CN102844322B - 制备二有机二卤代硅烷的方法 - Google Patents

制备二有机二卤代硅烷的方法 Download PDF

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Publication number
CN102844322B
CN102844322B CN201180019329.7A CN201180019329A CN102844322B CN 102844322 B CN102844322 B CN 102844322B CN 201180019329 A CN201180019329 A CN 201180019329A CN 102844322 B CN102844322 B CN 102844322B
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silicon
copper catalyst
catalyst
hydrogen
containing copper
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Chinese (zh)
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CN102844322A (zh
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D·卡佐利斯
罗伯特·托马斯·拉森
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Dow Silicones Corp
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Dow Corning Corp
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/12—Organo silicon halides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/12—Organo silicon halides
    • C07F7/121—Preparation or treatment not provided for in C07F7/14, C07F7/16 or C07F7/20
    • C07F7/125—Preparation or treatment not provided for in C07F7/14, C07F7/16 or C07F7/20 by reactions involving both Si-C and Si-halogen linkages, the Si-C and Si-halogen linkages can be to the same or to different Si atoms, e.g. redistribution reactions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/72—Copper
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/12—Organo silicon halides
    • C07F7/121—Preparation or treatment not provided for in C07F7/14, C07F7/16 or C07F7/20
    • C07F7/122—Preparation or treatment not provided for in C07F7/14, C07F7/16 or C07F7/20 by reactions involving the formation of Si-C linkages

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
CN201180019329.7A 2010-05-28 2011-03-31 制备二有机二卤代硅烷的方法 Active CN102844322B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US34924210P 2010-05-28 2010-05-28
US61/349,242 2010-05-28
PCT/US2011/030683 WO2011149588A1 (en) 2010-05-28 2011-03-31 A method for preparing a diorganodihalosilane

Publications (2)

Publication Number Publication Date
CN102844322A CN102844322A (zh) 2012-12-26
CN102844322B true CN102844322B (zh) 2015-09-23

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US (2) US8772525B2 (enExample)
EP (1) EP2576573B1 (enExample)
JP (1) JP5726294B2 (enExample)
KR (1) KR101839585B1 (enExample)
CN (1) CN102844322B (enExample)
WO (1) WO2011149588A1 (enExample)

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EP2528928A2 (en) 2010-01-26 2012-12-05 Dow Corning Corporation Method of preparing an organohalosilane
JP5726294B2 (ja) * 2010-05-28 2015-05-27 ダウ コーニング コーポレーションＤｏｗ Ｃｏｒｎｉｎｇ Ｃｏｒｐｏｒａｔｉｏｎ ジオルガノジハロシランの調製方法
US20130039831A1 (en) * 2011-01-25 2013-02-14 Aswini Dash Method of preparing a hydridohalosilane compound
US8865927B2 (en) * 2011-11-17 2014-10-21 Dow Corning Corporation Method for preparing a diorganodihalosilane
EP2834252A2 (en) * 2012-04-05 2015-02-11 Dow Corning Corporation A method for preparing an organofunctional compound
US20150005156A1 (en) 2012-04-16 2015-01-01 Dow Corning Corporation Processes for the Preparation of Silicon Containing Intermetallic Compounds and Intermetallic Compounds Prepared Thereby
US8865850B2 (en) 2012-06-14 2014-10-21 Dow Corning Corporation Method of selectively forming a reaction product in the presence of a metal silicide
US9296765B2 (en) 2012-08-13 2016-03-29 Dow Corning Corporation Method of preparing an organohalosilane
CN104583221B (zh) * 2012-10-16 2018-05-01 道康宁公司 制备卤化硅杂亚烃的方法
WO2014099125A1 (en) * 2012-12-19 2014-06-26 Dow Corning Corporation Method for preparing a diorganodihalosilane
WO2014149224A1 (en) * 2013-03-15 2014-09-25 Dow Corning Corporation Method for preparing a halosilane using copper silicides as catalysts
KR102299593B1 (ko) 2013-11-12 2021-09-09 다우 실리콘즈 코포레이션 할로실란의 제조 방법
WO2015100075A1 (en) * 2013-12-23 2015-07-02 Dow Corning Corporation Solid binary copper-silicon material catalysts for emissions control
US10081643B2 (en) 2014-12-18 2018-09-25 Dow Silicones Corporation Method for producing aryl-functional silanes

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US2380996A (en) * 1941-09-26 1945-08-07 Gen Electric Preparation of organosilicon halides
US4314908A (en) * 1979-10-24 1982-02-09 Union Carbide Corporation Preparation of reaction mass for the production of methylchlorosilane
US4973725A (en) * 1988-06-28 1990-11-27 Union Carbide Chemicals And Plastics Company Inc. Direct synthesis process for organohalohydrosilanes
US20060165580A1 (en) * 2005-01-26 2006-07-27 The Regents Of The University Of California Heterogeneous copper catalysts

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BE473151A (enExample) 1945-03-15
US2888476A (en) 1956-08-01 1959-05-26 Du Pont Preparation of long-chain alkylhalosilanes
US3057686A (en) 1957-08-01 1962-10-09 Du Pont Process for preparing silanes
JPS5747917B2 (enExample) 1974-08-20 1982-10-13
DE3024319C2 (de) 1980-06-27 1983-07-21 Wacker-Chemitronic Gesellschaft für Elektronik-Grundstoffe mbH, 8263 Burghausen Kontinuierliches Verfahren zur Herstellung von Trichlorsilan
FR2530638A1 (fr) 1982-07-26 1984-01-27 Rhone Poulenc Spec Chim Procede de preparation d'un melange a base de trichlorosilane utilisable pour la preparation de silicium de haute purete
US4526769A (en) 1983-07-18 1985-07-02 Motorola, Inc. Trichlorosilane production process
JPS63118069A (ja) * 1986-11-07 1988-05-23 Sumitomo Electric Ind Ltd 耐食性・耐摩耗性部材
US4946980A (en) 1988-10-17 1990-08-07 Dow Corning Corporation Preparation of organosilanes
US4888435A (en) 1989-06-22 1989-12-19 Dow Corning Corporation Integrated process for alkylation and redistribution of halosilanes
DE4041644A1 (de) 1990-12-22 1992-06-25 Nuenchritz Chemie Gmbh Verfahren zur reduktiven umwandlung von siliciumtetrachlorid in trichlorsilan
TW232751B (en) 1992-10-09 1994-10-21 Semiconductor Energy Res Co Ltd Semiconductor device and method for forming the same
DE19654154A1 (de) 1995-12-25 1997-06-26 Tokuyama Corp Verfahren zur Herstellung von Trichlorsilan
US7223879B2 (en) 1998-07-10 2007-05-29 Massachusetts Institute Of Technology Ligands for metals and improved metal-catalyzed processes based thereon
US6156380A (en) 1998-10-05 2000-12-05 Shin-Etsu Chemical Co., Ltd. Method for preparing contact mass for organohalosilane synthesis
US6528674B1 (en) * 2000-04-20 2003-03-04 General Electric Company Method for preparing a contact mass
DE10044796A1 (de) 2000-09-11 2002-04-04 Bayer Ag Verfahren zur Herstellung von Chlorsilanen
DE10061682A1 (de) 2000-12-11 2002-07-04 Solarworld Ag Verfahren zur Herstellung von Reinstsilicium
AU2003296892B2 (en) 2002-08-06 2006-01-05 Loma Linda University Substances for preventing and treating autoimmune diseases
US7716590B1 (en) 2002-10-28 2010-05-11 Oracle International Corporation Method and apparatus for dynamically updating a secondary form element based on a selection in a primary form element
US7559969B2 (en) 2003-09-19 2009-07-14 Sri International Methods and apparatuses for producing metallic compositions via reduction of metal halides
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DE102005046703A1 (de) 2005-09-29 2007-04-05 Wacker Chemie Ag Verfahren und Vorrichtung zur Hydrierung von Chlorsilanen
EP2039669A1 (en) 2007-09-19 2009-03-25 Max-Planck-Gesellschaft zur Förderung der Wissenschaften e.V. Use of a mixture of an ordered intermetallic compound and an inert material as a catalyst and corresponding hydrogenation processes
JP2009111202A (ja) 2007-10-31 2009-05-21 Panasonic Corp 半導体装置及びその製造方法
JP5726294B2 (ja) * 2010-05-28 2015-05-27 ダウ コーニング コーポレーションＤｏｗ Ｃｏｒｎｉｎｇ Ｃｏｒｐｏｒａｔｉｏｎ ジオルガノジハロシランの調製方法
DE102011005647A1 (de) 2011-03-16 2012-10-04 Evonik Degussa Gmbh Verbundverfahren zur Umstetzung von STC-haltigen und OCS-haltigen Nebenströmen zu wasserstoffhaltigen Chlorsilanen

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2380996A (en) * 1941-09-26 1945-08-07 Gen Electric Preparation of organosilicon halides
US4314908A (en) * 1979-10-24 1982-02-09 Union Carbide Corporation Preparation of reaction mass for the production of methylchlorosilane
US4973725A (en) * 1988-06-28 1990-11-27 Union Carbide Chemicals And Plastics Company Inc. Direct synthesis process for organohalohydrosilanes
US20060165580A1 (en) * 2005-01-26 2006-07-27 The Regents Of The University Of California Heterogeneous copper catalysts

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
Reactions during direct synthesis of alkylchlorosilanes. IV. Methylation of silicon tetrachloride in the synthesis of methylchlorosilanes;Lobusevich N. P.等,;《Zhurnal Obshchei Khimii》;19781231;第2534-2541页, 尤其是第2534页正文第2段和第2535页表1 *

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Publication number Publication date
US20130066096A1 (en) 2013-03-14
KR101839585B1 (ko) 2018-03-16
EP2576573B1 (en) 2015-06-24
JP2013528187A (ja) 2013-07-08
KR20130079349A (ko) 2013-07-10
WO2011149588A1 (en) 2011-12-01
US8772525B2 (en) 2014-07-08
CN102844322A (zh) 2012-12-26
US20140256975A1 (en) 2014-09-11
JP5726294B2 (ja) 2015-05-27
EP2576573A1 (en) 2013-04-10

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