CN103694198A - 用于制备环氧化物的方法 - Google Patents
用于制备环氧化物的方法 Download PDFInfo
- Publication number
- CN103694198A CN103694198A CN201410005014.2A CN201410005014A CN103694198A CN 103694198 A CN103694198 A CN 103694198A CN 201410005014 A CN201410005014 A CN 201410005014A CN 103694198 A CN103694198 A CN 103694198A
- Authority
- CN
- China
- Prior art keywords
- epoxide
- column plate
- feed zone
- halohydrin
- reactive distillation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/02—Synthesis of the oxirane ring
- C07D301/24—Synthesis of the oxirane ring by splitting off HAL—Y from compounds containing the radical HAL—C—C—OY
- C07D301/26—Y being hydrogen
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/009—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in combination with chemical reactions
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/02—Synthesis of the oxirane ring
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/32—Separation; Purification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
- C07D303/02—Compounds containing oxirane rings
- C07D303/04—Compounds containing oxirane rings containing only hydrogen and carbon atoms in addition to the ring oxygen atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
- C07D303/02—Compounds containing oxirane rings
- C07D303/08—Compounds containing oxirane rings with hydrocarbon radicals, substituted by halogen atoms, nitro radicals or nitroso radicals
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
Abstract
Description
Claims (18)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US8575808P | 2008-08-01 | 2008-08-01 | |
US61/085,758 | 2008-08-01 | ||
CN2009801306079A CN102112460A (zh) | 2008-08-01 | 2009-07-31 | 用于制备环氧化物的方法 |
Related Parent Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN2009801306079A Division CN102112460A (zh) | 2008-08-01 | 2009-07-31 | 用于制备环氧化物的方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN103694198A true CN103694198A (zh) | 2014-04-02 |
CN103694198B CN103694198B (zh) | 2016-03-02 |
Family
ID=41462254
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN2009801306079A Pending CN102112460A (zh) | 2008-08-01 | 2009-07-31 | 用于制备环氧化物的方法 |
CN201410005014.2A Expired - Fee Related CN103694198B (zh) | 2008-08-01 | 2009-07-31 | 用于制备环氧化物的方法 |
Family Applications Before (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN2009801306079A Pending CN102112460A (zh) | 2008-08-01 | 2009-07-31 | 用于制备环氧化物的方法 |
Country Status (8)
Country | Link |
---|---|
US (1) | US7985867B2 (zh) |
EP (1) | EP2321292B1 (zh) |
JP (1) | JP2011529914A (zh) |
KR (1) | KR20110036768A (zh) |
CN (2) | CN102112460A (zh) |
BR (1) | BRPI0910806A2 (zh) |
TW (1) | TWI368616B (zh) |
WO (1) | WO2010014898A2 (zh) |
Families Citing this family (27)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR101009858B1 (ko) * | 2003-11-20 | 2011-01-19 | 솔베이(소시에떼아노님) | 유기 화합물의 제조 방법 |
TWI321129B (en) * | 2005-05-20 | 2010-03-01 | Solvay | Process for preparing a chlorohydrin |
KR20080036555A (ko) * | 2005-05-20 | 2008-04-28 | 솔베이(소시에떼아노님) | 클로로히드린으로부터 출발하여 에폭시드를 제조하는 방법 |
EP1948583A2 (en) * | 2005-11-08 | 2008-07-30 | Solvay S.A. | Process for the manufacture of dichloropropanol by chlorination of glycerol |
EA200970011A1 (ru) * | 2006-06-14 | 2009-06-30 | Солвей (Сосьете Аноним) | Неочищенный продукт на основе глицерина, способ его очистки и его применение в производстве дихлорпропанола |
US20100032617A1 (en) * | 2007-02-20 | 2010-02-11 | Solvay (Societe Anonyme) | Process for manufacturing epichlorohydrin |
FR2913421B1 (fr) * | 2007-03-07 | 2009-05-15 | Solvay | Procede de fabrication de dichloropropanol. |
FR2913684B1 (fr) | 2007-03-14 | 2012-09-14 | Solvay | Procede de fabrication de dichloropropanol |
TW200911740A (en) | 2007-06-01 | 2009-03-16 | Solvay | Process for manufacturing a chlorohydrin |
TW200911773A (en) * | 2007-06-12 | 2009-03-16 | Solvay | Epichlorohydrin, manufacturing process and use |
TW200911693A (en) * | 2007-06-12 | 2009-03-16 | Solvay | Aqueous composition containing a salt, manufacturing process and use |
JP2011502032A (ja) * | 2007-10-02 | 2011-01-20 | ソルヴェイ(ソシエテ アノニム) | 容器の耐腐食性を向上させるためのケイ素を含有する組成物の使用 |
FR2925045B1 (fr) | 2007-12-17 | 2012-02-24 | Solvay | Produit a base de glycerol, procede pour son obtention et son utilisation dans la fabrication de dichloropropanol |
TWI478875B (zh) * | 2008-01-31 | 2015-04-01 | Solvay | 使水性組成物中之有機物質降解之方法 |
EA201071157A1 (ru) | 2008-04-03 | 2011-04-29 | Солвей (Сосьете Аноним) | Композиция, содержащая глицерин, способ ее получения и применение в производстве дихлорпропанола |
FR2935968B1 (fr) | 2008-09-12 | 2010-09-10 | Solvay | Procede pour la purification de chlorure d'hydrogene |
US8901823B2 (en) | 2008-10-24 | 2014-12-02 | Ilumisys, Inc. | Light and light sensor |
FR2939434B1 (fr) * | 2008-12-08 | 2012-05-18 | Solvay | Procede de traitement de glycerol. |
KR101705210B1 (ko) * | 2010-06-30 | 2017-02-09 | 롯데정밀화학 주식회사 | 클로로히드린류 조성물의 제조방법 및 그 방법에 의해 제조된 클로로히드린류 조성물을 사용하는 에피클로로히드린의 제조방법 |
KR101705208B1 (ko) * | 2010-06-30 | 2017-02-09 | 롯데정밀화학 주식회사 | 클로로히드린류 조성물의 제조방법 및 그 방법에 의해 제조된 클로로히드린류 조성물을 사용하는 에피클로로히드린의 제조방법 |
KR20140009163A (ko) | 2010-09-30 | 2014-01-22 | 솔베이(소시에떼아노님) | 천연유래 에피클로로히드린의 유도체 |
FR2966825B1 (fr) * | 2010-10-29 | 2014-05-16 | Solvay | Procede de fabrication d'epichlorhydrine |
US9527950B2 (en) * | 2011-09-27 | 2016-12-27 | Blue Cube Ip Llc | Reciprocating-plate column reactor for epoxidation of epoxy resins |
US8466302B1 (en) | 2011-12-21 | 2013-06-18 | Cpc Corporation, Taiwan | Process for producing propylene oxide |
US9422256B2 (en) | 2012-09-28 | 2016-08-23 | Conser Spa | Continuous process for producing epichlorohydrin from glycerol |
CN111632395A (zh) * | 2020-06-29 | 2020-09-08 | 山东凯泰科技股份有限公司 | 一种钠法环化生成环氧氯丙烷工艺系统 |
CN115253341A (zh) * | 2022-08-15 | 2022-11-01 | 惠州市红墙化学有限公司 | 一种环氧烷烃脱除转化的方法及装置 |
Family Cites Families (18)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2177419A (en) * | 1937-02-23 | 1939-10-24 | Shell Dev | Production of epihalohydrins |
NL261755A (zh) * | 1960-04-01 | 1900-01-01 | ||
DE1643847B2 (de) * | 1968-01-02 | 1974-09-05 | Chemische Werke Huels Ag, 4370 Marl | Verfahren zur Herstellung von Propylenoxid |
JPS5363303A (en) * | 1976-11-15 | 1978-06-06 | Showa Denko Kk | Purification of olefin oxides |
RO72086A2 (ro) | 1977-05-30 | 1981-11-24 | Combinatul Chimic,Ro | Procedeu si instalatie pentru fabricarea epiclorhidrinei |
JPS59196880A (ja) * | 1983-04-25 | 1984-11-08 | Mitsui Toatsu Chem Inc | エピクロルヒドリンの製造法 |
JPS60258171A (ja) | 1984-06-04 | 1985-12-20 | Showa Denko Kk | エピクロルヒドリンの製造方法 |
GB2173496B (en) | 1985-04-04 | 1989-01-05 | Inst Ciezkiej Syntezy Orga | Method for producing epichlorohydrin |
CN1005151B (zh) * | 1986-06-12 | 1989-09-13 | 天津大学 | 氯丙醇皂化制环氧丙烷方法的设备 |
JPH0662593B2 (ja) * | 1989-10-28 | 1994-08-17 | ダイソー株式会社 | エピクロルヒドリンの製造方法 |
JPH0625196B2 (ja) * | 1990-01-29 | 1994-04-06 | ダイソー株式会社 | エピクロルヒドリンの製造方法 |
FR2687149B1 (fr) | 1992-02-12 | 1995-11-03 | Roussel Uclaf | Nouveaux esters pyrethrinouides derives d'alcools thiazoliques, leur procede de preparation et leur application comme pesticides. |
US5532389A (en) | 1993-11-23 | 1996-07-02 | The Dow Chemical Company | Process for preparing alkylene oxides |
RO108962B1 (ro) | 1994-01-21 | 1994-10-31 | Sc Varachim Sa | Procedeu pentru fabricarea epiclorhidrinei |
JP3223267B2 (ja) * | 1997-12-25 | 2001-10-29 | 独立行政法人物質・材料研究機構 | 蛍石型またはその派生構造の酸化物焼結体とその製造方法 |
EP1059278B1 (en) * | 1999-06-08 | 2004-12-01 | Showa Denko Kabushiki Kaisha | Process for producing epichlorohydrin and intermediate thereof |
JP2002226471A (ja) * | 2001-01-31 | 2002-08-14 | Tokuyama Corp | プロピレンオキサイドの製造方法 |
US7910781B2 (en) | 2004-07-21 | 2011-03-22 | Dow Global Technologies Llc | Process for the conversion of a crude glycerol, crude mixtures of naturally derived multihydroxylated aliphatic hydrocarbons or esters thereof to a chlorohydrin |
-
2009
- 2009-07-21 TW TW098124514A patent/TWI368616B/zh not_active IP Right Cessation
- 2009-07-23 US US12/508,465 patent/US7985867B2/en not_active Expired - Fee Related
- 2009-07-31 EP EP09791046.7A patent/EP2321292B1/en not_active Not-in-force
- 2009-07-31 BR BRPI0910806-8A patent/BRPI0910806A2/pt not_active IP Right Cessation
- 2009-07-31 CN CN2009801306079A patent/CN102112460A/zh active Pending
- 2009-07-31 WO PCT/US2009/052399 patent/WO2010014898A2/en active Search and Examination
- 2009-07-31 CN CN201410005014.2A patent/CN103694198B/zh not_active Expired - Fee Related
- 2009-07-31 KR KR1020117004750A patent/KR20110036768A/ko not_active Application Discontinuation
- 2009-07-31 JP JP2011521355A patent/JP2011529914A/ja active Pending
Also Published As
Publication number | Publication date |
---|---|
BRPI0910806A2 (pt) | 2015-08-04 |
JP2011529914A (ja) | 2011-12-15 |
CN103694198B (zh) | 2016-03-02 |
KR20110036768A (ko) | 2011-04-08 |
EP2321292A2 (en) | 2011-05-18 |
WO2010014898A9 (en) | 2011-03-03 |
US7985867B2 (en) | 2011-07-26 |
US20100029959A1 (en) | 2010-02-04 |
WO2010014898A3 (en) | 2010-03-25 |
EP2321292B1 (en) | 2015-08-19 |
TW201006807A (en) | 2010-02-16 |
TWI368616B (en) | 2012-07-21 |
CN102112460A (zh) | 2011-06-29 |
WO2010014898A2 (en) | 2010-02-04 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C41 | Transfer of patent application or patent right or utility model | ||
CB02 | Change of applicant information |
Address after: American Michigan Applicant after: Dow Global Technologies Llc Address before: American Michigan Applicant before: Dow Global Technologies Inc. |
|
COR | Change of bibliographic data | ||
TA01 | Transfer of patent application right |
Effective date of registration: 20151218 Address after: American Michigan Applicant after: BLUE CUBE IP LLC Address before: American Michigan Applicant before: Dow Global Technologies Llc |
|
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
CF01 | Termination of patent right due to non-payment of annual fee | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160302 Termination date: 20160731 |