CN103666033B - A kind of novel UV solidifies serigraphy pearl ink and preparation method thereof - Google Patents
A kind of novel UV solidifies serigraphy pearl ink and preparation method thereof Download PDFInfo
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- CN103666033B CN103666033B CN201310593195.0A CN201310593195A CN103666033B CN 103666033 B CN103666033 B CN 103666033B CN 201310593195 A CN201310593195 A CN 201310593195A CN 103666033 B CN103666033 B CN 103666033B
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- serigraphy
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- cyclohexyl
- hydroxy
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- 238000002360 preparation method Methods 0.000 title claims description 8
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 14
- DAKWPKUUDNSNPN-UHFFFAOYSA-N Trimethylolpropane triacrylate Chemical compound C=CC(=O)OCC(CC)(COC(=O)C=C)COC(=O)C=C DAKWPKUUDNSNPN-UHFFFAOYSA-N 0.000 claims abstract description 10
- LJRSZGKUUZPHEB-UHFFFAOYSA-N 2-[2-(2-prop-2-enoyloxypropoxy)propoxy]propyl prop-2-enoate Chemical compound C=CC(=O)OC(C)COC(C)COC(C)COC(=O)C=C LJRSZGKUUZPHEB-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000004925 Acrylic resin Substances 0.000 claims abstract description 7
- 229920000178 Acrylic resin Polymers 0.000 claims abstract description 7
- 239000003513 alkali Substances 0.000 claims abstract description 7
- DIZPMCHEQGEION-UHFFFAOYSA-H aluminium sulfate (anhydrous) Chemical compound [Al+3].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O DIZPMCHEQGEION-UHFFFAOYSA-H 0.000 claims abstract description 7
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 7
- UHESRSKEBRADOO-UHFFFAOYSA-N ethyl carbamate;prop-2-enoic acid Chemical compound OC(=O)C=C.CCOC(N)=O UHESRSKEBRADOO-UHFFFAOYSA-N 0.000 claims abstract description 7
- 235000011187 glycerol Nutrition 0.000 claims abstract description 7
- 239000012860 organic pigment Substances 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 229920001169 thermoplastic Polymers 0.000 claims abstract description 7
- 239000004416 thermosoftening plastic Substances 0.000 claims abstract description 7
- WPYCRFCQABTEKC-UHFFFAOYSA-N Diglycidyl resorcinol ether Chemical compound C1OC1COC(C=1)=CC=CC=1OCC1CO1 WPYCRFCQABTEKC-UHFFFAOYSA-N 0.000 claims abstract description 4
- IAXXETNIOYFMLW-COPLHBTASA-N [(1s,3s,4s)-4,7,7-trimethyl-3-bicyclo[2.2.1]heptanyl] 2-methylprop-2-enoate Chemical compound C1C[C@]2(C)[C@@H](OC(=O)C(=C)C)C[C@H]1C2(C)C IAXXETNIOYFMLW-COPLHBTASA-N 0.000 claims abstract description 4
- AFZSMODLJJCVPP-UHFFFAOYSA-N dibenzothiazol-2-yl disulfide Chemical compound C1=CC=C2SC(SSC=3SC4=CC=CC=C4N=3)=NC2=C1 AFZSMODLJJCVPP-UHFFFAOYSA-N 0.000 claims abstract description 4
- 229940119545 isobornyl methacrylate Drugs 0.000 claims abstract description 4
- VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 claims abstract description 4
- 229910001862 magnesium hydroxide Inorganic materials 0.000 claims abstract description 4
- 239000000347 magnesium hydroxide Substances 0.000 claims abstract description 4
- 238000003756 stirring Methods 0.000 claims description 15
- 238000006243 chemical reaction Methods 0.000 claims description 9
- YSVQGHIOJPVICX-UHFFFAOYSA-N 1-(1-hydroxycyclohexyl)-1-phenylpropan-2-one Chemical compound C1CCCCC1(O)C(C(=O)C)C1=CC=CC=C1 YSVQGHIOJPVICX-UHFFFAOYSA-N 0.000 claims description 6
- ZTHYODDOHIVTJV-UHFFFAOYSA-N Propyl gallate Chemical compound CCCOC(=O)C1=CC(O)=C(O)C(O)=C1 ZTHYODDOHIVTJV-UHFFFAOYSA-N 0.000 claims description 6
- 239000012467 final product Substances 0.000 claims description 6
- 239000000843 powder Substances 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 4
- 150000005208 1,4-dihydroxybenzenes Chemical class 0.000 claims description 3
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 3
- 244000077995 Coix lacryma jobi Species 0.000 claims description 3
- FQYUMYWMJTYZTK-UHFFFAOYSA-N Phenyl glycidyl ether Chemical compound C1OC1COC1=CC=CC=C1 FQYUMYWMJTYZTK-UHFFFAOYSA-N 0.000 claims description 3
- 229920002367 Polyisobutene Polymers 0.000 claims description 3
- 239000006087 Silane Coupling Agent Substances 0.000 claims description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 239000003431 cross linking reagent Substances 0.000 claims description 3
- 239000010445 mica Substances 0.000 claims description 3
- 229910052618 mica group Inorganic materials 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- GEMHFKXPOCTAIP-UHFFFAOYSA-N n,n-dimethyl-n'-phenylcarbamimidoyl chloride Chemical compound CN(C)C(Cl)=NC1=CC=CC=C1 GEMHFKXPOCTAIP-UHFFFAOYSA-N 0.000 claims description 3
- 235000010388 propyl gallate Nutrition 0.000 claims description 3
- 239000002002 slurry Substances 0.000 claims description 3
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 3
- 230000000694 effects Effects 0.000 abstract description 5
- 238000007639 printing Methods 0.000 abstract description 5
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 239000000853 adhesive Substances 0.000 abstract description 2
- 230000001070 adhesive effect Effects 0.000 abstract description 2
- 238000010438 heat treatment Methods 0.000 abstract description 2
- 238000007650 screen-printing Methods 0.000 description 4
- 238000000034 method Methods 0.000 description 3
- 240000001624 Espostoa lanata Species 0.000 description 2
- 235000009161 Espostoa lanata Nutrition 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 101000831616 Homo sapiens Protachykinin-1 Proteins 0.000 description 1
- 240000008415 Lactuca sativa Species 0.000 description 1
- 102100024304 Protachykinin-1 Human genes 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 238000004134 energy conservation Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000005530 etching Methods 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000010428 oil painting Methods 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 235000012045 salad Nutrition 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 229920002994 synthetic fiber Polymers 0.000 description 1
- 239000004758 synthetic textile Substances 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
Landscapes
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses a kind of novel UV and solidify serigraphy pearl ink, it is characterized in that, made by the raw material of following weight portion: organic pigment 2-3, glycerine 6-10, aluminum sulfate 3-4, flower bulb alkali 1-2, urethane acrylate 21-23, tri (propylene glycol) diacrylate 12-15, trimethylolpropane triacrylate 8-10, thermoplastic acrylic resin 12-15, isobornyl methacrylate 11-13,1-hydroxy-cyclohexyl phenylacetone 5-8, magnesium hydroxide 1-2, resorcinol bisglycidyl ether 12-15, altax 1-2, auxiliary agent 4-5; Between the present invention and each stock, all have good adhesive force, hardening time is short, does not need heating, saves energy resource consumption, can obtain good printing effect at hard ground and soft ground, is applicable to the multiple mode of production and production requirement, high comprehensive performance.
Description
Technical field
The present invention relates to a kind of ink and preparation method thereof, particularly a kind of novel UV solidifies serigraphy pearl ink and preparation method thereof.
Background technology
Serigraphy is that silk fabrics, synthetic fabrics or woven wire are stretched tight on screen frame, adopts manual method of carving paint film or photochemistry plate-making to make screen printing forme. Modern screen printing technique, to utilize photosensitive material to make the flat carriers such as screen printing forme (the silk screen hole that makes picture and text part on screen printing forme is through hole, and the silk screen hole of non-graphic part is plugged) oil painting, etching, pictorial poster, business card, binding and layout front cover, commodity packaging, product tag, dyeing textile product, glass and metal etc. by photomechanical method.
Pearlescent pigment is as a kind of mode of printing of special-effect, rely on its unique pearly luster, make printed matter surface produce graceful unique, the soft pleasing reward effect of looking, there is the characteristic of anti-duplicating simultaneously, there is certain antifalse effect, in numerous mode of printings, take the course of its own, become popular one false proof with decorating printing technology. The application of pearly-lustre silk-screen ink can well embody the distinctive effect of pearly-lustre, is widely applied in fields such as banknote, security, Package and labels.
UV curable ink due in system containing solvent, there is efficient, wide adaptability, economy, energy-conservation, environmental friendliness, become tool novel ink with broad prospects for development.
Summary of the invention
The object of this invention is to provide a kind of novel UV and solidify serigraphy pearl ink and preparation method thereof.
In order to realize object of the present invention, the present invention passes through following scheme implementation:
A kind of novel UV solidifies serigraphy pearl ink, is made up: organic pigment 2-3, glycerine 6-10, aluminum sulfate 3-4, flower bulb alkali 1-2, urethane acrylate 21-23, tri (propylene glycol) diacrylate 12-15, trimethylolpropane triacrylate 8-10, thermoplastic acrylic resin 12-15, isobornyl methacrylate 11-13,1-hydroxy-cyclohexyl phenylacetone 5-8, magnesium hydroxide 1-2, resorcinol bisglycidyl ether 12-15, altax 1-2, auxiliary agent 4-5 of the raw material of following weight portion;
Described auxiliary agent is prepared from by the raw material of following weight portion: nano diatomite powder 0.2-0.3, nano mica powder 0.2-0.3, Silane coupling agent KH550 2-3, crosslinking agent TAC2-3, polyisobutene 2-3, hydroquinones 1-2, trimethylolpropane triacrylate 10-12, acrylic acid dimethylamino ethyl ester 2-3, phenyl glycidyl ether 1-2, cobalt naphthenate 2-3, n-propyl gallate 2-3, coix seed oil 1-2; Its preparation method is by each mixing of materials, is heated to 60-70 DEG C, and stirring reaction 30-40 minute, to obtain final product.
Novel UV of the present invention solidifies serigraphy pearl ink, made by following concrete steps: first add organic pigment, glycerine, aluminum sulfate, flower bulb alkali, urethane acrylate, tri (propylene glycol) diacrylate, trimethylolpropane triacrylate, thermoplastic acrylic resin to stir and evenly mix, be heated to 80-90 DEG C, stir 25-35 minute; Then add all the other residual components except 1-hydroxy-cyclohexyl phenylacetone, stirring reaction 3-5 hour; Finally be cooled to 60-70 DEG C, add 1-hydroxy-cyclohexyl phenylacetone, stirring reaction 40-50 minute, cooling after, grind obtain 20-40 μ m slurry, to obtain final product.
The invention has the beneficial effects as follows: between the present invention and each stock, all have good adhesive force, hardening time is short, do not need heating, save energy resource consumption, good printing effect be can obtain at hard ground and soft ground, the multiple mode of production and production requirement are applicable to, high comprehensive performance.
Specific embodiments
Below by instantiation, the present invention is described in detail.
A kind of novel UV solidifies serigraphy pearl ink, by following weight portion (kilogram) raw material make: organic pigment 2, glycerine 6, aluminum sulfate 3, flower bulb alkali 1, urethane acrylate 21, tri (propylene glycol) diacrylate 12, trimethylolpropane triacrylate 8, thermoplastic acrylic resin 12, isobornyl methacrylate 11,1-hydroxy-cyclohexyl phenylacetone 5, magnesium hydroxide 1, resorcinol bisglycidyl ether 12, altax 1, auxiliary agent 4;
Described auxiliary agent by following weight portion (kilogram) raw material be prepared from: nano diatomite powder 0.2, nano mica powder 0.2, Silane coupling agent KH550 2, crosslinking agent TAC2, polyisobutene 2, hydroquinones 1, trimethylolpropane triacrylate 10, acrylic acid dimethylamino ethyl ester 2, phenyl glycidyl ether 1, cobalt naphthenate 2, n-propyl gallate 2, coix seed oil 1; Its preparation method is by each mixing of materials, is heated to 60-70 DEG C, and stirring reaction 30-40 minute, to obtain final product.
Novel UV of the present invention solidifies serigraphy pearl ink, made by following concrete steps: first add organic pigment, glycerine, aluminum sulfate, flower bulb alkali, urethane acrylate, tri (propylene glycol) diacrylate, trimethylolpropane triacrylate, thermoplastic acrylic resin to stir and evenly mix, be heated to 80-90 DEG C, stir 25-35 minute; Then add all the other residual components except 1-hydroxy-cyclohexyl phenylacetone, stirring reaction 3-5 hour; Finally be cooled to 60-70 DEG C, add 1-hydroxy-cyclohexyl phenylacetone, stirring reaction 40-50 minute, cooling after, grind obtain 20-40 μ m slurry, to obtain final product.
The ink of gained, uses cross-hatching ox-hide tape stripping, draws compartment apart from 1mm, and 100% adheres to; Spirituous cotton balls is soaked in use, and 300 grams of pressure wipings 50 times, are as good as shape; Be soaked in salad oil (normal temperature) 8 hours, be as good as shape; Use is soaked with the cotton balls of salt solution, and 300 grams of pressure wipings 50 times, are as good as shape.
Claims (2)
1. a novel UV solidifies serigraphy pearl ink, it is characterized in that, be prepared from by the raw material of following weight portion: organic pigment 2-3, glycerine 6-10, aluminum sulfate 3-4, flower bulb alkali 1-2, urethane acrylate 21-23, tri (propylene glycol) diacrylate 12-15, trimethylolpropane triacrylate 8-10, thermoplastic acrylic resin 12-15, isobornyl methacrylate 11-13,1-hydroxy-cyclohexyl phenylacetone 5-8, magnesium hydroxide 1-2, resorcinol bisglycidyl ether 12-15, altax 1-2, auxiliary agent 4-5;
Described auxiliary agent is prepared from by the raw material of following weight portion: nano diatomite powder 0.2-0.3, nano mica powder 0.2-0.3, Silane coupling agent KH550 2-3, crosslinking agent TAC2-3, polyisobutene 2-3, hydroquinones 1-2, trimethylolpropane triacrylate 10-12, acrylic acid dimethylamino ethyl ester 2-3, phenyl glycidyl ether 1-2, cobalt naphthenate 2-3, n-propyl gallate 2-3, coix seed oil 1-2; Its preparation method is by each mixing of materials, is heated to 60-70 DEG C, and stirring reaction 30-40 minute, to obtain final product.
2. novel UV solidifies serigraphy pearl ink according to claim 1, it is characterized in that, made by following concrete steps: first add organic pigment, glycerine, aluminum sulfate, flower bulb alkali, urethane acrylate, tri (propylene glycol) diacrylate, trimethylolpropane triacrylate, thermoplastic acrylic resin to stir and evenly mix, be heated to 80-90 DEG C, stir 25-35 minute; Then add all the other residual components except 1-hydroxy-cyclohexyl phenylacetone, stirring reaction 3-5 hour; Finally be cooled to 60-70 DEG C, add 1-hydroxy-cyclohexyl phenylacetone, stirring reaction 40-50 minute, cooling after, grind obtain 20-40 μ m slurry, to obtain final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310593195.0A CN103666033B (en) | 2013-11-23 | 2013-11-23 | A kind of novel UV solidifies serigraphy pearl ink and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310593195.0A CN103666033B (en) | 2013-11-23 | 2013-11-23 | A kind of novel UV solidifies serigraphy pearl ink and preparation method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN103666033A CN103666033A (en) | 2014-03-26 |
| CN103666033B true CN103666033B (en) | 2016-05-04 |
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Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105315769B (en) * | 2015-11-30 | 2017-12-19 | 佛山市高明绿色德化工有限公司 | A kind of coloured UV ink of glass |
| CN109385918B (en) * | 2018-11-12 | 2021-02-12 | 广州市珠之江环保印花材料实业有限公司 | White glue for printing and dyeing and preparation method thereof |
| CN115466541A (en) * | 2022-08-03 | 2022-12-13 | 佛山市兴洲玻璃科技有限公司 | Method for cutting tempered ink glass in different places |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101665641A (en) * | 2009-09-25 | 2010-03-10 | 林国顺 | Ultraviolet curing embossed printing ink |
| CN101974267A (en) * | 2010-11-04 | 2011-02-16 | 中钞油墨有限公司 | Aqueous ultraviolet light curing pearlescent silk screen ink and preparation method thereof |
| CN102295858A (en) * | 2010-06-25 | 2011-12-28 | 深圳市顾康力化工有限公司 | Photo-curable screen printing ink and preparation method thereof |
| CN102533000A (en) * | 2011-12-28 | 2012-07-04 | 深圳市通产丽星股份有限公司 | Ultraviolet light curing ink and preparation method thereof |
| CN102634251A (en) * | 2012-04-10 | 2012-08-15 | 中钞油墨有限公司 | Photo-curing silk screen pearly-luster ink applicable to different printing substrates and preparation method thereof |
-
2013
- 2013-11-23 CN CN201310593195.0A patent/CN103666033B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101665641A (en) * | 2009-09-25 | 2010-03-10 | 林国顺 | Ultraviolet curing embossed printing ink |
| CN102295858A (en) * | 2010-06-25 | 2011-12-28 | 深圳市顾康力化工有限公司 | Photo-curable screen printing ink and preparation method thereof |
| CN101974267A (en) * | 2010-11-04 | 2011-02-16 | 中钞油墨有限公司 | Aqueous ultraviolet light curing pearlescent silk screen ink and preparation method thereof |
| CN102533000A (en) * | 2011-12-28 | 2012-07-04 | 深圳市通产丽星股份有限公司 | Ultraviolet light curing ink and preparation method thereof |
| CN102634251A (en) * | 2012-04-10 | 2012-08-15 | 中钞油墨有限公司 | Photo-curing silk screen pearly-luster ink applicable to different printing substrates and preparation method thereof |
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| CN103666033A (en) | 2014-03-26 |
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Inventor after: Zheng Yi Inventor before: Wan Hongxia Inventor before: Chen Keliang |
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| TR01 | Transfer of patent right |
Effective date of registration: 20170508 Address after: 515410, Xinjin Road, Longhu District, Guangdong, Shantou Patentee after: Shantou Rui Chi Printing Co., Ltd. Address before: The economic development zone of Anhui province Tongling city four road 244000 No. 3201 Patentee before: Tongling Fangzheng Plastic Industrial Technology Co., Ltd. |