CN102822137B - 在液相中制备不对称的叔丁基仲胺的方法 - Google Patents

在液相中制备不对称的叔丁基仲胺的方法 Download PDF

Info

Publication number
CN102822137B
CN102822137B CN201180017705.9A CN201180017705A CN102822137B CN 102822137 B CN102822137 B CN 102822137B CN 201180017705 A CN201180017705 A CN 201180017705A CN 102822137 B CN102822137 B CN 102822137B
Authority
CN
China
Prior art keywords
aldehyde
hydrogenation
tert
butylamine
formula
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201180017705.9A
Other languages
English (en)
Chinese (zh)
Other versions
CN102822137A (zh
Inventor
C·W·维格博斯
C·米勒
J-P·梅尔德
B·施泰因
H·迈斯奈尔
G·哈德莱恩
N·古特弗鲁特
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Publication of CN102822137A publication Critical patent/CN102822137A/zh
Application granted granted Critical
Publication of CN102822137B publication Critical patent/CN102822137B/zh
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/24—Preparation of compounds containing amino groups bound to a carbon skeleton by reductive alkylation of ammonia, amines or compounds having groups reducible to amino groups, with carbonyl compounds
    • C07C209/26—Preparation of compounds containing amino groups bound to a carbon skeleton by reductive alkylation of ammonia, amines or compounds having groups reducible to amino groups, with carbonyl compounds by reduction with hydrogen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CN201180017705.9A 2010-04-07 2011-04-06 在液相中制备不对称的叔丁基仲胺的方法 Expired - Fee Related CN102822137B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP10159254.1 2010-04-07
EP10159254 2010-04-07
PCT/EP2011/055372 WO2011124619A1 (de) 2010-04-07 2011-04-06 Verfahren zur herstellung von unsymmetrischen sekundären tert-butylaminen in der flüssigphase

Publications (2)

Publication Number Publication Date
CN102822137A CN102822137A (zh) 2012-12-12
CN102822137B true CN102822137B (zh) 2015-05-27

Family

ID=43875677

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201180017705.9A Expired - Fee Related CN102822137B (zh) 2010-04-07 2011-04-06 在液相中制备不对称的叔丁基仲胺的方法

Country Status (5)

Country Link
EP (1) EP2556046B1 (enExample)
JP (1) JP5911469B2 (enExample)
CN (1) CN102822137B (enExample)
ES (1) ES2524888T3 (enExample)
WO (1) WO2011124619A1 (enExample)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2013173976A (ja) * 2012-02-24 2013-09-05 Jfe Steel Corp 冷延鋼板の製造方法およびその製造設備
JP6624490B2 (ja) * 2015-07-17 2019-12-25 国立研究開発法人産業技術総合研究所 メチルアミノ基を有する芳香族化合物又はフラン誘導体の製造法
WO2018007207A1 (de) 2016-07-07 2018-01-11 Basf Se Verfahren zur herstellung von sekundären, cycloaliphatischen aminen
CN110294678A (zh) * 2019-05-08 2019-10-01 山东汉鸿新材料科技有限公司 脂肪双烷基仲胺和甲醛制备n-甲基双烷基叔胺的方法
EP4077270A4 (en) 2019-12-19 2024-03-13 Syensqo Sa METHOD FOR PRODUCING TWIN-TAIL TRIAMINES
CN116023270A (zh) * 2021-10-26 2023-04-28 中国石油化工股份有限公司 醇氨化制备有机胺的方法

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1492863A (fr) 1966-03-31 1967-08-25 Electrochimie Soc Perfectionnements aux procédés de fabrication de nu-méthylbutylamine
JP3345957B2 (ja) * 1993-04-15 2002-11-18 富士レビオ株式会社 アミン誘導体及びその製造方法
DE19859776B4 (de) * 1998-12-23 2008-06-19 Basf Se Verfahren zur Herstellung von Aminen
DE10122758B4 (de) 2001-05-11 2012-03-15 Oxea Gmbh Verfahren zur Herstellung von gemischten, sekundären Aminen
DE10153411A1 (de) 2001-10-30 2003-05-15 Basf Ag Verfahren zur Auftrennung von wasserhaltigen Rohamingemischen aus der Aminsynthese
DE10153410A1 (de) 2001-10-30 2003-05-15 Basf Ag Verfahren zur Auftrennung von wasserhaltigen Rohamingemischen aus der Aminsynthese
EP2236502B1 (en) 2007-12-27 2014-03-05 Ouchi Shinko Chemical Industrial Co., Ltd. Sulfenamide, vulcanization accelerator containing the sulfenamide for rubber, and process for producing the vulcanization accelerator

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
O.BAYER et al..Herstellung sekundarer Amine.《Methoden der organischen Chemie》.Georg Thieme Verlag,Stuttgart,1957,618-620. *
Synthesis of the β-Adrenergic Blocking Agent Timolol from Optically Active Precursors;Leonard M. Weinstock et al.;《JOURNAL OF ORGANIC CHEMISTRY》;19761231;第41卷(第19期);3121-3124 *
The synthesis of baclofen and GABOB via Rh(II) catalyzed intramolecular C–H insertion of α-diazoacetamides;Zhenliang Chen et al.;《Tetrahedron》;20041218;第61卷(第6期);1579–1586 *

Also Published As

Publication number Publication date
JP5911469B2 (ja) 2016-04-27
ES2524888T3 (es) 2014-12-15
WO2011124619A1 (de) 2011-10-13
EP2556046A1 (de) 2013-02-13
CN102822137A (zh) 2012-12-12
EP2556046B1 (de) 2014-10-08
JP2013523799A (ja) 2013-06-17

Similar Documents

Publication Publication Date Title
US8445726B2 (en) Process for preparing unsymmetric secondary tert-butylamines in the liquid phase
CN102822137B (zh) 在液相中制备不对称的叔丁基仲胺的方法
US8450530B2 (en) Process for preparing unsymmetric secondary tert-butylamines in the gas phase
US10093603B2 (en) Apparatus for preparing glycol and method of preparing the same
US8987523B2 (en) Method for obtaining ditrimethylolpropane and trimethylolpropane-enriched product streams from the side-streams in trimethylolpropane production
KR20160061395A (ko) 메타크롤레인의 생산 및 직접 산화적 에스테르화를 위한 그의 조건화/배수 방법
CN104039752B (zh) 在液相中制备仲胺的方法
CN1890203A (zh) 制备三环癸烷二醛的方法
KR101364249B1 (ko) 3-메틸-1,5-펜탄디올의 제조 방법
KR20180047255A (ko) 트리메틸올프로판의 제조장치 및 이를 이용한 제조방법
KR101294526B1 (ko) 고순도 ｎ-에틸메틸아민 및 이의 제조 방법
US20030187303A1 (en) Process for producing diamines
US9115110B2 (en) Method for recovering di-trimethylolpropane and trimethylolpropane-enriched product streams from the side streams of trimethylolpropane production
JP2008184409A (ja) アルキルアミン含有混合物の蒸留法及びアルキルアミン類の製造方法
US9045451B2 (en) Method for recovering di-trimethylolpropane and trimethylolpropane-enriched product streams from the side streams of trimethylolpropane production
WO2023140165A1 (ja) 多価アルコール類の製造方法
CN102884039B (zh) 在气相中制备不对称叔丁基仲胺的方法
US2678950A (en) Process of producing acrolein
US2691049A (en) Process fob the production of
TWI552988B (zh) ３－羥基－２，２－二甲基丙醛水溶液之濃縮方法
US20120101307A1 (en) Process for the preparation of 1-methyl-1-alkoxycyclopentanes
KR20030038375A (ko) 메틸아민의 제조 방법
EP1893556B1 (en) Process for preparing tetrafluorobenzene carbaldehyde alkyl acetal
HK1055939A (en) Process for producing diamines from dialdehydes
HK1178513A (en) Method for obtaining ditrimethylolpropane and trimethylolpropane-enriched product streams from the side-streams in trimethylolpropane production

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20150527

Termination date: 20170406