CN102985362A - LiPO2F2的制造 - Google Patents

LiPO2F2的制造 Download PDF

Info

Publication number
CN102985362A
CN102985362A CN2011800336981A CN201180033698A CN102985362A CN 102985362 A CN102985362 A CN 102985362A CN 2011800336981 A CN2011800336981 A CN 2011800336981A CN 201180033698 A CN201180033698 A CN 201180033698A CN 102985362 A CN102985362 A CN 102985362A
Authority
CN
China
Prior art keywords
solution
lipo
lipo2f2
carbonic acid
solvent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN2011800336981A
Other languages
English (en)
Chinese (zh)
Inventor
普拉西多·加西亚-胡安
阿尔夫·舒尔茨
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Solvay SA
Original Assignee
Solvay SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Solvay SA filed Critical Solvay SA
Publication of CN102985362A publication Critical patent/CN102985362A/zh
Pending legal-status Critical Current

Links

Classifications

    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/056—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes
    • H01M10/0564—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes the electrolyte being constituted of organic materials only
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/26—Phosphates
    • C01B25/455—Phosphates containing halogen
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D15/00—Lithium compounds
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/052—Li-accumulators
    • H01M10/0525—Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/056—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/056—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes
    • H01M10/0564—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes the electrolyte being constituted of organic materials only
    • H01M10/0566—Liquid materials
    • H01M10/0567—Liquid materials characterised by the additives
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/056—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes
    • H01M10/0564—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes the electrolyte being constituted of organic materials only
    • H01M10/0566—Liquid materials
    • H01M10/0568—Liquid materials characterised by the solutes
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Manufacturing & Machinery (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Materials Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Secondary Cells (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
CN2011800336981A 2010-07-08 2011-06-30 LiPO2F2的制造 Pending CN102985362A (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP10168886 2010-07-08
EP10168886.9 2010-07-08
PCT/EP2011/061026 WO2012004187A2 (en) 2010-07-08 2011-06-30 Manufacture of lipo2f2

Publications (1)

Publication Number Publication Date
CN102985362A true CN102985362A (zh) 2013-03-20

Family

ID=42732822

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2011800336981A Pending CN102985362A (zh) 2010-07-08 2011-06-30 LiPO2F2的制造

Country Status (7)

Country Link
US (1) US20130115522A1 (enExample)
EP (1) EP2590895A2 (enExample)
JP (1) JP2013539448A (enExample)
KR (1) KR20130041184A (enExample)
CN (1) CN102985362A (enExample)
TW (1) TW201213228A (enExample)
WO (1) WO2012004187A2 (enExample)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106829908A (zh) * 2016-12-23 2017-06-13 山东海容电源材料有限公司 一种二氟磷酸锂的制备方法及含有二氟磷酸锂的锂离子电池非水电解液
CN110342486A (zh) * 2019-07-22 2019-10-18 湖北百杰瑞新材料股份有限公司 一种二氟磷酸锂的制备方法
CN112758904A (zh) * 2019-11-22 2021-05-07 多氟多化工股份有限公司 一种二氟磷酸锂的制备方法
CN112811407A (zh) * 2019-11-15 2021-05-18 多氟多化工股份有限公司 一种二氟磷酸锂的制备方法

Families Citing this family (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2012016924A1 (en) 2010-08-04 2012-02-09 Solvay Sa Manufacture of lipo2f2 from pof3 or pf5
KR101614235B1 (ko) * 2012-03-14 2016-04-20 스텔라 케미파 코포레이션 디플루오로인산염의 제조방법
JP5980617B2 (ja) * 2012-08-09 2016-08-31 三洋電機株式会社 非水電解質二次電池及びその製造方法
EP2712843A1 (de) * 2012-09-28 2014-04-02 LANXESS Deutschland GmbH Herstellung von hochreinem Lithiumdifluorphosphat
JP2016516004A (ja) 2013-02-22 2016-06-02 メルク・シャープ・アンド・ドーム・コーポレーションＭｅｒｃｋ Ｓｈａｒｐ ＆ Ｄｏｈｍｅ Ｃｏｒｐ． 抗糖尿病二環式化合物
JP5715725B2 (ja) * 2013-06-07 2015-05-13 ステラケミファ株式会社 ジフルオロリン酸塩の精製方法
JP5666734B2 (ja) 2013-06-07 2015-02-12 ステラケミファ株式会社 ジフルオロリン酸塩の製造方法
WO2015051496A1 (en) 2013-10-08 2015-04-16 Merck Sharp & Dohme Corp. Antidiabetic tricyclic compounds
WO2015089809A1 (en) 2013-12-19 2015-06-25 Merck Sharp & Dohme Corp. Antidiabetic substituted heteroaryl compounds
WO2015176267A1 (en) 2014-05-22 2015-11-26 Merck Sharp & Dohme Corp. Antidiabetic tricyclic compounds
JP6405745B2 (ja) * 2014-06-27 2018-10-17 ダイキン工業株式会社 ジフルオロリン酸リチウムの製造方法
WO2016022742A1 (en) 2014-08-08 2016-02-11 Merck Sharp & Dohme Corp. Antidiabetic bicyclic compounds
WO2016022448A1 (en) 2014-08-08 2016-02-11 Merck Sharp & Dohme Corp. Antidiabetic bicyclic compounds
US10100042B2 (en) 2014-08-08 2018-10-16 Merck Sharp & Dohme Corp. [5,6]—fused bicyclic antidiabetic compounds
WO2016019587A1 (en) 2014-08-08 2016-02-11 Merck Sharp & Dohme Corp. [7, 6]-fused bicyclic antidiabetic compounds
JP5822044B1 (ja) * 2015-04-17 2015-11-24 宇部興産株式会社 非水電解液、並びにそれを用いたリチウムイオン二次電池及びリチウムイオンキャパシタ
WO2018106518A1 (en) 2016-12-06 2018-06-14 Merck Sharp & Dohme Corp. Antidiabetic heterocyclic compounds
WO2018118670A1 (en) 2016-12-20 2018-06-28 Merck Sharp & Dohme Corp. Antidiabetic spirochroman compounds
JP6921128B2 (ja) * 2017-01-20 2021-08-18 三井化学株式会社 ジフルオロリン酸リチウムの製造方法
CN109422256A (zh) * 2017-08-28 2019-03-05 天津金牛电源材料有限责任公司 一种二氟磷酸碱金属盐的制备方法
JP7020749B2 (ja) * 2018-03-26 2022-02-16 三井化学株式会社 ジフルオロリン酸リチウムの製造方法
KR101925051B1 (ko) * 2018-08-02 2019-02-22 주식회사 천보 디플루오로인산리튬염 결정체를 고순도로 제조하는 방법 및 이를 이용한 2차 전지용 비수계 전해액
KR102231049B1 (ko) * 2020-09-09 2021-03-23 주식회사 천보 용해성이 우수한 디플루오로인산리튬염 결정체를 고순도로 제조하는 방법 및 이를 이용한 2차 전지용 비수계 전해액
CN113060718A (zh) * 2021-03-29 2021-07-02 兰州理工大学 废旧锂离子电池回收电解液制备二氟磷酸锂的方法
KR102709477B1 (ko) * 2023-10-06 2024-09-24 주식회사 천보 디플루오로인산리튬염 결정체를 고순도로 제조하는 방법 및 이를 이용한 2차 전지용 비수계 전해액

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4880714A (en) 1989-02-27 1989-11-14 Duracell Inc. Method for preparing non-aqueous electrolytes
JP3173225B2 (ja) 1993-05-26 2001-06-04 ソニー株式会社 非水電解液二次電池
CA2104718C (en) 1993-08-24 1999-11-16 Huanyu Mao Simplified preparation of lipf6 based electrolyte for non-aqueous batteries
JPH07254415A (ja) 1993-12-20 1995-10-03 Wilson Greatbatch Ltd 電気化学電池およびその電圧遅延を減少させる方法
DE10016816A1 (de) 2000-04-05 2001-10-11 Solvay Fluor & Derivate Verwendung von Alkoxyestern
JP4674444B2 (ja) * 2003-04-18 2011-04-20 三菱化学株式会社 ジフルオロリン酸塩の製造方法、二次電池用非水系電解液及び非水系電解液二次電池
JP4604505B2 (ja) * 2004-02-09 2011-01-05 三菱化学株式会社 ジフルオロリン酸リチウムの製造方法、ならびに、非水系電解液及びこれを用いた非水系電解液二次電池
KR101227445B1 (ko) * 2004-10-19 2013-01-29 미쓰비시 가가꾸 가부시키가이샤 디플루오로인산염의 제조 방법, 이차전지용 비수계 전해질용액 및 비수계 전해질 이차전지
JP5228270B2 (ja) * 2004-10-19 2013-07-03 三菱化学株式会社 ジフルオロリン酸塩の製造方法、二次電池用非水系電解液及び非水系電解液二次電池
WO2006137177A1 (ja) * 2005-06-20 2006-12-28 Mitsubishi Chemical Corporation ジフルオロリン酸塩の製造方法、二次電池用非水系電解液及び非水系電解液二次電池
EP2061115B1 (en) * 2006-08-22 2015-04-01 Mitsubishi Chemical Corporation Lithium difluorophosphate, electrolytic solution containing lithium difluorophosphate, process for producing lithium difluorophosphate, process for producing nonaqueous electrolytic solution, nonaqueous electrolytic solution, and nonaqueous-electrolytic-solution secondary cell employing the same
JP5277550B2 (ja) * 2007-03-12 2013-08-28 セントラル硝子株式会社 ジフルオロリン酸リチウムの製造方法及びこれを用いた非水電解液電池
WO2012004188A1 (en) * 2010-07-08 2012-01-12 Solvay Sa Manufacture of lipo2f2 and crystalline lipo2f2

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106829908A (zh) * 2016-12-23 2017-06-13 山东海容电源材料有限公司 一种二氟磷酸锂的制备方法及含有二氟磷酸锂的锂离子电池非水电解液
CN110342486A (zh) * 2019-07-22 2019-10-18 湖北百杰瑞新材料股份有限公司 一种二氟磷酸锂的制备方法
CN110342486B (zh) * 2019-07-22 2022-09-30 湖北百杰瑞新材料股份有限公司 一种二氟磷酸锂的制备方法
CN112811407A (zh) * 2019-11-15 2021-05-18 多氟多化工股份有限公司 一种二氟磷酸锂的制备方法
CN112811407B (zh) * 2019-11-15 2023-10-31 多氟多新材料股份有限公司 一种二氟磷酸锂的制备方法
CN112758904A (zh) * 2019-11-22 2021-05-07 多氟多化工股份有限公司 一种二氟磷酸锂的制备方法

Also Published As

Publication number Publication date
EP2590895A2 (en) 2013-05-15
WO2012004187A2 (en) 2012-01-12
US20130115522A1 (en) 2013-05-09
WO2012004187A3 (en) 2012-03-08
KR20130041184A (ko) 2013-04-24
JP2013539448A (ja) 2013-10-24
TW201213228A (en) 2012-04-01

Similar Documents

Publication Publication Date Title
CN102985362A (zh) LiPO2F2的制造
CN103222102B (zh) 非水电解液
KR101668293B1 (ko) 리튬비스(플루오로술포닐)이미드의 제조방법
KR101695072B1 (ko) 펜타시클릭 음이온 염의 제조 방법
EP3332441B1 (en) Nonaqueous electrolyte compositions comprising lithium oxalato phosphates
CN104080780B (zh) 氟化的麦德鲁姆酸的衍生物、其制备方法、及其作为溶剂添加剂的用途
CN102985361A (zh) LiPO2F2和晶体LiPO2F2的制造
CN103874657A (zh) 制造含LiPO2F2和LiPF6的混合物
US9343774B2 (en) Method for producing a lithium hexafluorophosphate concentrated liquid
TWI598292B (zh) 五氟化磷之製造方法、六氟化磷酸鋰之製造方法、六氟化磷酸鋰、電池用非水電解液及鋰二次電池
CN109997258A (zh) 含有六元环环状硫酸酯的电解质
JP2009187958A (ja) 非水電解液およびリチウム二次電池
JP4810867B2 (ja) リチウムイオン電池用電解液の製造方法
CN103987691A (zh) 用于制造1,1’-二氟取代的碳酸二烷基酯的方法、其异构体以及含它的电解质组合物
CN108408711A (zh) 一种二氟磷酸锂的制备方法
KR100971065B1 (ko) 리튬이온전지용 전해액의 제조방법 및 이를 사용한리튬이온전지
WO2011155267A1 (ja) リチウムイオン電池用電解液の製造方法およびその電解液を用いたリチウムイオン電池
KR20230112800A (ko) 불화수소 함량이 저감된 카보네이트 용제 중의 비스(플루오로설포닐)이미드 리튬염의 제조방법
JP2005060261A (ja) ビス（２，２，３，４，４，４−ヘキサフルオロブチル）カーボネートおよびその製造方法、および非水系電解液
JP5151121B2 (ja) リチウムイオン電池用電解液の製造方法およびそれを用いたリチウムイオン電池
JP2014234358A (ja) カーボネート化合物及びその製造方法
KR102677153B1 (ko) 불화수소가 저감된 리튬 비스(플루오로설포닐)이미드의 카보네이트 용액 제조방법
JP4470902B2 (ja) 非水電解液およびリチウム二次電池
JP2006210259A (ja) 非水電解液
KR20250031405A (ko) 리튬 비스(플루오로설포닐)이미드의 프로피오네이트 용액 및 그 제조방법

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C02 Deemed withdrawal of patent application after publication (patent law 2001)
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20130320