CN103666030A - UV curing ink for printing of digital product touch screen glass and preparation method of UV curing ink - Google Patents
UV curing ink for printing of digital product touch screen glass and preparation method of UV curing ink Download PDFInfo
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- CN103666030A CN103666030A CN201310593168.3A CN201310593168A CN103666030A CN 103666030 A CN103666030 A CN 103666030A CN 201310593168 A CN201310593168 A CN 201310593168A CN 103666030 A CN103666030 A CN 103666030A
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- digital product
- screen glass
- printing
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- Granted
Links
- 238000003848 UV Light-Curing Methods 0.000 title claims abstract description 13
- 239000011521 glass Substances 0.000 title claims abstract description 13
- 238000007639 printing Methods 0.000 title claims abstract description 13
- 238000002360 preparation method Methods 0.000 title claims description 8
- YNAVUWVOSKDBBP-UHFFFAOYSA-N Morpholine Chemical compound C1COCCN1 YNAVUWVOSKDBBP-UHFFFAOYSA-N 0.000 claims abstract description 14
- WGLPBDUCMAPZCE-UHFFFAOYSA-N Trioxochromium Chemical compound O=[Cr](=O)=O WGLPBDUCMAPZCE-UHFFFAOYSA-N 0.000 claims abstract description 7
- APUPEJJSWDHEBO-UHFFFAOYSA-P ammonium molybdate Chemical compound [NH4+].[NH4+].[O-][Mo]([O-])(=O)=O APUPEJJSWDHEBO-UHFFFAOYSA-P 0.000 claims abstract description 7
- 229940010552 ammonium molybdate Drugs 0.000 claims abstract description 7
- 235000018660 ammonium molybdate Nutrition 0.000 claims abstract description 7
- 239000011609 ammonium molybdate Substances 0.000 claims abstract description 7
- KTWOOEGAPBSYNW-UHFFFAOYSA-N ferrocene Chemical compound [Fe+2].C=1C=C[CH-]C=1.C=1C=C[CH-]C=1 KTWOOEGAPBSYNW-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- ZDQNWDNMNKSMHI-UHFFFAOYSA-N 1-[2-(2-prop-2-enoyloxypropoxy)propoxy]propan-2-yl prop-2-enoate Chemical compound C=CC(=O)OC(C)COC(C)COCC(C)OC(=O)C=C ZDQNWDNMNKSMHI-UHFFFAOYSA-N 0.000 claims abstract description 4
- POAOYUHQDCAZBD-UHFFFAOYSA-N 2-butoxyethanol Chemical compound CCCCOCCO POAOYUHQDCAZBD-UHFFFAOYSA-N 0.000 claims abstract description 4
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 claims abstract description 4
- QBLDFAIABQKINO-UHFFFAOYSA-N barium borate Chemical compound [Ba+2].[O-]B=O.[O-]B=O QBLDFAIABQKINO-UHFFFAOYSA-N 0.000 claims abstract description 4
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 claims abstract description 4
- PWWSSIYVTQUJQQ-UHFFFAOYSA-N distearyl thiodipropionate Chemical compound CCCCCCCCCCCCCCCCCCOC(=O)CCSCCC(=O)OCCCCCCCCCCCCCCCCCC PWWSSIYVTQUJQQ-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000000976 ink Substances 0.000 claims description 16
- 238000003756 stirring Methods 0.000 claims description 15
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 9
- 238000006243 chemical reaction Methods 0.000 claims description 9
- 239000012752 auxiliary agent Substances 0.000 claims description 7
- JHPBZFOKBAGZBL-UHFFFAOYSA-N (3-hydroxy-2,2,4-trimethylpentyl) 2-methylprop-2-enoate Chemical compound CC(C)C(O)C(C)(C)COC(=O)C(C)=C JHPBZFOKBAGZBL-UHFFFAOYSA-N 0.000 claims description 6
- ZNQVEEAIQZEUHB-UHFFFAOYSA-N 2-ethoxyethanol Chemical compound CCOCCO ZNQVEEAIQZEUHB-UHFFFAOYSA-N 0.000 claims description 6
- LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 claims description 6
- 239000004593 Epoxy Substances 0.000 claims description 6
- ISAOCJYIOMOJEB-UHFFFAOYSA-N benzoin Chemical compound C=1C=CC=CC=1C(O)C(=O)C1=CC=CC=C1 ISAOCJYIOMOJEB-UHFFFAOYSA-N 0.000 claims description 6
- 239000000975 dye Substances 0.000 claims description 6
- 150000002734 metacrylic acid derivatives Chemical class 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- 239000000049 pigment Substances 0.000 claims description 6
- 239000000843 powder Substances 0.000 claims description 6
- GHMLBKRAJCXXBS-UHFFFAOYSA-N resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 4
- 244000077995 Coix lacryma jobi Species 0.000 claims description 3
- FQYUMYWMJTYZTK-UHFFFAOYSA-N Phenyl glycidyl ether Chemical compound C1OC1COC1=CC=CC=C1 FQYUMYWMJTYZTK-UHFFFAOYSA-N 0.000 claims description 3
- 229920002367 Polyisobutene Polymers 0.000 claims description 3
- ZTHYODDOHIVTJV-UHFFFAOYSA-N Propyl gallate Chemical compound CCCOC(=O)C1=CC(O)=C(O)C(O)=C1 ZTHYODDOHIVTJV-UHFFFAOYSA-N 0.000 claims description 3
- 239000006087 Silane Coupling Agent Substances 0.000 claims description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 3
- 244000028419 Styrax benzoin Species 0.000 claims description 3
- 235000000126 Styrax benzoin Nutrition 0.000 claims description 3
- 235000008411 Sumatra benzointree Nutrition 0.000 claims description 3
- DAKWPKUUDNSNPN-UHFFFAOYSA-N Trimethylolpropane triacrylate Chemical compound C=CC(=O)OCC(CC)(COC(=O)C=C)COC(=O)C=C DAKWPKUUDNSNPN-UHFFFAOYSA-N 0.000 claims description 3
- 229960002130 benzoin Drugs 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 235000019439 ethyl acetate Nutrition 0.000 claims description 3
- 235000019382 gum benzoic Nutrition 0.000 claims description 3
- 239000003112 inhibitor Substances 0.000 claims description 3
- 239000010445 mica Substances 0.000 claims description 3
- 229910052618 mica group Inorganic materials 0.000 claims description 3
- GEMHFKXPOCTAIP-UHFFFAOYSA-N n,n-dimethyl-n'-phenylcarbamimidoyl chloride Chemical compound CN(C)C(Cl)=NC1=CC=CC=C1 GEMHFKXPOCTAIP-UHFFFAOYSA-N 0.000 claims description 3
- 230000003647 oxidation Effects 0.000 claims description 3
- 238000007254 oxidation reaction Methods 0.000 claims description 3
- 239000002002 slurry Substances 0.000 claims description 3
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 3
- 238000001723 curing Methods 0.000 abstract description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 239000004615 ingredient Substances 0.000 abstract 2
- KWVGIHKZDCUPEU-UHFFFAOYSA-N 2,2-dimethoxy-2-phenylacetophenone Chemical compound C=1C=CC=CC=1C(OC)(OC)C(=O)C1=CC=CC=C1 KWVGIHKZDCUPEU-UHFFFAOYSA-N 0.000 abstract 1
- FPZWZCWUIYYYBU-UHFFFAOYSA-N 2-(2-ethoxyethoxy)ethyl acetate Chemical compound CCOCCOCCOC(C)=O FPZWZCWUIYYYBU-UHFFFAOYSA-N 0.000 abstract 1
- POYODSZSSBWJPD-UHFFFAOYSA-N 2-methylprop-2-enoyloxy 2-methylprop-2-eneperoxoate Chemical compound CC(=C)C(=O)OOOC(=O)C(C)=C POYODSZSSBWJPD-UHFFFAOYSA-N 0.000 abstract 1
- CERQOIWHTDAKMF-UHFFFAOYSA-M Methacrylate Chemical compound CC(=C)C([O-])=O CERQOIWHTDAKMF-UHFFFAOYSA-M 0.000 abstract 1
- GHPGOEFPKIHBNM-UHFFFAOYSA-N antimony(3+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[Sb+3].[Sb+3] GHPGOEFPKIHBNM-UHFFFAOYSA-N 0.000 abstract 1
- 239000003963 antioxidant agent Substances 0.000 abstract 1
- 230000003078 antioxidant effect Effects 0.000 abstract 1
- 229910000423 chromium oxide Inorganic materials 0.000 abstract 1
- 238000005265 energy consumption Methods 0.000 abstract 1
- 238000011031 large-scale manufacturing process Methods 0.000 abstract 1
- 239000012860 organic pigment Substances 0.000 abstract 1
- 238000007650 screen-printing Methods 0.000 description 6
- 238000000034 method Methods 0.000 description 3
- 240000001624 Espostoa lanata Species 0.000 description 2
- 235000009161 Espostoa lanata Nutrition 0.000 description 2
- 239000004744 fabric Substances 0.000 description 2
- 101000831616 Homo sapiens Protachykinin-1 Proteins 0.000 description 1
- 240000008415 Lactuca sativa Species 0.000 description 1
- 102100024304 Protachykinin-1 Human genes 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000005530 etching Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 238000010428 oil painting Methods 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 235000012045 salad Nutrition 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 229920002994 synthetic fiber Polymers 0.000 description 1
- 239000004758 synthetic textile Substances 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses UV curing ink for printing of digital product touch screen glass, which is characterized in that the ink is prepared from the following raw materials in parts by weight: 1-3 parts of organic pigments, 20-24 parts of methacrylate, 12-15 parts of epoxy methacrylate, 2-3 parts of ammonium molybdate, 1-2 parts of chromium oxide, 1-2 parts of morpholine, 5-8 parts of glycol ether, 1-2 parts of ferrocene, 3-4 parts of 2-butoxyethanol, 3-4 parts of methacrylic acid, 10-14 parts of diethylene glycol monoethyl ether acetate, 5-8 parts of benzil dimethyl ketal, 6-9 parts of tripropylene glycol diacrylate, 5-8 parts of a 184 photoinitiator, 1-2 parts of an antioxidant DSTP, 1-2 parts of Sb2O3, 1-2 parts of barium metaborate and 4-5 parts of an accessory ingredient. According to the invention, the toughness of the ink is improved through the accessory ingredient, the ink is enabled to be uniformly dispersed, and the stability of the ink is maintained; the UV curing ink is high in curing speed, reduces energy consumption and time, improves the production efficiency, and is suitable for large scale production.
Description
Technical field
The present invention relates to a kind of ink and preparation method thereof, particularly a kind of UV curing inks for digital product touch-screen glass printing and preparation method thereof.
Background technology
Silk screen printing is that silk fabrics, synthetic fabrics or wire cloth are stretched tight on screen frame, adopts manual method of carving paint film or photochemistry plate-making to make screen printing forme.Modern screen printing technique, to utilize sensitive materials by photomechanical method, to make the flat carriers such as screen printing forme (making the silk screen hole of picture and text part on screen printing forme is through hole, and the silk screen hole of non-graphic part is plugged) oil painting, etching, pictorial poster, business card, binding and layout front cover, commodity packaging, product tag, dyeing textile product, touch-screen glass and metal etc.Ink is the screen printing ink that is conducive to two liquid response types of environment, essential superior printing stability while thering is touch screen glass printing, good sticking power and patience, filming after solidifying has good sticking power, water tolerance and chemoresistance, also has higher surface hardness and wear resistance simultaneously.
Summary of the invention
The object of this invention is to provide a kind of UV curing inks for digital product touch-screen glass printing and preparation method thereof.
In order to realize object of the present invention, the present invention passes through following scheme implementation:
For a UV curing inks for digital product touch-screen glass printing, by the raw material of following weight part, made: pigment dyestuff 1-3, methacrylic ester 20-24, epoxy methacrylates 12-15, ammonium molybdate 2-3, chromic oxide 1-2, morpholine 1-2, ethylene glycol ethyl ether 5-8, ferrocene 1-2,2-butoxy-ethanol 3-4, methacrylic acid 3-4, diethylene glycol ether acetic ester 10-14, benzoin dimethylether 5-8, tripropylene glycol diacrylate 6-9,184 light trigger 5-8, oxidation inhibitor DSTP 1-2, Sb2O31-2, barium metaborate 1-2, auxiliary agent 4-5;
Described auxiliary agent is prepared from by the raw material of following weight part: nano diatomite powder 0.2-0.3, nano mica powder 0.2-0.3, Silane coupling agent KH550 2-3, linking agent TAC2-3, polyisobutene 2-3, Resorcinol 1-2, Viscoat 295 10-12, vinylformic acid dimethylamino ethyl ester 2-3, phenyl glycidyl ether 1-2, cobalt naphthenate 2-3, Tenox PG 2-3, coix seed oil 1-2; Its preparation method is by each mixing of materials, is heated to 60-70 ℃, and stirring reaction 30-40 minute, obtains.
UV curing inks for digital product touch-screen glass printing of the present invention, by following concrete steps, made: first add pigment dyestuff, methacrylic ester, epoxy methacrylates, ammonium molybdate, chromic oxide, morpholine, ethylene glycol ethyl ether, ferrocene stirring and evenly mixing, be heated to 80-90 ℃, stir 25-35 minute; Then add all the other remaining components except 184 light triggers, stirring reaction 3-5 hour; Finally be cooled to 60-70 ℃, add 184 light triggers, stirring reaction 40-50 minute, cooling after, grind and to obtain 20-40 μ m slurry, obtain.
The invention has the beneficial effects as follows: auxiliary agent of the present invention has improved the toughness of ink, make distributes ink even, and maintained the stability of ink; Curing speed of the present invention is fast, energy efficient and time, improved production efficiency, and be applicable to scale operation.
Specific embodiments
Below by specific examples, the present invention is described in detail.
For a UV curing inks for digital product touch-screen glass printing, by following weight part (kilogram) raw material make: pigment dyestuff 1, methacrylic ester 20, epoxy methacrylates 12, ammonium molybdate 2, chromic oxide 1, morpholine 1, ethylene glycol ethyl ether 5, ferrocene 1,2-butoxy-ethanol 3, methacrylic acid 3, diethylene glycol ether acetic ester 10, benzoin dimethylether 5, tripropylene glycol diacrylate 6,184 light triggers 5, oxidation inhibitor DSTP 1, Sb2O31, barium metaborate 1, auxiliary agent 4;
Described auxiliary agent by following weight part (kilogram) raw material be prepared from: nano diatomite powder 0.2, nano mica powder 0.2, Silane coupling agent KH550 2, linking agent TAC2, polyisobutene 2, Resorcinol 1, Viscoat 295 10, vinylformic acid dimethylamino ethyl ester 2, phenyl glycidyl ether 1, cobalt naphthenate 2, Tenox PG 2, coix seed oil 1; Its preparation method is by each mixing of materials, is heated to 60-70 ℃, and stirring reaction 30-40 minute, obtains.
UV curing inks for digital product touch-screen glass printing of the present invention, by following concrete steps, made: first add pigment dyestuff, methacrylic ester, epoxy methacrylates, ammonium molybdate, chromic oxide, morpholine, ethylene glycol ethyl ether, ferrocene stirring and evenly mixing, be heated to 80-90 ℃, stir 25-35 minute; Then add all the other remaining components except 184 light triggers, stirring reaction 3-5 hour; Finally be cooled to 60-70 ℃, add 184 light triggers, stirring reaction 40-50 minute, cooling after, grind and to obtain 20-40 μ m slurry, obtain.
The ink of gained, is used cross-hatching ox-hide tape stripping, draws compartment apart from 1mm, and 100% adheres to; Spirituous cotton balls is soaked in use, and 300 grams of pressure wipings 50 times, are as good as shape; Be soaked in salad oil (normal temperature) 8 hours, be as good as shape; Use is soaked with the cotton balls of salt solution, and 300 grams of pressure wipings 50 times, are as good as shape.
Claims (2)
1. the UV curing inks for digital product touch-screen glass printing, it is characterized in that, raw material by following weight part is made: pigment dyestuff 1-3, methacrylic ester 20-24, epoxy methacrylates 12-15, ammonium molybdate 2-3, chromic oxide 1-2, morpholine 1-2, ethylene glycol ethyl ether 5-8, ferrocene 1-2, 2-butoxy-ethanol 3-4, methacrylic acid 3-4, diethylene glycol ether acetic ester 10-14, benzoin dimethylether 5-8, tripropylene glycol diacrylate 6-9, 184 light trigger 5-8, oxidation inhibitor DSTP 1-2, Sb2O31-2, barium metaborate 1-2, auxiliary agent 4-5,
Described auxiliary agent is prepared from by the raw material of following weight part: nano diatomite powder 0.2-0.3, nano mica powder 0.2-0.3, Silane coupling agent KH550 2-3, linking agent TAC2-3, polyisobutene 2-3, Resorcinol 1-2, Viscoat 295 10-12, vinylformic acid dimethylamino ethyl ester 2-3, phenyl glycidyl ether 1-2, cobalt naphthenate 2-3, Tenox PG 2-3, coix seed oil 1-2; Its preparation method is by each mixing of materials, is heated to 60-70 ℃, and stirring reaction 30-40 minute, obtains.
2. according to claim 1 for the UV curing inks of digital product touch-screen glass printing, it is characterized in that, by following concrete steps, made: first add pigment dyestuff, methacrylic ester, epoxy methacrylates, ammonium molybdate, chromic oxide, morpholine, ethylene glycol ethyl ether, ferrocene stirring and evenly mixing, be heated to 80-90 ℃, stir 25-35 minute; Then add all the other remaining components except 184 light triggers, stirring reaction 3-5 hour; Finally be cooled to 60-70 ℃, add 184 light triggers, stirring reaction 40-50 minute, cooling after, grind and to obtain 20-40 μ m slurry, obtain.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310593168.3A CN103666030B (en) | 2013-11-23 | 2013-11-23 | A kind of UV cured printing ink for digital product touch-screen glass printing and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310593168.3A CN103666030B (en) | 2013-11-23 | 2013-11-23 | A kind of UV cured printing ink for digital product touch-screen glass printing and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103666030A true CN103666030A (en) | 2014-03-26 |
| CN103666030B CN103666030B (en) | 2016-05-04 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310593168.3A Active CN103666030B (en) | 2013-11-23 | 2013-11-23 | A kind of UV cured printing ink for digital product touch-screen glass printing and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103666030B (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101469152A (en) * | 2007-12-27 | 2009-07-01 | 深圳富泰宏精密工业有限公司 | Ink composition and use method thereof |
| CN101580661A (en) * | 2009-06-05 | 2009-11-18 | 刘恒全 | touch screen protection ink |
| CN102093782A (en) * | 2011-03-30 | 2011-06-15 | 北京神彩优维喷墨材料科技有限公司 | Ultraviolet-cured digital painting ink and preparation method thereof |
| CN102702849A (en) * | 2012-06-05 | 2012-10-03 | 无锡金桥精细油墨有限公司 | Ultraviolet-light-cured glass transparent ink and preparation method thereof |
-
2013
- 2013-11-23 CN CN201310593168.3A patent/CN103666030B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101469152A (en) * | 2007-12-27 | 2009-07-01 | 深圳富泰宏精密工业有限公司 | Ink composition and use method thereof |
| CN101580661A (en) * | 2009-06-05 | 2009-11-18 | 刘恒全 | touch screen protection ink |
| CN102093782A (en) * | 2011-03-30 | 2011-06-15 | 北京神彩优维喷墨材料科技有限公司 | Ultraviolet-cured digital painting ink and preparation method thereof |
| CN102702849A (en) * | 2012-06-05 | 2012-10-03 | 无锡金桥精细油墨有限公司 | Ultraviolet-light-cured glass transparent ink and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN103666030B (en) | 2016-05-04 |
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| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A UV cured ink and its preparation method for touch screen glass printing of digital products Effective date of registration: 20231113 Granted publication date: 20160504 Pledgee: Shanghai Yudi Aviation Supplies Co.,Ltd. Pledgor: TONGLING FOUNDER PLASTICS TECHNOLOGY Co.,Ltd. Registration number: Y2023980065339 |
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Date of cancellation: 20231219 Granted publication date: 20160504 Pledgee: Shanghai Yudi Aviation Supplies Co.,Ltd. Pledgor: TONGLING FOUNDER PLASTICS TECHNOLOGY Co.,Ltd. Registration number: Y2023980065339 |
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| PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A UV cured ink and its preparation method for touch screen glass printing of digital products Granted publication date: 20160504 Pledgee: Shanghai Yudi Aviation Supplies Co.,Ltd. Pledgor: TONGLING FOUNDER PLASTICS TECHNOLOGY Co.,Ltd. Registration number: Y2024980000266 |
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| PE01 | Entry into force of the registration of the contract for pledge of patent right |