CN102199491B - 一种医用杉木油提取的方法 - Google Patents
一种医用杉木油提取的方法 Download PDFInfo
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- CN102199491B CN102199491B CN201110096617A CN201110096617A CN102199491B CN 102199491 B CN102199491 B CN 102199491B CN 201110096617 A CN201110096617 A CN 201110096617A CN 201110096617 A CN201110096617 A CN 201110096617A CN 102199491 B CN102199491 B CN 102199491B
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- china fir
- alcohol
- polar solvent
- methyl alcohol
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- 238000000605 extraction Methods 0.000 title claims abstract description 22
- 239000010627 cedar oil Substances 0.000 title abstract description 7
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims abstract description 132
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 59
- 239000000463 material Substances 0.000 claims abstract description 53
- 239000012046 mixed solvent Substances 0.000 claims abstract description 37
- 239000012454 non-polar solvent Substances 0.000 claims abstract description 22
- 239000002798 polar solvent Substances 0.000 claims abstract description 22
- 238000000034 method Methods 0.000 claims abstract description 11
- 238000001704 evaporation Methods 0.000 claims abstract description 8
- 244000050510 Cunninghamia lanceolata Species 0.000 claims description 72
- UHOVQNZJYSORNB-UHFFFAOYSA-N monobenzene Natural products C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims description 56
- 238000002203 pretreatment Methods 0.000 claims description 28
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 claims description 21
- 239000002023 wood Substances 0.000 claims description 10
- 239000000284 extract Substances 0.000 claims description 8
- 230000008020 evaporation Effects 0.000 claims description 7
- 238000009472 formulation Methods 0.000 claims description 7
- 238000003754 machining Methods 0.000 claims description 7
- 239000000203 mixture Substances 0.000 claims description 7
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims description 7
- 239000000843 powder Substances 0.000 claims description 3
- -1 sawdust Substances 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- SVURIXNDRWRAFU-OGMFBOKVSA-N cedrol Chemical compound C1[C@]23[C@H](C)CC[C@H]3C(C)(C)[C@@H]1[C@@](O)(C)CC2 SVURIXNDRWRAFU-OGMFBOKVSA-N 0.000 abstract 1
- 229940026455 cedrol Drugs 0.000 abstract 1
- PCROEXHGMUJCDB-UHFFFAOYSA-N cedrol Natural products CC1CCC2C(C)(C)C3CC(C)(O)CC12C3 PCROEXHGMUJCDB-UHFFFAOYSA-N 0.000 abstract 1
- SVURIXNDRWRAFU-UHFFFAOYSA-N juniperanol Natural products C1C23C(C)CCC3C(C)(C)C1C(O)(C)CC2 SVURIXNDRWRAFU-UHFFFAOYSA-N 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 abstract 1
- 238000005516 engineering process Methods 0.000 description 5
- 239000002994 raw material Substances 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 239000004593 Epoxy Substances 0.000 description 1
- 241001098499 Lanceolata Species 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- JJTQQGNEXQKQRF-BIGJJFBESA-N cedrane Chemical compound C1[C@]23[C@H](C)CC[C@H]3C(C)(C)[C@@H]1[C@H](C)CC2 JJTQQGNEXQKQRF-BIGJJFBESA-N 0.000 description 1
- 229930002312 cedrane Natural products 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000012797 qualification Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 230000009897 systematic effect Effects 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 239000002916 wood waste Substances 0.000 description 1
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- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Fats And Perfumes (AREA)
Abstract
Description
Claims (1)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201110096617A CN102199491B (zh) | 2011-04-18 | 2011-04-18 | 一种医用杉木油提取的方法 |
Applications Claiming Priority (1)
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CN201110096617A CN102199491B (zh) | 2011-04-18 | 2011-04-18 | 一种医用杉木油提取的方法 |
Publications (2)
Publication Number | Publication Date |
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CN102199491A CN102199491A (zh) | 2011-09-28 |
CN102199491B true CN102199491B (zh) | 2012-10-03 |
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CN201110096617A Expired - Fee Related CN102199491B (zh) | 2011-04-18 | 2011-04-18 | 一种医用杉木油提取的方法 |
Country Status (1)
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CN (1) | CN102199491B (zh) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111849643A (zh) * | 2020-07-28 | 2020-10-30 | 福建省建瓯市金路实业有限公司 | 杉木油的蒸馏提取方法 |
CN111849644A (zh) * | 2020-07-28 | 2020-10-30 | 福建省建瓯市金路实业有限公司 | 杉木油的制备方法及设备 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
RU2137821C1 (ru) * | 1998-07-20 | 1999-09-20 | Институт химии и химической технологии СО РАН | Способ переработки пихтовой коры |
CN101024754A (zh) * | 2006-02-22 | 2007-08-29 | 粟国江 | 天然树脂提取工艺及装置 |
CN101885977A (zh) * | 2010-07-06 | 2010-11-17 | 贵州省锦屏县华绿炭素有限公司 | 一种杉木屑提取杉木油联产活性炭的方法 |
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2011
- 2011-04-18 CN CN201110096617A patent/CN102199491B/zh not_active Expired - Fee Related
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
RU2137821C1 (ru) * | 1998-07-20 | 1999-09-20 | Институт химии и химической технологии СО РАН | Способ переработки пихтовой коры |
CN101024754A (zh) * | 2006-02-22 | 2007-08-29 | 粟国江 | 天然树脂提取工艺及装置 |
CN101885977A (zh) * | 2010-07-06 | 2010-11-17 | 贵州省锦屏县华绿炭素有限公司 | 一种杉木屑提取杉木油联产活性炭的方法 |
Non-Patent Citations (1)
Title |
---|
刘娟.杉木化学成分及药理作用研究进展.《辽宁中医药大学学报》.2010,第12卷(第9期),8-9. * |
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CN102199491A (zh) | 2011-09-28 |
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Owner name: HEYI BIOLOGICAL SCIENCE AND TECHNOLOGY CO., LTD., Free format text: FORMER OWNER: CENTRAL SOUTH UNIVERSITY OF FORESTRY AND TECHNOLOGY Effective date: 20120907 |
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Inventor after: Ma Qingzhi Inventor after: OuYang Hui Inventor after: Hu Jiagang Inventor before: Ma Qingzhi |
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Free format text: CORRECT: INVENTOR; FROM: MA QINGZHI TO: MA QINGZHI OU YANGHUI HU JIAGANG Free format text: CORRECT: ADDRESS; FROM: 410004 CHANGSHA, HUNAN PROVINCE TO: 416000 XIANGXI TUJIA AND MIAO AUTONOMOUS PREFECTURE, HUNAN PROVINCE |
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Effective date of registration: 20120907 Address after: 416000 No. 69 Renmin South Road, Hunan, Jishou Patentee after: Heyi Biological Science and Technology Co.,Ltd. Xiangxi Autonomous Prefecture Address before: 410004 Shaoshan South Road, Hunan, No. 498, No. Patentee before: Central South University of Forestry and Technology |
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