CN110339124A - A kind of cosmetic face cream and preparation method thereof for whitening spot-removing - Google Patents
A kind of cosmetic face cream and preparation method thereof for whitening spot-removing Download PDFInfo
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- CN110339124A CN110339124A CN201910779560.4A CN201910779560A CN110339124A CN 110339124 A CN110339124 A CN 110339124A CN 201910779560 A CN201910779560 A CN 201910779560A CN 110339124 A CN110339124 A CN 110339124A
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- face cream
- cosmetic face
- whitening spot
- hamamelis
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/342—Alcohols having more than seven atoms in an unbroken chain
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/927—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of insects, e.g. shellac
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
Abstract
The cosmetic face cream and preparation method thereof that the invention discloses a kind of for whitening spot-removing.The raw material of the cosmetic face cream is made of Herba Saussureae Involueratae extract, glycyrrhiza glabra extract, hamamelis extract, different ethylhexyl palmitate, sad Propylheptyl, flores aurantii essential oil, borage oil etc..Preparation method of the cosmetic face cream for whitening spot-removing is specifically that will carry out high-temperature stirring in the investment reaction kettle such as different ethylhexyl palmitate, sad Propylheptyl, then it is added as cetostearyl alcohol, stearine etc. through primary mix made of homogeneous, sub-mixtures are obtained after stirring homogeneous, Herba Saussureae Involueratae extract isoreactivity ingredient will be added after sub-mixtures again vacuum homogeneous in emulsion pot and obtain ultimate mixture, most obtains finished product cosmetic face cream after cooling, addition auxiliary agent afterwards.The cosmetic face cream for being used for whitening spot-removing has preferable whitening spot-removing effect, and healthy and safe, there is preferable application prospect in face skin nursing.
Description
Technical field
The present invention relates to cosmetic technical fields, more particularly to a kind of cosmetic face cream for whitening spot-removing and its preparation
Method.
Background technique
Color spot is always for a long time the big problem for perplexing human skin, and in particular with the growth at age, skin goes out
The probability of existing color spot also obviously increases.The reason of color spot formation, is mainly since there are many pigment is thin for the distribution of human epidermal lower layer
Born of the same parents, catalysis oxidation of the chromatophore through internal tyrosinase and form melanin, melanin increases and unevenly assembles in skin
And form color spot.Furthermore the reason of different color spot type formation, is also different, if freckle is the reason of heredity, chloasma mostly
Be mostly with cyasma because sunburn is then the influence due to ultraviolet light caused by Endocrine and metabolism disorder, senile plaque be by
In skin and internal metabolism of pigment slowly and caused by.All the time, whitening spot-removing is all the topic that people earnestly pay close attention to.It wants
Want to achieve the purpose that whitening, nti-freckle, can pass through following two main path: one is the generations for preventing pigment；It is another then be
Promote the chromocrinia generated external out.The skin-color that needs to inhibit to generate or excrete is known as melanin, lipofuscin and leaf
Red pigment.Melanin and phylloerythrin (also known as carrot element) are physiologic agents, there is certain physiological function, harmless；And
Lipofuscin is then the substance being harmful to the human body.According to the pigmented influence degree of human skin, inhibit and exclude melanin
It is the main method of whitening, cosmetics use.Face cream is the most important step of basic skin care, the effective component energy in face cream
Enough preferably by percutaneous absorption, and face cream can form layer protecting film outside facial skin, reduce the dust in air to skin
The stimulation that skin generates.However most of whitening spot-removing face cream can generate different degrees of stimulation injury to skin, while also
Certain side effect, adverse effect can be brought to human health by addition to this adding the allogenic material containing heavy metal.
Summary of the invention
The problem of not being able to satisfy consumer demand still based on current whitening spot-removing face cream, the present invention provide a kind of for whitening
Cosmetic face cream of nti-freckle and preparation method thereof.
A kind of cosmetic face cream for whitening spot-removing, the raw material of the cosmetic face cream by mass percentage, form as follows:
Herba Saussureae Involueratae extract 1.7~2.9%
Glycyrrhiza glabra extract 1.2~2.5%
Hamamelis extract 0.6~0.8%
Cetostearyl alcohol 5.5~6.0%
Stearine 1.5~5.5%
Glycerol 6.0~10.0%
Different ethylhexyl palmitate 4.0~6.0%
Sad Propylheptyl 0.5~7.5%
Beeswax 2.5~3.5%
Flores aurantii essential oil 1.8~2.2%
Borage oil 0.05~0.15%
Essence 0.01~0.03%
Antioxidant 0.02~0.05%
Preservative 0.1~0.2%
Deionized water surplus.
The above-mentioned cosmetic face cream for whitening spot-removing contains Herba Saussureae Involueratae extract, glycyrrhiza glabra extract, hamamelis
The functional components such as extract, flores aurantii essential oil, borage oil, each functional components except play itself possessed by basic effect with
Outside, synergistic function is also unexpectedly shown, human endocrine and function can be adjusted from body metabolism level, from basic
On play the beautification function of whitening spot-removing.The cosmetic face cream has effect, suitable for the colour of skin is more black and crowd with facial colour spot
It uses.
The Herba Saussureae Involueratae extract, glycyrrhiza glabra extract and hamamelis extract in one of the embodiments,
The preparation method comprises the following steps:
Lanatechead saussurea herb with flower, glycyrrhiza glabra and hamamelis are crushed respectively, are sieved, being added to weight is 30 times, volumetric concentration
For in 70~80% ethanol solution, ultrasonic extraction 4~6 hours at 50 DEG C, ultrasonic power 250W then takes and clears
The heart, filtering, then by filtrate vacuum degree be -0.08MPa under conditions of rotary evaporation, extract concentrated solution is obtained, most afterwards through cold
Jelly is dried to obtain Herba Saussureae Involueratae extract, glycyrrhiza glabra extract and hamamelis extract.
The raw material of the cosmetic face cream by mass percentage, forms as follows in one of the embodiments:
Herba Saussureae Involueratae extract 2.3%
Glycyrrhiza glabra extract 1.8%
Hamamelis extract 0.7%
Cetostearyl alcohol 5.8%
Stearine 3.5%
Glycerol 8.0%
Different ethylhexyl palmitate 5.0%
Sad Propylheptyl 4.0%
Beeswax 3.0%
Flores aurantii essential oil 2.0%
Borage oil 0.1%
Essence 0.02%
Antioxidant 0.03%
Preservative 0.15%
Deionized water surplus.
The essence is any one in ginger extrait, flavoring rose essence, lavender oil in one of the embodiments,
Kind.
The antioxidant is selected from butylated hydroxy anisole, allantoin, hydroxypropyl tetrahydro pyrrole in one of the embodiments,
Any one muttered in triol.
Any one of the preservative in Nipasol, sorbic acid, triclosan in one of the embodiments,.
The present invention also provides the preparation methods of the above-mentioned cosmetic face cream for whitening spot-removing, comprise the steps of:
(1) cetostearyl alcohol, stearine, glycerol, deionized water are put into homogenizer, according to 1200~1800
Rev/min rate homogenous disperse 30~40 minutes, obtain primary mix；
(2) by different ethylhexyl palmitate, sad Propylheptyl, beeswax, borage oil investment reaction kettle, reaction is improved
Kettle temperature degree stirs 15~25 minutes under 300~500 revs/min of rate to 88~92 DEG C, walks then to being added in reaction kettle
Suddenly (1) resulting primary mix stirs homogeneous 30~50 minutes under 1800~2000 revs/min of rate, obtains secondary
Mixture；
(3) sub-mixtures that step (2) obtains are transferred in emulsion pot, emulsion pot is vacuumized, keep emulsion pot
Internal temperature is 65~75 DEG C, according to rate homogeneous 8~10 minutes of 2000~2200 revs/min, inside subsequent pot to be emulsified
When temperature is down to 55 DEG C or less, Herba Saussureae Involueratae extract, glycyrrhiza glabra extract, hamamelis are added into emulsion pot and extracts
Object obtains ultimate mixture according still further to rate homogeneous 18~20 minutes of 2400~2600 revs/min；
(4) after the ultimate mixture that step (3) obtains is cooled to room temperature, flores aurantii essential oil, essence, antioxygen are added thereto
Agent, preservative are stirred evenly according to 120~160 revs/min of rate, obtain finished product face cream.
The preparation method of the above-mentioned cosmetic face cream for whitening spot-removing, process conditions are mild, controllability is strong, and product quality is steady
Fixed, production cost economy is suitable for large-scale production.
Emulsion pot is evacuated to -0.06~-0.1MPa in the step (3) in one of the embodiments,.
The application that the present invention also provides described for the cosmetic face cream of whitening spot-removing in face skin nursing.
Specific embodiment
In order to make the foregoing objectives, features and advantages of the present invention clearer and more comprehensible, below in conjunction with specific embodiment,
The present invention will be described in further detail.It should be appreciated that the specific embodiments described herein are only used to explain this hair
It is bright, it is not intended to limit the present invention.
Unless otherwise defined, all technical and scientific terms used herein and belong to technical field of the invention
The normally understood meaning of technical staff is identical.Term as used herein in the specification of the present invention is intended merely to description tool
The purpose of the embodiment of body, it is not intended that in the limitation present invention.Term " and or " used herein includes one or more
Any and all combinations of relevant listed item.
Raw materials used and reagent is commercially available common raw material and reagent in following embodiment.
A kind of cosmetic face cream for whitening spot-removing, the raw material of the cosmetic face cream by mass percentage, form as follows:
Herba Saussureae Involueratae extract 1.7~2.9%
Glycyrrhiza glabra extract 1.2~2.5%
Hamamelis extract 0.6~0.8%
Cetostearyl alcohol 5.5~6.0%
Stearine 1.5~5.5%
Glycerol 6.0~10.0%
Different ethylhexyl palmitate 4.0~6.0%
Sad Propylheptyl 0.5~7.5%
Beeswax 2.5~3.5%
Flores aurantii essential oil 1.8~2.2%
Borage oil 0.05~0.15%
Essence 0.01~0.03%
Antioxidant 0.02~0.05%
Preservative 0.1~0.2%
Deionized water surplus.
Wherein, saussurea involucrata is the herbaceous plant of composite family phoenix hair Chrysanthemum saussurea involucrata subgenus, mainly includes snow lotus of big bud flower, Saussurea laniceps
The wounded in the battle complete stool of flower, mouse song lanatechead saussurea herb with flower, saussurea medusa flower etc..Contain more rich Flavonoid substances in lanatechead saussurea herb with flower, has anti-
The property of oxidation, can help skin it is anti-oxidant, promote dermal fibroblast proliferation, more particularly to help skin resist UVB and
The ultraviolet light of UVA irradiates, and protects skin, reduces damage, prevents skin photoage, and non-stimulated to skin.
Wherein, glycyrrhiza glabra extract can go deep into inside skin and keep high activity, effectively inhibit melanin production process
In a variety of enzymes activity, be a kind of fast, efficient, safe, green sun-proof, whitening cosmetics additive.With time fruit
Licorice also has effects that prevent pachylosis and anti-inflammatory, antibacterial.
Wherein, hamamelis is derived from the shrub in Eastern North America area, gives birth in moist region.Hamamelis mentions
The main component for taking object includes tannic acid, gallic acid, catechin, procyanidine, Protoapigenone, essential oil, choline and saponin.
Hamamelis extract has nature convergence, can play and nourish skin and promotion vasoconstrictor effects.
Wherein, flores aurantii essential oil be close to transparent light yellow liquid, main chemical compositions have australene, amphene, nopinene,
α-terpinenes, nerol, neryl acetate, fanesol, acid esters and indoles.Flores aurantii essential oil can enhance cell viability, side
Synergidae regeneration, increases skin elasticity；Whitening, moisturizing, light spot, nourish crease-resistant, restore delicate, are suitble to stemness, sensitivity and other
Problem skin.Its penetrating power is more than 70 times of common skin care ingredient, can penetrate into skin basal layer, decomposes skin melanin, flesh
Skin is purified by interior, increasingly attains white, is shone powder and is moistened pale brilliance.
Wherein, borage oil is suitble to the flesh of all skin, especially adult form rich in natural gamma-Linolenic acid is enriched
Skin is good skin renewal agent.Borage oil can effectively improve it is coarse it is dry and astringent, prevent cell water loss, increase skin
Saturating white sense.Damaged cell can also be repaired, improve self maintenance ability of cell, and with cellular matrix collective effect, be built into
Holomyarian skin barrier is presented skin full, compact, healthy.
The above-mentioned cosmetic face cream for whitening spot-removing contains Herba Saussureae Involueratae extract, glycyrrhiza glabra extract, hamamelis
The functional components such as extract, flores aurantii essential oil, borage oil, each functional components except play itself possessed by basic effect with
Outside, synergistic function is also unexpectedly shown, human endocrine and function can be adjusted from body metabolism level, from basic
On play the beautification function of whitening spot-removing.The cosmetic face cream has effect, suitable for the colour of skin is more black and crowd with facial colour spot
It uses.
In a preferred embodiment, the Herba Saussureae Involueratae extract, glycyrrhiza glabra extract and hamamelis are extracted
Object the preparation method comprises the following steps:
Lanatechead saussurea herb with flower, glycyrrhiza glabra and hamamelis are crushed respectively, are sieved, being added to weight is 30 times, volumetric concentration
For in 70~80% ethanol solution, ultrasonic extraction 4~6 hours at 50 DEG C, ultrasonic power 250W then takes and clears
The heart, filtering, then by filtrate vacuum degree be -0.08MPa under conditions of rotary evaporation, extract concentrated solution is obtained, most afterwards through cold
Jelly is dried to obtain Herba Saussureae Involueratae extract, glycyrrhiza glabra extract and hamamelis extract.
In a preferred embodiment, the raw material of the cosmetic face cream by mass percentage, forms as follows:
Herba Saussureae Involueratae extract 2.3%
Glycyrrhiza glabra extract 1.8%
Hamamelis extract 0.7%
Cetostearyl alcohol 5.8%
Stearine 3.5%
Glycerol 8.0%
Different ethylhexyl palmitate 5.0%
Sad Propylheptyl 4.0%
Beeswax 3.0%
Flores aurantii essential oil 2.0%
Borage oil 0.1%
Essence 0.02%
Antioxidant 0.03%
Preservative 0.15%
Deionized water surplus.
In a preferred embodiment, the essence is any in ginger extrait, flavoring rose essence, lavender oil
It is a kind of.
In a preferred embodiment, the antioxidant is selected from butylated hydroxy anisole, allantoin, hydroxypropyl tetrahydro
Any one in pyrans triol.
In a preferred embodiment, the preservative is any one in Nipasol, sorbic acid, triclosan
Kind.
The present invention also provides the preparation methods of the above-mentioned cosmetic face cream for whitening spot-removing, comprise the steps of:
(1) cetostearyl alcohol, stearine, glycerol, deionized water are put into homogenizer, according to 1200~1800
Rev/min rate homogenous disperse 30~40 minutes, obtain primary mix；
(2) by different ethylhexyl palmitate, sad Propylheptyl, beeswax, borage oil investment reaction kettle, reaction is improved
Kettle temperature degree stirs 15~25 minutes under 300~500 revs/min of rate to 88~92 DEG C, walks then to being added in reaction kettle
Suddenly (1) resulting primary mix stirs homogeneous 30~50 minutes under 1800~2000 revs/min of rate, obtains secondary
Mixture；
(3) sub-mixtures that step (2) obtains are transferred in emulsion pot, emulsion pot is vacuumized, keep emulsion pot
Internal temperature is 65~75 DEG C, according to rate homogeneous 8~10 minutes of 2000~2200 revs/min, inside subsequent pot to be emulsified
When temperature is down to 55 DEG C or less, Herba Saussureae Involueratae extract, glycyrrhiza glabra extract, hamamelis are added into emulsion pot and extracts
Object obtains ultimate mixture according still further to rate homogeneous 18~20 minutes of 2400~2600 revs/min；
(4) after the ultimate mixture that step (3) obtains is cooled to room temperature, flores aurantii essential oil, essence, antioxygen are added thereto
Agent, preservative are stirred evenly according to 120~160 revs/min of rate, obtain finished product face cream.
In a preferred embodiment, emulsion pot is evacuated to -0.06~-0.1MPa in the step (3).
The application that the present invention also provides above-mentioned for the cosmetic face cream of whitening spot-removing in face skin nursing.
Below by embodiment, the present invention is furture elucidated.It should be pointed out that the present invention is not intended to be limited to the reality
Apply example.
Embodiment 1
The cosmetic face cream formula for whitening spot-removing of the present embodiment is as follows:
Herba Saussureae Involueratae extract 1.7%
Glycyrrhiza glabra extract 1.2%
Hamamelis extract 0.6%
Cetostearyl alcohol 5.5%
Stearine 1.5%
Glycerol 6.0%
Different ethylhexyl palmitate 4.0%
Sad Propylheptyl 0.5%
Beeswax 2.5%
Flores aurantii essential oil 1.8%
Borage oil 0.05%
Essence 0.01%
Antioxidant 0.02%
Preservative 0.1%
Deionized water surplus.
The cosmetic face cream for whitening spot-removing of the present embodiment is prepared as follows:
(1) lanatechead saussurea herb with flower, glycyrrhiza glabra and hamamelis are crushed respectively, is sieved, being added to weight is 30 times, volume
In the ethanol solution that concentration is 70%, ultrasonic extraction 4 hours at 50 DEG C, ultrasonic power 250W then takes supernatant centrifugation, mistake
Filter, then by filtrate under conditions of vacuum degree is -0.08MPa rotary evaporation, obtain extract concentrated solution, it is last freeze-dried
Obtain Herba Saussureae Involueratae extract, glycyrrhiza glabra extract and hamamelis extract
(2) cetostearyl alcohol, stearine, glycerol, deionized water are put into homogenizer, according to 1200 revs/min
The rate homogenous disperse of clock 30 minutes, obtains primary mix；
(3) by different ethylhexyl palmitate, sad Propylheptyl, beeswax, borage oil investment reaction kettle, reaction is improved
Kettle temperature degree stirs 15 minutes under 300 revs/min of rate to 88 DEG C, resulting just then to step (2) are added in reaction kettle
Grade mixture, stirs homogeneous 30 minutes under 1800 revs/min of rate, obtains sub-mixtures；
(4) sub-mixtures that step (3) obtains are transferred in emulsion pot, emulsion pot is vacuumized, keep emulsion pot
Internal temperature is 65 DEG C, according to rate homogeneous 8 minutes of 2000 revs/min, subsequent pot internal temperature to be emulsified be down to 55 DEG C with
When lower, into emulsion pot be added Herba Saussureae Involueratae extract, glycyrrhiza glabra extract, hamamelis extract, according still further to 2400 turns/
Rate homogeneous 18 minutes of minute, obtain ultimate mixture；
(5) after the ultimate mixture that step (4) obtains is cooled to room temperature, flores aurantii essential oil, essence, antioxygen are added thereto
Agent, preservative are stirred evenly according to 120 revs/min of rate, are obtained finished product face cream, are denoted as S1.
Embodiment 2
The cosmetic face cream formula for whitening spot-removing of the present embodiment is as follows:
Herba Saussureae Involueratae extract 2.3%
Glycyrrhiza glabra extract 1.8%
Hamamelis extract 0.7%
Cetostearyl alcohol 5.8%
Stearine 3.5%
Glycerol 8.0%
Different ethylhexyl palmitate 5.0%
Sad Propylheptyl 4.0%
Beeswax 3.0%
Flores aurantii essential oil 2.0%
Borage oil 0.1%
Essence 0.02%
Antioxidant 0.03%
Preservative 0.15%
Deionized water surplus.
The cosmetic face cream for whitening spot-removing of the present embodiment is prepared as follows:
(1) lanatechead saussurea herb with flower, glycyrrhiza glabra and hamamelis are crushed respectively, is sieved, being added to weight is 30 times, volume
In the ethanol solution that concentration is 75%, ultrasonic extraction 5 hours at 50 DEG C, ultrasonic power 250W then takes supernatant centrifugation, mistake
Filter, then by filtrate under conditions of vacuum degree is -0.08MPa rotary evaporation, obtain extract concentrated solution, it is last freeze-dried
Obtain Herba Saussureae Involueratae extract, glycyrrhiza glabra extract and hamamelis extract
(2) cetostearyl alcohol, stearine, glycerol, deionized water are put into homogenizer, according to 1500 revs/min
The rate homogenous disperse of clock 35 minutes, obtains primary mix；
(3) by different ethylhexyl palmitate, sad Propylheptyl, beeswax, borage oil investment reaction kettle, reaction is improved
Kettle temperature degree stirs 20 minutes under 400 revs/min of rate to 90 DEG C, resulting just then to step (2) are added in reaction kettle
Grade mixture, stirs homogeneous 40 minutes under 1900 revs/min of rate, obtains sub-mixtures；
(4) sub-mixtures that step (3) obtains are transferred in emulsion pot, emulsion pot is vacuumized, keep emulsion pot
Internal temperature is 70 DEG C, according to rate homogeneous 9 minutes of 2100 revs/min, subsequent pot internal temperature to be emulsified be down to 55 DEG C with
When lower, into emulsion pot be added Herba Saussureae Involueratae extract, glycyrrhiza glabra extract, hamamelis extract, according still further to 2500 turns/
Rate homogeneous 19 minutes of minute, obtain ultimate mixture；
(5) after the ultimate mixture that step (4) obtains is cooled to room temperature, flores aurantii essential oil, essence, antioxygen are added thereto
Agent, preservative are stirred evenly according to 140 revs/min of rate, are obtained finished product face cream, are denoted as S2.
Embodiment 3
The cosmetic face cream formula for whitening spot-removing of the present embodiment is as follows:
Herba Saussureae Involueratae extract 2.9%
Glycyrrhiza glabra extract 2.5%
Hamamelis extract 0.8%
Cetostearyl alcohol 6.0%
Stearine 5.5%
Glycerol 10.0%
Different ethylhexyl palmitate 6.0%
Sad Propylheptyl 7.5%
Beeswax 3.5%
Flores aurantii essential oil 2.2%
Borage oil 0.15%
Essence 0.03%
Antioxidant 0.05%
Preservative 0.2%
Deionized water surplus.
The cosmetic face cream for whitening spot-removing of the present embodiment is prepared as follows:
(1) lanatechead saussurea herb with flower, glycyrrhiza glabra and hamamelis are crushed respectively, is sieved, being added to weight is 30 times, volume
In the ethanol solution that concentration is 80%, ultrasonic extraction 6 hours at 50 DEG C, ultrasonic power 250W then takes supernatant centrifugation, mistake
Filter, then by filtrate under conditions of vacuum degree is -0.08MPa rotary evaporation, obtain extract concentrated solution, it is last freeze-dried
Obtain Herba Saussureae Involueratae extract, glycyrrhiza glabra extract and hamamelis extract
(2) cetostearyl alcohol, stearine, glycerol, deionized water are put into homogenizer, according to 1800 revs/min
The rate homogenous disperse of clock 40 minutes, obtains primary mix；
(3) by different ethylhexyl palmitate, sad Propylheptyl, beeswax, borage oil investment reaction kettle, reaction is improved
Kettle temperature degree stirs 25 minutes under 500 revs/min of rate to 92 DEG C, resulting just then to step (2) are added in reaction kettle
Grade mixture, stirs homogeneous 50 minutes under 2000 revs/min of rate, obtains sub-mixtures；
(4) sub-mixtures that step (3) obtains are transferred in emulsion pot, emulsion pot is vacuumized, keep emulsion pot
Internal temperature is 75 DEG C, according to rate homogeneous 10 minutes of 2200 revs/min, subsequent pot internal temperature to be emulsified be down to 55 DEG C with
When lower, into emulsion pot be added Herba Saussureae Involueratae extract, glycyrrhiza glabra extract, hamamelis extract, according still further to 2600 turns/
Rate homogeneous 20 minutes of minute, obtain ultimate mixture；
(5) after the ultimate mixture that step (4) obtains is cooled to room temperature, flores aurantii essential oil, essence, antioxygen are added thereto
Agent, preservative are stirred evenly according to 160 revs/min of rate, are obtained finished product face cream, are denoted as S3.
Comparative example 1
Substantially with embodiment 2, difference is the formula and preparation method of the cosmetic face cream of this comparative example, does not add saussurea involucrata
Flower extract, final cosmetic face cream obtained are denoted as C1.
Comparative example 2
Substantially with embodiment 2, difference is the formula and preparation method of the cosmetic face cream of this comparative example, does not add light fruit
Licorice, final cosmetic face cream obtained are denoted as C2.
Comparative example 3
Substantially with embodiment 2, difference is the formula and preparation method of the cosmetic face cream of this comparative example, does not add North America
Hamamelis extract, final cosmetic face cream obtained are denoted as C3.
Comparative example 4
Substantially with embodiment 1, difference is the formula and preparation method of the cosmetic face cream of this comparative example, does not add flores aurantii
Essential oil, final cosmetic face cream obtained are denoted as C4.
Comparative example 5
Substantially with embodiment 1, difference is the formula and preparation method of the cosmetic face cream of this comparative example, does not add coloured glaze
Lettuce oil, final cosmetic face cream obtained are denoted as C5.
Performance test
Cosmetic face cream prepared by Examples 1 to 3 and comparative example 1~5 is subjected to using effect performance test.
Select the age at 25~45 years old, the more black and women population with color spot of blee is as test object, at random
Be divided into 8 groups, every group of 15 people, each group skin of face situation, in terms of the difference that there are no significant, 1~8 group of difference
Cosmetic face cream S1~the S3 and comparative example 1~5 that the embodiment of the present invention 1~3 is prepared are smeared in daily early, two periods of evening
Cosmetic face cream C1~the C5 being prepared is each primary, after being used continuously one month, carries out effect assessment using the method for marking.
Full marks are 5 points, and 4~5 points of expression improvements are splendid；3~4 points of expression improvements are good；2~3 points of expression improvements one
As；2 points of following presentations are not affected significantly effect, and last each group is made even respectively, and the specific situation that scores is as shown in table 1:
Table 1
| The scoring of user's colour of skin improvement | The scoring of user's color spot improvement | |
| S1 | 4.0 | 4.2 |
| S2 | 4.3 | 4.4 |
| S3 | 4.1 | 4.0 |
| C1 | 3.9 | 3.1 |
| C2 | 2.8 | 3.7 |
| C3 | 3.7 | 3.9 |
| C4 | 3.2 | 3.6 |
| C5 | 3.8 | 4.0 |
Test result is as shown above, the cosmetic face cream of embodiment S1~S3 group and the cosmetic face cream of comparative example C1~C5 group
It compares, more excellent colour of skin improvement and color spot improvement, and the beauty of embodiment S2 is all had for user
Face cream has most excellent using effect.It can be seen that and of the invention dispel for whitening from the case where embodiment and comparative example
Herba Saussureae Involueratae extract, glycyrrhiza glabra extract, hamamelis extract, flores aurantii essential oil, coloured glaze in the cosmetic face cream ingredient of spot
In the case that glass lettuce oil, which produces using effect, to be significantly affected, and mentioned component is used in conjunction with, using effect compared to
Lack any one ingredient and have and be extremely obviously improved, it is seen that produces synergistic work between above-mentioned several ingredients
With having a good application prospect.
The embodiments described above only express several embodiments of the present invention, and the description thereof is more specific and detailed, but simultaneously
It cannot therefore be construed as limiting the scope of the patent.It should be pointed out that coming for those of ordinary skill in the art
It says, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to protection of the invention
Range.
Claims (9)
1. a kind of cosmetic face cream for whitening spot-removing, which is characterized in that the raw material of the cosmetic face cream by mass percentage,
It forms as follows:
Herba Saussureae Involueratae extract 1.7~2.9%
Glycyrrhiza glabra extract 1.2~2.5%
Hamamelis extract 0.6~0.8%
Cetostearyl alcohol 5.5~6.0%
Stearine 1.5~5.5%
Glycerol 6.0~10.0%
Different ethylhexyl palmitate 4.0~6.0%
Sad Propylheptyl 0.5~7.5%
Beeswax 2.5~3.5%
Flores aurantii essential oil 1.8~2.2%
Borage oil 0.05~0.15%
Essence 0.01~0.03%
Antioxidant 0.02~0.05%
Preservative 0.1~0.2%
Deionized water surplus.
2. the cosmetic face cream according to claim 1 for whitening spot-removing, which is characterized in that the Herba Saussureae Involueratae extract,
Glycyrrhiza glabra extract and hamamelis extract the preparation method comprises the following steps:
Lanatechead saussurea herb with flower, glycyrrhiza glabra and hamamelis are crushed respectively, are sieved, being added to weight is 30 times, volumetric concentration 70
In~80% ethanol solution, ultrasonic extraction 4~6 hours at 50 DEG C, ultrasonic power 250W then takes supernatant centrifugation, mistake
Filter, then by filtrate under conditions of vacuum degree is -0.08MPa rotary evaporation, obtain extract concentrated solution, it is last freeze-dried
Obtain Herba Saussureae Involueratae extract, glycyrrhiza glabra extract and hamamelis extract.
3. the cosmetic face cream according to claim 1 for whitening spot-removing, which is characterized in that the raw material of the cosmetic face cream
By mass percentage, it forms as follows:
Herba Saussureae Involueratae extract 2.3%
Glycyrrhiza glabra extract 1.8%
Hamamelis extract 0.7%
Cetostearyl alcohol 5.8%
Stearine 3.5%
Glycerol 8.0%
Different ethylhexyl palmitate 5.0%
Sad Propylheptyl 4.0%
Beeswax 3.0%
Flores aurantii essential oil 2.0%
Borage oil 0.1%
Essence 0.02%
Antioxidant 0.03%
Preservative 0.15%
Deionized water surplus.
4. described in any item cosmetic face creams for whitening spot-removing according to claim 1~3, which is characterized in that the essence
Any one in ginger extrait, flavoring rose essence, lavender oil.
5. described in any item cosmetic face creams for whitening spot-removing according to claim 1~3, which is characterized in that the antioxygen
Any one of agent in butylated hydroxy anisole, allantoin, hydroxypropyl oxinane triol.
6. described in any item cosmetic face creams for whitening spot-removing according to claim 1~3, which is characterized in that the anti-corrosion
Any one of agent in Nipasol, sorbic acid, triclosan.
7. a kind of preparation method of the cosmetic face cream as described in any one of claims 1 to 6 for whitening spot-removing, feature exist
In comprising the steps of:
(1) by cetostearyl alcohol, stearine, glycerol, deionized water investment homogenizer in, according to 1200~1800 turns/
Rate homogenous disperse 30~40 minutes of minute, obtain primary mix；
(2) by different ethylhexyl palmitate, sad Propylheptyl, beeswax, borage oil investment reaction kettle, reaction kettle temperature is improved
Degree stirs 15~25 minutes under 300~500 revs/min of rate to 88~92 DEG C, then to step is added in reaction kettle
(1) resulting primary mix stirs homogeneous 30~50 minutes under 1800~2000 revs/min of rate, obtains secondary mixed
Close object；
(3) sub-mixtures that step (2) obtains are transferred in emulsion pot, emulsion pot is vacuumized, kept inside emulsion pot
Temperature is 65~75 DEG C, according to rate homogeneous 8~10 minutes of 2000~2200 revs/min, subsequent pot internal temperature to be emulsified
When being down to 55 DEG C or less, Herba Saussureae Involueratae extract, glycyrrhiza glabra extract, hamamelis extract are added into emulsion pot, then
According to rate homogeneous 18~20 minutes of 2400~2600 revs/min, ultimate mixture is obtained；
(4) after the ultimate mixture that step (3) obtains is cooled to room temperature, flores aurantii essential oil, essence, anti-oxidant is added thereto
Agent, preservative are stirred evenly according to 120~160 revs/min of rate, obtain finished product face cream.
8. the preparation method of the cosmetic face cream according to claim 7 for whitening spot-removing, which is characterized in that the step
(3) emulsion pot is evacuated to -0.06~-0.1MPa in.
9. described in any item answering in face skin nursing of the cosmetic face cream for whitening spot-removing according to claim 1~6
With.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110960478A (en) * | 2019-12-04 | 2020-04-07 | 广州博科健康科技集团有限公司 | Freckle-removing cream containing umbilical cord extract and preparation method thereof |
| CN112587463A (en) * | 2020-07-26 | 2021-04-02 | 广州元美盛化妆品有限公司 | Long-acting skin care composition for removing freckles and concealing blemishes and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102670456A (en) * | 2012-06-06 | 2012-09-19 | 广州舒泰生物技术有限公司 | Multi-effect facial cream and preparation method thereof |
| CN107669566A (en) * | 2017-11-22 | 2018-02-09 | 佛山汇沐化学科技有限公司 | A kind of spot-eliminating composition |
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2019
- 2019-08-22 CN CN201910779560.4A patent/CN110339124A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102670456A (en) * | 2012-06-06 | 2012-09-19 | 广州舒泰生物技术有限公司 | Multi-effect facial cream and preparation method thereof |
| CN107669566A (en) * | 2017-11-22 | 2018-02-09 | 佛山汇沐化学科技有限公司 | A kind of spot-eliminating composition |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110960478A (en) * | 2019-12-04 | 2020-04-07 | 广州博科健康科技集团有限公司 | Freckle-removing cream containing umbilical cord extract and preparation method thereof |
| CN112587463A (en) * | 2020-07-26 | 2021-04-02 | 广州元美盛化妆品有限公司 | Long-acting skin care composition for removing freckles and concealing blemishes and preparation method thereof |
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Application publication date: 20191018 |