CN102670456A - Multi-effect facial cream and preparation method thereof - Google Patents
Multi-effect facial cream and preparation method thereof Download PDFInfo
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- CN102670456A CN102670456A CN2012101837654A CN201210183765A CN102670456A CN 102670456 A CN102670456 A CN 102670456A CN 2012101837654 A CN2012101837654 A CN 2012101837654A CN 201210183765 A CN201210183765 A CN 201210183765A CN 102670456 A CN102670456 A CN 102670456A
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Abstract
The invention provides a multi-effect facial cream and a preparation method thereof. The multi-effect facial cream comprises the following components in percentage by weight: component A including 60 to 80 % of water, 0.1 to 0.6 % of ceramide, 0.1 to 0.2 % of allantoin, 0.1 to 0.35 % of xanthan gum, and 0.5 to 1.5 % of SEPIPLUS265; component B including 2 to 8 % of 1,3 butanediol and 0.01 to 0.1 % of glabridin; component C including 1 to 3 % of acetyl tetrapeptide-9, 2 to 5 % of mentha piperita extracting solution, 0.1 to 0.3 % of preservative and 0.1 to 0.5 % of essence; component D including 2.0 to 4.0 % of EMULIUMDELTA, 0.5 to 2 % of wool grease, 2 to 6 % of jojoba oil, 0.5 to 2.0 % of cetostearyl alcohol, 2 to 6 % of caprylic acid propyl heptanoic ester and 1 to 5 % of PDMS (polydimethylsiloxane); and if the amount of the facial cream is 100%, the component A occupies 60 to 80%, the component B occupies 2 to 10%, the component C occupies 5 to 9%, and the component D occupies 12 to 22%. The preparation method comprises the following steps: 1), heating the component A and the component D to 80 DEG C through an electric furnace respectively; 2), stirring the component A through a stirrer, slowly adding the component D into the component A, and homogenizing for 2 minutes through a homogenizer after addition; 3), cooling down to 40 DEG C while stirring through the stirrer, adding the component B, stirring to dissolve, and stirring through the stirrer evenly after adding the component C; and 4) discharging, thus the facial cream is made.
Description
Technical field
The present invention relates to a kind of facial cream, refer to especially a kind of integrate preserve moisture, whiten, the multiple-effect washing cream of defying age, antiallergic multiple efficacies.
Background technology
Have much on the market at present whiten, preserve moisture, the cosmetics of single effects such as defying age, antiallergic; Wanting to reach above effect must all will use by each cosmetics; Modern's rhythm of life is more and more faster, and is unrealistic like this, also can bring financial burden to consumer simultaneously.
Summary of the invention
To the single present situation of existing facial cream effect, the technical problem that the present invention will solve is: provide a kind of integrate preserve moisture, whiten, the multiple-effect washing cream of defying age, antiallergic multiple efficacies.
To this, the present invention provides a kind of multiple-effect washing cream, by weight percentage, is made up of following component:
A component: water 60-80%, ceramide 0.1-0.6%, allantoin 0.1-0.25%, HANSHENGJIAO 0.1-0.35%, SEPIPLUS 265:0.5-1.5%;
B component: 1,3 butanediol 2-8%, glabridin 0.01-0.1%;
C component: acetyl group tetrapeptide-9:1-3%, Mentha piperita extracting solution 2-5%, antiseptic 0.1-0.3%, essence 0.1-0.5%;
D component: EMULIUM DELTA:2.0-4.0%, lanoline 0.5-2%, Jojoba oil 2-6%, cetearyl alcohol 0.5-2.0%, sad propyl group heptyl ester 2-6%, polydimethylsiloxane 1-5%;
In multiple-effect washing cream is 100%, and said A component is 60-80%, and said B component is 2-10%, and said C component is 5-9%, and said D component is 12-22%.
Wherein, said SEPIPLUS 265 is that France matches the raw material of releasing at the beginning of the BIC Corp 2004, and it contains acrylamide, ammonium acrylate copolymer, polyisobutylene and polysorbate-20.
Said antiseptic adopts the DMDM hydantoin.
Said essence adopts Fructus Citri Limoniae essence, purchases the Ke Dao company in Shanghai.
Said EMULIUM DELTA is the raw material that the good method lion company of France released in 1998, and it contains spermol, glyceryl stearate, PEG-75 stearate, spermol polyethers-20 and stearyl alcohol polyethers-20.
The present invention also provides a kind of method for preparing multiple-effect washing cream, comprises following step:
1) A component and D component are heated to 80 ℃ with electric furnace respectively;
2) the A component is stirred with blender, simultaneously the D component is slowly added in the A component, after adding, reuse homogenizer homogenizing 2 minutes;
3) limit is stirred the limit with blender and is cooled to 40 ℃ with cold water, adds the B component, stirring and dissolving, then add the C component after, the reuse blender stirs;
4) multiple-effect washing cream is promptly processed in discharging.
Preferably, the mixing speed of said blender is 200r/min.
Preferably, the time that adds said D component is 1 minute.
Preferably, the homogenizing speed of said homogenizer is 2000r/min.
The invention has the beneficial effects as follows: the invention provides a kind of multiple-effect washing cream because multiple-effect washing cream of the present invention simultaneously Pear Power, preserve moisture, defying age, antiallergic effect, specifically comprise:
1. white-skinned face function: the multiple-effect washing cream among the present invention is through having inhibitory action to main melanin synthetic proteins enzyme-tyrosinase activity, dopachrome interconvertible enzyme activity etc.; Just can reach the melanic effect of good restraining as long as add very little consumption, thereby reach white-skinned face function.
2. moisture-keeping efficacy: the multiple-effect washing cream among the present invention is adsorbed on skin surface and forms liquid crystal, makes the skin feel good; After the skin absorbs, quick and degree of depth ground association moisture forms long-acting preserving moisture.
3. senile-resistant efficacy: the multiple-effect washing cream among the present invention works on photoprotein polysaccharide and I collagen type; Can form the functional network of closely knit, regular collagen fabric; Improve the degree of packing and the structure of skin, experiment confirm has good aging resistance function.
4. antiallergic effect: thus the multiple-effect washing cream among the present invention is through reducing main inflammatory mediator inflammation-inhibiting reaction, can stimulate the generation of β-Nei calf peptide-" happiness " neuropeptide simultaneously, makes skin present the state that health is releived.
5. the multiple-effect washing cream among the present invention has no side effect to skin, and effect is obvious, be fit to the crowd of various age levels, and manufacturing process of the present invention is simple, does not need complex apparatus and technology, and cost is low.
Description of drawings
Fig. 1 is the dermal melanin variation figure among the embodiment 4 among the present invention.
Fig. 2 is skin moisture changes of contents figure among the embodiment 5 among the present invention.
Fig. 3 is R2 among the embodiment 6 among the present invention, R5, R7 value variation diagram.
The specific embodiment
Below in conjunction with accompanying drawing, more excellent embodiment of the present invention is done further detailed description:
Embodiment 1:A component is by 75.9 gram water, and 0.3 restrains ceramide, 0.15 gram allantoin, and 0.2 gram HANSHENGJIAO, 0.7 gram SEPIPLUS 265 forms; The B component is made up of 4 gram 1,3 butanediols and 0.05 gram glabridin; The C component is by 2 gram acetyl group tetrapeptides-9,3 gram Mentha piperita extracting solution, 0.2 gram DMDM hydantoin, and 0.2 gram Fructus Citri Limoniae essence is formed; The D component is made up of 2.5 gram EMULIUM DELTA, 0.8 gram lanoline, 4 gram Jojoba oils, 1 gram cetearyl alcohol, the sad propyl group heptyl ester of 3 grams, 2 gram polydimethylsiloxane.
Concrete steps are following: 1) A component and D component are heated to 80 ℃ with electric furnace respectively; 2) the A component is stirred (mixing speed 200r/min) with blender, simultaneously the D component is slowly added in the A component, after adding, reuse homogenizer homogenizing 2 minutes (homogenizing speed 2000r/min); 3) limit is stirred the limit with blender and is cooled to 40 ℃ with cold water, adds the B component, stirring and dissolving, then add the C component after, the reuse blender stirs; 4) multiple-effect washing cream is promptly processed in discharging.
Example 2:A component: water 78.1%, ceramide 0.1%, allantoin 0.25%, HANSHENGJIAO 0.35%, SEPIPLUS 265 0.5%; B component: 1,3 butanediol 2.0%, glabridin 0.1%; The C component contains acetyl group tetrapeptide-9 1.0%, Mentha piperita extracting solution 5.0%, DMDM hydantoin 0.1%, Fructus Citri Limoniae essence 0.5%; The D component contains EMULIUM DELTA 2%, lanoline 0.5%, Jojoba oil 6%, cetearyl alcohol 0.5%, sad propyl group heptyl ester 2.0%, polydimethylsiloxane 1.0%.
Concrete steps are following: 1) A component and D component are heated to 80 ℃ with electric furnace respectively; 2) the A component is stirred (mixing speed 200r/min) with blender, simultaneously the D component is slowly added in the A component, after adding, reuse homogenizer homogenizing 2 minutes (homogenizing speed 2000r/min); 3) limit is stirred the limit with blender and is cooled to 40 ℃ with cold water, adds the B component, stirring and dissolving, then add the C component after, the reuse blender stirs; 4) multiple-effect washing cream is promptly processed in discharging.
Embodiment 3:A component contains water 63.29%, ceramide 0.6%, allantoin 0.1%, HANSHENGJIAO 0.1%, SEPIPLUS 265:1.5%; The B component contains 1,3 butanediol 8.0%, glabridin 0.01%; The C component contains acetyl group tetrapeptide-9 3.0%, Mentha piperita extracting solution 2.0%, DMDM hydantoin 0.3%, Fructus Citri Limoniae essence 0.1%; The D component contains EMULIUM DELTA:4%, lanoline 2%, Jojoba oil 2%, cetearyl alcohol 2%, sad propyl group heptyl ester 6.0%, polydimethylsiloxane 5%.
Concrete steps are following: 1) A component and D component are heated to 80 ℃ with electric furnace respectively; 2) the A component is stirred (mixing speed 200r/min) with blender, simultaneously the D component is slowly added in the A component, after adding, reuse homogenizer homogenizing 2 minutes (homogenizing speed 2000r/min); 3) limit is stirred the limit with blender and is cooled to 40 ℃ with cold water, adds the B component, stirring and dissolving, then add the C component after, the reuse blender stirs; 4) multiple-effect washing cream is promptly processed in discharging.
Experiment proof: have through the prepared facial cream that obtains of test proof preserve moisture, whiten, defying age and antiallergic effect.Select for use embodiment 1 prepared facial cream to test, concrete effect is tested as follows:
Embodiment 4: the whitening effect test
Test instrunment: the skin elasticity Cotometer MPA580 main frame that German Courage+Khazaka company (German CK company) makes, employed probe is dermal melanin and red pigment Mexameter MX18 test probe.
Experimenter's quantity and condition: the normal subjects women in 30 35-45 years.
Test zone: the place between the eyebrows middle is down 2cm chin area, the left and right cheek region of nose and pupil intersection place of 2cm forehead zone, lower lip middle up.
Testing procedure: measure the blank value of test zone cleaning back 30min earlier, press the product description consumption then and use step, sample is evenly coated face.Sooner or later adhere to every day using, must not use other cosmetics, used for 8 weeks continuously, test the dermal melanin of the 1st week, 2 weeks, 3 weeks, 4 weeks, 6 weeks, 8 all pilot regions respectively.Same experimenter's test is accomplished by same survey crew.Through test these 30 experimenters use before and after the variation of dermal melanin numbers (meansigma methods) assess the skin whitening efficacy of this product, the black prime number changes as shown in table 1:
Table 1: dermal melanin changes
| Test period (week) | 0 | 1 | 2 | 3 | 4 | 6 | 8 |
| Melanin (meansigma methods) | 320 | 310 | 300 | 285 | 225 | 180 | 170 |
Annotate: melanin:＜100 represent hypomelanism, easily sunburn; 100-200 is normal, and skin is more pale;＞200 melanin are more, and skin protection power is strong, and skin is more black.
As can beappreciated from fig. 1, use this frost back the 3rd all melanic numerical value to have more significantly and descend, the 5th week just was tending towards normal value, and 6-8 week melanin descends and tends towards stability, in normal range.The melanin rate of descent is 46.88%, proves this white Magnesium Ascorbylphosphate.
Embodiment 5: the moistening effect test
Test instrunment: the skin elasticity Cotometer MPA580 main frame that German Courage+Khazaka company (German CK company) makes, employed probe is a skin moisture content Cornemeter CM825 test probe.
Experimenter's quantity and condition: the normal subjects women in 30 35-45 years.
Test zone: two 4 * 4cm pilot regions of the inboard labelling of experimenter's left hand forearm, interregional at a distance from 2cm.
Testing procedure: use test sample in zone therein, another zone is as blank contrast.Measure earlier each test zone cleaning and dry the blank value of back 0.5h with clean napkin, by the consumption of every square centimeter in 2.0 ± 0.1 mg samples, the use latex finger cot is evenly coated sample in the trial zone then.Measure the skin moisture content that 0.5h, 1h, 1.5h, 2h, 4h, 6h, 8h are tried zone and blank zone after smearing respectively, same experimenter's test is accomplished by same survey crew.Tried the skin moisture-keeping effect that this product is assessed in the variation regional and skin moisture content that blank is regional through test, test data changes as shown in table 2:
Table 2: skin moisture changes of contents
| Test period (week) | 0 | 0.5 | 1 | 1.5 | 2 | 4 | 6 | 8 |
| Blank value (meansigma methods) | 29.5 | 30.9 | 32.4 | 31.5 | 28.3 | 29.1 | 30.5 | 31.7 |
| Moisture (meansigma methods) | 31.6 | 32.5 | 45.5 | 51.0 | 53.2 | 54.7 | 58.0 | 52.4 |
Annotate: the pairing value of abscissa zero graduation is the test zone cleaning and dries the measured blank value of 0.5h afterwards with clean napkin.
As can beappreciated from fig. 2; Using this facial cream to be tried regional moisture after 1 hour has more obviously and to increase, and moisture keeps increasing always, after 6 hours, just begins to have slight decline; The 8th hour moisture 52.4% proves that this facial cream has moisture-keeping efficacy.
Embodiment 6: the defying age measure of merit
Test instrunment: the skin elasticity Cotometer MPA580 main frame that German Courage+Khazaka company (German CK company) makes, employed probe is a Reviscometer RV600 elastic fibrous tissue test probe.
Experimenter's quantity and condition: the normal subjects women in 30 35-45 years
Test zone: the place between the eyebrows middle is down 2cm chin area, the left and right cheek region of nose and pupil intersection place of 2cm forehead zone, lower lip middle up.
Testing procedure: blank value (R2, R5, R7, R2=Ua/Uf wherein, R5=Ur/Ue, R7=Ur/Uf, the Uf--skin maximum tension amount of measuring earlier test zone cleaning back 30min;
After the Ue--constant negative pressure is added on the skin; 0.1 the amount of tension of skin during second, location elastic part amount of tension; After the Ur--cancellation negative pressure, the skin attitude that will restore to the original state rapidly is divided into elastic score value Ur equally, promptly cancels negative pressure after 0.1 second, and recovery value and the viscoelasticity of skin partly are worth, or title plasticity partly is worth; Ua--is from the recovery value of cancellation negative pressure skin when the follow-on test skin surface adds negative pressure more next time), press product description consumption and use step then, sample is evenly coated face.Sooner or later adhere to every day using, must not use other cosmetics, used for 8 weeks continuously, test the R2 of the skin of the 1st week, 2 weeks, 3 weeks, 4 weeks, 6 weeks, 8 all pilot regions respectively, R5, R7.Same experimenter's test is accomplished by same survey crew.Through the R2 of skin before and after the test use, R5, the R7 value changes the skin anti-aging effect of assessing this product, R2, R5, the R7 value changes as follows:
Table 3:R2, R5, the R7 value changes
In the table 3, R2, R5, R7 are more near 1, and skin elasticity is good more, can be got by Fig. 3; Prepared first week of facial cream back R2, R5, R7 increase to some extent, the 4th all R2, R5, R7 rise obviously; 4-8 week R2, R5, the R7 value levels off to 1, this shows that this frost has increase skin elasticity, senile-resistant efficacy.
Embodiment 7: the antiallergic measure of merit
Experimenter's quantity and condition: the normal subjects women in 30 35-45 years.
Testing procedure: two 4 * 4cm pilot regions of the inboard labelling of experimenter's left hand forearm, interregional at a distance from 2cm.Use test sample in zone therein, used 5 days as blank contrast continuously in another zone, uses lactic acid solutions in these two zones then, characterizes this frost and have the antiallergic analgesic activity through detecting sensation of pricking.
Test result: 80% experimenter feels not use the test zone tingle of the prepared facial cream of the present invention to use this white test zone not have obvious sensation of pricking, proves that this frost has the antiallergic effect.
Can know by above test result, the multiple-effect washing cream Pear Power among the present invention, preserve moisture, defying age and antiallergic analgesic activity.
Above content is to combine concrete preferred implementation to the further explain that the present invention did, and can not assert that practical implementation of the present invention is confined to these explanations.For the those of ordinary skill of technical field under the present invention, under the prerequisite that does not break away from the present invention's design, can also make some simple deduction or replace, all should be regarded as belonging to protection scope of the present invention.
Claims (9)
1. a multiple-effect washing cream is characterized in that, by weight percentage, is made up of following component:
A component: water 60-80%, ceramide 0.1-0.6%, allantoin 0.1-0.25%, HANSHENGJIAO 0.1-0.35%, SEPIPLUS 265:0.5-1.5%;
B component: 1,3 butanediol 2-8%, glabridin 0.01-0.1%;
C component: acetyl group tetrapeptide-9:1-3%, Mentha piperita extracting solution 2-5%, antiseptic 0.1-0.3%, essence 0.1-0.5%;
D component: EMULIUM DELTA:2.0-4.0%, lanoline 0.5-2%, Jojoba oil 2-6%, cetearyl alcohol 0.5-2.0%, sad propyl group heptyl ester 2-6%, polydimethylsiloxane 1-5%;
In multiple-effect washing cream is 100%, and said A component is 60-80%, and said B component is 2-10%, and said C component is 5-9%, and said D component is 12-22%.
2. multiple-effect washing cream as claimed in claim 1 is characterized in that, said SEPIPLUS 265 is the mixture of acrylamide, ammonium acrylate copolymer, polyisobutylene and polysorbate-20.
3. multiple-effect washing cream as claimed in claim 1 is characterized in that, said antiseptic adopts the DMDM hydantoin.
4. multiple-effect washing cream as claimed in claim 1 is characterized in that, said essence adopts Fructus Citri Limoniae essence.
5. multiple-effect washing cream as claimed in claim 1 is characterized in that, said EMULIUM DELTA is the mixture of spermol, glyceryl stearate, PEG-75 stearate, spermol polyethers-20 and stearyl alcohol polyethers-20.
6. a method for preparing multiple-effect washing cream is characterized in that, comprises that said method comprises following several steps like each described multiple-effect washing cream of claim 1 to 5:
1) A component and D component are heated to 80 ℃ with electric furnace respectively;
2) the A component is stirred with blender, simultaneously the D component is slowly added in the A component, after adding, reuse homogenizer homogenizing 2 minutes;
3) limit is stirred the limit with blender and is cooled to 40 ℃ with cold water, adds the B component, stirring and dissolving, then add the C component after, the reuse blender stirs;
4) multiple-effect washing cream is promptly processed in discharging.
7. method as claimed in claim 6 is characterized in that, the mixing speed of said blender is 200r/min.
8. method as claimed in claim 6 is characterized in that, the time of said adding D component is 1 minute.
9. method as claimed in claim 6 is characterized in that, the homogenizing speed of said homogenizer is 2000r/min.
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| CN104173212A (en) * | 2014-09-10 | 2014-12-03 | 百莲凯国际企业管理（北京）有限公司 | Regenerative cream and preparation technology thereof |
| CN104257536A (en) * | 2014-09-04 | 2015-01-07 | 刘永东 | Horse oil moisturizing cream for babies and preparation method of horse oil moisturizing cream |
| CN104306196A (en) * | 2014-09-24 | 2015-01-28 | 中华人民共和国惠州出入境检验检疫局 | Multi-effect whitening and skin tendering compound essential oil and preparation method thereof |
| CN105496815A (en) * | 2015-12-21 | 2016-04-20 | 韩后化妆品有限公司 | Stable sun cream adopting double gel systems and preparation method of sun cream |
| CN110339124A (en) * | 2019-08-22 | 2019-10-18 | 台州市奥拉克医疗美容整形门诊部有限公司 | A kind of cosmetic face cream and preparation method thereof for whitening spot-removing |
| CN111568811A (en) * | 2020-05-21 | 2020-08-25 | 鹂诺生物医药科技(上海)有限公司 | Skin-care cream and preparation method thereof |
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| CN102670456B (en) | 2013-06-12 |
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