CN102811627A - 处理糖苷的混合物以获得更纯的形式的一种或多种这些糖苷的方法 - Google Patents

处理糖苷的混合物以获得更纯的形式的一种或多种这些糖苷的方法 Download PDF

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Publication number
CN102811627A
CN102811627A CN2011800151398A CN201180015139A CN102811627A CN 102811627 A CN102811627 A CN 102811627A CN 2011800151398 A CN2011800151398 A CN 2011800151398A CN 201180015139 A CN201180015139 A CN 201180015139A CN 102811627 A CN102811627 A CN 102811627A
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Prior art keywords
reb
slurry
rebaudioside
liquid phase
solid phase
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CN2011800151398A
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English (en)
Chinese (zh)
Inventor
A·埃里克森
J·J·哈恩
A·S·迈尔森
A·K·奥莫斯
T·A·鲁尼穆斯
K·M·斯托罗
C·A·泰勒
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Cargill Inc
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Cargill Inc
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Priority to CN201710007545.9A priority Critical patent/CN106986905B/zh
Publication of CN102811627A publication Critical patent/CN102811627A/zh
Pending legal-status Critical Current

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    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/30—Artificial sweetening agents
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H15/00—Compounds containing hydrocarbon or substituted hydrocarbon radicals directly attached to hetero atoms of saccharide radicals
    • C07H15/20—Carbocyclic rings
    • C07H15/24—Condensed ring systems having three or more rings
    • C07H15/256—Polyterpene radicals
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H15/00—Compounds containing hydrocarbon or substituted hydrocarbon radicals directly attached to hetero atoms of saccharide radicals
    • C07H15/20—Carbocyclic rings
    • C07H15/24—Condensed ring systems having three or more rings
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof
    • A23L2/52—Adding ingredients
    • A23L2/60—Sweeteners
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/30—Artificial sweetening agents
    • A23L27/33—Artificial sweetening agents containing sugars or derivatives
    • A23L27/36—Terpene glycosides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H1/00—Processes for the preparation of sugar derivatives
    • C07H1/06—Separation; Purification
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Nutrition Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Genetics & Genomics (AREA)
  • General Health & Medical Sciences (AREA)
  • Biotechnology (AREA)
  • Molecular Biology (AREA)
  • Biochemistry (AREA)
  • Proteomics, Peptides & Aminoacids (AREA)
  • Saccharide Compounds (AREA)
  • Seasonings (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Processing Of Solid Wastes (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Compounds Of Unknown Constitution (AREA)
CN2011800151398A 2010-01-28 2011-01-27 处理糖苷的混合物以获得更纯的形式的一种或多种这些糖苷的方法 Pending CN102811627A (zh)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710007545.9A CN106986905B (zh) 2010-01-28 2011-01-27 处理糖苷的混合物以获得更纯的形式的一种或多种这些糖苷的方法

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US29916010P 2010-01-28 2010-01-28
US61/299,160 2010-01-28
PCT/US2011/022741 WO2011094423A1 (en) 2010-01-28 2011-01-27 Methods to treat mixtures of glycosides to obtain one or more of these glycosides in more pure form

Related Child Applications (1)

Application Number Title Priority Date Filing Date
CN201710007545.9A Division CN106986905B (zh) 2010-01-28 2011-01-27 处理糖苷的混合物以获得更纯的形式的一种或多种这些糖苷的方法

Publications (1)

Publication Number Publication Date
CN102811627A true CN102811627A (zh) 2012-12-05

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CN2011800151398A Pending CN102811627A (zh) 2010-01-28 2011-01-27 处理糖苷的混合物以获得更纯的形式的一种或多种这些糖苷的方法
CN201710007545.9A Expired - Fee Related CN106986905B (zh) 2010-01-28 2011-01-27 处理糖苷的混合物以获得更纯的形式的一种或多种这些糖苷的方法

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CN201710007545.9A Expired - Fee Related CN106986905B (zh) 2010-01-28 2011-01-27 处理糖苷的混合物以获得更纯的形式的一种或多种这些糖苷的方法

Country Status (14)

Country Link
US (2) US9024012B2 (https=)
EP (1) EP2528455A4 (https=)
JP (1) JP2013518118A (https=)
KR (1) KR20120117895A (https=)
CN (2) CN102811627A (https=)
AR (1) AR080051A1 (https=)
AU (1) AU2011210818B2 (https=)
BR (1) BR112012018791A2 (https=)
CA (1) CA2788359C (https=)
MX (1) MX337550B (https=)
PE (1) PE20121696A1 (https=)
PY (1) PY1102598A (https=)
RU (1) RU2012136639A (https=)
WO (1) WO2011094423A1 (https=)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103458706A (zh) * 2011-01-28 2013-12-18 泰特&莱尔组分美国公司 含有莱鲍迪甙b的甜叶菊掺合物
CN103709215A (zh) * 2013-12-31 2014-04-09 天津北洋百川生物技术有限公司 一种从甜菊糖结晶母液糖中提取莱鲍迪甙d的方法
CN105037458A (zh) * 2015-07-23 2015-11-11 诸城市浩天药业有限公司 一种甜菊糖d苷晶型a、其制备方法及其应用
CN109456371A (zh) * 2018-10-16 2019-03-12 桂林莱茵生物科技股份有限公司 一种高效甜菊糖苷混合物的制备方法

Families Citing this family (28)

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KR20120027363A (ko) 2009-06-16 2012-03-21 이피씨 (베이징) 내추럴 프로덕츠 컴퍼니, 리미티드 뒷맛을 감소시키거나 제거하기 위한 레바우디오사이드 ｄ를 포함하는 조성물 및 그의 제조 방법
AU2011210818B2 (en) * 2010-01-28 2014-10-30 Cargill, Incorporated Methods to treat mixtures of glycosides to obtain one or more of these glycosides in more pure form
US20150344512A1 (en) 2011-12-19 2015-12-03 Purecircle Usa Inc. Methods of purifying steviol glycosides and uses of the same
US9578895B2 (en) 2010-08-23 2017-02-28 Epc (Beijing) Natural Products Co., Ltd. Rebaudioside A and stevioside compositions
WO2012068457A1 (en) 2010-11-19 2012-05-24 Cargill, Incorporated Method for the enrichment of rebaudioside b and/or rebaudioside d in stevia-derived glycoside compositions using adsorb-desorb chromatography with a macroporous neutral adsorbent resin
US9510611B2 (en) * 2010-12-13 2016-12-06 Purecircle Sdn Bhd Stevia composition to improve sweetness and flavor profile
US8962698B2 (en) 2011-01-28 2015-02-24 Tate & Lyle Ingredients Americas Llc Rebaudioside-mogroside V blends
ES2717431T3 (es) 2011-02-10 2019-06-21 Purecircle Usa Composición a base de estevia
US9795156B2 (en) 2011-03-17 2017-10-24 E.P.C (Beijing) Plant Pharmaceutical Technology Co., Ltd Rebaudioside B and derivatives
WO2013066490A1 (en) * 2011-09-06 2013-05-10 Pepsico, Inc. Rebaudioside d sweeteners and food products sweetened with rebaudioside d
EP4124245A1 (en) 2011-12-19 2023-02-01 The Coca-Cola Company Beverage comprising rebaudioside x
GB201217700D0 (en) 2012-08-01 2012-11-14 Tate & Lyle Ingredients Sweetener compositions containing rebaudioside B
MX2015003684A (es) 2012-09-25 2015-06-15 Cargill Inc Mezclas de esteviosidos.
HK1222515A1 (zh) 2012-12-19 2017-07-07 可口可乐公司 用於提高莱鲍迪苷x溶解度的组合物和方法
US20140171519A1 (en) 2012-12-19 2014-06-19 Indra Prakash Compositions and methods for improving rebaudioside x solubility
EP3714699B1 (en) 2013-06-07 2024-12-18 PureCircle USA Inc. Stevia extract containing selected steviol glycosides as flavor, salty and sweetness profile modifier
US10905146B2 (en) 2013-07-12 2021-02-02 The Coca-Cola Company Compositions for improving rebaudioside M solubility
US10264811B2 (en) 2014-05-19 2019-04-23 Epc Natural Products Co., Ltd. Stevia sweetener with improved solubility
US10357052B2 (en) 2014-06-16 2019-07-23 Sweet Green Fields USA LLC Rebaudioside A and stevioside with improved solubilities
US10485256B2 (en) 2014-06-20 2019-11-26 Sweet Green Fields International Co., Limited Stevia sweetener with improved solubility with a cyclodextrin
EP3017708B1 (en) * 2014-10-24 2018-05-02 Red Bull GmbH Sweetening composition
US20170258121A1 (en) * 2014-11-24 2017-09-14 Cargill, Incorporated Glycoside compositions
CA2985669C (en) 2015-05-20 2022-05-03 Cargill, Incorporated Glycoside compositions
US11251343B2 (en) * 2017-02-08 2022-02-15 Current Lighting Solutions, Llc LED design of lower CCT utilizing PFS phosphor
EP3691468A4 (en) 2017-10-06 2021-10-20 Cargill, Incorporated EASILY SOLUBLE STEVIOL GLYCOSIDE COMPOSITIONS
WO2020210118A1 (en) 2019-04-06 2020-10-15 Cargill, Incorporated Sensory modifiers
JP2020031640A (ja) * 2019-10-04 2020-03-05 カーギル インコーポレイテッド 配糖体混合物
WO2022132971A1 (en) * 2020-12-16 2022-06-23 Corn Products Development, Inc. Method for purifying a crude composition comprising one or more steviol glycosides

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US5962678A (en) * 1996-09-13 1999-10-05 Alberta Research Council Method of extracting selected sweet glycosides from the Stevia rebaudiana plant
CN101090642A (zh) * 2004-10-18 2007-12-19 甜美绿色田野有限责任公司 生产纯新蛇菊苷a的高收率方法
CN101220062A (zh) * 2008-01-23 2008-07-16 石任兵 一种同时制备甜菊苷和莱鲍迪苷a的方法
WO2008091547A2 (en) * 2007-01-22 2008-07-31 Cargill, Incorporated Method of producing purified rebaudioside a compositions using solvent/antisolvent crystallization
CN101472487A (zh) * 2006-06-19 2009-07-01 可口可乐公司 甜菊双糖苷a组合物及其纯化方法

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JPS51142570A (en) 1975-06-04 1976-12-08 Morita Kagaku Kogyo Method of imparting sweetness to food or pharmaceutical agent
JPS5262300A (en) 1975-11-13 1977-05-23 Ajinomoto Co Inc Isolation of bibaudioside-a by crystallization
JPS56121454A (en) 1980-02-27 1981-09-24 Ajinomoto Co Inc Separation of stevioside and rebaudioside a by crystallization
JPS56121453A (en) 1980-02-27 1981-09-24 Ajinomoto Co Inc Separation of stevioside and rebaudioside a
US4361697A (en) 1981-05-21 1982-11-30 F. K. Suzuki International, Inc. Extraction, separation and recovery of diterpene glycosides from Stevia rebaudiana plants
US4599403A (en) * 1985-10-07 1986-07-08 Harold Levy Method for recovery of stevioside
ATE97910T1 (de) 1987-07-21 1993-12-15 Roger H Giovanetto Verfahren zur gewinnung von steviosiden aus pflanzlichem rohmaterial.
JP3111203B2 (ja) 1987-12-26 2000-11-20 中里 隆憲 ステビア新品種に属する植物
CN1243835A (zh) 1998-08-05 2000-02-09 黑龙江垦区海林甜菊糖有限责任公司 莱苞迪甙a提取方法
WO2006038221A1 (en) * 2004-10-04 2006-04-13 Council Of Scientific And Industrial Research Process for production of steviosides from stevia rebaudiana bertoni
US7838044B2 (en) * 2004-12-21 2010-11-23 Purecircle Sdn Bhd Extraction, separation and modification of sweet glycosides from the Stevia rebaudiana plant
US7862845B2 (en) * 2005-10-11 2011-01-04 Purecircle Sdn Bhd Process for manufacturing a sweetener and use thereof
US8791253B2 (en) 2006-06-19 2014-07-29 The Coca-Cola Company Rebaudioside A composition and method for purifying rebaudioside A
US8017168B2 (en) * 2006-11-02 2011-09-13 The Coca-Cola Company High-potency sweetener composition with rubisco protein, rubiscolin, rubiscolin derivatives, ace inhibitory peptides, and combinations thereof, and compositions sweetened therewith
CN101200480B (zh) * 2006-12-15 2011-03-30 成都华高药业有限公司 莱鲍迪甙a的提取方法
WO2010118218A1 (en) * 2009-04-09 2010-10-14 Cargill, Incorporated Sweetener composition comprising high solubility form of rebaudioside a and method of making
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Publication number Priority date Publication date Assignee Title
US5962678A (en) * 1996-09-13 1999-10-05 Alberta Research Council Method of extracting selected sweet glycosides from the Stevia rebaudiana plant
CN101090642A (zh) * 2004-10-18 2007-12-19 甜美绿色田野有限责任公司 生产纯新蛇菊苷a的高收率方法
CN101472487A (zh) * 2006-06-19 2009-07-01 可口可乐公司 甜菊双糖苷a组合物及其纯化方法
WO2008091547A2 (en) * 2007-01-22 2008-07-31 Cargill, Incorporated Method of producing purified rebaudioside a compositions using solvent/antisolvent crystallization
CN101220062A (zh) * 2008-01-23 2008-07-16 石任兵 一种同时制备甜菊苷和莱鲍迪苷a的方法

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103458706A (zh) * 2011-01-28 2013-12-18 泰特&莱尔组分美国公司 含有莱鲍迪甙b的甜叶菊掺合物
CN108464425A (zh) * 2011-01-28 2018-08-31 泰特&莱尔组分美国公司 甜叶菊提取物和甜味组合物
CN103458706B (zh) * 2011-01-28 2018-09-14 泰特&莱尔组分美国公司 含有莱鲍迪甙b的甜叶菊掺合物
CN108464425B (zh) * 2011-01-28 2021-10-01 泰特&莱尔组分美国公司 甜叶菊提取物和甜味组合物
CN103709215A (zh) * 2013-12-31 2014-04-09 天津北洋百川生物技术有限公司 一种从甜菊糖结晶母液糖中提取莱鲍迪甙d的方法
CN103709215B (zh) * 2013-12-31 2016-01-06 天津北洋百川生物技术有限公司 一种从甜菊糖结晶母液糖中提取莱鲍迪甙d的方法
CN105037458A (zh) * 2015-07-23 2015-11-11 诸城市浩天药业有限公司 一种甜菊糖d苷晶型a、其制备方法及其应用
CN105037458B (zh) * 2015-07-23 2018-12-28 诸城市浩天药业有限公司 一种甜菊糖d苷晶型a、其制备方法及其应用
US10611789B2 (en) 2015-07-23 2020-04-07 Zhucheng Haotian Pharm Co., Ltd Crystalline form A of rebaudioside D, and preparation method and application therefor
CN109456371A (zh) * 2018-10-16 2019-03-12 桂林莱茵生物科技股份有限公司 一种高效甜菊糖苷混合物的制备方法

Also Published As

Publication number Publication date
CN106986905B (zh) 2019-07-26
CA2788359C (en) 2019-01-08
BR112012018791A2 (pt) 2015-09-01
CA2788359A1 (en) 2011-08-04
RU2012136639A (ru) 2014-03-10
US20120289687A1 (en) 2012-11-15
MX337550B (es) 2016-03-10
CN106986905A (zh) 2017-07-28
EP2528455A1 (en) 2012-12-05
US9024012B2 (en) 2015-05-05
EP2528455A4 (en) 2013-11-27
AU2011210818A1 (en) 2012-08-23
AU2011210818B2 (en) 2014-10-30
PY1102598A (es) 2014-08-01
WO2011094423A1 (en) 2011-08-04
MX2012008546A (es) 2012-09-07
US20160009749A1 (en) 2016-01-14
PE20121696A1 (es) 2012-12-16
JP2013518118A (ja) 2013-05-20
AR080051A1 (es) 2012-03-07
KR20120117895A (ko) 2012-10-24

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