CN103666033A - Novel UV (ultraviolet) curing silk-screen printing pearly-luster ink and preparation method thereof - Google Patents
Novel UV (ultraviolet) curing silk-screen printing pearly-luster ink and preparation method thereof Download PDFInfo
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- CN103666033A CN103666033A CN201310593195.0A CN201310593195A CN103666033A CN 103666033 A CN103666033 A CN 103666033A CN 201310593195 A CN201310593195 A CN 201310593195A CN 103666033 A CN103666033 A CN 103666033A
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- screen printing
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- acetone
- viscoat
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- 238000007650 screen-printing Methods 0.000 title claims abstract description 16
- 238000002360 preparation method Methods 0.000 title claims description 8
- 239000002932 luster Substances 0.000 title abstract 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 20
- DAKWPKUUDNSNPN-UHFFFAOYSA-N Trimethylolpropane triacrylate Chemical compound C=CC(=O)OCC(CC)(COC(=O)C=C)COC(=O)C=C DAKWPKUUDNSNPN-UHFFFAOYSA-N 0.000 claims abstract description 10
- YSVQGHIOJPVICX-UHFFFAOYSA-N 1-(1-hydroxycyclohexyl)-1-phenylpropan-2-one Chemical compound C1CCCCC1(O)C(C(=O)C)C1=CC=CC=C1 YSVQGHIOJPVICX-UHFFFAOYSA-N 0.000 claims abstract description 7
- LJRSZGKUUZPHEB-UHFFFAOYSA-N 2-[2-(2-prop-2-enoyloxypropoxy)propoxy]propyl prop-2-enoate Chemical compound C=CC(=O)OC(C)COC(C)COC(C)COC(=O)C=C LJRSZGKUUZPHEB-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229920000178 Acrylic resin Polymers 0.000 claims abstract description 7
- 239000004925 Acrylic resin Substances 0.000 claims abstract description 7
- DIZPMCHEQGEION-UHFFFAOYSA-H aluminium sulfate (anhydrous) Chemical compound [Al+3].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O DIZPMCHEQGEION-UHFFFAOYSA-H 0.000 claims abstract description 7
- UHESRSKEBRADOO-UHFFFAOYSA-N ethyl carbamate;prop-2-enoic acid Chemical compound OC(=O)C=C.CCOC(N)=O UHESRSKEBRADOO-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 229920001169 thermoplastic Polymers 0.000 claims abstract description 7
- 239000004416 thermosoftening plastic Substances 0.000 claims abstract description 7
- 239000000463 material Substances 0.000 claims abstract description 5
- IAXXETNIOYFMLW-COPLHBTASA-N [(1s,3s,4s)-4,7,7-trimethyl-3-bicyclo[2.2.1]heptanyl] 2-methylprop-2-enoate Chemical compound C1C[C@]2(C)[C@@H](OC(=O)C(=C)C)C[C@H]1C2(C)C IAXXETNIOYFMLW-COPLHBTASA-N 0.000 claims abstract description 4
- 229940119545 isobornyl methacrylate Drugs 0.000 claims abstract description 4
- VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 claims abstract description 4
- 239000000347 magnesium hydroxide Substances 0.000 claims abstract description 4
- 229910001862 magnesium hydroxide Inorganic materials 0.000 claims abstract description 4
- 238000003756 stirring Methods 0.000 claims description 15
- 238000006243 chemical reaction Methods 0.000 claims description 9
- 239000000049 pigment Substances 0.000 claims description 7
- 239000003513 alkali Substances 0.000 claims description 6
- 239000012752 auxiliary agent Substances 0.000 claims description 6
- 239000000975 dye Substances 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- 239000000843 powder Substances 0.000 claims description 6
- GHMLBKRAJCXXBS-UHFFFAOYSA-N resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 claims description 6
- 244000077995 Coix lacryma jobi Species 0.000 claims description 3
- WPYCRFCQABTEKC-UHFFFAOYSA-N Diglycidyl resorcinol ether Chemical compound C1OC1COC(C=1)=CC=CC=1OCC1CO1 WPYCRFCQABTEKC-UHFFFAOYSA-N 0.000 claims description 3
- FQYUMYWMJTYZTK-UHFFFAOYSA-N Phenyl glycidyl ether Chemical compound C1OC1COC1=CC=CC=C1 FQYUMYWMJTYZTK-UHFFFAOYSA-N 0.000 claims description 3
- 229920002367 Polyisobutene Polymers 0.000 claims description 3
- ZTHYODDOHIVTJV-UHFFFAOYSA-N Propyl gallate Chemical compound CCCOC(=O)C1=CC(O)=C(O)C(O)=C1 ZTHYODDOHIVTJV-UHFFFAOYSA-N 0.000 claims description 3
- 239000006087 Silane Coupling Agent Substances 0.000 claims description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- AFZSMODLJJCVPP-UHFFFAOYSA-N dibenzothiazol-2-yl disulfide Chemical compound C1=CC=C2SC(SSC=3SC4=CC=CC=C4N=3)=NC2=C1 AFZSMODLJJCVPP-UHFFFAOYSA-N 0.000 claims description 3
- 239000010445 mica Substances 0.000 claims description 3
- 229910052618 mica group Inorganic materials 0.000 claims description 3
- GEMHFKXPOCTAIP-UHFFFAOYSA-N n,n-dimethyl-n'-phenylcarbamimidoyl chloride Chemical compound CN(C)C(Cl)=NC1=CC=CC=C1 GEMHFKXPOCTAIP-UHFFFAOYSA-N 0.000 claims description 3
- 239000002002 slurry Substances 0.000 claims description 3
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 3
- 230000000694 effects Effects 0.000 abstract description 5
- 238000007639 printing Methods 0.000 abstract description 5
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 239000000758 substrate Substances 0.000 abstract 2
- UUODQIKUTGWMPT-UHFFFAOYSA-N 2-fluoro-5-(trifluoromethyl)pyridine Chemical compound FC1=CC=C(C(F)(F)F)C=N1 UUODQIKUTGWMPT-UHFFFAOYSA-N 0.000 abstract 1
- 239000004115 Sodium Silicate Substances 0.000 abstract 1
- 238000005265 energy consumption Methods 0.000 abstract 1
- 235000011187 glycerol Nutrition 0.000 abstract 1
- 239000012860 organic pigment Substances 0.000 abstract 1
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 abstract 1
- 229910052911 sodium silicate Inorganic materials 0.000 abstract 1
- 238000000034 method Methods 0.000 description 3
- 240000001624 Espostoa lanata Species 0.000 description 2
- 235000009161 Espostoa lanata Nutrition 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000004744 fabric Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 101000831616 Homo sapiens Protachykinin-1 Proteins 0.000 description 1
- 240000008415 Lactuca sativa Species 0.000 description 1
- 102100024304 Protachykinin-1 Human genes 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 238000004134 energy conservation Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000005530 etching Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000010428 oil painting Methods 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 235000012045 salad Nutrition 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 229920002994 synthetic fiber Polymers 0.000 description 1
- 239000004758 synthetic textile Substances 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
Landscapes
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses novel UV (ultraviolet) curing silk-screen printing pearly-luster ink which is characterized by being prepared from the following raw materials in parts by weight: 2-3 parts of an organic pigment, 6-10 parts of glycerin, 3-4 parts of aluminum sulfate, 1-2 parts of sodium silicate, 21-23 parts of urethane acrylate, 12-15 parts of tri(propylene glycol) diacrylate, 8-10 parts of trimethylolpropane triacrylate, 12-15 parts of thermoplastic acrylic resin, 11-13 parts of isobornyl methacrylate, 5-8 parts of 1-hydroxyl cyclohexyl phenyl acetone, 1-2 parts of magnesium hydroxide, 12-15 parts of resorcinol diglycidyl ether, 1-2 parts of an accelerator DM and 4-5 parts of an aid. According to the ink, good adhesiveness with printed materials is achieved, the curing time is short, the energy consumption is reduced, very good printing effects on a hard substrate and a soft substrate can be obtained, various production modes and production requirements are met, and the comprehensive performance is excellent.
Description
Technical field
The present invention relates to a kind of ink and preparation method thereof, particularly a kind of novel UV solidifies silk screen printing pearl ink and preparation method thereof.
Background technology
Silk screen printing is that silk fabrics, synthetic fabrics or wire cloth are stretched tight on screen frame, adopts manual method of carving paint film or photochemistry plate-making to make screen printing forme.Modern screen printing technique, to utilize sensitive materials by photomechanical method, to make the flat carriers such as screen printing forme (making the silk screen hole of picture and text part on screen printing forme is through hole, and the silk screen hole of non-graphic part is plugged) oil painting, etching, pictorial poster, business card, binding and layout front cover, commodity packaging, product tag, dyeing textile product, glass and metal etc.
Pearly pigment is as a kind of mode of printing of special-effect, rely on its unique pearliness, make printed matter surface produce graceful unique, the soft pleasing reward effect of looking, the characteristic simultaneously with anti-duplicating, there is certain antifalse effect, in numerous mode of printings, take the course of its own, become popular a kind of false proof and decorating printing technology.The application of pearly-lustre silk-screen ink can well embody the distinctive effect of pearly-lustre, in fields such as banknote, security, Package and labels, is widely applied.
UV curable ink due in system containing solvent, there is efficient, wide adaptability, economy, energy-conservation, environmental friendliness, become tool novel ink with broad prospects for development.
Summary of the invention
The object of this invention is to provide a kind of novel UV and solidify silk screen printing pearl ink and preparation method thereof.
In order to realize object of the present invention, the present invention passes through following scheme implementation:
Novel UV solidifies a silk screen printing pearl ink, by the raw material of following weight part, is made: pigment dyestuff 2-3, glycerol 6-10, Tai-Ace S 150 3-4, flower bulb alkali 1-2, urethane acrylate 21-23, tri (propylene glycol) diacrylate 12-15, Viscoat 295 8-10, thermoplastic acrylic resin 12-15, isobornyl methacrylate 11-13,1-hydroxy-cyclohexyl phenyl-acetone 5-8, magnesium hydroxide 1-2, Resorcinol bisglycidyl ether 12-15, altax 1-2, auxiliary agent 4-5;
Described auxiliary agent is prepared from by the raw material of following weight part: nano diatomite powder 0.2-0.3, nano mica powder 0.2-0.3, Silane coupling agent KH550 2-3, linking agent TAC2-3, polyisobutene 2-3, Resorcinol 1-2, Viscoat 295 10-12, vinylformic acid dimethylamino ethyl ester 2-3, phenyl glycidyl ether 1-2, cobalt naphthenate 2-3, Tenox PG 2-3, coix seed oil 1-2; Its preparation method is by each mixing of materials, is heated to 60-70 ℃, and stirring reaction 30-40 minute, obtains.
Novel UV of the present invention solidifies silk screen printing pearl ink, by following concrete steps, made: first add pigment dyestuff, glycerol, Tai-Ace S 150, flower bulb alkali, urethane acrylate, tri (propylene glycol) diacrylate, Viscoat 295, thermoplastic acrylic resin stirring and evenly mixing, be heated to 80-90 ℃, stir 25-35 minute; Then add all the other remaining components except 1-hydroxy-cyclohexyl phenyl-acetone, stirring reaction 3-5 hour; Finally be cooled to 60-70 ℃, add 1-hydroxy-cyclohexyl phenyl-acetone, stirring reaction 40-50 minute, cooling after, grind and to obtain 20-40 μ m slurry, obtain.
The invention has the beneficial effects as follows: between the present invention and each stock, all have good sticking power, set time is short, do not need heating, save energy consumes, at hard ground and soft ground, good printing effect be can obtain, the multiple mode of production and production requirement are applicable to, high comprehensive performance.
Specific embodiments
Below by specific examples, the present invention is described in detail.
Novel UV solidifies a silk screen printing pearl ink, by following weight part (kilogram) raw material make: pigment dyestuff 2, glycerol 6, Tai-Ace S 150 3, flower bulb alkali 1, urethane acrylate 21, tri (propylene glycol) diacrylate 12, Viscoat 295 8, thermoplastic acrylic resin 12, isobornyl methacrylate 11,1-hydroxy-cyclohexyl phenyl-acetone 5, magnesium hydroxide 1, Resorcinol bisglycidyl ether 12, altax 1, auxiliary agent 4;
Described auxiliary agent by following weight part (kilogram) raw material be prepared from: nano diatomite powder 0.2, nano mica powder 0.2, Silane coupling agent KH550 2, linking agent TAC2, polyisobutene 2, Resorcinol 1, Viscoat 295 10, vinylformic acid dimethylamino ethyl ester 2, phenyl glycidyl ether 1, cobalt naphthenate 2, Tenox PG 2, coix seed oil 1; Its preparation method is by each mixing of materials, is heated to 60-70 ℃, and stirring reaction 30-40 minute, obtains.
Novel UV of the present invention solidifies silk screen printing pearl ink, by following concrete steps, made: first add pigment dyestuff, glycerol, Tai-Ace S 150, flower bulb alkali, urethane acrylate, tri (propylene glycol) diacrylate, Viscoat 295, thermoplastic acrylic resin stirring and evenly mixing, be heated to 80-90 ℃, stir 25-35 minute; Then add all the other remaining components except 1-hydroxy-cyclohexyl phenyl-acetone, stirring reaction 3-5 hour; Finally be cooled to 60-70 ℃, add 1-hydroxy-cyclohexyl phenyl-acetone, stirring reaction 40-50 minute, cooling after, grind and to obtain 20-40 μ m slurry, obtain.
The ink of gained, is used cross-hatching ox-hide tape stripping, draws compartment apart from 1mm, and 100% adheres to; Spirituous cotton balls is soaked in use, and 300 grams of pressure wipings 50 times, are as good as shape; Be soaked in salad oil (normal temperature) 8 hours, be as good as shape; Use is soaked with the cotton balls of salt solution, and 300 grams of pressure wipings 50 times, are as good as shape.
Claims (2)
1. a novel UV solidifies silk screen printing pearl ink, it is characterized in that, by the raw material of following weight part, made: pigment dyestuff 2-3, glycerol 6-10, Tai-Ace S 150 3-4, flower bulb alkali 1-2, urethane acrylate 21-23, tri (propylene glycol) diacrylate 12-15, Viscoat 295 8-10, thermoplastic acrylic resin 12-15, isobornyl methacrylate 11-13,1-hydroxy-cyclohexyl phenyl-acetone 5-8, magnesium hydroxide 1-2, Resorcinol bisglycidyl ether 12-15, altax 1-2, auxiliary agent 4-5;
Described auxiliary agent is prepared from by the raw material of following weight part: nano diatomite powder 0.2-0.3, nano mica powder 0.2-0.3, Silane coupling agent KH550 2-3, linking agent TAC2-3, polyisobutene 2-3, Resorcinol 1-2, Viscoat 295 10-12, vinylformic acid dimethylamino ethyl ester 2-3, phenyl glycidyl ether 1-2, cobalt naphthenate 2-3, Tenox PG 2-3, coix seed oil 1-2; Its preparation method is by each mixing of materials, is heated to 60-70 ℃, and stirring reaction 30-40 minute, obtains.
2. novel UV solidifies silk screen printing pearl ink according to claim 1, it is characterized in that, by following concrete steps, made: first add pigment dyestuff, glycerol, Tai-Ace S 150, flower bulb alkali, urethane acrylate, tri (propylene glycol) diacrylate, Viscoat 295, thermoplastic acrylic resin stirring and evenly mixing, be heated to 80-90 ℃, stir 25-35 minute; Then add all the other remaining components except 1-hydroxy-cyclohexyl phenyl-acetone, stirring reaction 3-5 hour; Finally be cooled to 60-70 ℃, add 1-hydroxy-cyclohexyl phenyl-acetone, stirring reaction 40-50 minute, cooling after, grind and to obtain 20-40 μ m slurry, obtain.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310593195.0A CN103666033B (en) | 2013-11-23 | 2013-11-23 | A kind of novel UV solidifies serigraphy pearl ink and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310593195.0A CN103666033B (en) | 2013-11-23 | 2013-11-23 | A kind of novel UV solidifies serigraphy pearl ink and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103666033A true CN103666033A (en) | 2014-03-26 |
| CN103666033B CN103666033B (en) | 2016-05-04 |
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| CN201310593195.0A Active CN103666033B (en) | 2013-11-23 | 2013-11-23 | A kind of novel UV solidifies serigraphy pearl ink and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105315769A (en) * | 2015-11-30 | 2016-02-10 | 佛山市高明绿色德化工有限公司 | Colored UV ink for glass |
| CN109385918A (en) * | 2018-11-12 | 2019-02-26 | 广州市珠之江环保印花材料实业有限公司 | Printing and dyeing PVA glue and preparation method thereof |
| CN115466541A (en) * | 2022-08-03 | 2022-12-13 | 佛山市兴洲玻璃科技有限公司 | Method for cutting tempered ink glass in different places |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101665641A (en) * | 2009-09-25 | 2010-03-10 | 林国顺 | Ultraviolet curing embossed printing ink |
| CN101974267A (en) * | 2010-11-04 | 2011-02-16 | 中钞油墨有限公司 | Aqueous ultraviolet light curing pearlescent silk screen ink and preparation method thereof |
| CN102295858A (en) * | 2010-06-25 | 2011-12-28 | 深圳市顾康力化工有限公司 | Photo-curable screen printing ink and preparation method thereof |
| CN102533000A (en) * | 2011-12-28 | 2012-07-04 | 深圳市通产丽星股份有限公司 | Ultraviolet light curing ink and preparation method thereof |
| CN102634251A (en) * | 2012-04-10 | 2012-08-15 | 中钞油墨有限公司 | Photo-curing silk screen pearly-luster ink applicable to different printing substrates and preparation method thereof |
-
2013
- 2013-11-23 CN CN201310593195.0A patent/CN103666033B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101665641A (en) * | 2009-09-25 | 2010-03-10 | 林国顺 | Ultraviolet curing embossed printing ink |
| CN102295858A (en) * | 2010-06-25 | 2011-12-28 | 深圳市顾康力化工有限公司 | Photo-curable screen printing ink and preparation method thereof |
| CN101974267A (en) * | 2010-11-04 | 2011-02-16 | 中钞油墨有限公司 | Aqueous ultraviolet light curing pearlescent silk screen ink and preparation method thereof |
| CN102533000A (en) * | 2011-12-28 | 2012-07-04 | 深圳市通产丽星股份有限公司 | Ultraviolet light curing ink and preparation method thereof |
| CN102634251A (en) * | 2012-04-10 | 2012-08-15 | 中钞油墨有限公司 | Photo-curing silk screen pearly-luster ink applicable to different printing substrates and preparation method thereof |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105315769A (en) * | 2015-11-30 | 2016-02-10 | 佛山市高明绿色德化工有限公司 | Colored UV ink for glass |
| CN105315769B (en) * | 2015-11-30 | 2017-12-19 | 佛山市高明绿色德化工有限公司 | A kind of coloured UV ink of glass |
| CN109385918A (en) * | 2018-11-12 | 2019-02-26 | 广州市珠之江环保印花材料实业有限公司 | Printing and dyeing PVA glue and preparation method thereof |
| CN109385918B (en) * | 2018-11-12 | 2021-02-12 | 广州市珠之江环保印花材料实业有限公司 | White glue for printing and dyeing and preparation method thereof |
| CN115466541A (en) * | 2022-08-03 | 2022-12-13 | 佛山市兴洲玻璃科技有限公司 | Method for cutting tempered ink glass in different places |
Also Published As
| Publication number | Publication date |
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| CN103666033B (en) | 2016-05-04 |
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Inventor after: Zheng Yi Inventor before: Wan Hongxia Inventor before: Chen Keliang |
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Effective date of registration: 20170508 Address after: 515410, Xinjin Road, Longhu District, Guangdong, Shantou Patentee after: Shantou Rui Chi Printing Co., Ltd. Address before: The economic development zone of Anhui province Tongling city four road 244000 No. 3201 Patentee before: Tongling Fangzheng Plastic Industrial Technology Co., Ltd. |
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