CN103666030B - A kind of UV cured printing ink for digital product touch-screen glass printing and preparation method thereof - Google Patents
A kind of UV cured printing ink for digital product touch-screen glass printing and preparation method thereof Download PDFInfo
- Publication number
- CN103666030B CN103666030B CN201310593168.3A CN201310593168A CN103666030B CN 103666030 B CN103666030 B CN 103666030B CN 201310593168 A CN201310593168 A CN 201310593168A CN 103666030 B CN103666030 B CN 103666030B
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- ink
- screen glass
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- printing
- auxiliary agent
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- 238000007639 printing Methods 0.000 title claims abstract description 24
- 239000011521 glass Substances 0.000 title claims abstract description 13
- 238000002360 preparation method Methods 0.000 title claims description 8
- YNAVUWVOSKDBBP-UHFFFAOYSA-N Morpholine Chemical compound C1COCCN1 YNAVUWVOSKDBBP-UHFFFAOYSA-N 0.000 claims abstract description 14
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 9
- LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 claims abstract description 8
- ISAOCJYIOMOJEB-UHFFFAOYSA-N benzoin Chemical compound C=1C=CC=CC=1C(O)C(=O)C1=CC=CC=C1 ISAOCJYIOMOJEB-UHFFFAOYSA-N 0.000 claims abstract description 8
- ZNQVEEAIQZEUHB-UHFFFAOYSA-N 2-ethoxyethanol Chemical compound CCOCCO ZNQVEEAIQZEUHB-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000004593 Epoxy Substances 0.000 claims abstract description 7
- CERQOIWHTDAKMF-UHFFFAOYSA-M Methacrylate Chemical compound CC(=C)C([O-])=O CERQOIWHTDAKMF-UHFFFAOYSA-M 0.000 claims abstract description 7
- WGLPBDUCMAPZCE-UHFFFAOYSA-N Trioxochromium Chemical compound O=[Cr](=O)=O WGLPBDUCMAPZCE-UHFFFAOYSA-N 0.000 claims abstract description 7
- APUPEJJSWDHEBO-UHFFFAOYSA-P ammonium molybdate Chemical compound [NH4+].[NH4+].[O-][Mo]([O-])(=O)=O APUPEJJSWDHEBO-UHFFFAOYSA-P 0.000 claims abstract description 7
- 229940010552 ammonium molybdate Drugs 0.000 claims abstract description 7
- 235000018660 ammonium molybdate Nutrition 0.000 claims abstract description 7
- 239000011609 ammonium molybdate Substances 0.000 claims abstract description 7
- 229910000423 chromium oxide Inorganic materials 0.000 claims abstract description 7
- KTWOOEGAPBSYNW-UHFFFAOYSA-N ferrocene Chemical compound [Fe+2].C=1C=C[CH-]C=1.C=1C=C[CH-]C=1 KTWOOEGAPBSYNW-UHFFFAOYSA-N 0.000 claims abstract description 7
- 150000002734 metacrylic acid derivatives Chemical class 0.000 claims abstract description 7
- 239000012860 organic pigment Substances 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- ZDQNWDNMNKSMHI-UHFFFAOYSA-N 1-[2-(2-prop-2-enoyloxypropoxy)propoxy]propan-2-yl prop-2-enoate Chemical compound C=CC(=O)OC(C)COC(C)COCC(C)OC(=O)C=C ZDQNWDNMNKSMHI-UHFFFAOYSA-N 0.000 claims abstract description 4
- POAOYUHQDCAZBD-UHFFFAOYSA-N 2-butoxyethanol Chemical compound CCCCOCCO POAOYUHQDCAZBD-UHFFFAOYSA-N 0.000 claims abstract description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 claims abstract description 4
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 claims abstract description 4
- 244000028419 Styrax benzoin Species 0.000 claims abstract description 4
- 235000000126 Styrax benzoin Nutrition 0.000 claims abstract description 4
- 235000008411 Sumatra benzointree Nutrition 0.000 claims abstract description 4
- 239000003963 antioxidant agent Substances 0.000 claims abstract description 4
- 230000003078 antioxidant effect Effects 0.000 claims abstract description 4
- QBLDFAIABQKINO-UHFFFAOYSA-N barium borate Chemical compound [Ba+2].[O-]B=O.[O-]B=O QBLDFAIABQKINO-UHFFFAOYSA-N 0.000 claims abstract description 4
- 229960002130 benzoin Drugs 0.000 claims abstract description 4
- 235000019382 gum benzoic Nutrition 0.000 claims abstract description 4
- 238000003756 stirring Methods 0.000 claims description 15
- 239000000047 product Substances 0.000 claims description 11
- 238000006243 chemical reaction Methods 0.000 claims description 9
- ZTHYODDOHIVTJV-UHFFFAOYSA-N Propyl gallate Chemical compound CCCOC(=O)C1=CC(O)=C(O)C(O)=C1 ZTHYODDOHIVTJV-UHFFFAOYSA-N 0.000 claims description 6
- 239000012467 final product Substances 0.000 claims description 6
- 239000000843 powder Substances 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 4
- 150000005208 1,4-dihydroxybenzenes Chemical class 0.000 claims description 3
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 3
- 244000077995 Coix lacryma jobi Species 0.000 claims description 3
- FQYUMYWMJTYZTK-UHFFFAOYSA-N Phenyl glycidyl ether Chemical compound C1OC1COC1=CC=CC=C1 FQYUMYWMJTYZTK-UHFFFAOYSA-N 0.000 claims description 3
- 229920002367 Polyisobutene Polymers 0.000 claims description 3
- 239000006087 Silane Coupling Agent Substances 0.000 claims description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 3
- DAKWPKUUDNSNPN-UHFFFAOYSA-N Trimethylolpropane triacrylate Chemical compound C=CC(=O)OCC(CC)(COC(=O)C=C)COC(=O)C=C DAKWPKUUDNSNPN-UHFFFAOYSA-N 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 239000003431 cross linking reagent Substances 0.000 claims description 3
- 239000010445 mica Substances 0.000 claims description 3
- 229910052618 mica group Inorganic materials 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- GEMHFKXPOCTAIP-UHFFFAOYSA-N n,n-dimethyl-n'-phenylcarbamimidoyl chloride Chemical compound CN(C)C(Cl)=NC1=CC=CC=C1 GEMHFKXPOCTAIP-UHFFFAOYSA-N 0.000 claims description 3
- 235000010388 propyl gallate Nutrition 0.000 claims description 3
- 239000002002 slurry Substances 0.000 claims description 3
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 3
- 238000005265 energy consumption Methods 0.000 abstract description 2
- 238000011031 large-scale manufacturing process Methods 0.000 abstract description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- PWWSSIYVTQUJQQ-UHFFFAOYSA-N distearyl thiodipropionate Chemical compound CCCCCCCCCCCCCCCCCCOC(=O)CCSCCC(=O)OCCCCCCCCCCCCCCCCCC PWWSSIYVTQUJQQ-UHFFFAOYSA-N 0.000 abstract 1
- 238000007650 screen-printing Methods 0.000 description 5
- 238000000034 method Methods 0.000 description 3
- 240000001624 Espostoa lanata Species 0.000 description 2
- 235000009161 Espostoa lanata Nutrition 0.000 description 2
- 239000000853 adhesive Substances 0.000 description 2
- 230000001070 adhesive effect Effects 0.000 description 2
- 101000831616 Homo sapiens Protachykinin-1 Proteins 0.000 description 1
- 240000008415 Lactuca sativa Species 0.000 description 1
- 102100024304 Protachykinin-1 Human genes 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000005530 etching Methods 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000010428 oil painting Methods 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 235000012045 salad Nutrition 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 229920002994 synthetic fiber Polymers 0.000 description 1
- 239000004758 synthetic textile Substances 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses a kind of UV cured printing ink for digital product touch-screen glass printing, it is characterized in that, raw material by following weight portion is made: organic pigment 1-3, methacrylate 20-24, epoxy methacrylates 12-15, ammonium molybdate 2-3, chromium oxide 1-2, morpholine 1-2, ethylene glycol ethyl ether 5-8, ferrocene 1-2, 2-butoxy-ethanol 3-4, methacrylic acid 3-4, diethylene glycol ether acetate 10-14, benzoin dimethylether 5-8, tripropylene glycol diacrylate 6-9, 184 light trigger 5-8, antioxidant DSTP? 1-2, Sb2O31-2, barium metaborate 1-2, auxiliary agent 4-5, auxiliary agent of the present invention has improved the toughness of ink, makes distributes ink even, and has maintained the stability of ink, curing rate of the present invention is fast, saves energy consumption and time, has improved production efficiency, is applicable to large-scale production.
Description
Technical field
The present invention relates to a kind of ink and preparation method thereof, particularly a kind of UV cured printing ink for digital product touch-screen glass printing and preparation method thereof.
Background technology
Serigraphy is that silk fabrics, synthetic fabrics or woven wire are stretched tight on screen frame, adopts manual method of carving paint film or photochemistry plate-making to make screen printing forme. Modern screen printing technique, to utilize photosensitive material to make the flat carriers such as screen printing forme (the silk screen hole that makes picture and text part on screen printing forme is through hole, and the silk screen hole of non-graphic part is plugged) oil painting, etching, pictorial poster, business card, binding and layout front cover, commodity packaging, product tag, dyeing textile product, touch-screen glass and metal etc. by photomechanical method. Ink is the screen printing ink that is conducive to two liquid response types of environment, essential superior printing stability while thering is touch screen glass printing, good adhesive force and patience, film after solidifying has good adhesive force, resistance to water and chemoresistance, also has higher case hardness and wearability simultaneously.
Summary of the invention
The object of this invention is to provide a kind of UV cured printing ink for digital product touch-screen glass printing and preparation method thereof.
In order to realize object of the present invention, the present invention passes through following scheme implementation:
For a UV cured printing ink for digital product touch-screen glass printing, made by the raw material of following weight portion: organic pigment 1-3, methacrylate 20-24, epoxy methacrylates 12-15, ammonium molybdate 2-3, chromium oxide 1-2, morpholine 1-2, ethylene glycol ethyl ether 5-8, ferrocene 1-2,2-butoxy-ethanol 3-4, methacrylic acid 3-4, diethylene glycol ether acetate 10-14, benzoin dimethylether 5-8, tripropylene glycol diacrylate 6-9,184 light trigger 5-8, antioxidant DSTP1-2, Sb2O31-2, barium metaborate 1-2, auxiliary agent 4-5;
Described auxiliary agent is prepared from by the raw material of following weight portion: nano diatomite powder 0.2-0.3, nano mica powder 0.2-0.3, Silane coupling agent KH550 2-3, crosslinking agent TAC2-3, polyisobutene 2-3, hydroquinones 1-2, trimethylolpropane triacrylate 10-12, acrylic acid dimethylamino ethyl ester 2-3, phenyl glycidyl ether 1-2, cobalt naphthenate 2-3, n-propyl gallate 2-3, coix seed oil 1-2; Its preparation method is by each mixing of materials, is heated to 60-70 DEG C, and stirring reaction 30-40 minute, to obtain final product.
UV cured printing ink for digital product touch-screen glass printing of the present invention, made by following concrete steps: first add organic pigment, methacrylate, epoxy methacrylates, ammonium molybdate, chromium oxide, morpholine, ethylene glycol ethyl ether, ferrocene to stir and evenly mix, be heated to 80-90 DEG C, stir 25-35 minute; Then add all the other residual components except 184 light triggers, stirring reaction 3-5 hour; Finally be cooled to 60-70 DEG C, add 184 light triggers, stirring reaction 40-50 minute, cooling after, grind obtain 20-40 μ m slurry, to obtain final product.
The invention has the beneficial effects as follows: auxiliary agent of the present invention has improved the toughness of ink, make distributes ink even, and maintained the stability of ink; Curing rate of the present invention is fast, saves energy consumption and time, has improved production efficiency, is applicable to large-scale production.
Specific embodiments
Below by instantiation, the present invention is described in detail.
For a UV cured printing ink for digital product touch-screen glass printing, by following weight portion (kilogram) raw material make: organic pigment 1, methacrylate 20, epoxy methacrylates 12, ammonium molybdate 2, chromium oxide 1, morpholine 1, ethylene glycol ethyl ether 5, ferrocene 1,2-butoxy-ethanol 3, methacrylic acid 3, diethylene glycol ether acetate 10, benzoin dimethylether 5, tripropylene glycol diacrylate 6,184 light triggers 5, antioxidant DSTP1, Sb2O31, barium metaborate 1, auxiliary agent 4;
Described auxiliary agent by following weight portion (kilogram) raw material be prepared from: nano diatomite powder 0.2, nano mica powder 0.2, Silane coupling agent KH550 2, crosslinking agent TAC2, polyisobutene 2, hydroquinones 1, trimethylolpropane triacrylate 10, acrylic acid dimethylamino ethyl ester 2, phenyl glycidyl ether 1, cobalt naphthenate 2, n-propyl gallate 2, coix seed oil 1; Its preparation method is by each mixing of materials, is heated to 60-70 DEG C, and stirring reaction 30-40 minute, to obtain final product.
UV cured printing ink for digital product touch-screen glass printing of the present invention, made by following concrete steps: first add organic pigment, methacrylate, epoxy methacrylates, ammonium molybdate, chromium oxide, morpholine, ethylene glycol ethyl ether, ferrocene to stir and evenly mix, be heated to 80-90 DEG C, stir 25-35 minute; Then add all the other residual components except 184 light triggers, stirring reaction 3-5 hour; Finally be cooled to 60-70 DEG C, add 184 light triggers, stirring reaction 40-50 minute, cooling after, grind obtain 20-40 μ m slurry, to obtain final product.
The ink of gained, uses cross-hatching ox-hide tape stripping, draws compartment apart from 1mm, and 100% adheres to; Spirituous cotton balls is soaked in use, and 300 grams of pressure wipings 50 times, are as good as shape; Be soaked in salad oil (normal temperature) 8 hours, be as good as shape; Use is soaked with the cotton balls of salt solution, and 300 grams of pressure wipings 50 times, are as good as shape.
Claims (2)
1. the UV cured printing ink for digital product touch-screen glass printing, it is characterized in that, raw material by following weight portion is prepared from: organic pigment 1-3, methacrylate 20-24, epoxy methacrylates 12-15, ammonium molybdate 2-3, chromium oxide 1-2, morpholine 1-2, ethylene glycol ethyl ether 5-8, ferrocene 1-2, 2-butoxy-ethanol 3-4, methacrylic acid 3-4, diethylene glycol ether acetate 10-14, benzoin dimethylether 5-8, tripropylene glycol diacrylate 6-9, 184 light trigger 5-8, antioxidant DSTP1-2, Sb2O31-2, barium metaborate 1-2, auxiliary agent 4-5, described auxiliary agent is prepared from by the raw material of following weight portion: nano diatomite powder 0.2-0.3, nano mica powder 0.2-0.3, Silane coupling agent KH550 2-3, crosslinking agent TAC2-3, polyisobutene 2-3, hydroquinones 1-2, trimethylolpropane triacrylate 10-12, acrylic acid dimethylamino ethyl ester 2-3, phenyl glycidyl ether 1-2, cobalt naphthenate 2-3, n-propyl gallate 2-3, coix seed oil 1-2, its preparation method is by each mixing of materials, is heated to 60-70 DEG C, and stirring reaction 30-40 minute, to obtain final product.
2. according to claim 1 for the UV cured printing ink of digital product touch-screen glass printing, it is characterized in that, made by following concrete steps: first add organic pigment, methacrylate, epoxy methacrylates, ammonium molybdate, chromium oxide, morpholine, ethylene glycol ethyl ether, ferrocene to stir and evenly mix, be heated to 80-90 DEG C, stir 25-35 minute; Then add all the other residual components except 184 light triggers, stirring reaction 3-5 hour; Finally be cooled to 60-70 DEG C, add 184 light triggers, stirring reaction 40-50 minute, cooling after, grind obtain 20-40 μ m slurry, to obtain final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310593168.3A CN103666030B (en) | 2013-11-23 | 2013-11-23 | A kind of UV cured printing ink for digital product touch-screen glass printing and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310593168.3A CN103666030B (en) | 2013-11-23 | 2013-11-23 | A kind of UV cured printing ink for digital product touch-screen glass printing and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103666030A CN103666030A (en) | 2014-03-26 |
| CN103666030B true CN103666030B (en) | 2016-05-04 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310593168.3A Active CN103666030B (en) | 2013-11-23 | 2013-11-23 | A kind of UV cured printing ink for digital product touch-screen glass printing and preparation method thereof |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101469152A (en) * | 2007-12-27 | 2009-07-01 | 深圳富泰宏精密工业有限公司 | Ink composition and use method thereof |
| CN101580661A (en) * | 2009-06-05 | 2009-11-18 | 刘恒全 | touch screen protection ink |
| CN102093782A (en) * | 2011-03-30 | 2011-06-15 | 北京神彩优维喷墨材料科技有限公司 | Ultraviolet-cured digital painting ink and preparation method thereof |
| CN102702849A (en) * | 2012-06-05 | 2012-10-03 | 无锡金桥精细油墨有限公司 | Ultraviolet-light-cured glass transparent ink and preparation method thereof |
-
2013
- 2013-11-23 CN CN201310593168.3A patent/CN103666030B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101469152A (en) * | 2007-12-27 | 2009-07-01 | 深圳富泰宏精密工业有限公司 | Ink composition and use method thereof |
| CN101580661A (en) * | 2009-06-05 | 2009-11-18 | 刘恒全 | touch screen protection ink |
| CN102093782A (en) * | 2011-03-30 | 2011-06-15 | 北京神彩优维喷墨材料科技有限公司 | Ultraviolet-cured digital painting ink and preparation method thereof |
| CN102702849A (en) * | 2012-06-05 | 2012-10-03 | 无锡金桥精细油墨有限公司 | Ultraviolet-light-cured glass transparent ink and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN103666030A (en) | 2014-03-26 |
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| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A UV cured ink and its preparation method for touch screen glass printing of digital products Effective date of registration: 20231113 Granted publication date: 20160504 Pledgee: Shanghai Yudi Aviation Supplies Co.,Ltd. Pledgor: TONGLING FOUNDER PLASTICS TECHNOLOGY Co.,Ltd. Registration number: Y2023980065339 |
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Date of cancellation: 20231219 Granted publication date: 20160504 Pledgee: Shanghai Yudi Aviation Supplies Co.,Ltd. Pledgor: TONGLING FOUNDER PLASTICS TECHNOLOGY Co.,Ltd. Registration number: Y2023980065339 |
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| PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A UV cured ink and its preparation method for touch screen glass printing of digital products Granted publication date: 20160504 Pledgee: Shanghai Yudi Aviation Supplies Co.,Ltd. Pledgor: TONGLING FOUNDER PLASTICS TECHNOLOGY Co.,Ltd. Registration number: Y2024980000266 |
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