CN105560082A - Improved peelable soak-off gel and preparation method thereof - Google Patents
Improved peelable soak-off gel and preparation method thereof Download PDFInfo
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- CN105560082A CN105560082A CN201610099313.6A CN201610099313A CN105560082A CN 105560082 A CN105560082 A CN 105560082A CN 201610099313 A CN201610099313 A CN 201610099313A CN 105560082 A CN105560082 A CN 105560082A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q3/00—Manicure or pedicure preparations
- A61Q3/02—Nail coatings
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/38—Polysiloxanes modified by chemical after-treatment
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/42—Colour properties
- A61K2800/43—Pigments; Dyes
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/95—Involves in-situ formation or cross-linking of polymers
Abstract
The invention discloses improved peelable soak-off gel. The improved peelable soak-off gel is prepared from, by weight, 50-80 parts of UV curing resin A, 50-80 parts of UV curing resin B, 50-80 parts of reactive diluent, 0.05-0.1 part of flatting agent, 1-10 parts of wetting agent, 0.2-1 part of defoaming agent, 1-10 parts of color paste and 3-5 parts of photoinitiator. The invention further provides a preparation method of the improved peelable soak-off gel. Wetting agent, flatting agent, defoaming agent and color paste are added into a high-speed disperser, UV curing resin A, UV curing resin B, reactive diluent, thickening agent and photoinitiator are added after dispersion, dispersion continues to be conducted, and materials are evenly mixed to obtain the improved peelable soak-off gel. The improved peelable soak-off gel has rapid curing capacity after being used for coating and irradiated by a 395-nm UV-LED lamp and can be widely used for the technical field of nail beautifying of various people and the like.
Description
Technical field
The invention belongs to polymeric material field, relate to a kind of nail polish glue, strippable property nail polish glue of a kind of improvement specifically and preparation method thereof.
Background technology
Ms to manicure like come from one and have deep love for.Nail polish glue is applied to fingernail with instrument when using, and after common UV light source light source treatment with irradiation, cross-linking polymerization occurs, the nail polish adhesive curing thing of generation beautiful in colour, glittering and translucent full, change irregularly infinite, be the favorite of ladies.Compared with the light source curing mode of common UV, UV-LED light source has the plurality of advantages such as luminous efficiency is high, the life-span is long, response speed is fast, heat release is few, energy-saving and environmental protection, substitutes common UV light source gradually.Along with the quickening that the abundant of city life and rhythm of life convert, ladies have liked the fingernail of allegro conversion oneself.Peelable nail polish glue is easy to use, peels off when needing to take off without cleaner with regard to whole of energy, easily, is particularly suitable for child and uses.But current peelable nail polish glue generally with the addition of peelable component in the formula of nail polish glue, makes troubles to the production of nail polish glue and use.
Based on above background, need to develop a kind of can fast setting, have from peeling off component, there is the strippable property nail polish glue and preparation method thereof of decorative effect, improvement that peeling effect is good simultaneously.
Summary of the invention
For above-mentioned technical problem of the prior art, strippable property nail polish glue that the invention provides a kind of improvement and preparation method thereof, strippable property nail polish glue of described this improvement and preparation method thereof will solve peelable nail polish glue of the prior art and generally in the formula of nail polish glue, with the addition of peelable component, to the technical problem that the production of nail polish glue and use are made troubles.
The invention provides a kind of strippable property nail polish glue of improvement, calculate by weight, its raw material composition and content as follows:
The chemical constitution of described UV cured resin A is as follows:
Wherein: m is the integer within the scope of 1-30;
The preparation method of described UV cured resin A comprises the steps:
1) by weight, following component is taken:
2) above-mentioned gained methyl and phenyl hydrogen-containing silicon oil and double pentaerythritol methacrylate are joined in a reaction vessel, then polymerization inhibitor is added, pass into protective gas, stir and heat, being warming up to 60 ~ 80 DEG C, adding catalyst, stir lower constant temperature 3 ~ 5h, stop heating, treat that temperature drops to room temperature, obtain UV cured resin A;
Described UV cured resin B is hyperbranched UV cured resin;
Described levelling agent is any one or two or more mixture in enlightening height TegoGlide410, German BYK Bi Ke BYK-UV3510, BYK-341, BYK-344, BYK-345, BYK-346, BYK-347 or BYK-348;
Described UV wetting agent is one or both mixture in the NP-100 of LG-DOW company or German BYK333 levelling agent;
Described defoamer is any one or two or more mixture in German BYK Bi Ke BYK-024, BYK-025, BYK-035, BYK-037, BYK-038, BYK-044 or BYK-038;
Described light trigger A be in BASF Irgacure1173, Irgacure184D, IrgacureTPO, Irgacure369, Irgacure651, Irgacure379, Irgacure819, Irgacure907 or macromolecular photoinitiator EsacureKIP150 any one or two or more mixture;
Described photoinitiator b is any one or two or more mixture in BASF BASF light trigger Irgacure2959, IRGACURE500 or IRGACURE819DW.
Further, the strippable property nail polish glue of above-mentioned a kind of improvement, calculates by weight, its raw material composition and content as follows:
Wherein, the preparation method of described UV cured resin A is:
20 parts of methyl and phenyl hydrogen-containing silicon oils and 10 parts of double pentaerythritol methacrylates are joined in a reaction vessel, then the polymerization inhibitor of 0.005 part is added, pass into protective gas, stir and heat, being warming up to 60 DEG C, adding 0.03 part of catalyst, stir lower constant temperature 3h, stop heating, treat that temperature drops to room temperature, obtain UV cured resin A;
Described UV cured resin C be double pentaerythritol methacrylate, diethylene glycol diacrylate, oxolane acrylate in mass ratio 1:1:1 composition mixture;
Described levelling agent is enlightening height TegoGlide410;
Described wetting agent is the NP-100 of LG-DOW company;
Described defoamer is the mixture of German BYK-035, BYK-037 1:1 in mass ratio;
Described mill base is a kind of temperature sensing color changing color slurry of changeable colour;
Described light trigger A be BASF Irgacure1173, Irgacure184D, IrgacureTPO in mass ratio 1:1:1 composition mixture;
Described photoinitiator b be BASF BASF light trigger Irgacure2959, IRGACURE500 in mass ratio 1:1 composition mixture.
Further, the strippable property nail polish glue of above-mentioned a kind of improvement, calculates by weight, its raw material composition and content as follows:
Wherein, the preparation method of described UV cured resin A is:
Above-mentioned 60 parts of methyl and phenyl hydrogen-containing silicon oils and 20 parts of double pentaerythritol methacrylates are joined in a reaction vessel, add the polymerization inhibitor of 0.01 part again, pass into protective gas, stir and heat, being warming up to 60 DEG C, adding 0.05 part of catalyst, stir lower constant temperature 5h, stop heating, treat that temperature drops to room temperature, obtain UV cured resin A;
Described UV cured resin C be double pentaerythritol methacrylate, diethylene glycol diacrylate, oxolane acrylate in mass ratio 2:1:1 composition mixture;
Described levelling agent be German BYK-345, BYK-346 in mass ratio 1:1 composition mixture;
Described wetting agent is German BYK333;
Described defoamer be German BYK Bi Ke BYK-024, BYK-025 in mass ratio 1:1 composition mixture;
Described mill base is a kind of temperature sensing color changing color slurry of changeable colour;
Described light trigger A is BASF Irgacure184D, IrgacureTPO, Irgacure369 1:1:1 many kinds of mixture in mass ratio;
Described photoinitiator b be BASF BASF light trigger Irgacure2959, IRGACURE500 in mass ratio 2:1 composition mixture.
Present invention also offers the preparation method of the strippable property nail polish glue of above-mentioned a kind of improvement, comprise the steps:
1) UV cured resin A, UV cured resin B, reactive diluent, levelling agent, wetting agent, defoamer, mill base and light trigger is taken according to parts by weight;
2) in the high speed dispersor controlling rotating speed 300-400r/min, wetting agent, levelling agent, defoamer and mill base is added, after disperseing 15-20min under 600-800r/min rotating speed, rotating speed is down to 250 ~ 350r/min, add UV cured resin A, UV cured resin B and light trigger A, photoinitiator b, continue dispersion 5-10min, mix homogeneously, the strippable property nail polish glue be namely improved.
The reaction equation of above-mentioned UV cured resin A is as follows:
The present invention, owing to have employed the UV cured resin A of multi-functional acrylate and having the hyperbranched UV cured resin of dissaving structure, makes it have at 395nmUV-LED, the rapid shaping ability under the irradiation of lamp source.Through the surface of the microscope slide of the strippable property nail polish glue of UV nail polish light irradiation precoating improvement after the strippable property nail polish glue film of the improvement of gained of the present invention, according to the fingers-touch method (surface of the strippable property nail polish glue of the improvement of the cured a period of time that press...withes one's finger, using tack-free as completely crued standard, when solidifying completely with the strippable property nail polish glue improved, the shortest time used characterizes), after testing, the hardening time of the strippable property nail polish glue of quick-drying improvement of the present invention is 1-7s.UV cured resin A molecular structure as main film forming substance of the present invention is organosilicon structures, there is very low surface energy, reduce the interaction between film and base material, make it to embody better rippability, peel strength adopts Shenzhen newly to think carefully, and the CMT5104 electronic tension tester of company at room temperature carries out the stripping test of 180 ° by GB/T2790-1995 standard " adhesive 180 ° of peeling strength test methods ", draw speed 50mm/min, recording peel strength is 0.21 ~ 0.25kN/m.The chameleon pigment that the strippable property nail polish glue of the improvement of gained of the present invention adds brings Protean color to the strippable property nail polish glue improved.
The present invention compares with prior art, and its technological progress is significant.The present invention has the quick setting capabilities under 395nmUV-LED lamp source is irradiated, and has and covers with paint, lacquer, colour wash, etc. bright changeable, the feature such as strippable property is good of convenient and swift, color, have high glaze simultaneously, do not add the peelable effect of remover with regard to realizing.And, preparation method of the present invention due to technique simple, easy to control, the maturation that therefore possesses skills, the feature such as quick, efficient, and be suitable for suitability for industrialized production.The present invention can widely use the technical fields such as the manicure of all kinds of crowd.
Detailed description of the invention
Below by embodiment, the present invention is described in further detail, but do not limit the present invention.
In the raw material that various embodiments of the present invention are used except the special producer that shows and specification, other raw materials are commercially available, and specification is chemical pure.
The model of the various equipment that the present invention is used and the information of manufacturer as follows:
GFJ-0.4 type high speed dispersor, Shanghai Xin Nuo instrument and equipment company limited produces.
Embodiment 1
A strippable property nail polish glue for improvement, calculates by weight, its raw material composition and content as follows:
Wherein said UV cured resin A calculates by weight, its composition and content as follows:
Described UV cured resin A is prepared as follows:
Above-mentioned 20 parts of methyl and phenyl hydrogen-containing silicon oils and 10 parts of double pentaerythritol methacrylates are joined in the there-necked flask of 500ml; add the polymerization inhibitor of 0.005 part again; pass into protective gas; stir and heat, being warming up to 60 DEG C, adding 0.03 part of catalyst; stir lower constant temperature 3h; stop heating, treat that flask temperature drops to room temperature, obtain UV cured resin A.
Described levelling agent is enlightening height TegoGlide410;
Described wetting agent is the NP-100 of LG-DOW company;
Described defoamer is the mixture of German BYK-035, BYK-037 1:1 in mass ratio;
Described mill base is a kind of temperature sensing color changing color slurry of changeable colour;
Described light trigger A be BASF Irgacure1173, Irgacure184D, IrgacureTPO in mass ratio 1:1:1 composition mixture;
Described photoinitiator b be BASF BASF light trigger Irgacure2959, IRGACURE500 in mass ratio 1:1 composition mixture;
The preparation method of the strippable property nail polish glue of above-mentioned a kind of improvement, specifically comprises the steps:
(1) preparation of the strippable property nail polish glue, improved
According to formula, 1 part of wetting agent, 0.05 part of levelling agent, 0.2 part of defoamer and 1 part of mill base is added in the GFJ-0.4 type high speed dispersor (Shanghai Xin Nuo instrument and equipment company limited) controlling rotating speed 300r/min, after disperseing 15min under 600r/min rotating speed, rotating speed is down to 300r/min, add 50 parts of UV cured resin A, 50 parts of UV cured resin B, 50 parts of reactive diluents, 3 parts of light trigger A and 3 part photoinitiator bs, continue dispersion 10min, mix homogeneously, the strippable property nail polish glue be namely improved.
The surface of the microscope slide of the strippable property nail polish glue improved through the UV-LED light irradiation precoating of 395nm after the strippable property nail polish glue film of the improvement of gained of the present invention, according to the fingers-touch method (surface of the strippable property nail polish glue of the improvement of the cured a period of time that press...withes one's finger, using tack-free as completely crued standard, when solidifying completely with the strippable property nail polish glue improved, the shortest time used characterizes), after testing, the hardening time of the strippable property nail polish glue of quick-drying improvement of the present invention is 1s.
The CMT5104 electronic tension tester that peel strength adopts Shenzhen newly to think carefully company at room temperature carries out the stripping test of 180 ° by GB/T2790-1995 standard " adhesive 180 ° of peeling strength test methods ", draw speed 50mm/min; Recording peel strength is 0.25kN/m; Therefore, curing rate higher after the strippable property nail polish glue film of the improvement of gained of the present invention, easily peels off.
Embodiment 2
A strippable property nail polish glue for improvement, calculates by weight, its raw material composition and content as follows:
Wherein said UV cured resin A calculates by weight, its composition and content as follows:
Described UV cured resin A is prepared as follows:
60 parts of methyl and phenyl hydrogen-containing silicon oils and 20 parts of double pentaerythritol methacrylates are joined in the there-necked flask of 500ml; add the polymerization inhibitor of 0.01 part again; pass into protective gas; stir and heat, being warming up to 80 DEG C, adding 0.05 part of catalyst; stir lower constant temperature 5h; stop heating, treat that flask temperature drops to room temperature, obtain UV cured resin A.
Described levelling agent be German BYK-345, BYK-346 in mass ratio 1:1 composition mixture;
Described wetting agent is German BYK333;
Described defoamer be German BYK Bi Ke BYK-024, BYK-025 in mass ratio 1:1 composition mixture;
Described mill base is a kind of temperature sensing color changing color slurry of changeable colour;
Described light trigger A is BASF Irgacure184D, IrgacureTPO, Irgacure369 1:1:1 many kinds of mixture in mass ratio;
Described photoinitiator b be BASF BASF light trigger Irgacure2959, IRGACURE500 in mass ratio 2:1 composition mixture;
The preparation method of the strippable property nail polish glue of above-mentioned a kind of improvement, specifically comprises the steps:
According to formula, 10 parts of wetting agent, 0.1 part of levelling agent, 1 part of defoamer and 10 parts of mill bases are added in the GFJ-0.4 type high speed dispersor (Shanghai Xin Nuo instrument and equipment company limited) controlling rotating speed 400r/min, after disperseing 20min under 800r/min rotating speed, rotating speed is down to 300r/min, add 80 parts of UV cured resin A, 80 parts of UV cured resin B, 80 parts of reactive diluents, 5 parts of light trigger A and 5 part photoinitiator bs, continue dispersion 10min, mix homogeneously, the strippable property nail polish glue be namely improved.
The surface of the microscope slide of the strippable property nail polish glue improved through the UV-LED light irradiation precoating of 395nm after the strippable property nail polish glue film of the improvement of gained of the present invention, according to the fingers-touch method (surface of the strippable property nail polish glue of the improvement of the cured a period of time that press...withes one's finger, using tack-free as completely crued standard, when solidifying completely with the strippable property nail polish glue improved, the shortest time used characterizes), after testing, the hardening time of the strippable property nail polish glue of quick-drying improvement of the present invention is 7s.Color changeable effect is presented after solidification.
The CMT5104 electronic tension tester that peel strength adopts Shenzhen newly to think carefully company at room temperature carries out the stripping test of 180 ° by GB/T2790-1995 standard " adhesive 180 ° of peeling strength test methods ", draw speed 50mm/min; Recording peel strength is 0.21kN/m; Therefore, curing rate higher after the strippable property nail polish glue film of the improvement of gained of the present invention, easily peels off.
In sum, what the strippable property nail polish glue of improvement of the present invention adopted is UV curing formula, and the high speed curable of UV improves its curing rate, only has 1 ~ 7s; That adds has toughening effect UV cured resin C, makes the strippable property nail polish glue of improvement have certain toughness.UV cured resin A molecular structure as main film forming substance is organosilicon structures, has very low surface energy, reduces the interaction between film and base material, and making it to embody better rippability peel strength is 0.21 ~ 0.25kN/m.
Described content be only the present invention conceive under basic explanation, and according to any equivalent transformation that technical scheme of the present invention is done, all should protection scope of the present invention be belonged to.
Claims (4)
1. improve a strippable property nail polish glue, it is characterized in that calculating by weight, its raw material composition and content as follows:
The chemical constitution of described UV cured resin A is as follows:
Wherein: m is the integer within the scope of 1-30; The preparation method of described UV cured resin A comprises the steps:
1) by weight, following component is taken:
2) above-mentioned gained methyl and phenyl hydrogen-containing silicon oil and double pentaerythritol methacrylate are joined in a reaction vessel, then polymerization inhibitor is added, pass into protective gas, stir and heat, being warming up to 60 ~ 80 DEG C, adding catalyst, stir lower constant temperature 3 ~ 5h, stop heating, treat that temperature drops to room temperature, obtain UV cured resin A;
Described UV cured resin B is hyperbranched UV cured resin;
Described levelling agent is any one or two or more mixture in enlightening height TegoGlide410, German BYK Bi Ke BYK-UV3510, BYK-341, BYK-344, BYK-345, BYK-346, BYK-347 or BYK-348;
Described UV wetting agent is one or both mixture in the NP-100 of LG-DOW company or German BYK333 levelling agent;
Described defoamer is any one or two or more mixture in German BYK Bi Ke BYK-024, BYK-025, BYK-035, BYK-037, BYK-038, BYK-044 or BYK-038;
Described light trigger A be in BASF Irgacure1173, Irgacure184D, IrgacureTPO, Irgacure369, Irgacure651, Irgacure379, Irgacure819, Irgacure907 or macromolecular photoinitiator EsacureKIP150 any one or two or more mixture;
Described photoinitiator b is any one or two or more mixture in BASF BASF light trigger Irgacure2959, IRGACURE500 or IRGACURE819DW.
2. the strippable property nail polish glue of a kind of improvement according to claim 1, is characterized in that calculating by weight, its raw material composition and content as follows:
Wherein, the preparation method of described UV cured resin A is:
20 parts of methyl and phenyl hydrogen-containing silicon oils and 10 parts of double pentaerythritol methacrylates are joined in a reaction vessel, then the polymerization inhibitor of 0.005 part is added, pass into protective gas, stir and heat, being warming up to 60 DEG C, adding 0.03 part of catalyst, stir lower constant temperature 3h, stop heating, treat that temperature drops to room temperature, obtain UV cured resin A;
Described UV cured resin C be double pentaerythritol methacrylate, diethylene glycol diacrylate, oxolane acrylate in mass ratio 1:1:1 composition mixture;
Described levelling agent is enlightening height TegoGlide410;
Described wetting agent is the NP-100 of LG-DOW company;
Described defoamer is the mixture of German BYK-035, BYK-037 1:1 in mass ratio;
Described mill base is a kind of temperature sensing color changing color slurry of changeable colour;
Described light trigger A be BASF Irgacure1173, Irgacure184D, IrgacureTPO in mass ratio 1:1:1 composition mixture;
Described photoinitiator b be BASF BASF light trigger Irgacure2959, IRGACURE500 in mass ratio 1:1 composition mixture.
3. the strippable property nail polish glue of a kind of improvement according to claim 1, is characterized in that calculating by weight, its raw material composition and content as follows:
Wherein, the preparation method of described UV cured resin A is:
Above-mentioned 60 parts of methyl and phenyl hydrogen-containing silicon oils and 20 parts of double pentaerythritol methacrylates are joined in a reaction vessel, add the polymerization inhibitor of 0.01 part again, pass into protective gas, stir and heat, being warming up to 60 DEG C, adding 0.05 part of catalyst, stir lower constant temperature 5h, stop heating, treat that temperature drops to room temperature, obtain UV cured resin A;
Described UV cured resin C be double pentaerythritol methacrylate, diethylene glycol diacrylate, oxolane acrylate in mass ratio 2:1:1 composition mixture;
Described levelling agent be German BYK-345, BYK-346 in mass ratio 1:1 composition mixture;
Described wetting agent is German BYK333;
Described defoamer be German BYK Bi Ke BYK-024, BYK-025 in mass ratio 1:1 composition mixture;
Described mill base is a kind of temperature sensing color changing color slurry of changeable colour;
Described light trigger A is BASF Irgacure184D, IrgacureTPO, Irgacure369 1:1:1 many kinds of mixture in mass ratio;
Described photoinitiator b be BASF BASF light trigger Irgacure2959, IRGACURE500 in mass ratio 2:1 composition mixture.
4. the preparation method of the strippable property nail polish glue of a kind of improvement described in claim, is characterized in that comprising the steps:
1) UV cured resin A, UV cured resin B, reactive diluent, levelling agent, wetting agent, defoamer, mill base and light trigger is taken according to parts by weight;
2) in the high speed dispersor controlling rotating speed 300-400r/min, wetting agent, levelling agent, defoamer and mill base is added, after disperseing 15-20min under 600-800r/min rotating speed, rotating speed is down to 250 ~ 350r/min, add UV cured resin A, UV cured resin B and light trigger A, photoinitiator b, continue dispersion 5-10min, mix homogeneously, the strippable property nail polish glue be namely improved.
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| CN201610099313.6A CN105560082B (en) | 2016-02-23 | 2016-02-23 | Improved strippable property nail polish glue and preparation method thereof |
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| CN201610099313.6A CN105560082B (en) | 2016-02-23 | 2016-02-23 | Improved strippable property nail polish glue and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107281010A (en) * | 2017-06-23 | 2017-10-24 | 梁萍 | A kind of nail polish glue containing plants essential oil and preparation method thereof |
| CN108586754A (en) * | 2018-05-14 | 2018-09-28 | 中科广化（重庆）新材料研究院有限公司 | A kind of hyperbranched silicone acrylic resin and the preparation method and application thereof |
| CN110204726A (en) * | 2019-06-11 | 2019-09-06 | 上海本诺电子材料有限公司 | A kind of preparation method of organosilicon modified crylic acid resin |
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| JP2006327941A (en) * | 2005-05-23 | 2006-12-07 | Daito Kasei Kogyo Kk | Aqueous nail polish |
| CN105125421A (en) * | 2015-09-29 | 2015-12-09 | 上海应用技术学院 | UV solidified water-based strippable polish gum and preparation method thereof |
| CN105213221A (en) * | 2015-10-08 | 2016-01-06 | 上海应用技术学院 | A kind of quick-drying nail polish glue and preparation method thereof |
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2016
- 2016-02-23 CN CN201610099313.6A patent/CN105560082B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2006327941A (en) * | 2005-05-23 | 2006-12-07 | Daito Kasei Kogyo Kk | Aqueous nail polish |
| CN105125421A (en) * | 2015-09-29 | 2015-12-09 | 上海应用技术学院 | UV solidified water-based strippable polish gum and preparation method thereof |
| CN105213221A (en) * | 2015-10-08 | 2016-01-06 | 上海应用技术学院 | A kind of quick-drying nail polish glue and preparation method thereof |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107281010A (en) * | 2017-06-23 | 2017-10-24 | 梁萍 | A kind of nail polish glue containing plants essential oil and preparation method thereof |
| CN108586754A (en) * | 2018-05-14 | 2018-09-28 | 中科广化（重庆）新材料研究院有限公司 | A kind of hyperbranched silicone acrylic resin and the preparation method and application thereof |
| CN110204726A (en) * | 2019-06-11 | 2019-09-06 | 上海本诺电子材料有限公司 | A kind of preparation method of organosilicon modified crylic acid resin |
| CN110204726B (en) * | 2019-06-11 | 2022-02-11 | 上海本诺电子材料有限公司 | Preparation method of organic silicon modified acrylic resin |
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| CN105560082B (en) | 2019-03-05 |
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