CN102670456B - Multi-effect facial cream and preparation method thereof - Google Patents

Abstract

The invention provides a multi-effect facial cream and a preparation method thereof. The multi-effect facial cream comprises the following components in percentage by weight: component A including 60 to 80 % of water, 0.1 to 0.6 % of ceramide, 0.1 to 0.2 % of allantoin, 0.1 to 0.35 % of xanthan gum, and 0.5 to 1.5 % of SEPIPLUS265; component B including 2 to 8 % of 1,3 butanediol and 0.01 to 0.1 % of glabridin; component C including 1 to 3 % of acetyl tetrapeptide-9, 2 to 5 % of mentha piperita extracting solution, 0.1 to 0.3 % of preservative and 0.1 to 0.5 % of essence; component D including 2.0 to 4.0 % of EMULIUMDELTA, 0.5 to 2 % of wool grease, 2 to 6 % of jojoba oil, 0.5 to 2.0 % of cetostearyl alcohol, 2 to 6 % of caprylic acid propyl heptanoic ester and 1 to 5 % of PDMS (polydimethylsiloxane); and if the amount of the facial cream is 100%, the component A occupies 60 to 80%, the component B occupies 2 to 10%, the component C occupies 5 to 9%, and the component D occupies 12 to22%. The preparation method comprises the following steps: 1), heating the component A and the component D to 80 DEG C through an electric furnace respectively; 2), stirring the component A through astirrer, slowly adding the component D into the component A, and homogenizing for 2 minutes through a homogenizer after addition; 3), cooling down to 40 DEG C while stirring through the stirrer, adding the component B, stirring to dissolve, and stirring through the stirrer evenly after adding the component C; and 4) discharging, thus the facial cream is made.

Description

A kind of multiple-effect washing cream and preparation method thereof

Technical field

The present invention relates to a kind of facial cream, espespecially a kind of multiple-effect washing cream that integrates moisturizing, whitening, defying age, antiallergic multiple efficacies.

Background technology

The cosmetics that the single effects such as a lot of whitenings, moisturizing, defying age, antiallergic are arranged at present on the market, wanting to reach above effect must all will use by each cosmetics, modern's rhythm of life is more and more faster, and is unrealistic like this, also can bring financial burden to consumer simultaneously.

Summary of the invention

For the existing single present situation of facial cream effect, the technical problem to be solved in the present invention is: a kind of multiple-effect washing cream that integrates moisturizing, whitening, defying age, antiallergic multiple efficacies is provided.

To this, the invention provides a kind of multiple-effect washing cream, by weight percentage, formed by following component:

A component: water 60-80%, ceramide 0.1-0.6%, allantoin 0.1-0.25%, HANSHENGJIAO 0.1-0.35%, SEPIPLUS 265:0.5-1.5%;

B component: 1,3 butanediol 2-8%, glabridin 0.01-0.1%;

C component: acetyl group tetrapeptide-9:1-3%, Mentha piperita extracting solution 2-5%, antiseptic 0.1-0.3%, essence 0.1-0.5%;

D component: EMULIUM DELTA:2.0-4.0%, lanoline 0.5-2%, Jojoba oil 2-6%, cetearyl alcohol 0.5-2.0%, sad propyl group heptyl ester 2-6%, polydimethylsiloxane 1-5%;

Take multiple-effect washing cream as 100%, described A component is 60-80%, and described B component is 2-10%, and described C component is 5-9%, and described D component is 12-22%.

Wherein, described SEPIPLUS 265 is that France matches the raw material of releasing at the beginning of BIC Corp 2004, and it contains acrylamide, ammonium acrylate copolymer, polyisobutylene and polysorbate-20.

Described antiseptic adopts the DMDM hydantoin.

Described essence adopts Fructus Citri Limoniae essence, purchases in Shanghai Ke Dao company.

Described EMULIUM DELTA is the raw material that France good method lion company released in 1998, and it contains spermol, glyceryl stearate, PEG-75 stearate, spermol polyethers-20 and stearyl alcohol polyethers-20.

The present invention also provides a kind of method for preparing multiple-effect washing cream, comprises following step:

1) A component and D component are heated to 80 ℃ with electric furnace respectively;

2) the A component is stirred with blender, simultaneously the D component is slowly added in the A component, after adding, then used the homogenizer homogenizing 2 minutes;

3) limit is stirred the limit with blender and is cooled to 40 ℃ with cold water, adds the B component, and stirring and dissolving after then adding the C component, then stirs with blender;

4) multiple-effect washing cream is namely made in discharging.

Preferably, the mixing speed of described blender is 200r/min.

Preferably, adding the time of described D component is 1 minute.

Preferably, the homogenizing speed of described homogenizer is 2000r/min.

The invention has the beneficial effects as follows: the invention provides a kind of multiple-effect washing cream, because multiple-effect washing cream of the present invention has whitening, moisturizing, defying age, antiallergic effect simultaneously, specifically comprise:

1. white-skinned face function: the multiple-effect washing cream in the present invention is by having inhibitory action to main melanin synthetic proteins enzyme-tyrosinase activity, dopachrome interconvertible enzyme activity etc., just can reach the effect of good check melanin as long as add very little consumption, thereby reach white-skinned face function.

2. moisture-keeping efficacy: the multiple-effect washing cream in the present invention is adsorbed on skin surface and forms liquid crystal, makes the skin feel good; After skin absorbed, quick and degree of depth ground association moisture formed long-acting moisturizing.

3. senile-resistant efficacy: the multiple-effect washing cream in the present invention works on photoprotein polysaccharide and NTx albumen, can form the functional network of closely knit, regular collagen fabric, improve the degree of packing and the structure of skin, experiment confirm has good aging resistance function.

4. antiallergic effect: thus the multiple-effect washing cream in the present invention is by reducing main inflammatory mediator inflammation-inhibiting reaction, can stimulate the generation of β-Nei calf peptide-" happiness " neuropeptide simultaneously, makes skin present the state that health is releived.

5. without any side effect, successful be fit to the crowd of various age levels, and manufacturing process of the present invention is simple, does not need complicated equipment and process to skin for the multiple-effect washing cream in the present invention, and cost is low.

Description of drawings

Fig. 1 is the dermal melanin variation figure in embodiment 4 in the present invention.

Fig. 2 is skin moisture changes of contents figure in embodiment 5 in the present invention.

Fig. 3 is R2 in embodiment 6 in the present invention, R5, R7 value variation diagram.

The specific embodiment

Below in conjunction with accompanying drawing, more excellent embodiment of the present invention is described in further detail:

Embodiment 1:A component is by 75.9 gram water, 0.3 gram ceramide, and 0.15 gram allantoin, 0.2 gram HANSHENGJIAO, 0.7 gram SEPIPLUS 265 forms; The B component is comprised of 4 gram 1,3 butanediols and 0.05 gram glabridin; The C component is by 2 gram acetyl group tetrapeptides-9,3 gram Mentha piperita extracting solution, 0.2 gram DMDM hydantoin, and 0.2 gram Fructus Citri Limoniae essence forms; The D component is comprised of 2.5 gram EMULIUM DELTA, 0.8 gram lanoline, 4 gram Jojoba oils, 1 gram cetearyl alcohol, the 3 sad propyl group heptyl esters of gram, 2 gram polydimethylsiloxane.

Concrete steps are as follows: 1) A component and D component are heated to 80 ℃ with electric furnace respectively; 2) the A component is stirred (mixing speed 200r/min) with blender, simultaneously the D component is slowly added in the A component, after adding, then use the homogenizer homogenizing 2 minutes (homogenizing speed 2000r/min); 3) limit is stirred the limit with blender and is cooled to 40 ℃ with cold water, adds the B component, and stirring and dissolving after then adding the C component, then stirs with blender; 4) multiple-effect washing cream is namely made in discharging.

Example 2:A component: water 78.1%, ceramide 0.1%, allantoin 0.25%, HANSHENGJIAO 0.35%, SEPIPLUS 265 0.5%; B component: 1,3 butanediol 2.0%, glabridin 0.1%; The C component contains acetyl group tetrapeptide-9 1.0%, Mentha piperita extracting solution 5.0%, DMDM hydantoin 0.1%, Fructus Citri Limoniae essence 0.5%; The D component contains EMULIUM DELTA 2%, lanoline 0.5%, Jojoba oil 6%, cetearyl alcohol 0.5%, sad propyl group heptyl ester 2.0%, polydimethylsiloxane 1.0%.

Concrete steps are as follows: 1) A component and D component are heated to 80 ℃ with electric furnace respectively; 2) the A component is stirred (mixing speed 200r/min) with blender, simultaneously the D component is slowly added in the A component, after adding, then use the homogenizer homogenizing 2 minutes (homogenizing speed 2000r/min); 3) limit is stirred the limit with blender and is cooled to 40 ℃ with cold water, adds the B component, and stirring and dissolving after then adding the C component, then stirs with blender; 4) multiple-effect washing cream is namely made in discharging.

Embodiment 3:A component contains water 63.29%, ceramide 0.6%, allantoin 0.1%, HANSHENGJIAO 0.1%, SEPIPLUS 265:1.5%; The B component contains 1,3 butanediol 8.0%, glabridin 0.01%; The C component contains acetyl group tetrapeptide-9 3.0%, Mentha piperita extracting solution 2.0%, DMDM hydantoin 0.3%, Fructus Citri Limoniae essence 0.1%; The D component contains EMULIUM DELTA:4%, lanoline 2%, Jojoba oil 2%, cetearyl alcohol 2%, sad propyl group heptyl ester 6.0%, polydimethylsiloxane 5%.

Concrete steps are as follows: 1) A component and D component are heated to 80 ℃ with electric furnace respectively; 2) the A component is stirred (mixing speed 200r/min) with blender, simultaneously the D component is slowly added in the A component, after adding, then use the homogenizer homogenizing 2 minutes (homogenizing speed 2000r/min); 3) limit is stirred the limit with blender and is cooled to 40 ℃ with cold water, adds the B component, and stirring and dissolving after then adding the C component, then stirs with blender; 4) multiple-effect washing cream is namely made in discharging.

Experimental results show that: prove that by test preparation-obtained facial cream has moisturizing, whitening, defying age and antiallergic effect.Select the prepared facial cream of embodiment 1 to test, concrete efficacy test is as follows:

Embodiment 4: the whitening effect test

Test instrunment: the skin elasticity Cotometer MPA580 main frame that German Courage+Khazaka company (German CK company) makes, the probe that uses is dermal melanin and red pigment Mexameter MX18 test probe.

Experimenter's quantity and condition: the normal subjects women in 30 35-45 years.

Test zone: up down the left and right cheek in 2cm chin area, nose and pupil intersection place is regional in 2cm forehead zone, lower lip middle for the place between the eyebrows middle.

Testing procedure: first measure the blank value of the rear 30min of test zone cleaning, then press the product description consumption and use step, sample is evenly coated face.Sooner or later adhere to every day using, must not use other cosmetics, used continuously for 8 weeks, test respectively the dermal melanin of the 1st week, 2 weeks, 3 weeks, 4 weeks, 6 weeks, 8 all pilot regions.Same experimenter's test is completed by same survey crew.By test these 30 experimenters use before and after the variation of dermal melanin numbers (meansigma methods) assess the skin whitening efficacy of this product, the black prime number changes as shown in table 1:

Table 1: dermal melanin changes

Test period (week)	0	1	2	3	4	6	8
								Melanin (meansigma methods)	320	310	300	285	225	180	170

Annotate: melanin:＜100 represent hypomelanism, easily sunburn; 100-200 is normal, and skin is more pale;＞200 melanin are more, and skin protection power is strong, and skin is more black.

As can be seen from Figure 1, use rear the 3rd all melanic numerical value of this frost that obvious decline is arranged, the 5th week just was tending towards normal value, and 6-8 week melanin descends and tends towards stability, in normal range.The melanin rate of descent is 46.88%, proves that this frost has white-skinned face function.

Embodiment 5: the moistening effect test

Test instrunment: the skin elasticity Cotometer MPA580 main frame that German Courage+Khazaka company (German CK company) makes, the probe that uses is skin moisture content Cornemeter CM825 test probe.

Experimenter's quantity and condition: the normal subjects women in 30 35-45 years.

Test zone: two 4 * 4cm pilot regions of the inboard labelling of experimenter's left hand forearm, interregional every 2cm.

Testing procedure: use test sample in zone therein, another zone is as blank contrast.First measure each test zone and clean and use clean napkin to dry the blank value of rear 0.5h, then by the consumption of every square centimeter, 2.0 ± 0.1 mg sample, use latex finger cot that sample is evenly coated in the trial zone.Smear the rear skin moisture content of measuring respectively 0.5h, 1h, 1.5h, 2h, 4h, 6h, the tested zone of 8h and blank zone, same experimenter's test is completed by same survey crew.The skin moisture-keeping effect of this product is assessed in the variation of the skin moisture content by testing tested zone and blank zone, and test data changes as shown in table 2:

Table 2: skin moisture changes of contents

Test period (week)	0	0.5	1	1.5	2	4	6	8
									Blank value (meansigma methods)	29.5	30.9	32.4	31.5	28.3	29.1	30.5	31.7
Moisture (meansigma methods)	31.6	32.5	45.5	51.0	53.2	54.7	58.0	52.4

Annotate: the corresponding value of abscissa zero graduation is that test zone cleans and use clean napkin to dry the measured blank value of rear 0.5h.

As can be seen from Figure 2, use this facial cream after 1 hour tested regional moisture have more obviously and to increase, and moisture keeps increasing always, until just begin to have slight decline after 6 hours, the moisture 52.4% of the 8th hour proves that this facial cream has moisture-keeping efficacy.

Embodiment 6: the defying age measure of merit

Test instrunment: the skin elasticity Cotometer MPA580 main frame that German Courage+Khazaka company (German CK company) makes, the probe that uses are Reviscometer RV600 elastic fibrous tissue test probes.

Experimenter's quantity and condition: the normal subjects women in 30 35-45 years

Test zone: up down the left and right cheek in 2cm chin area, nose and pupil intersection place is regional in 2cm forehead zone, lower lip middle for the place between the eyebrows middle.

Testing procedure: blank value (R2, R5, R7, R2=Ua/Uf wherein, R5=Ur/Ue, R7=Ur/Uf, the Uf--skin maximum tension amount of first measuring 30min after test zone cleaning;

After the Ue--constant negative pressure is added on skin; 0.1 the amount of tension of skin during second, location elastic part amount of tension; After Ur--cancelled negative pressure, the skin attitude that will restore to the original state rapidly was divided into elastic score value Ur equally, namely cancels negative pressure after 0.1 second, and recovery value and the viscoelasticity of skin partly are worth, or claim the plastic value; Ua--is from cancel the recovery value of negative pressure skin when the follow-on test skin surface adds negative pressure more next time), then press product description consumption and use step, sample is evenly coated face.Sooner or later adhere to every day using, must not use other cosmetics, used continuously for 8 weeks, test respectively the R2 of the skin of the 1st week, 2 weeks, 3 weeks, 4 weeks, 6 weeks, 8 all pilot regions, R5, R7.Same experimenter's test is completed by same survey crew.The R2 of skin before and after using by test, R5, the R7 value changes the skin anti-aging effect of assessing this product, R2, R5, the R7 value changes as follows:

Table 3:R2, R5, the R7 value changes

In table 3, R2, R5, R7 are more near 1, and skin elasticity is better, can be got by Fig. 3, prepared facial cream R2 after the first week, R5, R7 increase to some extent, the 4th all R2, R5, R7 rise obviously, 4-8 week R2, R5, the R7 value levels off to 1, this shows that this frost has increase skin elasticity, senile-resistant efficacy.

Embodiment 7: the antiallergic measure of merit

Experimenter's quantity and condition: the normal subjects women in 30 35-45 years.

Testing procedure: two 4 * 4cm pilot regions of the inboard labelling of experimenter's left hand forearm, interregional every 2cm.Use test sample in zone therein, used 5 days continuously as blank contrast in another zone, then uses lactic acid solutions in these two zones, characterizes this frost and have the antiallergic analgesic activity by detecting sensation of pricking.

Test result: 80% experimenter feels not use the test zone tingle of the prepared facial cream of the present invention to use this white test zone there is no obvious sensation of pricking, proves that this frost has the antiallergic effect.

By above test result as can be known, the multiple-effect washing cream in the present invention has whitening, moisturizing, defying age and antiallergic analgesic activity.

Above content is in conjunction with concrete preferred implementation further description made for the present invention, can not assert that concrete enforcement of the present invention is confined to these explanations.For the general technical staff of the technical field of the invention, without departing from the inventive concept of the premise, can also make some simple deduction or replace, all should be considered as belonging to protection scope of the present invention.

Claims (4)

1. a multiple-effect washing cream, is characterized in that, by weight percentage, is comprised of following component:

A component: water 60-80%, ceramide 0.1-0.6%, allantoin 0.1-0.25%, HANSHENGJIAO 0.1-0.35%, SEPIPLUS265:0.5-1.5%;

B component: 1,3 butylene glycol 2-8%, glabridin 0.01-0.1%;

C component: acetyl group tetrapeptide-9:1-3%, Mentha piperita extracting solution 2-5%, antiseptic 0.1-0.3%, essence 0.1-0.5%;

D component: EMULIUM DELTA:2.0-4.0%, lanoline 0.5-2%, Jojoba oil 2-6%, cetearyl alcohol 0.5-2.0%, sad propyl group heptyl ester 2-6%, polydimethylsiloxane 1-5%;

Take multiple-effect washing cream as 100%, described A component is 60-80%, and described B component is 2-10%, and described C component is 5-9%, and described D component is 12-22%; Described SEPIPLUS 265 is the mixture of acrylamide/ammonium acrylate copolymer, polyisobutylene and polysorbate-20; Described EMULIUM DELTA is the mixture of spermol, glyceryl stearate, PEG-75 stearate, spermol polyethers-20 and stearyl alcohol polyethers-20.

2. multiple-effect washing cream as claimed in claim 1, is characterized in that, described antiseptic adopts the DMDM hydantoin.

3. multiple-effect washing cream as claimed in claim 1, is characterized in that, described essence adopts Fructus Citri Limoniae essence.

4. a method for preparing multiple-effect washing cream, is characterized in that, comprises multiple-effect washing cream as described in the claims 1 to 3 any one, and described method is following several step:

1) A component and D component are heated to 80 ℃ with electric furnace respectively;

2) the A component is stirred with blender, mixing speed is 200r/min, simultaneously the D component is slowly added in the A component, and adding the time of D component is 1 minute, after adding, then uses the homogenizer homogenizing 2 minutes, and homogenizing speed is 2000r/min;

3) limit is stirred the limit with blender and is cooled to 40 ℃ with cold water, adds the B component, and stirring and dissolving after then adding the C component, then stirs with blender;

4) multiple-effect washing cream is namely made in discharging.

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