CN110200898B - Multi-effect mask composition and preparation method and application thereof - Google Patents
Multi-effect mask composition and preparation method and application thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9728—Fungi, e.g. yeasts
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61Q19/08—Anti-ageing preparations
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
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Abstract
The invention relates to a mask composition, and in particular relates to a multi-effect mask composition as well as a preparation method and application thereof. The multi-effect mask composition is prepared from the following raw materials in percentage by weight: 0.05-0.5% of thickening agent, 5-20% of humectant, 0.1-0.8% of preservative, 2-10% of other additives and the balance of water, wherein the other additives comprise skin conditioner. The invention has the advantages of moisture preservation, anti-aging, anti-inflammation and good whitening effect.
Description
Technical Field
The invention relates to the technical field of cosmetics, and in particular relates to a multi-effect mask composition as well as a preparation method and application thereof.
Background
The mask is a carrier of beauty care products, and the existing masks made of blended powder, kaolin, non-woven fabrics, silk masks, biological fiber masks and non-woven fabrics are widely used. The mask is a category of skin care products, and the most important purpose of the mask is to make up for the cleaning work of makeup removal and face washing, and realize other maintenance functions such as moisturizing, whitening, anti-aging, grease balancing and the like by matching with other essential ingredients on the basis.
The facial mask is not required to be popular urgently, and the adhesive type moisturizing facial mask is only used after the tearing type facial mask is used and the nose acne is removed. That effect is absolutely not equal to going to the beauty salon to do the face. The real facial mask is prepared by firstly carrying out subtraction on skin, namely deeply cleaning, removing cutin and removing oxidized grease, and then carrying out addition on the skin, namely carrying out maintenance work such as whitening, anti-aging, grease balancing and the like on the basis of water replenishing and moisture retention. The principle of the facial mask is that the facial mask is covered on the face for a short time, so that outside air and pollution are temporarily isolated, the skin temperature is increased, pores of the skin are expanded, sweat gland secretion and metabolism are promoted, the oxygen content of the skin is increased, products of epidermal cell metabolism and accumulated grease substances are favorably removed from the skin, water in the facial mask permeates into the horny layer of the epidermis, the skin becomes soft, and the skin is naturally bright and elastic.
With the continuous improvement of the living standard of people, people pursue various skin care products and beauty care products more and more. The mask is a carrier of a beauty treatment product, and is popular and accepted by the masses due to the advantages of convenient use, quick response and the like. The facial mask carries a certain amount of substances with the functions of maintaining, repairing and the like through carriers of various materials, so that the skin is naturally bright and elastic. However, due to environmental pollution, consumers are in a bad environment for a long time, and adverse reactions such as inflammation and allergy are easily generated on the skin under the influence of external pollution and microorganisms. Therefore, the mask needs to have multiple effects of resisting aging, resisting inflammation and whitening on the basis of moisturizing.
Purslane is also called longevity grass in China, and contains a large amount of flavonoids, epinephrine, polysaccharides, various vitamins, amino acids and other compounds. The herba Portulacae extract has antiallergic, antiinflammatory, and skin irritation resisting effects, and is used in cosmetics for removing acne.
The lemon extract is extracted from the fruit of Rutaceae plant Citrus aurantium or Citrus depressa, the main components of the extract comprise limonene (up to 90 percent), citral, octanal, nonanal, decanal, dodecanal, pinene, camphene, linalool, linalyl acetate, geranyl acetate, neryl acetate and the like, and the extract has a very good promoting effect on the activity of luciferase, so that the extract has an anti-inflammatory effect; it also has effects in promoting skin metabolism and resisting aging.
The papain is a protease, so the papain can act on the aged horny layer on the skin of a human body, promote the degeneration, decomposition and removal of the aged horny layer, promote the metabolism of the skin, reduce the phenomenon of darkening of the skin caused by the sun and has the whitening effect.
The shiitake extract has cell activating effect and fibronectin promoting effect, wherein the fibronectin contains collagen fibers and elastin fibers, which is helpful for reducing wrinkles, reflects the skin activating effect on the promotion of laminin and adenosine triphosphate generation, and can be used in anti-aging, anti-wrinkle and skin-firming cosmetics; meanwhile, the whitening cream also has a certain inhibiting effect on the activity of melanocytes and has the whitening effect.
Chinese patent application CN109363997A discloses a deep moisturizing cream and a preparation method thereof, which solve the defects of poor moisturizing effect, certain irritation and poor moisturizing effect in the prior art, and is prepared by mixing the following raw materials in parts by weight: a humectant; an emollient; an emulsifier; skin conditioner: beta-glucan 0.3-0.8%, allantoin 0.05-0.2%, and purslane extract 0.3-0.8%; thickening agent: carbomer 0.03-0.1%; neutralizing agent: 0.03-0.08% of triethanolamine; preservative: 1,2-hexanediol 0.3-0.8%, p-hydroxyacetophenone 0.2-0.5%, essence 0.01-0.1%, and the balance of deionized water. The deep moisturizing cream provided by the patent has no alcohol, hormone or pigment, can effectively prevent the water loss of the skin, can strengthen the defense capability of the skin and can resist external stimulation. However, the moisturizing effect of the patent needs to be further improved, multiple effects of moisturizing, anti-aging, anti-inflammation and whitening cannot be realized, and the components of the product of the patent are complex and the cost is high.
Therefore, it is very necessary to develop a multi-effect mask composition and a method for preparing the same, which can solve the above technical problems.
Disclosure of Invention
The invention aims to overcome the defects of the prior art and provides a multi-effect mask composition with good moisturizing, anti-aging, anti-inflammatory and whitening effects, and a preparation method and application thereof.
The invention is realized by the following technical scheme:
the multi-effect mask composition is prepared from the following raw materials in percentage by weight: 0.05-0.5% of thickening agent, 5-20% of humectant, 0.1-0.8% of preservative, 2-10% of other additives and the balance of water, wherein the other additives comprise a skin conditioner.
Preferably, the thickener is at least one of carbomer, sodium carbomer, xanthan gum, hydroxyethyl cellulose and sodium alginate.
More preferably, the thickener is at least one of carbomer, sodium carbomer, hydroxyethyl cellulose, sodium alginate.
More preferably, the thickener is at least one of carbomer and hydroxyethyl cellulose.
Preferably, the humectant is at least one of propylene glycol, glycerin, trehalose, butylene glycol, sorbitol, dipropylene glycol, 1,2-pentanediol, and polyglycerol-10.
More preferably, the humectant is at least one of propylene glycol, trehalose, butylene glycol, sorbitol, dipropylene glycol, 1,2-pentanediol, and polyglycerol-10.
More preferably, the humectant is at least one of propylene glycol, trehalose, butylene glycol, sorbitol, and polyglycerol-10.
More preferably, the humectant is at least one of propylene glycol, trehalose, and butylene glycol.
More preferably, the propylene glycol is 1,3-propanediol.
More preferably, the butanediol is 1,3-butanediol.
Preferably, the preservative is at least one of phenoxyethanol, methylparaben, benzoic acid and potassium sorbate.
More preferably, the preservative is at least one of phenoxyethanol, methylparaben and potassium sorbate.
Preferably, the other additives include emulsifiers, skin conditioners, stabilizers.
More preferably, the further additive is a mixture of emulsifiers, skin conditioners, stabilizers.
More preferably, the mass ratio of the emulsifier to the skin conditioner to the stabilizer is 2-10.
More preferably, the emulsifier is at least one of sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane, polysorbate, hydrogenated soybean lecithin, hemicellulose, hydrogenated castor oil-40, mineral oil, babassu seed oil glyceryl polyether-8 ester.
More preferably, the emulsifier is at least one of sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane, polysorbate, hydrogenated soybean lecithin, hydrogenated castor oil-40, and babassu seed oil glyceryl polyether-8 ester.
More preferably, the emulsifier is at least one of sodium acrylate/sodium acryloyldimethyl taurate copolymer, polysorbate, hydrogenated soybean lecithin, hydrogenated castor oil-40.
More preferably, the stabilizer is at least one of triethanolamine, sodium hydroxide, potassium hydroxide and sodium bicarbonate.
More preferably, the stabilizer is at least one of triethanolamine, sodium hydroxide and sodium bicarbonate.
More preferably, the stabilizer is at least one of triethanolamine and sodium bicarbonate. .
More preferably, the skin conditioner is at least one of purslane extract, shiitake extract, lemon extract, papain, allantoin, and hydrolyzed pearl.
The herba Portulacae extract contains alkaloids and flavonoids, and can be used as antiinflammatory, antiinflammatory and antiallergic components in cosmetics.
The lemon extract has a very good promoting effect on the activity of luciferase, which indicates that the lemon extract has an anti-inflammatory effect; the activation of cathepsin can enhance the metabolism of skin and has the function of anti-aging.
Allantoin, also known as 5-ureylethanolamide, ureidoacetolactam, ureidohydantoin, uretidione, is a hydantoin derivative. The allantoin is an amphoteric compound, can be combined with various substances to form a double salt, has the effects of protecting from light, sterilizing, preventing corrosion, relieving pain and resisting oxidation, can keep the skin moisture, moisten and soften, and is a special additive for cosmetics such as beauty, hairdressing and the like.
The lemon extract, allantoin and purslane extract have a synergistic anti-inflammatory effect.
The papain is a protease, so the papain can act on the aged horny layer on the skin of a human body, promote the degeneration, decomposition and removal of the aged horny layer, promote the metabolism of the skin, reduce the phenomenon of darkening of the skin caused by the sun and has the whitening effect.
The lentinus edodes extract has the effects of activating cells and promoting the generation of fibronectin, wherein the fibronectin comprises collagen fibers and elastin fibers, which are beneficial to reducing wrinkles, the skin-activating effect is reflected by the promotion of the generation of laminin and adenosine triphosphate, and the lentinus edodes extract can be used in anti-aging, anti-wrinkle and skin-firming cosmetics; meanwhile, the whitening cream also has a certain inhibiting effect on the activity of melanocytes and has the whitening effect.
The hydrolyzed pearl is rich in various amino acids, microelements and vitamin B, and can increase skin cell activity.
More preferably, the skin conditioner is a mixture of purslane extract, shiitake extract, lemon extract, papain, allantoin, hydrolyzed pearls.
More preferably, the skin conditioner consists of the following components in parts by weight: 0.1-1 part of purslane extract, 0.4-1.2 parts of mushroom extract, 0.001-0.1 part of lemon extract, 0.001-0.1 part of papain, 0.1-0.5 part of allantoin and 0.5-2 parts of hydrolyzed pearl.
According to the invention, under the synergistic anti-inflammatory action of the lemon extract, the allantoin and the purslane extract, papain is added to remove dead skin and aged cuticle on the skin, so as to promote the absorption of the facial mask composition liquid by the skin, meanwhile, the lentinan extract contains lentinan, can activate the fibrin of cells, is beneficial to the anti-aging and firming effects of the skin, and under the synergistic action of the hydrolyzed pearls rich in various amino acids and vitamins, the nutrition absorption of the skin is facilitated, the skin is brightened, and the multiple requirements of consumers can be met.
Preferably, the raw materials of the multi-effect mask composition further comprise essence and a coloring agent.
The coloring agent and the essence are added according to the requirements of consumers, and the odor type of the essence and the color number of the coloring agent are selected and matched according to the requirements of the consumers.
More preferably, the mass fraction of the essence is 0-0.01%.
More preferably, the mass fraction of the colorant is 0 to 0.5%.
The invention also relates to a preparation method of the multi-effect mask composition, which comprises the following steps:
(1) Mixing the thickener, the humectant and water according to the formula ratio to obtain a substance A;
(2) Mixing the emulsifier with the substance A according to the formula ratio to obtain a substance B;
(3) Mixing the stabilizer with the substance B according to the formula amount to obtain a substance C;
(4) Mixing the skin conditioner and the preservative with the substance C according to the formula amount to obtain the skin care product.
Preferably, the step (1) includes the steps of: mixing the thickener, humectant and water, heating to 75-85 deg.C, and homogenizing for 3-8min to obtain substance A.
Preferably, the step (2) includes the steps of: mixing emulsifier and substance A, and homogenizing for 3-5min to obtain substance B.
More preferably, the emulsifier is dispersed beforehand before being mixed with substance a.
Preferably, the step (3) includes the steps of: mixing the stabilizer with the substance B according to the formula amount, and keeping the temperature at 75-80 ℃ for 15-25min to obtain a substance C.
Preferably, the step (4) includes the steps of: cooling to 40-50 deg.C, and mixing with skin conditioner, antiseptic and substance C.
The invention also relates to an application of the multi-effect facial mask composition or the multi-effect facial mask composition prepared by the preparation method in facial masks.
The beneficial effects of the invention are:
according to the skin conditioner, under the synergistic anti-inflammatory action of the lemon extract, the allantoin and the purslane extract, papain is added to remove dead skin and aged cuticle on the skin, so that the absorption of the facial mask composition by the skin is promoted, meanwhile, the lentinan extract contains lentinan, and the cell fibrin can be activated, and under the synergistic action of hydrolyzed pearls rich in various amino acids and vitamins, the skin conditioner is beneficial to the anti-aging and firming effects of the skin and the nutrient absorption of the skin, so that the skin is brightened, and the components in the skin conditioner have synergistic action, so that the multiple requirements of consumers can be met.
The invention limits the adding sequence of each raw material in the preparation process, is beneficial to better mixing of each raw material, better exerts the synergistic effect among the raw materials, and has the multiple effects of moisturizing, whitening, anti-aging and anti-inflammation under the condition of limited temperature and time.
Detailed Description
The invention will be further described with reference to specific embodiments, and the advantages and features of the invention will become apparent as the description proceeds. These examples are illustrative only and do not limit the scope of the present invention in any way. It will be understood by those skilled in the art that various changes in form and details may be made therein without departing from the spirit and scope of the invention, and that such changes and modifications may be made without departing from the spirit and scope of the invention.
Example 1
A multi-effect mask composition comprises the following raw materials in percentage by weight: carbomer 0.05%,1,3-propylene glycol 5%, phenoxyethanol 0.1%, other additives 2%, and the balance water, wherein the other additives are a mixture of sodium acrylate/sodium acryloyldimethyl taurate copolymer, a skin conditioner, and triethanolamine, and the mass ratio of the three is 2;
the skin conditioner consists of the following components in parts by weight: 0.1 part of purslane extract, 0.4 part of mushroom extract, 0.001 part of lemon extract, 0.001 part of papain, 0.1 part of allantoin and 0.5 part of hydrolyzed pearl.
The preparation method of the mask composition comprises the following steps:
(1) Mixing carbomer, 1,3-propylene glycol and water according to the formula ratio, heating to 75 ℃ in an emulsifying pot, and homogenizing for 3min to obtain a substance A;
(2) Adding the sodium acrylate/sodium acryloyldimethyl taurate copolymer in the formula ratio into an emulsifying pot to neutralize the substance A, and homogenizing for 3min to obtain a substance B;
(3) Adding triethanolamine with formula amount into an emulsifying pot, mixing with the substance B, stirring to completely dissolve, and keeping the temperature at 75 ℃ for 15min to obtain a substance C;
(4) Cooling the emulsifying pot to 40 ℃, adding the skin conditioner, the phenoxyethanol and the substance C according to the formula ratio, and uniformly stirring to obtain the skin-care cream.
Example 2
A multi-effect mask composition comprises the following raw materials in percentage by weight: 0.5% of xanthan gum, 20% of trehalose, 0.8% of methyl hydroxybenzoate, 10% of other additives, 0.01% of rose essence (purchased from Huadong essence and spice Co., ltd., guangzhou city), 0.5% of lemon yellow CI19140 and the balance of water, wherein the other additives are a mixture of isohexadecane, a skin conditioner and potassium hydroxide, and the mass ratio of the three is 10;
the skin conditioner consists of the following components in parts by weight: 1 part of purslane extract, 1.2 parts of mushroom extract, 0.1 part of lemon extract, 0.1 part of papain, 0.5 part of allantoin and 2 parts of hydrolyzed pearl.
The preparation method of the mask composition comprises the following steps:
(1) Mixing xanthan gum, trehalose and water according to the formula ratio, heating to 85 ℃ in an emulsifying pot, and homogenizing for 8min to obtain a substance A;
(2) Adding the pre-dispersed isohexadecane in the formula amount into an emulsifying pot to neutralize the substance A, and homogenizing for 5min to obtain a substance B;
(3) Adding potassium hydroxide with the formula amount into an emulsifying pot, mixing with the substance B, stirring until the potassium hydroxide is completely dissolved, and keeping the temperature at 80 ℃ for 25min to obtain a substance C;
(4) And cooling the emulsifying pot to 50 ℃, adding the skin conditioner, the methyl hydroxybenzoate and the substance C in the formula amount, and uniformly stirring to obtain a substance D.
(5) Then cooling to 45 ℃, adding the colorant, the essence and the substance D, and uniformly stirring to obtain the product.
Example 3
A multi-effect mask composition comprises the following raw materials in percentage by weight: 0.25% of hydroxyethyl cellulose, 10% of polyglycerol-10%, 0.4% of benzoic acid, 6% of other additives and the balance of water, wherein the other additives are a mixture of hydrogenated soybean lecithin, a skin conditioner and sodium hydroxide, and the mass ratio of the three is 6;
the skin conditioner consists of the following components in parts by weight: 0.5 part of purslane extract, 0.8 part of mushroom extract, 0.05 part of lemon extract, 0.05 part of papain, 0.3 part of allantoin and 1.0 part of hydrolyzed pearl.
The preparation method of the mask composition comprises the following steps:
(1) Mixing hydroxyethyl cellulose, polyglycerol-10 and water according to formula ratio, heating to 80 deg.C in emulsifying pot, and homogenizing for 5min to obtain substance A;
(2) Adding hydrogenated soybean lecithin with formula ratio into an emulsifying pot to neutralize the substance A, and homogenizing for 4min to obtain a substance B;
(3) Adding sodium hydroxide with the formula amount into an emulsifying pot, mixing with the substance B, stirring until the sodium hydroxide is completely dissolved, and keeping the temperature at 78 ℃ for 20min to obtain a substance C;
(4) Cooling the emulsifying pot to 45 ℃, adding the skin conditioner, the benzoic acid and the substance C in the formula amount, and uniformly stirring to obtain the skin-care cream.
Example 4
A multi-effect mask composition comprises the following raw materials in percentage by weight: 0.25% of sodium alginate, 12% of sorbitol, 0.4% of potassium sorbate, 6% of other additives and the balance of water, wherein the other additives are a mixture of babassu seed oil glycerol polyether-8 esters, a skin conditioner and sodium bicarbonate, and the mass ratio of the three is 6;
the skin conditioner consists of the following components in parts by weight: 0.5 part of purslane extract, 0.8 part of mushroom extract, 0.05 part of lemon extract, 0.05 part of papain, 0.3 part of allantoin and 1.5 parts of hydrolyzed pearl.
The preparation method of the mask composition comprises the following steps:
(1) Mixing sodium alginate, sorbitol and water, heating to 80 deg.C in emulsifying pot, and homogenizing for 5min to obtain substance A;
(2) Adding the Babesia seed oil glyceryl polyether-8 esters into an emulsifying pot according to the formula ratio to neutralize the substance A, and homogenizing for 4min to obtain a substance B;
(3) Adding sodium bicarbonate with formula amount into an emulsifying pot, mixing with the substance B, stirring to completely dissolve, and keeping the temperature at 78 deg.C for 20min to obtain substance C;
(4) Cooling the emulsifying pot to 45 ℃, adding the skin conditioner, the potassium sorbate and the substance C in the formula amount, and uniformly stirring to obtain the skin-care cream.
Example 5
A multi-effect mask composition comprises the following raw materials in percentage by weight: carbomer 0.3%,1,3-propylene glycol 15%, phenoxyethanol 0.5%, other additives 6%, the balance water, the other additives are hydrogenated castor oil-40, skin conditioner, triethanolamine mixture, the mass ratio of the three is 8;
the skin conditioner consists of the following components in parts by weight: 0.5 part of purslane extract, 1.0 part of mushroom extract, 0.08 part of lemon extract, 0.05 part of papain, 0.5 part of allantoin and 1.0 part of hydrolyzed pearl.
The preparation method of the mask composition comprises the following steps:
(1) Mixing carbomer, 1,3-propylene glycol and water according to the formula ratio, heating to 80 ℃ in an emulsifying pot, and homogenizing for 5min to obtain a substance A;
(2) Adding hydrogenated castor oil-40 in formula amount into emulsifying pot to neutralize substance A, mixing, and homogenizing for 3min to obtain substance B;
(3) Adding triethanolamine with formula amount into an emulsifying pot, mixing with the substance B, stirring to dissolve completely, and keeping the temperature at 75 deg.C for 20min to obtain substance C;
(4) Cooling the emulsifying pot to 45 ℃, adding the skin conditioner, the phenoxyethanol and the substance C according to the formula ratio, and uniformly stirring to obtain the skin-care cream.
Comparative example 1
Compared with the example 5, the multi-effect mask composition is different only in the mass fractions of the components, and the rest conditions are the same, and specifically comprises the following steps:
carbomer 0.01%,1,3-propylene glycol 15%, phenoxyethanol 1%, other additives 15%, and the balance water, wherein the other additives are a mixture of hydrogenated castor oil-40, a skin conditioner, and triethanolamine, and the mass ratio of the three is 8;
the skin conditioner consists of the following components in parts by weight: 0.5 part of purslane extract, 1.0 part of mushroom extract, 0.08 part of lemon extract, 0.05 part of papain, 0.5 part of allantoin and 1.0 part of hydrolyzed pearl.
Comparative example 2
Compared with the example 5, the multi-effect facial mask composition is only different from the skin conditioner in components, and the rest conditions are the same, and specifically the following conditions are adopted:
the skin conditioner consists of the following components in parts by weight: 0.5 part of Yunnan camellia extract, 1.0 part of mushroom extract, 0.08 part of lemon extract, 0.05 part of papain, 0.5 part of allantoin and 1.0 part of hydrolyzed pearl.
Comparative example 3
Compared with the example 5, the multi-effect facial mask composition is different only in the mass fraction of each component in the skin conditioner, and the rest conditions are the same, and specifically comprises the following steps:
the skin conditioner consists of the following components in parts by weight: 1.5 parts of purslane extract, 1.5 parts of mushroom extract, 0.15 part of lemon extract, 0.15 part of papain, 1.0 part of allantoin and 2.5 parts of hydrolyzed pearl.
Comparative example 4
Compared with the example 5, the multi-effect mask composition is different only in the adding sequence of the raw materials in the preparation process, and the rest conditions are the same, and specifically comprises the following steps:
the preparation method of the mask composition comprises the following steps:
(1) Mixing carbomer, 1,3-propylene glycol and water according to the formula ratio, heating to 80 ℃ in an emulsifying pot, and homogenizing for 5min to obtain a substance A;
(2) Adding phenoxyethanol and triethanolamine in a formula amount into an emulsifying pot to be mixed with the substance A, stirring until the phenoxyethanol and the triethanolamine are completely dissolved, and keeping the temperature at 75 ℃ for 20min to obtain a substance B;
(3) Adding hydrogenated castor oil-40 with formula amount into an emulsifying pot, mixing with the substance B, and homogenizing for 3min to obtain a substance C;
(4) Cooling the emulsifying pot to 45 ℃, adding the skin conditioner and the substance C according to the formula amount, and uniformly stirring to obtain the skin conditioner.
Test example 1 test for patch on human body
The test method comprises the following steps: selecting 90 healthy subjects aged 20-40 years; the subjects had not used anti-inflammatory drugs or cosmetics for the last two months, and were randomly divided into 9 groups of 10 persons each, and subjected to the mask composition tests of examples 1 to 5 and comparative examples 1 to 4. The mask compositions of examples 1 to 5 and comparative examples 1 to 4 of the present invention were put into a spot tester (non-irritating tape was used for the spot tester) in an amount of 0.03g. The non-irritating adhesive tape with the facial mask composition was applied to the inner side of the forearm of the subject, one side was the control area and the other side was the test area, and was applied to the skin by gently pressing with the palm for 24 hours. After the mask composition was removed, the skin reaction was observed at 0.5, 12, 24, and 48 hours, respectively, and the results were recorded according to the skin reaction grading standards in "cosmetic sanitation Specification".
And (3) test results: the results of the human skin patch test show that all the subjects pass the patch test and observe skin reactions at 0.5, 12, 24 and 48 hours, wherein examples 1 to 5 and comparative examples 2 to 4 have no adverse reactions such as erythema, pimple and blister, and comparative example 1 has 1 case with slight erythema, which indicates that the product of the invention is safe and has no irritation.
Test example 2 moisture retention test
Selecting 90 healthy volunteers between 20-45 years old, randomly dividing into 9 groups, randomly dividing each group into 10 persons, testing the skin moisture content of the volunteers by using an SK IV digital skin moisture tester before testing, washing the backs of hands by using clean water under the environment of room temperature and humidity of 40-60%, and respectively soaking equivalent and sufficient facial mask compositions of examples 1-5 and comparative examples 1-4 for 30min3×3cm 2 Applying the non-woven cotton on the same appointed skin part, removing the non-woven cotton after 20min, testing the moisture content of the skin of a subject by using an SK IV digital skin moisture tester 0min, 30min and 60min after removing the non-woven cotton, and calculating the change amplitude of the moisture content of the skin after 0min, 30min and 60min, wherein the calculation formula is as follows: width of change in skin moisture content = [ (moisture content of skin after use-moisture content of skin before use)/moisture content of skin before use]X 100%, the test results are shown in table 1.
TABLE 1 skin moisture content variation amplitude results
Test example 3 anti-aging and whitening Effect test
105 female healthy volunteers aged 20-45 years are selected and randomly divided into 7 groups, 15 persons in each group are cleaned, and then the facial masks prepared in the examples 1,3, 5 and 1-4 are used one piece (25 mL of facial mask liquid and facial mask cloth made of the same material) after each face cleaning, and are used for 2 times every week and for the same time. After 1 month of continuous use, the anti-aging and whitening effect evaluation of the product by volunteers was collected, and the results are shown in table 2.
TABLE 2 anti-aging and whitening test results
The technical means disclosed by the scheme of the invention are not limited to the technical means disclosed by the technical means, and the technical scheme also comprises the technical scheme formed by any combination of the technical characteristics. While the foregoing is directed to embodiments of the present invention, it will be appreciated by those skilled in the art that various changes may be made in the embodiments without departing from the principles of the invention, and that such changes and modifications are intended to be included within the scope of the invention.
Claims (5)
1. The multi-effect mask composition is characterized by comprising the following raw materials in percentage by weight: 0.05-0.5% of a thickening agent, 5-20% of a humectant, 0.1-0.8% of a preservative, 2-10% of other additives and the balance of water, wherein the other additives comprise an emulsifier, a skin conditioner and a stabilizer, and the mass ratio of the emulsifier to the skin conditioner to the stabilizer is (2-10); the emulsifier is hydrogenated castor oil-40; the stabilizer is triethanolamine;
the skin conditioner comprises the following components in parts by weight: 0.1-1 part of purslane extract, 0.4-1.2 parts of mushroom extract, 0.001-0.1 part of lemon extract, 0.001-0.1 part of papain, 0.1-0.5 part of allantoin and 0.5-2 parts of hydrolyzed pearl;
the preparation method of the multi-effect mask composition comprises the following steps:
(1) Mixing the thickener, the humectant and water according to the formula ratio to obtain a substance A;
(2) Mixing the emulsifier with the substance A according to the formula ratio to obtain a substance B;
(3) Mixing the stabilizer with the substance B according to the formula amount to obtain a substance C;
(4) Mixing the skin conditioner and the preservative with the substance C according to the formula amount to obtain the skin care product.
2. The multi-effect mask composition of claim 1, wherein the thickener is at least one of carbomer, sodium carbomer, xanthan gum, hydroxyethyl cellulose, sodium alginate; the humectant is at least one of propylene glycol, glycerol, trehalose, butanediol, sorbitol, dipropylene glycol, 1,2-pentanediol and polyglycerol-10; the antiseptic is at least one of phenoxyethanol, methyl hydroxybenzoate, benzoic acid, and potassium sorbate.
3. A method of preparing a multi-effect mask composition according to any one of claims 1-2, comprising the steps of:
(1) Mixing the thickener, the humectant and water according to the formula ratio to obtain a substance A;
(2) Mixing the emulsifier with the substance A according to the formula amount to obtain a substance B;
(3) Mixing the stabilizer with the substance B according to the formula amount to obtain a substance C;
(4) Mixing the skin conditioner and the preservative with the substance C according to the formula amount to obtain the skin care product.
4. The method of claim 3, comprising the steps of:
(1) Mixing the thickener, humectant and water according to the formula ratio, heating to 75-85 deg.C, and homogenizing for 3-8min to obtain substance A;
(2) Mixing emulsifier and substance A, and homogenizing for 3-5min to obtain substance B;
(3) Mixing the stabilizer with the substance B according to the formula amount, and keeping the temperature at 75-80 ℃ for 15-25min to obtain a substance C;
(4) Cooling to 40-50 deg.C, and mixing with skin conditioner, antiseptic and substance C.
5. Use of the multi-effect mask composition according to any one of claims 1 to 2 or the multi-effect mask composition prepared by the preparation method according to any one of claims 3 to 4 in a mask.
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| CN111616856A (en) * | 2020-07-15 | 2020-09-04 | 重庆美莱整形美容医院有限公司 | Multi-effect cold compress plaster |
| CN112057352A (en) * | 2020-09-28 | 2020-12-11 | 李友贵 | Whitening, skin-tendering, moisturizing and health-preserving mask |
| CN112089678A (en) * | 2020-10-28 | 2020-12-18 | 北海市海真珠化妆品有限公司 | Preservative-free moisturizing pearl facial mask and preparation method thereof |
| CN114504544A (en) * | 2022-01-20 | 2022-05-17 | 广东柏俐臣生物科技有限公司 | Facial mask liquid containing lactobacillus soybean milk fermentation product filtrate and preparation method thereof |
| CN115475274A (en) * | 2022-10-14 | 2022-12-16 | 云飞生物药业(吉林)有限公司 | Skin repair dressing |
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