A kind of preparation method of skin-protection type makeup remover wet tissue
Technical field
The present invention relates to cosmetics of everyday use technical field, more particularly to a kind of preparation method of skin-protection type makeup remover wet tissue.
Background technology
Cleaning is the first step of skin care, therefore cleaning makeup removing tool has very important significance, and not only to remove skin table
The color make-up in face, the dirt in pore will also enable the skin to keep acid-base balance, horny layer to be softened, metabolism energy
Power is strengthened.Sense stricto makeup removing can only understand the dirt of skin surface, it is impossible to profound level cleaning, it will affect skin to shield
The absorption of skin product.Before early in the twentieth century, some will remove very heavy on the face color make-up and greasy, and what is generally used is one
A little baby oil or other oils and fatss, this makeup removing thought with oil soluble oil is quite right, can be very good to dispose color make-up, but but will
Wash the greasy of new addition and be cumbersome thing, and substantial amounts of oils and fatss can block skin pore.Until nineteen sixty, day
It is that, come removal heavy make-up, but oils and fatss do not allow easy cleaning again with oils and fatss that performer is witnessed during operation in one's original domicile make up artist Shu Uemera, from
And a kind of composition of emulsifying agent is with the addition of in makeup remover, easily can be combined with the color make-up greasy dirt on skin, then by water
The mode of emulsifying, it is during flushing that the dirt on skin is fully erased.
Makeup-removing wet tissue, facilitates handy, and the color make-up and dirt on daytime has just been taken away in gently one brush, eliminate many steps and when
Between, it is pressed for time or the limited occasion of condition, such as in travelling way, encamp, go to the places such as gymnasium to guarantee to use
Cleansing milk and clear water wash one's face, then makeup-removing wet tissue is a good succedaneum.
Makeup-removing wet tissue, produced together with liquid medicine is mixed by non-woven fabrics in full-automatic facial tissues machine, also will can be made
Makeup remover is equably sprayed on non-woven fabrics and is obtained;At present, the processing technology of makeup remover is also gradually improved, various effects, is suitable for
It is also more and more in the makeup remover of different skin;But wet tissue single function on the market, especially stability are preferable, affinity
Preferably, the makeup remover wet tissue for repairing the making of skin-protection type makeup remover does not temporarily find, needs to be increased.
The content of the invention
The present invention is in view of the shortcomings of the prior art, there is provided a kind of preparation method of skin-protection type makeup remover wet tissue, tool
Body technique scheme is as follows:
A kind of preparation method of skin-protection type makeup remover wet tissue, comprises the steps:
The preparation of step one, makeup remover
Following makeup remover raw material is weighed according to weight portion:40 ~ 45 parts of Fructus rhois chinensiss fruit oil, 10 ~ 17 parts of olive oil, lauryl alcohol polyoxy second
9 ~ 11 parts of alkene ether, 5 ~ 6 parts of Gemini surface active agent, 13 ~ 15 parts of Fructus rhois chinensiss leaf polyphenol, 5 ~ 6 parts of Radix Angelicae Sinensis extract, aloe 5 ~ 6
Part, 2 parts of glycerol, 0.5 part of sodium benzoate, 0.5 part of quintessence oil;Makeup remover raw material is mixed 20 ~ 30 minutes at 25 ~ 30 DEG C,
Then ultrasonic disperse obtains final product the makeup remover after 1 ~ 2 hour at 100Hz frequency of vibration and 35 ~ 45 DEG C;
Step 2, immersion
Non-woven fabrics are divided into into 30, every heap, are neatly arranged and about 2 ~ 3 minutes is soaked in makeup remover;
Step 3, extruding
After non-woven fabrics immersion is finished, put into extruding in extruder and obtain wet tissue in 30 ~ 40 seconds, follow after the makeup removing recovery of oil for squeezing out
Ring is utilized;
Step 4, pruning
Cut off the unnecessary burr of wet tissue;
Step 5, packaging
The wet tissue pruned is fitted in packaging bag, then packaging bag is sealed using sealing machine, the packaging bag after sealing
Cased immediately.
In makeup remover of the present invention:
Fructus rhois chinensiss fruit oil:Also known as Galla Chinensiss tree, five times of bavins etc. belong to machaka or Qiao of Anacardiaceae Rhus to Fructus rhois chinensiss
Wood.Fructus rhois chinensiss fruit oil rich in mineral substances, protein, it is necessary to fatty acid.Containing a large amount of undersaturated fat in Fructus rhois chinensiss fruit oil
Acid, adds Fructus rhois chinensiss fruit oil in makeup remover so that while makeup removing so that Fructus rhois chinensiss fruit oil can penetrate into atomic little sky
In gap so as to powerful permeability, using on human body skin, the air in pore gap can be driven out of, and be permeated
It is absorbed simultaneously in nutrient to subcutaneous tissue, dermal respiration will not be not only hindered, promote the microgranule in pore gap to discharge,
And skin health can be made, skin care to promote vis medicatrix naturae and metabolism, so as to reach the effect of maintenance skin, sensitive flesh
Skin can also be safe to use.
Olive oil is rich in vitamin, mineral, especially protein, it is necessary to fatty acid, ɑ-linolenic acid, wherein enriching not
Satisfied fatty acid and Vitamin E, can be absorbed by the skin, and moisten nutrition skin quality, glossy pool and high resilience, reduce wrinkle, slow down
Aging.
Polyoxyethylene lauryl ether, is one of kind minimum to skin irritation in surfactant, is that the present invention is adopted
Emulsifying agent, it enable to makeup remover of the present invention have it is as clear as crystal, it is not stratified, do not precipitate, from the temperature to skin
For degree, than Tween 80, polysorbas20 is more preferable.
Fructus rhois chinensiss leaf polyphenol, in being extracted from leaf of the Chinese sumac, there is the very strong harmful free radicals that eliminate, anti-aging effects,
Antibacterial, bactericidal action.Therefore after adding in this makeup remover, storage period can be extended, being capable of the various nutrition of effective protection makeup remover
Composition.
Aloe, is that one kind can bring moisturizing to skin rich in nicotinic acid, vitamin B6 etc., and moisturizing, whitening is calm, disappears
Inflammation, releives, skin lightening, the comprehensive effect such as reparation.
Glycerol, can be with the moisture in absorption air so that skin keeps moistening.
Sodium benzoate is preservative, and sodium benzoate is used cooperatively with Fructus rhois chinensiss leaf polyphenol, can significantly extend storage period, no
But the makeup remover is after storage 180 days, muddiness, flocculation will not still occur;And wet tissue of the present invention was in storage 180 days
Afterwards, remain to normally use.
Radix Angelicae Sinensis extract of the present invention is commercially available or adopts and prepare with the following method:Radix Angelicae Sinensis add water or ethanol is carried
Take, concentrate, be dried;Or further using in alcohol deposition method, water back dissolution method, organic solvent extractionprocess, flocculent precipitation, column chromatography
After one or more are used in combination and are suitably refined, crush, mixing is sieved, and is checked, and obtains final product Radix Angelicae Sinensis extract.Radix Angelicae Sinensis are carried
Take thing and include volatile oil composition and organic acid, predominantly succinic acid, Yan acid, uracil, adenine, ligustilide, vitamin
B12, Vitamin E, sitoesterol, folinic acid, butylidenephthalide, ferulic acid etc..Due to its peat-reek, therefore it is easy to distinguish
Recognize.Skin after it can remove ornaments and formal dress in makeup remover is safeguarded, with suppression melanin generation, the pigmentosa skin wrinkle of elimination
Point, removes acne and comedo.
Used as the improvement of above-mentioned technical proposal, the Gemini surface active agent is N, N '-dialkyl group (8/12/16)-N, N '-
Glucosulfone Malondiamide nonionic Gemini surface active agent.The Gemini surface active agent also may be selected glucose amide it is non-from
Sub- Gemini surface active agent.Wherein, N, N '-dialkyl group (8/12/16)-N, N '-glucosulfone Malondiamide nonionic Shuangzi table
Face activating agent, with good biological degradability, skin compatibility and splendid Environmental compatibility, also with good hard water resistance
Ability, with lower critical micelle concentration, more preferable solubilization.
Used as the improvement of above-mentioned technical proposal, the quintessence oil is the one kind in Herba Lysimachiae foenum-graeci quintessence oil, Flos Rosae Rugosae quintessence oil, osmanthus essential oil
Or it is various.
Using the present invention provide makeup remover as TRPV1 receptor antagonists, TRPV1 refer to " transient voltage sensor sun from
Subchannel, subclass V, member 1 ", the passage is a protein, by TRPV1 coded by said gene in human gene;TRPV1 is
One part gates non-selective cation channel, can be swashed by various exogen and endogenous physics and chemical stimulation
Send out, for example:Temperature more than 43 DEG C, pH value it is low(Sour environment), Endocannabinoids anandamide, N- arachidonics
Acyl group dopamine and capsaicin(The effective ingredient of Fructus Capsici);This passage is found to be present in central nervous system and tip god
In Jing systems, and it is related to the transmission and modulation of the pain sensation, and integrates various same pain informations, proves through human test, can
Effectively to block the burning sensation and the sensation of pricking that are caused by capsaicin, so as to alleviate the sense of discomfort of skin, be conducive to improving skin
Tolerance threshold values, and then improve the reparation function of skin.
Beneficial effects of the present invention:Preparation process is simple of the present invention, wet tissue good stability, excellent affinity, makeup removing effect
Good, storage period is long, is difficult to go mouldy;Makeup remover in makeup remover wet tissue of the present invention proves through human test, can be effective
Burning sensation and sensation of pricking that blocking is caused by capsaicin, so as to alleviate the sense of discomfort of skin, are conducive to improving the tolerance valve of skin
Value, and then improve the reparation function of skin;When therefore being wiped to skin or removed ornaments and formal dress using makeup remover wet tissue of the present invention,
Especially to when scribbling the skin of higher stimulus cosmetics, sensitive skin and being wiped or removed ornaments and formal dress, the makeup remover wet tissue pair
Skin zest is little, is not likely to produce sense of discomfort, and skin effect is good.
Specific embodiment
In order that the objects, technical solutions and advantages of the present invention become more apparent, with reference to embodiments, to the present invention
It is further elaborated.It should be appreciated that specific embodiment described herein is not used to only to explain the present invention
Limit the present invention.
Embodiment 1
Weigh Fructus rhois chinensiss fruit oil 42Kg, olive oil 15Kg, polyoxyethylene lauryl ether 10Kg, Gemini surface active agent 5Kg, salt skin
Wooden leaf polyphenol 15Kg, Radix Angelicae Sinensis extract 5Kg, aloe 5Kg, glycerol 2Kg, sodium benzoate 0.5Kg, quintessence oil 0.5Kg;25 ~ 30
Makeup remover raw material is mixed 20 ~ 30 minutes at DEG C, then ultrasonic disperse 1 ~ 2 is little at 100Hz frequency of vibration and 35 ~ 45 DEG C
When after obtain final product the makeup remover X;
Step 2, immersion
Non-woven fabrics are divided into into 30, every heap, are neatly arranged and about 2 ~ 3 minutes is soaked in makeup remover X;
Step 3, extruding
After non-woven fabrics immersion is finished, put into extruding in extruder and obtain wet tissue A in 30 ~ 40 seconds, after the makeup removing recovery of oil for squeezing out
Recycle;
Step 4, pruning
Cut off the unnecessary burr of wet tissue;
Step 5, packaging
The wet tissue pruned is fitted in packaging bag, then packaging bag is sealed using sealing machine, the packaging bag after sealing
Cased immediately.
Embodiment 2
Weigh Fructus rhois chinensiss fruit oil 40Kg, olive oil 17Kg, polyoxyethylene lauryl ether 9Kg, Gemini surface active agent 6Kg, salt skin
Wooden leaf polyphenol 13Kg, Radix Angelicae Sinensis extract 6Kg, aloe 6Kg, glycerol 2Kg, sodium benzoate 0.5Kg, quintessence oil 0.5Kg;25 ~ 30
Makeup remover raw material is mixed 20 ~ 30 minutes at DEG C, then ultrasonic disperse 1 ~ 2 is little at 100Hz frequency of vibration and 35 ~ 45 DEG C
When after obtain final product the makeup remover Y;
Step 2, immersion
Non-woven fabrics are divided into into 30, every heap, are neatly arranged and about 2 ~ 3 minutes is soaked in makeup remover Y;
Step 3, extruding
After non-woven fabrics immersion is finished, put into extruding in extruder and obtain wet tissue B in 30 ~ 40 seconds, after the makeup removing recovery of oil for squeezing out
Recycle;
Step 4, pruning
Cut off the unnecessary burr of wet tissue;
Step 5, packaging
The wet tissue pruned is fitted in packaging bag, then packaging bag is sealed using sealing machine, the packaging bag after sealing
Cased immediately.
Embodiment 3
Weigh Fructus rhois chinensiss fruit oil 45Kg, olive oil 10Kg, polyoxyethylene lauryl ether 11Kg, Gemini surface active agent 6Kg, salt skin
Wooden leaf polyphenol 15Kg, Radix Angelicae Sinensis extract 5Kg, aloe 5Kg, glycerol 2Kg, sodium benzoate 0.5Kg, quintessence oil 0.5Kg;25 ~ 30
Makeup remover raw material is mixed 20 ~ 30 minutes at DEG C, then ultrasonic disperse 1 ~ 2 is little at 100Hz frequency of vibration and 35 ~ 45 DEG C
When after obtain final product the makeup remover Z;
Step 2, immersion
Non-woven fabrics are divided into into 30, every heap, are neatly arranged and about 2 ~ 3 minutes is soaked in makeup remover Z;
Step 3, extruding
After non-woven fabrics immersion is finished, put into extruding in extruder and obtain wet tissue C in 30 ~ 40 seconds, after the makeup removing recovery of oil for squeezing out
Recycle;
Step 4, pruning
Cut off the unnecessary burr of wet tissue;
Step 5, packaging
The wet tissue pruned is fitted in packaging bag, then packaging bag is sealed using sealing machine, the packaging bag after sealing
Cased immediately.
Control experiment 1
Weigh Fructus rhois chinensiss fruit oil 42Kg, olive oil 30Kg, polyoxyethylene lauryl ether 10Kg, Gemini surface active agent 5Kg, Radix Angelicae Sinensis
Extract 5Kg, aloe 5Kg, glycerol 2Kg, sodium benzoate 0.5Kg, quintessence oil 0.5Kg;Makeup remover raw material is mixed at 25 ~ 30 DEG C
Stirring 20 ~ 30 minutes is closed, then ultrasonic disperse obtains final product the makeup remover after 1 ~ 2 hour at 100Hz frequency of vibration and 35 ~ 45 DEG C
M;
Step 2, immersion
Non-woven fabrics are divided into into 30, every heap, are neatly arranged and about 2 ~ 3 minutes is soaked in makeup remover M;
Step 3, extruding
After non-woven fabrics immersion is finished, put into extruding in extruder and obtain wet tissue D in 30 ~ 40 seconds.
Control experiment 2
Weigh olive oil 72Kg, polyoxyethylene lauryl ether 10Kg, Gemini surface active agent 5Kg, Radix Angelicae Sinensis extract 5Kg, Aloe
Oily 5Kg, glycerol 2Kg, sodium benzoate 0.5Kg, quintessence oil 0.5Kg;Makeup remover raw material is mixed into 20 ~ 30 points at 25 ~ 30 DEG C
Clock, then ultrasonic disperse obtains final product the makeup remover N after 1 ~ 2 hour at 100Hz frequency of vibration and 35 ~ 45 DEG C;
Step 2, immersion
Non-woven fabrics are divided into into 30, every heap, are neatly arranged and about 2 ~ 3 minutes is soaked in makeup remover N;
Step 3, extruding
After non-woven fabrics immersion is finished, put into extruding in extruder and obtain wet tissue E in 30 ~ 40 seconds.
Control experiment 3
Weigh Fructus rhois chinensiss fruit oil 57Kg, olive oil 15Kg, polyoxyethylene lauryl ether 10Kg, Gemini surface active agent 5Kg, Radix Angelicae Sinensis
Extract 5Kg, aloe 5Kg, glycerol 2Kg, sodium benzoate 0.5Kg, quintessence oil 0.5Kg;Makeup remover raw material is mixed at 25 ~ 30 DEG C
Stirring 20 ~ 30 minutes is closed, then ultrasonic disperse obtains final product the makeup remover after 1 ~ 2 hour at 100Hz frequency of vibration and 35 ~ 45 DEG C
P;
Step 2, immersion
Non-woven fabrics are divided into into 30, every heap, are neatly arranged and about 2 ~ 3 minutes is soaked in makeup remover P;
Step 3, extruding
After non-woven fabrics immersion is finished, put into extruding in extruder and obtain wet tissue F in 30 ~ 40 seconds.
The sensitive skin confirmatory experiment of protection
1), experimental principle:Sensitive skin is generally along with the overreaction of peripheral nerve, especially TRPV1 overacfivities institute
The bad sensations such as caused calcination twinge.Research shows sensitivity and readme of the TRPV1 receptors of peripheral nerve for capsaicin
Sensitive skin phenomenon there is obvious dependency;Using sample as specific TRPV1 antagonisies, and prove through human test
The burning sensation and sensation of pricking caused by capsaicin can be effectively blocked, so as to effectively alleviate the sense of discomfort of skin.To improve
The measuring accuracy of the sensitive skin confirmatory experiment of protection, is easy to experimenter significantly to distinguish each group experiment and clearly exactly in list
Impression when testing described in secondary experiment, therefore replace the makeup remover wet tissue to be protected using makeup remover of the present invention
Sensitive skin confirmatory experiment.
2), test article:It is the makeup remover Y in makeup remover X, embodiment 2, the makeup remover Z in embodiment 3 in embodiment 1, right
Makeup remover N, the makeup remover P in control experiment 3, Pure Olive Oil, quality in makeup remover M, the control experiment 2 according to the facts tested in 1 point
Number is 1 ‰ capsaicin ethanol solution, and the capsaicin ethanol solution that mass fraction is 1 ‰ is labeled as into L.
3), tested crowd:60 collegegirl volunteers.
4), method of testing:L is first applied to face 1 minute by experimenter, evaluates the sensation of pricking and burning sensation of face;Then again
Makeup remover X or makeup remover Y or makeup remover Z or makeup remover M or makeup remover N or makeup remover P or Pure Olive Oil are smeared toward face, is smeared
The sensation of pricking and burning sensation of 3 minutes inner evaluation faces after end, according to following grade scoring:0(Without sensation)、1(Slightly
Feel)、2(Acceptable sensation)、3(Keen sensation)、4(Sensation strongly), the sensitivity of capsaicin is remembered
Record, as a result as shown in Table 1 and Table 2:
Table 1 feeds back conclusive table to Fructus Capsici sensitivity testses situation
Table 2 feeds back conclusive table to Fructus Capsici sensitivity testses situation
The component table of each makeup remover of table 3(Mass fraction)
|
Fructus rhois chinensiss fruit oil |
Olive oil |
Polyoxyethylene lauryl ether |
Gemini surface active agent |
Fructus rhois chinensiss leaf polyphenol |
Radix Angelicae Sinensis extract |
Aloe |
Glycerol |
Sodium benzoate |
Quintessence oil |
X |
42% |
15% |
10% |
5% |
15% |
5% |
5% |
2% |
0.5% |
0.5% |
Y |
40% |
17% |
9% |
6% |
13% |
6% |
6% |
2% |
0.5% |
0.5% |
Z |
45% |
10% |
11% |
6% |
15% |
5% |
5% |
2% |
0.5% |
0.5% |
M |
42% |
30% |
10% |
5% |
0% |
5% |
5% |
2% |
0.5% |
0.5% |
N |
0% |
72% |
10% |
5% |
0% |
5% |
5% |
2% |
0.5% |
0.5% |
P |
57% |
15% |
10% |
5% |
0% |
5% |
5% |
2% |
0.5% |
0.5% |
As can be found from Table 1, in the embodiment of the present invention makeup remover X, makeup remover Y, makeup remover Z can significantly reduce capsaicin
Burning sensation, sensation of pricking, prurituss and the fiber crops for bringing.Skin is improved effect between makeup remover X, makeup remover Y, makeup remover Z three
It is more or less the same.With reference to Tables 1 and 2 analysis, the effect is significant that makeup remover X improves to skin is better than makeup remover M, makeup remover N and unloads
Adornment oil P, analyzes in conjunction with table 3:In makeup remover X, Fructus rhois chinensiss fruit oil or Fructus rhois chinensiss leaf polyphenol are respectively provided with suppression capsaicin and bring
The effect of the uncomfortable reaction of skin, also, Fructus rhois chinensiss fruit oil and Fructus rhois chinensiss leaf polyphenol coordinated can significantly inhibit capsaicin and bring
The uncomfortable reaction of skin.Therefore, makeup remover X, makeup remover Y, the makeup remover Z that the present invention is provided, can with sensitive skin of releiving
Effectively suppress capsaicin to bring the uncomfortable reaction of skin, the tolerance threshold values of skin is favorably improved to the adjustment effect of skin.
That is, when wet tissue A, wet tissue B, wet tissue C are wiped to skin or removed ornaments and formal dress, especially to scribbling higher stimulus cosmetics
Skin, sensitive skin when being wiped or being removed ornaments and formal dress, wet tissue A, wet tissue B, wet tissue C are little to skin zest, are not likely to produce discomfort
Sense, skin effect is good.
Stability test
10g makeup remover X, 10g makeup remover Y, 10g makeup remover Z, 3 wet tissue A, 3 wet tissue B, 3 wet tissue C are taken, room is each placed in
In warm couveuse, in 50 DEG C of couveuses and in -10 ~ 40 DEG C of temperature cycling case, the sight of 6 months is then carried out to its stability
Examine.Observation result is shown in following table.
The stability test situation of table 4
Moisture retention is tested
50 cosmetic women of 20 ~ 35 years old are chosen, is divided into 5 groups, per group of 10 people, using wet tissue A, wet tissue B, wet tissue C, wet tissue D, wet
Towel E, wet tissue F are removed ornaments and formal dress, and other skin care item are not smeared after makeup removing.It is tested each to be tested using moisture of skin tester mushu
The skin moisture content of person.Before makeup removing, using moisture of skin tester in steady temperature(24℃)And constant humidity(45%)Bar
The skin moisture content of each experimenter is determined under part, and as reference value, 0 hour, 2 hours, 4 hours and 8 hours after makeup removing
With the change of the skin moisture content of 12 hours.Measurement result is shown in table 5 below.
The subjects skin's moisture retention test case of table 5
By the result of table 5 can be seen that using the ratio of skin moisture content at once after wet tissue A, wet tissue B, wet tissue C use wet tissue D,
Skin moisture content at once after wet tissue E, wet tissue F is more, and skin moisturization continues 12 hours or the longer time, also
It can be seen that the raising of rhus glabra oil content can effectively improve the performance of keeping humidity of makeup remover wet tissue of the present invention.
In the above-described embodiments, Radix Angelicae Sinensis extract, sodium benzoate are enabled in rhus glabra using ultrasonic disperse technology
Oil, olive oil, polyoxyethylene lauryl ether, Gemini surface active agent, Fructus rhois chinensiss leaf polyphenol, aloe, glycerol, the mixing of quintessence oil
It is uniformly dispersed in thing.
Presently preferred embodiments of the present invention is the foregoing is only, not to limit the present invention, all essences in the present invention
Any modification, equivalent and improvement made within god and principle etc., should be included within the scope of the present invention.