CN103666097A - UV printing ink for silk-screen printing and preparation method thereof - Google Patents
UV printing ink for silk-screen printing and preparation method thereof Download PDFInfo
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- CN103666097A CN103666097A CN201310601045.XA CN201310601045A CN103666097A CN 103666097 A CN103666097 A CN 103666097A CN 201310601045 A CN201310601045 A CN 201310601045A CN 103666097 A CN103666097 A CN 103666097A
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- printing ink
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- phenyl ketone
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- 238000007650 screen-printing Methods 0.000 title claims abstract description 16
- 238000002360 preparation method Methods 0.000 title claims description 8
- 238000007639 printing Methods 0.000 title abstract 6
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 claims abstract description 14
- 239000002994 raw material Substances 0.000 claims abstract description 9
- 239000004721 Polyphenylene oxide Substances 0.000 claims abstract description 7
- DAKWPKUUDNSNPN-UHFFFAOYSA-N Trimethylolpropane triacrylate Chemical compound C=CC(=O)OCC(CC)(COC(=O)C=C)COC(=O)C=C DAKWPKUUDNSNPN-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229910052782 aluminium Inorganic materials 0.000 claims abstract description 7
- 239000004411 aluminium Substances 0.000 claims abstract description 7
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000003822 epoxy resin Substances 0.000 claims abstract description 7
- YDKNBNOOCSNPNS-UHFFFAOYSA-N methyl 1,3-benzoxazole-2-carboxylate Chemical compound C1=CC=C2OC(C(=O)OC)=NC2=C1 YDKNBNOOCSNPNS-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229910052901 montmorillonite Inorganic materials 0.000 claims abstract description 7
- 229920002037 poly(vinyl butyral) polymer Polymers 0.000 claims abstract description 7
- 229920000647 polyepoxide Polymers 0.000 claims abstract description 7
- 229920000570 polyether Polymers 0.000 claims abstract description 7
- KCTAWXVAICEBSD-UHFFFAOYSA-N prop-2-enoyloxy prop-2-eneperoxoate Chemical compound C=CC(=O)OOOC(=O)C=C KCTAWXVAICEBSD-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 6
- -1 acrylic ester Chemical class 0.000 claims abstract description 5
- 239000006087 Silane Coupling Agent Substances 0.000 claims abstract description 4
- 238000003756 stirring Methods 0.000 claims description 15
- 238000006243 chemical reaction Methods 0.000 claims description 10
- 239000002585 base Substances 0.000 claims description 9
- RWCCWEUUXYIKHB-UHFFFAOYSA-N benzophenone Chemical compound C=1C=CC=CC=1C(=O)C1=CC=CC=C1 RWCCWEUUXYIKHB-UHFFFAOYSA-N 0.000 claims description 9
- 239000012752 auxiliary agent Substances 0.000 claims description 7
- OEOIWYCWCDBOPA-UHFFFAOYSA-N 6-methyl-heptanoic acid Chemical compound CC(C)CCCCC(O)=O OEOIWYCWCDBOPA-UHFFFAOYSA-N 0.000 claims description 6
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims description 6
- DHKHKXVYLBGOIT-UHFFFAOYSA-N acetaldehyde Diethyl Acetal Natural products CCOC(C)OCC DHKHKXVYLBGOIT-UHFFFAOYSA-N 0.000 claims description 6
- 125000002777 acetyl group Chemical class [H]C([H])([H])C(*)=O 0.000 claims description 6
- 239000000975 dye Substances 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- HDZGCSFEDULWCS-UHFFFAOYSA-N monomethylhydrazine Chemical compound CNN HDZGCSFEDULWCS-UHFFFAOYSA-N 0.000 claims description 6
- 239000000049 pigment Substances 0.000 claims description 6
- 239000000843 powder Substances 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 4
- YXIWHUQXZSMYRE-UHFFFAOYSA-N 1,3-benzothiazole-2-thiol Chemical compound C1=CC=C2SC(S)=NC2=C1 YXIWHUQXZSMYRE-UHFFFAOYSA-N 0.000 claims description 3
- KDVYCTOWXSLNNI-UHFFFAOYSA-N 4-t-Butylbenzoic acid Chemical compound CC(C)(C)C1=CC=C(C(O)=O)C=C1 KDVYCTOWXSLNNI-UHFFFAOYSA-N 0.000 claims description 3
- 244000077995 Coix lacryma jobi Species 0.000 claims description 3
- 229920002367 Polyisobutene Polymers 0.000 claims description 3
- ZTHYODDOHIVTJV-UHFFFAOYSA-N Propyl gallate Chemical compound CCCOC(=O)C1=CC(O)=C(O)C(O)=C1 ZTHYODDOHIVTJV-UHFFFAOYSA-N 0.000 claims description 3
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 3
- APZPSKFMSWZPKL-UHFFFAOYSA-N [3-hydroxy-2,2-bis(hydroxymethyl)propyl] 2-methylprop-2-enoate Chemical compound CC(=C)C(=O)OCC(CO)(CO)CO APZPSKFMSWZPKL-UHFFFAOYSA-N 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 239000010445 mica Substances 0.000 claims description 3
- 229910052618 mica group Inorganic materials 0.000 claims description 3
- SLCVBVWXLSEKPL-UHFFFAOYSA-N neopentyl glycol Chemical compound OCC(C)(C)CO SLCVBVWXLSEKPL-UHFFFAOYSA-N 0.000 claims description 3
- 229940117969 neopentyl glycol Drugs 0.000 claims description 3
- 229920005989 resin Polymers 0.000 claims description 3
- 239000011347 resin Substances 0.000 claims description 3
- 229910000077 silane Inorganic materials 0.000 claims description 3
- 239000002002 slurry Substances 0.000 claims description 3
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 3
- 238000001035 drying Methods 0.000 abstract description 3
- BAVYZALUXZFZLV-UHFFFAOYSA-N Methylamine Chemical compound NC BAVYZALUXZFZLV-UHFFFAOYSA-N 0.000 abstract 2
- 239000012956 1-hydroxycyclohexylphenyl-ketone Substances 0.000 abstract 1
- MQDJYUACMFCOFT-UHFFFAOYSA-N bis[2-(1-hydroxycyclohexyl)phenyl]methanone Chemical compound C=1C=CC=C(C(=O)C=2C(=CC=CC=2)C2(O)CCCCC2)C=1C1(O)CCCCC1 MQDJYUACMFCOFT-UHFFFAOYSA-N 0.000 abstract 1
- 238000005265 energy consumption Methods 0.000 abstract 1
- 239000012860 organic pigment Substances 0.000 abstract 1
- 239000000976 ink Substances 0.000 description 23
- 238000000034 method Methods 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 240000001624 Espostoa lanata Species 0.000 description 2
- 235000009161 Espostoa lanata Nutrition 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000004744 fabric Substances 0.000 description 2
- XXMIOPMDWAUFGU-UHFFFAOYSA-N hexane-1,6-diol Chemical compound OCCCCCCO XXMIOPMDWAUFGU-UHFFFAOYSA-N 0.000 description 2
- 239000002932 luster Substances 0.000 description 2
- 238000006116 polymerization reaction Methods 0.000 description 2
- 101000831616 Homo sapiens Protachykinin-1 Proteins 0.000 description 1
- 240000008415 Lactuca sativa Species 0.000 description 1
- 206010034972 Photosensitivity reaction Diseases 0.000 description 1
- 102100024304 Protachykinin-1 Human genes 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 239000003344 environmental pollutant Substances 0.000 description 1
- 238000005530 etching Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 238000010428 oil painting Methods 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 238000000016 photochemical curing Methods 0.000 description 1
- 230000036211 photosensitivity Effects 0.000 description 1
- 231100000719 pollutant Toxicity 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 235000012045 salad Nutrition 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 229920002994 synthetic fiber Polymers 0.000 description 1
- 239000004758 synthetic textile Substances 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 238000002211 ultraviolet spectrum Methods 0.000 description 1
Landscapes
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses a UV printing ink for silk-screen printing. The UV printing ink is characterized by being prepared from the following raw materials in parts by weight: 1 to 3 parts of organic pigment, 10 to 12 parts of neopentyl glycol diacrylate, 1 to 2 parts of aluminium isocaprylate, 2 to 3 parts of aluminium chloride, 1 to 2 parts of na-montmorillonite, 25 to 30 parts of epoxy acrylate, 1 to 2 parts of polyvinyl butyral, 5 to 8 parts of 1-hydroxy-cyclohexyl phenyl ketone, 10 to 12 parts of polyether acrylic ester, 6 to 9 parts of 1,6-HDDA, 10 to 12 parts of trimethylolpropane triacrylate, 13 to 17 parts of E-42 epoxy resin, 3 to 4 parts of metanilic methylamine, 1 to 2 parts of an accelerant M, 1 to 2 parts of a silane coupling agent KH-550 and 4 to 5 parts of an addition agent. The addition agent improves the toughness of the printing ink, enables the printing ink to be dispersed uniformly, and maintains the stability of the printing ink; the raw materials are rich in source, low in price, convenient to use and low in cost, the product quality is easy to control, the drying speed is high, and the energy consumption is low.
Description
Technical field
The present invention relates to a kind of ink and preparation method thereof, particularly UV ink and preparation method thereof for a kind of silk screen printing.
Background technology
Silk screen printing is that silk fabrics, synthetic fabrics or wire cloth are stretched tight on screen frame, adopts manual method of carving paint film or photochemistry plate-making to make screen printing forme.Modern screen printing technique, to utilize sensitive materials by photomechanical method, to make the flat carriers such as screen printing forme (making the silk screen hole of picture and text part on screen printing forme is through hole, and the silk screen hole of non-graphic part is plugged) oil painting, etching, pictorial poster, business card, binding and layout front cover, commodity packaging, product tag, dyeing textile product, glass and metal etc.
Ultraviolet light polymerization (UV) ink refers under uviolizing, utilizes the UV-light of different wave length and energy to make ink film forming and dry ink.Utilize different UV spectrum, can produce different-energy, the monomer polymerization in different ink vehicles is become to polymkeric substance, so the look film of UV ink has good machinery and chemical property.The major advantage of UV ink has: (1) is without solvent; (2) rate of drying is fast, and power consumption is few; (3) good luster, bright in luster; (4) water-fast, resistance to solvent, wear resisting property is good.In UV ink, light trigger is a kind of light activated compound that is subject to, and after absorb light is shone, is excited into free radical, and energy is transferred to photosensitivity molecule or photocrosslinking agent, makes UV China ink that photocuring reaction occur.UV China ink has become a kind of more ripe ink technology at present, and its pollutant emission is almost nil.Except not containing solvent, UV China ink is also just like being difficult for scumming, and site is clear, the bright-coloured light of mass colour, the advantage such as chemical resistance is excellent, low-consuming.
Summary of the invention
The object of this invention is to provide UV ink and preparation method thereof for a kind of silk screen printing.
In order to realize object of the present invention, the present invention passes through following scheme implementation:
A kind of silk screen printing UV ink, raw material by following weight part is made: pigment dyestuff 1-3, neopentylglycol diacrylate 10-12, isocaprylic acid aluminium 1-2, aluminum chloride 2-3, na-montmorillonite 1-2, epoxy acrylate 25-30, polyvinyl butyral acetal 1-2,1-hydroxyl-ring base in the sixth of the twelve Earthly Branches phenyl ketone 5-8, polyether acrylate 10-12,1,6 hexanediol diacrylate 6-9, Viscoat 295 10-12, E-42 epoxy resin 13-17, amino methylamine 3-4, captax 1-2, silane resin acceptor kh-550 1-2, auxiliary agent 4-5;
Described auxiliary agent is prepared from by the raw material of following weight part: nano diatomite powder 0.2-0.3, nano mica powder 0.2-0.3, double pentaerythritol methacrylate 10-12, neopentyl glycol 5-7, p-tert-butyl benzoic acid 1-2, linking agent TAC2-3, polyisobutene 2-3, silane coupling agent KH560 1-2, Tenox PG 2-3, coix seed oil 1-2; Its preparation method is by each mixing of materials, is heated to 60-70 ℃, and stirring reaction 30-40 minute, obtains.
Silk screen printing of the present invention UV ink, by following concrete steps, made: first add pigment dyestuff, neopentylglycol diacrylate, isocaprylic acid aluminium, aluminum chloride, na-montmorillonite, epoxy acrylate, polyvinyl butyral acetal, polyether acrylate, 1,6-hexanediyl ester, Viscoat 295, E-42 epoxy resin, an amino methylamine stirring and evenly mixing, be heated to 80-90 ℃, stir 25-35 minute; Then add all the other remaining components except 1-hydroxyl-ring base in the sixth of the twelve Earthly Branches phenyl ketone, stirring reaction 3-5 hour; Finally be cooled to 60-70 ℃, add 1-hydroxyl-ring base in the sixth of the twelve Earthly Branches phenyl ketone, stirring reaction 40-50 minute, cooling after, grind and to obtain 20-40 μ m slurry, obtain.
The invention has the beneficial effects as follows: auxiliary agent of the present invention has improved the toughness of ink, make distributes ink even, and maintained the stability of ink; Raw material sources of the present invention are abundant, and cheap, easy to use, cost is low, and quality product is easily controlled, and rate of drying is fast, and power consumption is few.
Specific embodiments
Below by specific examples, the present invention is described in detail.
A kind of silk screen printing UV ink, by following weight part (kilogram) raw material make: pigment dyestuff 1, neopentylglycol diacrylate 10, isocaprylic acid aluminium 1, aluminum chloride 2, na-montmorillonite 1, epoxy acrylate 25, polyvinyl butyral acetal 1,1-hydroxyl-ring base in the sixth of the twelve Earthly Branches phenyl ketone 5, polyether acrylate 10,1,6 hexanediol diacrylate 6, Viscoat 295 10, E-42 epoxy resin 13, an amino methylamine 3, captax 1, silane resin acceptor kh-550 1, auxiliary agent 4;
Described auxiliary agent by following weight part (kilogram) raw material be prepared from: nano diatomite powder 0.2, nano mica powder 0.2, double pentaerythritol methacrylate 10, neopentyl glycol 5, p-tert-butyl benzoic acid 1, linking agent TAC2, polyisobutene 2, silane coupling agent KH560 1, Tenox PG 2, coix seed oil 1; Its preparation method is by each mixing of materials, is heated to 60-70 ℃, and stirring reaction 30-40 minute, obtains.
Silk screen printing of the present invention UV ink, by following concrete steps, made: first add pigment dyestuff, neopentylglycol diacrylate, isocaprylic acid aluminium, aluminum chloride, na-montmorillonite, epoxy acrylate, polyvinyl butyral acetal, polyether acrylate, 1,6-hexanediyl ester, Viscoat 295, E-42 epoxy resin, an amino methylamine stirring and evenly mixing, be heated to 80-90 ℃, stir 25-35 minute; Then add all the other remaining components except 1-hydroxyl-ring base in the sixth of the twelve Earthly Branches phenyl ketone, stirring reaction 3-5 hour; Finally be cooled to 60-70 ℃, add 1-hydroxyl-ring base in the sixth of the twelve Earthly Branches phenyl ketone, stirring reaction 40-50 minute, cooling after, grind and to obtain 20-40 μ m slurry, obtain.
The ink of gained, is used cross-hatching ox-hide tape stripping, draws compartment apart from 1mm, and 100% adheres to; Spirituous cotton balls is soaked in use, and 300 grams of pressure wipings 50 times, are as good as shape; Be soaked in salad oil (normal temperature) 8 hours, be as good as shape; Use is soaked with the cotton balls of salt solution, and 300 grams of pressure wipings 50 times, are as good as shape.
Claims (2)
1. a silk screen printing UV ink, it is characterized in that, raw material by following weight part is made: pigment dyestuff 1-3, neopentylglycol diacrylate 10-12, isocaprylic acid aluminium 1-2, aluminum chloride 2-3, na-montmorillonite 1-2, epoxy acrylate 25-30, polyvinyl butyral acetal 1-2, 1-hydroxyl-ring base in the sixth of the twelve Earthly Branches phenyl ketone 5-8, polyether acrylate 10-12, 1, 6-hexanediyl ester 6-9, Viscoat 295 10-12, E-42 epoxy resin 13-17, between amino methylamine 3-4, captax 1-2, silane resin acceptor kh-550 1-2, auxiliary agent 4-5,
Described auxiliary agent is prepared from by the raw material of following weight part: nano diatomite powder 0.2-0.3, nano mica powder 0.2-0.3, double pentaerythritol methacrylate 10-12, neopentyl glycol 5-7, p-tert-butyl benzoic acid 1-2, linking agent TAC2-3, polyisobutene 2-3, silane coupling agent KH560 1-2, Tenox PG 2-3, coix seed oil 1-2; Its preparation method is by each mixing of materials, is heated to 60-70 ℃, and stirring reaction 30-40 minute, obtains.
2. silk screen printing UV ink according to claim 1, it is characterized in that, by following concrete steps, made: first add pigment dyestuff, neopentylglycol diacrylate, isocaprylic acid aluminium, aluminum chloride, na-montmorillonite, epoxy acrylate, polyvinyl butyral acetal, polyether acrylate, 1,6-hexanediyl ester, Viscoat 295, E-42 epoxy resin, an amino methylamine stirring and evenly mixing, be heated to 80-90 ℃, stir 25-35 minute; Then add all the other remaining components except 1-hydroxyl-ring base in the sixth of the twelve Earthly Branches phenyl ketone, stirring reaction 3-5 hour; Finally be cooled to 60-70 ℃, add 1-hydroxyl-ring base in the sixth of the twelve Earthly Branches phenyl ketone, stirring reaction 40-50 minute, cooling after, grind and to obtain 20-40 μ m slurry, obtain.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310601045.XA CN103666097A (en) | 2013-11-25 | 2013-11-25 | UV printing ink for silk-screen printing and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310601045.XA CN103666097A (en) | 2013-11-25 | 2013-11-25 | UV printing ink for silk-screen printing and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103666097A true CN103666097A (en) | 2014-03-26 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310601045.XA Pending CN103666097A (en) | 2013-11-25 | 2013-11-25 | UV printing ink for silk-screen printing and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103666097A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107629540A (en) * | 2017-08-30 | 2018-01-26 | 王琪宇 | A kind of preparation method of light-curable ink |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1970656A (en) * | 2006-11-23 | 2007-05-30 | 北京印刷学院 | Thermoforming plastic printing ink adopting ultraviolet-infra red drying technology |
| CN102382514A (en) * | 2011-11-04 | 2012-03-21 | 江苏泰格油墨有限公司 | Ink for replacing aluminum foil lining paper and preparation method thereof |
| CN103342921A (en) * | 2013-07-29 | 2013-10-09 | 中国科学院化学研究所 | Ink with high hiding rate for ink-jet printing and application thereof to preparation of flexible plate |
-
2013
- 2013-11-25 CN CN201310601045.XA patent/CN103666097A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1970656A (en) * | 2006-11-23 | 2007-05-30 | 北京印刷学院 | Thermoforming plastic printing ink adopting ultraviolet-infra red drying technology |
| CN102382514A (en) * | 2011-11-04 | 2012-03-21 | 江苏泰格油墨有限公司 | Ink for replacing aluminum foil lining paper and preparation method thereof |
| CN103342921A (en) * | 2013-07-29 | 2013-10-09 | 中国科学院化学研究所 | Ink with high hiding rate for ink-jet printing and application thereof to preparation of flexible plate |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107629540A (en) * | 2017-08-30 | 2018-01-26 | 王琪宇 | A kind of preparation method of light-curable ink |
| CN107629540B (en) * | 2017-08-30 | 2020-09-04 | 广东泰金智能包装有限公司 | Preparation method of photo-curing ink |
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| PB01 | Publication | ||
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Application publication date: 20140326 |