AU2011210818B2 - Methods to treat mixtures of glycosides to obtain one or more of these glycosides in more pure form - Google Patents

Methods to treat mixtures of glycosides to obtain one or more of these glycosides in more pure form Download PDF

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Publication number
AU2011210818B2
AU2011210818B2 AU2011210818A AU2011210818A AU2011210818B2 AU 2011210818 B2 AU2011210818 B2 AU 2011210818B2 AU 2011210818 A AU2011210818 A AU 2011210818A AU 2011210818 A AU2011210818 A AU 2011210818A AU 2011210818 B2 AU2011210818 B2 AU 2011210818B2
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AU
Australia
Prior art keywords
reb
slurry
rebaudioside
glycosides
aging
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
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AU2011210818A
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English (en)
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AU2011210818A1 (en
Inventor
Aron Erickson
John Joseph Hahn
Allan S. Myerson
Andrew Keith Ohmes
Troy Allen Rhonemus
Kern M. Storo
Christopher Austin Tyler
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Cargill Inc
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Cargill Inc
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Publication date
Application filed by Cargill Inc filed Critical Cargill Inc
Publication of AU2011210818A1 publication Critical patent/AU2011210818A1/en
Application granted granted Critical
Publication of AU2011210818B2 publication Critical patent/AU2011210818B2/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/30—Artificial sweetening agents
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H15/00—Compounds containing hydrocarbon or substituted hydrocarbon radicals directly attached to hetero atoms of saccharide radicals
    • C07H15/20—Carbocyclic rings
    • C07H15/24—Condensed ring systems having three or more rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H15/00—Compounds containing hydrocarbon or substituted hydrocarbon radicals directly attached to hetero atoms of saccharide radicals
    • C07H15/20—Carbocyclic rings
    • C07H15/24—Condensed ring systems having three or more rings
    • C07H15/256—Polyterpene radicals
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof
    • A23L2/52—Adding ingredients
    • A23L2/60—Sweeteners
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/30—Artificial sweetening agents
    • A23L27/33—Artificial sweetening agents containing sugars or derivatives
    • A23L27/36—Terpene glycosides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H1/00—Processes for the preparation of sugar derivatives
    • C07H1/06—Separation; Purification
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Nutrition Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Genetics & Genomics (AREA)
  • General Health & Medical Sciences (AREA)
  • Biotechnology (AREA)
  • Molecular Biology (AREA)
  • Biochemistry (AREA)
  • Proteomics, Peptides & Aminoacids (AREA)
  • Saccharide Compounds (AREA)
  • Seasonings (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Processing Of Solid Wastes (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Compounds Of Unknown Constitution (AREA)
AU2011210818A 2010-01-28 2011-01-27 Methods to treat mixtures of glycosides to obtain one or more of these glycosides in more pure form Expired - Fee Related AU2011210818B2 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US29916010P 2010-01-28 2010-01-28
US61/299,160 2010-01-28
PCT/US2011/022741 WO2011094423A1 (en) 2010-01-28 2011-01-27 Methods to treat mixtures of glycosides to obtain one or more of these glycosides in more pure form

Publications (2)

Publication Number Publication Date
AU2011210818A1 AU2011210818A1 (en) 2012-08-23
AU2011210818B2 true AU2011210818B2 (en) 2014-10-30

Family

ID=44319766

Family Applications (1)

Application Number Title Priority Date Filing Date
AU2011210818A Expired - Fee Related AU2011210818B2 (en) 2010-01-28 2011-01-27 Methods to treat mixtures of glycosides to obtain one or more of these glycosides in more pure form

Country Status (14)

Country Link
US (2) US9024012B2 (https=)
EP (1) EP2528455A4 (https=)
JP (1) JP2013518118A (https=)
KR (1) KR20120117895A (https=)
CN (2) CN102811627A (https=)
AR (1) AR080051A1 (https=)
AU (1) AU2011210818B2 (https=)
BR (1) BR112012018791A2 (https=)
CA (1) CA2788359C (https=)
MX (1) MX337550B (https=)
PE (1) PE20121696A1 (https=)
PY (1) PY1102598A (https=)
RU (1) RU2012136639A (https=)
WO (1) WO2011094423A1 (https=)

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KR20120027363A (ko) 2009-06-16 2012-03-21 이피씨 (베이징) 내추럴 프로덕츠 컴퍼니, 리미티드 뒷맛을 감소시키거나 제거하기 위한 레바우디오사이드 ｄ를 포함하는 조성물 및 그의 제조 방법
AU2011210818B2 (en) * 2010-01-28 2014-10-30 Cargill, Incorporated Methods to treat mixtures of glycosides to obtain one or more of these glycosides in more pure form
US20150344512A1 (en) 2011-12-19 2015-12-03 Purecircle Usa Inc. Methods of purifying steviol glycosides and uses of the same
US9578895B2 (en) 2010-08-23 2017-02-28 Epc (Beijing) Natural Products Co., Ltd. Rebaudioside A and stevioside compositions
WO2012068457A1 (en) 2010-11-19 2012-05-24 Cargill, Incorporated Method for the enrichment of rebaudioside b and/or rebaudioside d in stevia-derived glycoside compositions using adsorb-desorb chromatography with a macroporous neutral adsorbent resin
US9510611B2 (en) * 2010-12-13 2016-12-06 Purecircle Sdn Bhd Stevia composition to improve sweetness and flavor profile
US8962698B2 (en) 2011-01-28 2015-02-24 Tate & Lyle Ingredients Americas Llc Rebaudioside-mogroside V blends
KR101797644B1 (ko) * 2011-01-28 2017-11-15 테이트 앤드 라일 인그리디언츠 어메리카즈 엘엘씨 레바우디오사이드 b를 포함하는 스테비아 블렌드
ES2717431T3 (es) 2011-02-10 2019-06-21 Purecircle Usa Composición a base de estevia
US9795156B2 (en) 2011-03-17 2017-10-24 E.P.C (Beijing) Plant Pharmaceutical Technology Co., Ltd Rebaudioside B and derivatives
WO2013066490A1 (en) * 2011-09-06 2013-05-10 Pepsico, Inc. Rebaudioside d sweeteners and food products sweetened with rebaudioside d
EP4124245A1 (en) 2011-12-19 2023-02-01 The Coca-Cola Company Beverage comprising rebaudioside x
GB201217700D0 (en) 2012-08-01 2012-11-14 Tate & Lyle Ingredients Sweetener compositions containing rebaudioside B
MX2015003684A (es) 2012-09-25 2015-06-15 Cargill Inc Mezclas de esteviosidos.
HK1222515A1 (zh) 2012-12-19 2017-07-07 可口可乐公司 用於提高莱鲍迪苷x溶解度的组合物和方法
US20140171519A1 (en) 2012-12-19 2014-06-19 Indra Prakash Compositions and methods for improving rebaudioside x solubility
EP3714699B1 (en) 2013-06-07 2024-12-18 PureCircle USA Inc. Stevia extract containing selected steviol glycosides as flavor, salty and sweetness profile modifier
US10905146B2 (en) 2013-07-12 2021-02-02 The Coca-Cola Company Compositions for improving rebaudioside M solubility
CN103709215B (zh) * 2013-12-31 2016-01-06 天津北洋百川生物技术有限公司 一种从甜菊糖结晶母液糖中提取莱鲍迪甙d的方法
US10264811B2 (en) 2014-05-19 2019-04-23 Epc Natural Products Co., Ltd. Stevia sweetener with improved solubility
US10357052B2 (en) 2014-06-16 2019-07-23 Sweet Green Fields USA LLC Rebaudioside A and stevioside with improved solubilities
US10485256B2 (en) 2014-06-20 2019-11-26 Sweet Green Fields International Co., Limited Stevia sweetener with improved solubility with a cyclodextrin
EP3017708B1 (en) * 2014-10-24 2018-05-02 Red Bull GmbH Sweetening composition
US20170258121A1 (en) * 2014-11-24 2017-09-14 Cargill, Incorporated Glycoside compositions
CA2985669C (en) 2015-05-20 2022-05-03 Cargill, Incorporated Glycoside compositions
CN105037458B (zh) * 2015-07-23 2018-12-28 诸城市浩天药业有限公司 一种甜菊糖d苷晶型a、其制备方法及其应用
US11251343B2 (en) * 2017-02-08 2022-02-15 Current Lighting Solutions, Llc LED design of lower CCT utilizing PFS phosphor
EP3691468A4 (en) 2017-10-06 2021-10-20 Cargill, Incorporated EASILY SOLUBLE STEVIOL GLYCOSIDE COMPOSITIONS
CN109456371A (zh) * 2018-10-16 2019-03-12 桂林莱茵生物科技股份有限公司 一种高效甜菊糖苷混合物的制备方法
WO2020210118A1 (en) 2019-04-06 2020-10-15 Cargill, Incorporated Sensory modifiers
JP2020031640A (ja) * 2019-10-04 2020-03-05 カーギル インコーポレイテッド 配糖体混合物
WO2022132971A1 (en) * 2020-12-16 2022-06-23 Corn Products Development, Inc. Method for purifying a crude composition comprising one or more steviol glycosides

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20060083838A1 (en) * 2004-10-18 2006-04-20 Sweet Aloha Farms, L.L.C. High yield method of producing pure rebaudioside A
US20070082103A1 (en) * 2005-10-11 2007-04-12 Stevian Biotechnology Corporation Sdn. Bhd Process for manufacturing a sweetner and use thereof
US20070292582A1 (en) * 2006-06-19 2007-12-20 The Coca-Cola Company Rebaudioside A Composition and Method for Purifying Rebaudioside A
WO2008091547A2 (en) * 2007-01-22 2008-07-31 Cargill, Incorporated Method of producing purified rebaudioside a compositions using solvent/antisolvent crystallization
WO2010118218A1 (en) * 2009-04-09 2010-10-14 Cargill, Incorporated Sweetener composition comprising high solubility form of rebaudioside a and method of making

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JPS56121454A (en) 1980-02-27 1981-09-24 Ajinomoto Co Inc Separation of stevioside and rebaudioside a by crystallization
JPS56121453A (en) 1980-02-27 1981-09-24 Ajinomoto Co Inc Separation of stevioside and rebaudioside a
US4361697A (en) 1981-05-21 1982-11-30 F. K. Suzuki International, Inc. Extraction, separation and recovery of diterpene glycosides from Stevia rebaudiana plants
US4599403A (en) * 1985-10-07 1986-07-08 Harold Levy Method for recovery of stevioside
ATE97910T1 (de) 1987-07-21 1993-12-15 Roger H Giovanetto Verfahren zur gewinnung von steviosiden aus pflanzlichem rohmaterial.
JP3111203B2 (ja) 1987-12-26 2000-11-20 中里 隆憲 ステビア新品種に属する植物
US5962678A (en) 1996-09-13 1999-10-05 Alberta Research Council Method of extracting selected sweet glycosides from the Stevia rebaudiana plant
CN1243835A (zh) 1998-08-05 2000-02-09 黑龙江垦区海林甜菊糖有限责任公司 莱苞迪甙a提取方法
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US7838044B2 (en) * 2004-12-21 2010-11-23 Purecircle Sdn Bhd Extraction, separation and modification of sweet glycosides from the Stevia rebaudiana plant
CN101472487B (zh) * 2006-06-19 2013-05-01 可口可乐公司 甜菊双糖苷a组合物及其纯化方法
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AU2011210818B2 (en) * 2010-01-28 2014-10-30 Cargill, Incorporated Methods to treat mixtures of glycosides to obtain one or more of these glycosides in more pure form

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US20060083838A1 (en) * 2004-10-18 2006-04-20 Sweet Aloha Farms, L.L.C. High yield method of producing pure rebaudioside A
US20070082103A1 (en) * 2005-10-11 2007-04-12 Stevian Biotechnology Corporation Sdn. Bhd Process for manufacturing a sweetner and use thereof
US20070292582A1 (en) * 2006-06-19 2007-12-20 The Coca-Cola Company Rebaudioside A Composition and Method for Purifying Rebaudioside A
WO2008091547A2 (en) * 2007-01-22 2008-07-31 Cargill, Incorporated Method of producing purified rebaudioside a compositions using solvent/antisolvent crystallization
WO2010118218A1 (en) * 2009-04-09 2010-10-14 Cargill, Incorporated Sweetener composition comprising high solubility form of rebaudioside a and method of making

Also Published As

Publication number Publication date
CN106986905B (zh) 2019-07-26
CA2788359C (en) 2019-01-08
BR112012018791A2 (pt) 2015-09-01
CA2788359A1 (en) 2011-08-04
RU2012136639A (ru) 2014-03-10
US20120289687A1 (en) 2012-11-15
CN102811627A (zh) 2012-12-05
MX337550B (es) 2016-03-10
CN106986905A (zh) 2017-07-28
EP2528455A1 (en) 2012-12-05
US9024012B2 (en) 2015-05-05
EP2528455A4 (en) 2013-11-27
AU2011210818A1 (en) 2012-08-23
PY1102598A (es) 2014-08-01
WO2011094423A1 (en) 2011-08-04
MX2012008546A (es) 2012-09-07
US20160009749A1 (en) 2016-01-14
PE20121696A1 (es) 2012-12-16
JP2013518118A (ja) 2013-05-20
AR080051A1 (es) 2012-03-07
KR20120117895A (ko) 2012-10-24

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MK25 Application lapsed reg. 22.2i(2) - failure to pay acceptance fee