CN110200898A - A kind of multiple-effect mask composition and the preparation method and application thereof - Google Patents
A kind of multiple-effect mask composition and the preparation method and application thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/66—Enzymes
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9728—Fungi, e.g. yeasts
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
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Abstract
The present invention relates to a kind of mask compositions, and in particular to a kind of multiple-effect mask composition and the preparation method and application thereof.The multiple-effect mask composition is made of raw material as follows by weight percentage: thickener 0.05-0.5%, moisturizer 5-20%, preservative 0.1-0.8%, other additives 2-10%, surplus is water, and other additives include skin conditioning agent.The present invention has the advantages that moisturizing, anti-ageing, anti-inflammatory, whitening effect is good.
Description
Technical field
The present invention relates to cosmetic technical fields, and in particular to a kind of multiple-effect mask composition and preparation method thereof with answer
With.
Background technique
Facial mask is a kind of carrier of face beautifying health keeping product, and powder reconciliation at present, kaolin, non-woven fabrics, silk mask, biology are fine
Tie up facial mask, nonwoven fabric facial mask material facial mask using very extensive.Facial mask is a classification in skin care item, most basic
Be most important purpose it is to make up makeup removing and wash one's face still insufficient cleaning, cooperates other essential ingredients real on this basis
Existing others maintenance function, such as replenishing water and preserving moisture, whitening and anti-aging, Sage Extract etc..
Do facial mask be not intended to it is anxious catch up with prevalence, only focus on and remove nose acne, used tearing type facial mask, with
Just hurry in the mounted moisture saver mask of patch again afterwards.That effect is absolutely not equal to beauty parlor and does face.Facial mask really is made, it should
It is first to do subtraction, i.e. deep layer cleaning, exfoliating, removal oxidation grease to skin, then do addition to skin, i.e., in replenishing water and preserving moisture
On the basis of do the maintenance works such as whitening and anti-aging, Sage Extract.The principle of facial mask, exactly using be covered on face it is of short duration when
Between, it is temporarily isolating extraneous air and pollution, improves skin temperature, the pore expansion of skin promotes sweat gland secretion and new old generation
It thanks, increase the oxygen content of skin, be conducive to skin and exclude the product of epidermal cell metabolism and the oil substances of accumulation,
Moisture in facial mask penetrates into the cuticula of epidermis, and skin becomes soft, and skin is naturally bright flexible.
With the continuous improvement of people's living standards, people are also more next for the pursuit of various skin care item and face beautifying health keeping product
It is higher.Facial mask is a kind of carrier of face beautifying health keeping product, easy to use due to having many advantages, such as, take effect it is quick and by numerous people
The masses like and receive.Facial mask carries a certain amount of substance with functions such as maintenance, reparations by the carrier of various types of materials,
So that skin is naturally bright and elastic.But due to the pollution of environment, long term consumer is in undesirable environment, skin
It is influenced to be easy to produce the adverse reactions such as inflammation, allergy by outside contamination and microorganism.Therefore, facial mask is on the basis of replenishing water and preserving moisture
On also need to have anti-ageing, anti-inflammatory, whitening multi-efficiency.
Purslane is also referred to as longevity grass in China, wherein containing a large amount of flavonoids, adrenin, polysaccharide and various dimensions
The compounds such as raw element, amino acid.Purslane extract is for having antiallergy, anti-inflammatory anti-inflammatory and resisting outer bound pair skin in cosmetics
Various stimulations, there are also acne-removal functions.
Lemon extract is extracted from rutaceae Canton lemon or the fruit of lemon, and main component has limonene (up to
90%), citral, octanal, aldehyde C-9, capraldehyde, lauric aldehyde, firpene, amphene, linalool, bergamio, geranyl acetate and second
Bitter orange flower ester etc., has extraordinary facilitation to the activity of luciferase, it is anti-inflammatory to illustrate that it has the function of；It can also enhance
The metabolism of skin plays the role of anti-ageing.
Papain is a kind of protein decomposition enzyme, thus papain may act on aging angle on human skin
Matter layer promotes it to degenerate, decomposes, removal, promoting skin metabolism, and the colour of skin deepens phenomenon caused by reducing because of solarization, has
Whitening effect.
Shitake Mushroom P.E has activation to cell, and to the facilitation that has of Filaggrin, Filaggrin is contained
Collagen fabric and elastic protein fiber help to reduce wrinkle, generate to laminin and adenosine triphyosphate
Promotion all reflect its skin-active act on, can be used for anti-ageing, wrinkle resistant, firming cosmetic；Also have to the activity of melanocyte simultaneously
Certain inhibiting effect, there is the effect of whitening.
Chinese patent application CN109363997A discloses a kind of deep water supplement moisturiser and preparation method, solves existing skill
Moistening effect present in art is bad, have the shortcomings that certain irritation, moisturizing effect is poor, is mixed by the raw material of following parts by weight
It closes: moisturizer；Emollient；Emulsifier；Skin conditioning agent: beta glucan 0.3-0.8%, allantoin 0.05-0.2%, horse
Sativa extract 0.3-0.8%；Thickener: carbomer 0.03-0.1%；Neutralizer: triethanolamine 0.03-0.08%；Anti-corrosion
Agent: 1,2- hexylene glycol 0.3-0.8%, parahydroxyacet-ophenone 0.2-0.5%, essence 0.01-0.1%, surplus are deionized water.It should
The deep water supplement moisturiser that patent provides, it is alcohol-free, without hormone, non-pigment, it can effectively prevent skin moisture loss, flesh can be strengthened
The defence capability of skin fights environmental stimuli.But the moistening effect of the patent needs to be further increased, and cannot achieve moisturizing, resists
It declines, is anti-inflammatory, whitening multi-efficiency, and the comparison of ingredients of the patented product is complicated, higher cost.
Therefore, a kind of multiple-effect mask composition and preparation method thereof that can solve above-mentioned technical problem of exploitation is very
It is necessary.
Summary of the invention
It is provided the purpose of the present invention is overcome the deficiencies in the prior art a kind of with moisturizing, anti-ageing, anti-inflammatory, whitening effect
Good multiple-effect mask composition and the preparation method and application thereof.
The present invention is achieved by the following technical programs:
A kind of multiple-effect mask composition, the multiple-effect mask composition are made of raw material as follows by weight percentage:
Thickener 0.05-0.5%, moisturizer 5-20%, preservative 0.1-0.8%, other additives 2-10%, surplus is water, described
Other additives include skin conditioning agent.
Preferably, the thickener be carbomer, carbomer sodium, xanthan gum, hydroxyethyl cellulose, in mosanom at least
It is a kind of.
It is highly preferred that the thickener is at least one of carbomer, carbomer sodium, hydroxyethyl cellulose, mosanom.
It is highly preferred that the thickener is at least one of carbomer, hydroxyethyl cellulose.
Preferably, the moisturizer is propylene glycol, glycerol, trehalose, butanediol, D-sorbite, dipropylene glycol, 1,2- penta
At least one of glycol, Natrulon H-10.
It is highly preferred that the moisturizer is propylene glycol, trehalose, butanediol, D-sorbite, dipropylene glycol, 1,2- penta 2
At least one of alcohol, Natrulon H-10.
It is highly preferred that the moisturizer be propylene glycol, trehalose, butanediol, D-sorbite, in Natrulon H-10 at least
It is a kind of.
It is highly preferred that the moisturizer is at least one of propylene glycol, trehalose, butanediol.
It is highly preferred that the propylene glycol is 1,3-PD.
It is highly preferred that the butanediol is 1,3-BDO.
Preferably, the preservative is at least one of Phenoxyethanol, methyl hydroxybenzoate, benzoic acid, potassium sorbate.
It is highly preferred that the preservative is at least one of Phenoxyethanol, methyl hydroxybenzoate, potassium sorbate.
Preferably, other described additives include emulsifier, skin conditioning agent, stabilizer.
It is highly preferred that other described additives are the mixture of emulsifier, skin conditioning agent, stabilizer.
It is highly preferred that the mass ratio of the emulsifier, skin conditioning agent, stabilizer is 2-10:10-20:1.
It is highly preferred that the emulsifier is sodium acrylate/sodium acryloyldimethyl taurate copolymers, isohexadecane, gathers
Sorbitol ester, hydrogenated soy phosphatidyl choline, hemicellulose, rilanit special -40, mineral oil, -8 ester of Babassu seed oil glycerin polyether
At least one of class.
It is highly preferred that the emulsifier is sodium acrylate/sodium acryloyldimethyl taurate copolymers, isohexadecane, gathers
At least one of sorbitol ester, hydrogenated soy phosphatidyl choline, rilanit special -40, -8 esters of Babassu seed oil glycerin polyether.
It is highly preferred that the emulsifier be sodium acrylate/sodium acryloyldimethyl taurate copolymers, polysorbate,
At least one of hydrogenated soy phosphatidyl choline, rilanit special -40.
It is highly preferred that the stabilizer is at least one of triethanolamine, sodium hydroxide, potassium hydroxide, sodium bicarbonate.
It is highly preferred that the stabilizer is at least one of triethanolamine, sodium hydroxide, sodium bicarbonate.
It is highly preferred that the stabilizer is at least one of triethanolamine, sodium bicarbonate.
It is highly preferred that the skin conditioning agent is purslane extract, Shitake Mushroom P.E, lemon extract, Papain
At least one of enzyme, allantoin, hydrolyzed pearl.
Purslane extract class containing alkaloids and Flavonoid substances, can be used as that anti-inflammatory is anti-inflammatory, antiallergy functional component is answered
For cosmetics.
Lemon extract has extraordinary facilitation to the activity of luciferase, and it is anti-inflammatory to illustrate that it has the function of；It is right
The metabolism of skin can be enhanced in the activation display of cathepsin, plays the role of anti-ageing.
Allantoin, alias Allantoin, Allantoin, Allantion, Allantoin are a kind of second
Interior ureide derivative.Since allantoin is a kind of amphoteric compound, double salt can be formed in conjunction with many kinds of substance, have and be protected from light, sterilize
Anti-corrosion, analgesic, antioxidation can make skin keep moisture, moist and softness, be the special efficacy addition of the cosmetics such as cosmetology
Agent.
Lemon extract and allantoin, purslane extract have collaboration anti-inflammatory effect in the present invention.
Papain is a kind of protein decomposition enzyme, thus papain may act on aging angle on human skin
Matter layer promotes it to degenerate, decomposes, removal, promoting skin metabolism, and the colour of skin deepens phenomenon caused by reducing because of solarization, has
Whitening effect.
Shitake Mushroom P.E has activation to cell, and to the facilitation that has of Filaggrin, Filaggrin is contained
Collagen fabric and elastic protein fiber help to reduce wrinkle, generate to laminin and adenosine triphyosphate
Promotion all reflect its skin-active act on, can be used for anti-ageing, wrinkle resistant, firming cosmetic；Also have to the activity of melanocyte simultaneously
Certain inhibiting effect, there is the effect of whitening.
Hydrolyzed pearl is rich in a variety of amino acid, microelement and vitamin B, can increase the vigor of skin cell.
It is highly preferred that the skin conditioning agent is purslane extract, Shitake Mushroom P.E, lemon extract, Papain
Enzyme, allantoin, hydrolyzed pearl mixture.
It is highly preferred that the skin conditioning agent is grouped as by the group of following weight percent: purslane extract 0.1-
1%, Shitake Mushroom P.E 0.4-1.2%, lemon extract 0.001-0.1%, papain 0.001-0.1%, allantoin
0.1-0.5%, hydrolyzed pearl 0.5-2%.
Under lemon extract, allantoin, purslane extract collaboration anti-inflammatory effect, addition papain is gone the present invention
Except the cuticula of dead skin and aging on skin, promote absorption of the skin to mask composition liquid, while Shitake Mushroom P.E contains
Lentinan is capable of the Filaggrin of active cell, facilitates anti-ageing, Firm the effect of skin, along with rich in a variety of ammonia
Under the synergistic effect of the hydrolyzed pearl of base acid and vitamin, it is more advantageous to the nutrient absorption of skin, highlights skin, is able to satisfy consumption
The multiple demand of person.
Preferably, the raw material of the multiple-effect mask composition further includes essence and colorant.
Colorant and essence are added according to consumer demand, and the odor type of essence and the color number of colorant are also that basis disappears
Expense person's demand is selected and is arranged in pairs or groups.
It is highly preferred that the mass fraction of the essence is 0-0.01%.
It is highly preferred that the mass fraction of the colorant is 0-0.5%.
The invention further relates to the preparation methods of above-mentioned multiple-effect mask composition, include the following steps:
(1) thickener of formula ratio, moisturizer, water are mixed, obtains substance A；
(2) emulsifier of formula ratio and substance A are mixed, obtains substance B；
(3) stabilizer of formula ratio is mixed with substance B, obtains substance C；
(4) skin conditioning agent of formula ratio, preservative are mixed with substance C to get.
Preferably, the step (1) includes the following steps: to mix in the thickener of formula ratio, moisturizer, water, is heated to
75-85 DEG C, homogeneous 3-8min obtains substance A.
Preferably, the step (2) includes the following steps: to mix the emulsifier of formula ratio and substance A, homogeneous 3-
5min obtains substance B.
It is highly preferred that the emulsifier is dispersed in advance before mixing with substance A.
Preferably, the step (3) includes the following steps: to mix the stabilizer of formula ratio with substance B, at 75-80 DEG C
15-25min is kept the temperature, substance C is obtained.
Preferably, the step (4) includes the following steps: to be cooled to 40-50 DEG C, by the skin conditioning agent of formula ratio, prevents
Rotten agent mixed with substance C to get.
The invention further relates to the multiple-effect mask compositions that above-mentioned multiple-effect mask composition or above-mentioned preparation method are prepared
Application in facial mask.
The beneficial effects of the present invention are:
Skin conditioning agent of the invention is under lemon extract, allantoin, purslane extract collaboration anti-inflammatory effect, addition
Papain removes the dead skin on skin and the cuticula of aging, promotes absorption of the skin to mask composition, while mushroom
Extract contains lentinan, is capable of the Filaggrin of active cell, along with the hydrolysis for being rich in a variety of amino acid and vitamin
Under the synergistic effect of pearl, facilitate the nutrient absorption of the anti-ageing of skin, skin tightening effect and skin, highlights skin, skin tune
Each component synergistic effect in agent is managed, the multiple demand of consumer is able to satisfy.
The present invention defines the order of addition of each raw material during the preparation process, is conducive to each raw material and is better mixed,
The cooperative effect between raw material is preferably played, the product using effect being prepared under limiting temperature and time is more preferable, has both
Moisturizing, whitening and anti-aging, anti-inflammatory multi-efficiency.
Specific embodiment
The invention will now be further described with reference to specific embodiments, the advantages and features of the present invention will be with description and
It is apparent.But examples are merely exemplary for these, and it is not intended to limit the scope of the present invention in any way.Those skilled in the art
Member it should be understood that without departing from the spirit and scope of the invention can details to technical solution of the present invention and form into
Row modifications or substitutions, but these modifications and replacement are fallen within the protection scope of the present invention.
Embodiment 1
A kind of multiple-effect mask composition, is made of raw material as follows by weight percentage: carbomer 0.05%, 1,3- third
Glycol 5%, Phenoxyethanol 0.1%, other additives 2%, surplus is water, wherein other additives are sodium acrylate/acryloyl
Dimethyltaurine sodium copolymer, skin conditioning agent, triethanolamine mixture, three's mass ratio be 2:10:1；
Skin conditioning agent is grouped as by the group of following weight percent: purslane extract 0.1%, Shitake Mushroom P.E
0.4%, lemon extract 0.001%, papain 0.001%, allantoin 0.1%, hydrolyzed pearl 0.5%.
The preparation method of mask composition:
(1) carbomer of formula ratio, 1,3-PD, water are mixed, 75 DEG C, homogeneous 3min are heated in emulsion pot,
Obtain substance A；
(2) emulsion pot neutralize material A is added in the sodium acrylate of formula ratio/sodium acryloyldimethyl taurate copolymers to mix
It closes, homogeneous 3min obtains substance B；
(3) triethanolamine of formula ratio is added in emulsion pot and is mixed with substance B, stirring is protected to being completely dissolved at 75 DEG C
Warm 15min, obtains substance C；
(4) emulsion pot is cooled to 40 DEG C, the skin conditioning agent of formula ratio is added, Phenoxyethanol is mixed with substance C, stirring
Uniformly to get.
Embodiment 2
A kind of multiple-effect mask composition, is made of raw material as follows by weight percentage: xanthan gum 0.5%, trehalose
20%, methyl hydroxybenzoate 0.8%, other additives 10%, 0.01% rose essence (it is limited to be purchased from the magnificent flavors and fragrances in Guangzhou
Company), 0.5% lemon yellow CI19140, surplus is water, wherein other additives are isohexadecane, skin conditioning agent, hydroxide
The mixture of potassium, three's mass ratio are 10:20:1；
Skin conditioning agent is grouped as by the group of following weight percent: purslane extract 1%, Shitake Mushroom P.E 1.2%,
Lemon extract 0.1%, papain 0.1%, allantoin 0.5%, hydrolyzed pearl 2%.
The preparation method of mask composition:
(1) xanthan gum of formula ratio, trehalose, water are mixed, 85 DEG C is heated in emulsion pot, homogeneous 8min obtains object
Matter A；
(2) emulsion pot neutralize material A is added in the pre-dispersed good isohexadecane of formula ratio to mix, homogeneous 5min obtains object
Matter B；
(3) potassium hydroxide of formula ratio is added in emulsion pot and is mixed with substance B, stirring is protected to being completely dissolved at 80 DEG C
Warm 25min, obtains substance C；
(4) emulsion pot is cooled to 50 DEG C, the skin conditioning agent of formula ratio is added, methyl hydroxybenzoate is mixed with substance C, stirring
Uniformly, substance D is obtained.
(5) 45 DEG C are cooled to then, be added colorant, essence and substance D be mixed and stirred for uniformly to get.
Embodiment 3
A kind of multiple-effect mask composition, is made of raw material as follows by weight percentage: hydroxyethyl cellulose 0.25%,
Natrulon H-10 12%, benzoic acid 0.4%, other additives 6%, surplus is water, wherein other additives are hydrogenated soybean ovum
Phosphatide, skin conditioning agent, sodium hydroxide mixture, three's mass ratio be 6:15:1；
Skin conditioning agent is grouped as by the group of following weight percent: purslane extract 0.5%, Shitake Mushroom P.E
0.8%, lemon extract 0.05%, papain 0.05%, allantoin 0.3%, hydrolyzed pearl 1.0%.
The preparation method of mask composition:
(1) hydroxyethyl cellulose of formula ratio, Natrulon H-10, water are mixed, 80 DEG C is heated in emulsion pot, homogeneous
5min obtains substance A；
(2) emulsion pot neutralize material A is added in the hydrogenated soy phosphatidyl choline of formula ratio to mix, homogeneous 4min obtains substance B；
(3) sodium hydroxide of formula ratio is added in emulsion pot and is mixed with substance B, stirring is protected to being completely dissolved at 78 DEG C
Warm 20min, obtains substance C；
(4) emulsion pot is cooled to 45 DEG C, the skin conditioning agent of formula ratio is added, benzoic acid is mixed with substance C, stirring is equal
It is even to get.
Embodiment 4
A kind of multiple-effect mask composition, is made of raw material as follows by weight percentage: mosanom 0.25%, sorbose
Alcohol 12%, potassium sorbate 0.4%, other additives 6%, surplus is water, other additives are Babassu seed oil glycerin polyether -8
Esters, skin conditioning agent, sodium bicarbonate mixture, three's mass ratio be 6:15:1；
Skin conditioning agent is grouped as by the group of following weight percent: purslane extract 0.5%, Shitake Mushroom P.E
0.8%, lemon extract 0.05%, papain 0.05%, allantoin 0.3%, hydrolyzed pearl 1.5%.
The preparation method of mask composition:
(1) mosanom of formula ratio, D-sorbite, water are mixed, 80 DEG C is heated in emulsion pot, homogeneous 5min is obtained
Substance A；
(2) emulsion pot neutralize material A is added in -8 esters of Babassu seed oil glycerin polyether of formula ratio to mix, homogeneous
4min obtains substance B；
(3) sodium bicarbonate of formula ratio is added in emulsion pot and is mixed with substance B, stirring is protected to being completely dissolved at 78 DEG C
Warm 20min, obtains substance C；
(4) emulsion pot is cooled to 45 DEG C, the skin conditioning agent of formula ratio is added, potassium sorbate is mixed with substance C, stirring
Uniformly to get.
Embodiment 5
A kind of multiple-effect mask composition, is made of raw material as follows by weight percentage: carbomer 0.3%, 1,3- third
Glycol 15%, Phenoxyethanol 0.5%, other additives 6%, surplus is water, other additives are rilanit special -40, skin
The mixture of conditioner, triethanolamine, three's mass ratio are 8:12:1；
Skin conditioning agent is grouped as by the group of following weight percent: purslane extract 0.5%, Shitake Mushroom P.E
1.0%, lemon extract 0.08%, papain 0.05%, allantoin 0.5%, hydrolyzed pearl 1.0%.
The preparation method of mask composition:
(1) carbomer of formula ratio, 1,3-PD, water are mixed, 80 DEG C, homogeneous 5min are heated in emulsion pot,
Obtain substance A；
(2) emulsion pot neutralize material A is added in the rilanit special -40 of formula ratio to mix, homogeneous 3min obtains substance B；
(3) triethanolamine of formula ratio is added in emulsion pot and is mixed with substance B, stirring is protected to being completely dissolved at 75 DEG C
Warm 20min, obtains substance C；
(4) emulsion pot is cooled to 45 DEG C, the skin conditioning agent of formula ratio is added, Phenoxyethanol is mixed with substance C, stirring
Uniformly to get.
Comparative example 1
A kind of multiple-effect mask composition, compared with Example 5, difference are only that each composition quality score is different, remaining
Part is all the same, specific as follows:
Carbomer 0.01%, 1,3-PD 15%, Phenoxyethanol 1%, other additives 15%, surplus is water, wherein
Other additives are the mixture of rilanit special -40, skin conditioning agent, triethanolamine, and three's mass ratio is 8:12:1；
Skin conditioning agent is grouped as by the group of following weight percent: purslane extract 0.5%, Shitake Mushroom P.E
1.0%, lemon extract 0.08%, papain 0.05%, allantoin 0.5%, hydrolyzed pearl 1.0%.
Comparative example 2
A kind of multiple-effect mask composition, compared with Example 5, difference are only that the ingredient of skin conditioning agent is different, remaining
Condition is all the same, specific as follows:
Skin conditioning agent is grouped as by the group of following weight percent: Yunnan camellia flower extract 0.5%, Shitake Mushroom P.E
1.0%, lemon extract 0.08%, papain 0.05%, allantoin 0.5%, hydrolyzed pearl 1.0%.
Comparative example 3
A kind of multiple-effect mask composition, compared with Example 5, difference are only that each composition quality score in skin conditioning agent
Difference, remaining condition is all the same, specific as follows:
Skin conditioning agent is grouped as by the group of following weight percent: purslane extract 1.5%, Shitake Mushroom P.E
1.5%, lemon extract 0.15%, papain 0.15%, allantoin 1.0%, hydrolyzed pearl 2.5%.
Comparative example 4
A kind of multiple-effect mask composition, compared with Example 5, difference are only that the order of addition of raw material in preparation process not
Together, remaining condition is all the same, specific as follows:
The preparation method of mask composition:
(1) carbomer of formula ratio, 1,3-PD, water are mixed, 80 DEG C, homogeneous 5min are heated in emulsion pot,
Obtain substance A；
(2) Phenoxyethanol of formula ratio, triethanolamine are added emulsion pot neutralize material A and mixed, stirring to being completely dissolved,
In 75 DEG C of heat preservation 20min, substance B is obtained；
(3) rilanit special -40 of formula ratio is added in emulsion pot and is mixed with substance B, homogeneous 3min obtains substance C；
(4) emulsion pot is cooled to 45 DEG C, the skin conditioning agent that formula ratio is added is mixed with substance C, is stirred evenly, i.e.,
?.1 human body patch test of test case
Test method: health volunteer of 90 ages of selection at 20-40 years old；Subject was not used anti-in nearly two months
Scorching drug or cosmetics, are randomly divided into 9 groups, and every group of 10 people carry out the mask composition test of embodiment 1-5 and comparative example 1-4.
The mask composition of the embodiment of the present invention 1-5 and comparative example 1-4 are put into spot tester (spot tester selects non-stimulated adhesive tape),
Dosage is 0.03g.Non-stimulated adhesive tape added with mask composition spreads on to the inner forearm of subject, side is check plot, one
Side is trial zone, is gently pressed with palm and is allowed to uniformly be pasted on skin, continues 24 hours.Remove mask composition after respectively at
0.5, observation dermoreaction in 12,24,48 hours, records its knot according to dermoreaction grade scale in " cosmetics health specification "
Fruit.
Test result: human skin patch test result shows all subjects by patch test, 0.5,12,24,
Observation dermoreaction in 48 hours, wherein it is bad anti-to there is not erythema, papule, blister etc. by embodiment 1-5 and comparative example 2-4
It answers, comparative example 1 has 1 skin slight erythema occur, illustrates product safety of the invention, non-stimulated.
2 moisturizing of test case test
90 people of healthy volunteer between 20~45 years old is chosen, is randomly divided into 9 groups, every group of 10 people use SK IV number before testing
Word moisture of skin tester tests the skin moisture content of volunteer, in the environment of room temperature, humidity 40-60%, with clean
Water cleans the back of the hand, then respectively with having impregnated equivalent and after enough embodiment 1-5 and comparative example 1-4 mask composition 30min
3 × 3cm2Non-woven cotton applies after same specified skin part, 20min while removing non-woven cotton, in remove non-woven cotton 0,
After 30min, 60min, the moisture content of the skin of subject is tested with SK IV digital skin moisture tester, and counts
It calculates as follows using skin moisture content amplitude of variation, calculation formula after 0,30min, 60min: the amplitude of variation of skin moisture content
=[(using the moisture content of the preceding skin of moisture content-use of rear skin)/using the moisture content of preceding skin] × 100%,
Test result is referring to table 1.
1 skin moisture content amplitude of variation result of table
Test case 3 is anti-ageing to be tested with whitening effect
105 ages are chosen in 20-45 years old women's health volunteer, are randomly divided into 7 groups, every group of 15 people are clean every time
Using the embodiment of the present invention 1, embodiment 3, embodiment 5 and the facial mask of comparative example 1-4 preparation behind face, a piece of (every is used every time
Facial mask liquid 25mL, the facial mask cloth of same material), it uses 2 times weekly, and identical using the time every time.After continuous use 1 month,
It acquires volunteer to evaluate the anti-ageing and whitening effect of product, the results are shown in Table 2.
Table 2 is anti-ageing with whitening test result
The technical means disclosed in the embodiments of the present invention is not limited to the technical means disclosed in the above technical means, and further includes
Technical solution consisting of any combination of the above technical features.The foregoing is a specific embodiment of the present invention, should refer to
Out, for those skilled in the art, without departing from the principle of the present invention, can also make several
Improvements and modifications, these modifications and embellishments are also considered to be within the scope of the present invention.
Claims (10)
1. a kind of multiple-effect mask composition, which is characterized in that the multiple-effect mask composition is by as follows by weight percentage
Raw material composition: thickener 0.05-0.5%, moisturizer 5-20%, preservative 0.1-0.8%, other additives 2-10%, surplus
For water, other additives include skin conditioning agent.
2. multiple-effect mask composition according to claim 1, which is characterized in that the thickener is carbomer, carbomer
At least one of sodium, xanthan gum, hydroxyethyl cellulose, mosanom；The moisturizer is propylene glycol, glycerol, trehalose, fourth two
At least one of alcohol, D-sorbite, dipropylene glycol, 1,2- pentanediol, Natrulon H-10；The preservative is Phenoxyethanol, hydroxyl
At least one of benzene methyl, benzoic acid, potassium sorbate.
3. multiple-effect mask composition according to claim 1, which is characterized in that other described additives include emulsifier,
Skin conditioning agent, stabilizer.
4. multiple-effect mask composition according to claim 3, which is characterized in that the emulsifier, skin conditioning agent, stabilization
The mass ratio of agent is 2-10:10-20:1.
5. multiple-effect mask composition according to claim 3, which is characterized in that the emulsifier is sodium acrylate/propylene
Acyl dimethyltaurine sodium copolymer, isohexadecane, polysorbate, hydrogenated soy phosphatidyl choline, hemicellulose, hydrogenated castor
At least one of oil -40, mineral oil, -8 esters of Babassu seed oil glycerin polyether；The stabilizer is triethanolamine, hydroxide
At least one of sodium, potassium hydroxide, sodium bicarbonate.
6. multiple-effect mask composition according to claim 3, which is characterized in that the skin conditioning agent is purslane extraction
At least one of object, Shitake Mushroom P.E, lemon extract, papain, allantoin, hydrolyzed pearl, it is preferable that the skin
Skin conditioner is the mixed of purslane extract, Shitake Mushroom P.E, lemon extract, papain, allantoin and hydrolyzed pearl
Close object.
7. multiple-effect mask composition according to claim 6, which is characterized in that the skin conditioning agent is by following weight hundred
The group of score is grouped as: purslane extract 0.1-1%, Shitake Mushroom P.E 0.4-1.2%, lemon extract 0.001-0.1%,
Papain 0.001-0.1%, allantoin 0.1-0.5%, hydrolyzed pearl 0.5-2%.
8. a kind of preparation method of any one of claim 1-7 multiple-effect mask composition, which is characterized in that including walking as follows
It is rapid:
(1) thickener of formula ratio, moisturizer, water are mixed, obtains substance A；
(2) emulsifier of formula ratio and substance A are mixed, obtains substance B；
(3) stabilizer of formula ratio is mixed with substance B, obtains substance C；
(4) skin conditioning agent of formula ratio, preservative are mixed with substance C to get.
9. preparation method according to claim 8, which comprises the steps of:
(1) thickener of formula ratio, moisturizer, water are mixed, is heated to 75-85 DEG C, homogeneous 3-8min obtains substance A；
(2) emulsifier of formula ratio and substance A are mixed, homogeneous 3-5min obtains substance B；
(3) stabilizer of formula ratio is mixed with substance B, in 75-80 DEG C of heat preservation 15-25min, obtains substance C；
(4) be cooled to 40-50 DEG C, the skin conditioning agent of formula ratio, preservative are mixed with substance C to get.
10. any one of any one of the claim 1-7 multiple-effect mask composition or claim 8-9 the preparation method preparation
Application of the obtained multiple-effect mask composition in facial mask.
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| CN112057352A (en) * | 2020-09-28 | 2020-12-11 | 李友贵 | Whitening, skin-tendering, moisturizing and health-preserving mask |
| CN112089678A (en) * | 2020-10-28 | 2020-12-18 | 北海市海真珠化妆品有限公司 | Preservative-free moisturizing pearl facial mask and preparation method thereof |
| CN114504544A (en) * | 2022-01-20 | 2022-05-17 | 广东柏俐臣生物科技有限公司 | Facial mask liquid containing lactobacillus soybean milk fermentation product filtrate and preparation method thereof |
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| CN110200898B (en) | 2023-01-24 |
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