CN101874591A - Fluffy granular composite low-sugar and low-calorie sweetener and preparation method thereof - Google Patents
Fluffy granular composite low-sugar and low-calorie sweetener and preparation method thereof Download PDFInfo
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- CN101874591A CN101874591A CN2009102345960A CN200910234596A CN101874591A CN 101874591 A CN101874591 A CN 101874591A CN 2009102345960 A CN2009102345960 A CN 2009102345960A CN 200910234596 A CN200910234596 A CN 200910234596A CN 101874591 A CN101874591 A CN 101874591A
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Abstract
The invention relates to a fluffy granular composite low-sugar and low-calorie sweetener and a preparation method. The sweetener comprises the following components: 40-50% of dextrose monohydrate, 20-40% of sorbitol, 2-4% of maltodextrin and 8-35% of sucralose. The process comprises the following steps: respectively adding the maltodextrin and the sucralose to a heating container and respectively adding deionized water for mixing; raising the temperature until dissolution; adding activated carbon to the solution respectively, filtering the mixture while the mixture is hot and collecting the filtrates respectively in storage tanks; and pumping the ground mixture of the dextrose monohydrate and the sorbitol into a fluidized bed with spraying from the bottom of the bed under positive pressure and ensuring the mixture to flow at high speed from bottom to top, applying negative pressure to the upper part of the fluidized bed with spraying so that the bed vibrates from top to bottom to ensure the materials to boil in the bed; using a multipoint spray gun at the side of the fluidized bed to continuously spray and disperse the refined sucralose solution on superfine sugar alcohols, then pumping the maltodextrin solution and carrying out continuous spray drying, thus obtaining the low-sugar and low-calorie sweetener. The preparation flow is simple and convenient and easy to operate and the sweetness of the product is 50-200 times that of the common sucrose.
Description
Technical field
The present invention relates to a kind of edible sweetener, relate in particular to a kind of fluffy granular composite low-sugar and low-calorie sweetener and preparation method thereof.
Background technology
Along with the increase of people because of too much bringing disease, people's demand safety, healthy low-sugar-content and low-calorie type sweetener with sugar; In production procedure, reach from raw material and put into the advanced preparation technology that finished product one step finishes; It is learnt from other's strong points to offset one's weaknesses, has complementary advantages to make between the sugar alcohol sweet taste on the formula for a product, can play during product uses and cover the effect that promotes mouthfeel with synergy, people thirst for satisfying under the low prerequisite of sugariness height, heat, and occupation modeization, with cane-sugar taste safety and Health low-sugar-content and low-calorie type sweetener roughly the same.
Summary of the invention
The objective of the invention is to overcome the deficiency that prior art exists, a kind of fluffy granular composite low-sugar and low-calorie sweetener and preparation method thereof is provided, adopt the scientific technology of easy operation control, the molten speed of product, mouthfeel, sugariness all are higher than the prior art optimum value.
Purpose of the present invention is achieved through the following technical solutions:
Fluffy granular composite low-sugar and low-calorie sweetener, characteristics are to comprise following composition (percentage by weight): Dextrose Monohydrate 40～50%, D-sorbite 20～40%, maltodextrin 2～4%, Sucralose 8～35%.
Further, above-mentioned fluffy granular composite low-sugar and low-calorie sweetener, wherein, Dextrose Monohydrate 40%, D-sorbite 22%, maltodextrin 3.2%, Sucralose 34.8%.
Further, above-mentioned fluffy granular composite low-sugar and low-calorie sweetener, described maltodextrin DE value is 10～20.
The preparation method of fluffy granular composite low-sugar and low-calorie sweetener of the present invention comprises following processing step:
1. maltodextrin, Sucralose are joined respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 52～80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned maltodextrin solution and the sucralose solution, be incubated 25～30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank of heat tracing;
4. will put in the spray-fluidized bed apparatus after Dextrose Monohydrate and the D-sorbite pulverizing, the mixed material of Dextrose Monohydrate and D-sorbite enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, pump into the above-mentioned maltodextrin solution that refines again, spray-drying obtains fluffy granular composite low-sugar and low-calorie sweetener continuously.
Again further, the preparation method of above-mentioned fluffy granular composite low-sugar and low-calorie sweetener joins maltodextrin, Sucralose respectively in the heating container, adds deionized water respectively and mixes; Be warming up to 60～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank that has heat tracing; Dextrose Monohydrate and D-sorbite reach 120～180 orders through pulverizing, be sent in the spray-fluidized bed apparatus, the mixed material of Dextrose Monohydrate and D-sorbite enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, control fluidized-bed layer temperature is at 35～80 ℃, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, after the mixing of sugar alcohol fluidisation loses surperficial moisture content, pump into the above-mentioned maltodextrin solution that refines again, spray drying granulation obtains fluffy granular composite low-sugar and low-calorie sweetener continuously.
Again further, the preparation method of above-mentioned fluffy granular composite low-sugar and low-calorie sweetener, the bed temperature scope of described fluidized bed with spraying is 35～80 ℃, wherein the bed temperature of phase I Sucralose spraying dispersion is 35～50 ℃, and the bed temperature of second stage maltodextrin mist projection granulating is 50～80 ℃.
Again further, the preparation method of above-mentioned fluffy granular composite low-sugar and low-calorie sweetener, in the phase I of described spraying mixed fluidized bed, the Sucralose spraying is dispersed in fluidisation and smashes on the fine sugar alcohol crystal body; In second stage, the maltodextrin spray drying granulation is on the noncrystal of mixing sugar alcohol.
Substantive distinguishing features and obvious improvement that technical solution of the present invention is outstanding are mainly reflected in:
The negative pressure fluid bed fluidization technique that adopts scientific formula, uses advanced is in conjunction with the multi-point atomizing method, and time sharing segment control appliance bed temperature efficiently solves even dispersion, coats problems such as granulation, drying.With Dextrose Monohydrate, D-sorbite, Sucralose is primary raw material; modify uniformly and coat by preparation method to sugariness; make product sweetness reach 50～200 times of common sucrose; products obtained therefrom does not have smell, does not have color; soluble in water; this fluffy granular composite low-sugar and low-calorie sweetener is easy to use, and its preparation process science is simple and easy to operate, is fit to very much large-scale production.
Description of drawings
Below in conjunction with accompanying drawing technical solution of the present invention is described further:
Fig. 1: process chart of the present invention.
The specific embodiment
Fluffy granular composite low-sugar and low-calorie sweetener of the present invention, its composition is: Dextrose Monohydrate 40～50%, D-sorbite 20～40%, maltodextrin 2～4%, Sucralose 8～35%.Ideal formulations is: Dextrose Monohydrate 40%, D-sorbite 22%, maltodextrin 3.2%, Sucralose 34.8%.
As shown in Figure 1, the preparation technology of fluffy granular composite low-sugar and low-calorie sweetener: at first, maltodextrin, Sucralose are joined respectively in the heating container, add deionized water respectively and mix; Be warming up to 52～80 ℃ of dissolvings respectively, and stir; Add active carbon in above-mentioned maltodextrin solution and the sucralose solution respectively, be incubated 25～30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank of heat tracing; At last, put into after Dextrose Monohydrate and D-sorbite pulverized in the spray-fluidized bed apparatus (heating temperature control and by the positive negative pressure boiling of equipment technology with the boiling that in fluid bed, circulates of sugar alcohol material, mix that fluidisation is anhydrated and fluffy processing, sugar alcohol mixtures material → malleation material quickens to flow from bottom to top → and negative pressure vibrates → makes material boiling up and down in fluid bed → by the fluid bed side multiple spot spray gun liquid material ejection fog-like liquid of naming a person for a particular job from top to bottom, be sprayed onto on the trickle solid material body of boiling), the mixed material of Dextrose Monohydrate and D-sorbite enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, the bed temperature that the spraying of control Sucralose disperses is 35～50 ℃, and the Sucralose even spraying is dispersed on the mixing sugar alcohol crystalline solid of powder; The rising bed temperature, at mixing sugar alcohol after fluidisation loses surface crystallization water, pump into the above-mentioned maltodextrin solution that refines again, continuous spray drying granulation, the bed temperature of maltodextrin mist projection granulating controlled well is 50～80 ℃, and the maltodextrin spray drying granulation is on the noncrystalline fluffy body of sugar alcohol; Obtain fluffy the shape product that even sugariness is modified.
Embodiment 1:
2.3 kilograms of maltodextrins and deionized water are dissolved in a stainless steel heating reaction pot for 20 kilograms, 8.7 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel heating reaction pot for 27 kilograms, material is heated to 62 ℃ by chuck in the pot, start stirring, add 1 kilogram of active carbon respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; 50 kilograms of Dextrose Monohydrates, 39 kilograms of D-sorbites, pulverizing reaches 130 orders through pulverizer, be sent in the spray-fluidized bed apparatus, the mixed material of Dextrose Monohydrate and D-sorbite enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, control fluidized-bed layer temperature is 35～50 ℃, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, at Dextrose Monohydrate, after the mixing of D-sorbite alcohol fluidisation loses surface crystallization water, pump into the above-mentioned maltodextrin solution that refines, continuous spray drying granulation is controlled air quantity and mist flow well, obtains the fluffy granular product that even sugariness is modified.
Embodiment 2:
2.5 kilograms of maltodextrins and deionized water are dissolved in a stainless steel heating reaction pot for 25 kilograms, 17.5 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel reaction pot for 25 kilograms, material is heated to 52 ℃ by chuck in the pot, start stirring, add 2 kilograms of active carbons respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; 45 kilograms of Dextrose Monohydrates, 35 kilograms of D-sorbites, reach 150 orders through pulverizing, be sent to and carry out the fluidisation mixing in the spray-fluidized bed apparatus, the mixed material of Dextrose Monohydrate and D-sorbite enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, 35～40 ℃ of control fluidized-bed layer temperature, even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, make Dextrose Monohydrate, after the mixing of D-sorbite alcohol fluidisation loses surface crystallization water, pumping into the above-mentioned maltodextrin solution that refines, continuous spray granulating and drying is controlled air quantity and mist flow well, obtains the fluffy granular product that even sugariness is modified.
Embodiment 3:
2.8 kilograms of maltodextrins and deionized water are dissolved in a stainless steel heating reaction pot for 30 kilograms, 26.2 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel heating reaction pot for 30 kilograms, material is heated to 60 ℃ by chuck in the pot, start stirring, add 3.0 kilograms of active carbons respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; 46 kilograms of Dextrose Monohydrates, 25 kilograms of D-sorbites, pulverizing reaches 160 orders through pulverizer, be sent in the spray-fluidized bed apparatus, the mixed material of Dextrose Monohydrate and D-sorbite enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, control 35～42 ℃ of fluidized-bed layer temperature well, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, at Dextrose Monohydrate, after the mixing of D-sorbite alcohol fluidisation loses surface crystallization water, pump into the above-mentioned maltodextrin solution that refines, continuous spray drying granulation is controlled air quantity and mist flow well, obtains the fluffy granular product that even sugariness is modified.
Embodiment 4:
3.2 kilograms of maltodextrins and deionized water are dissolved in a stainless steel heating reaction pot for 30 kilograms, 50 kilograms also another dissolves in stainless steel heating reaction pot with 34.8 kilograms of Sucraloses and deionized water, material is heated to 80 ℃ by chuck in the pot, start stirring, add 3.0 kilograms of active carbons respectively, be incubated 35 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; 40 kilograms of Dextrose Monohydrates, 22 kilograms of D-sorbites, pulverizing reaches 180 orders through pulverizer, be sent to fluidisation in the spray-fluidized bed apparatus, the mixed material of Dextrose Monohydrate and D-sorbite enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, control 35～50 ℃ of fluidized-bed layer temperature well, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, at Dextrose Monohydrate, after D-sorbite alcohol fluidisation loses surface crystallization water, pumping into the above-mentioned maltodextrin solution that refines, air quantity and mist flow are controlled in continuously spraying combination drying granulation well, obtain the fluffy granular product that even sugariness is adornd.
After testing, the fluffy granular composite low-sugar and low-calorie sweetener that adopts technical solution of the present invention to obtain, its main performance index sees Table 1.
Table 1
| Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 |
| Particle size | 30～60 orders | 30～60 orders | 30～60 orders | 30～60 orders |
| Sugariness (sucrose contrast) | 50 times | 100 times | 150 times | 200 times |
| Outward appearance | White particle | White particle | White particle | White particle |
| Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 |
| Bulk density (g/mm 3) | ??0.60 | ??0.62 | ??0.63 | ??0.66 |
The stability test of sweetener is to check sweetener to guarantee the ability that undergoes no deterioration within a certain period of time, and the sweetener product of the embodiment of the invention was stored 3 years at normal temperatures, phenomenons such as rotten and sugariness reduction occur, and stability is very superior.
The sugariness degree of modification of fluffy granular composite low-sugar and low-calorie sweetener of the present invention, will be according to the adjustment of Sucralose in consumption, usually select the common sucrose sugariness for use 50～200 times, the use needs that relatively are fit to food enterprise, form according to prescription, under same sugariness situation, people only are 1/50～1/200 of common sucrose to the absorption of heat, low-sugar-content and low-calorie sweetening agent is the sweet taste product of low-calorie, this sweetener can not cause blood sugar to raise, and satisfies three high crowds, the healthy people's of pursuit needs.
Show obviously that to sum up the present invention adopts scientific formula, uses advanced science and technology technology and method, products obtained therefrom does not have smell, do not have color, and is soluble in water, and it is very convenient that this fluffy granular low-sugar-content and low-calorie sweetening agent is used.Granularity, molten speed, mouthfeel, sugariness all are much better than the prior art value, and the scientific preparation process simple flow is easily gone, and are fit to very much large-scale production, are worth wide popularization and application in the field of business.
What need understand is: the above only is a preferred implementation of the present invention; for those skilled in the art; under the prerequisite that does not break away from the principle of the invention, can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (6)
1. fluffy granular composite low-sugar and low-calorie sweetener is characterized in that comprising following composition (percentage by weight): Dextrose Monohydrate 40～50%, D-sorbite 20～40%, maltodextrin 2～4%, Sucralose 8～35%.
2. fluffy granular composite low-sugar and low-calorie sweetener according to claim 1 is characterized in that its component has following percentage by weight: Dextrose Monohydrate 40%, D-sorbite 22%, maltodextrin 3.2%, Sucralose 34.8%.
3. fluffy granular composite low-sugar and low-calorie sweetener according to claim 1 and 2 is characterized in that: described maltodextrin DE value is 10～20.
4. the preparation method of the described fluffy granular composite low-sugar and low-calorie sweetener of claim 1 is characterized in that: comprise following processing step---
1. maltodextrin, Sucralose are joined respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 52～80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned maltodextrin solution and the sucralose solution, be incubated 25～30 minutes, filter while hot, filtrate is pooled in the storage tank of heat tracing stand-by respectively;
4. will put in the spray-fluidized bed apparatus after Dextrose Monohydrate and the D-sorbite pulverizing, the mixed material of Dextrose Monohydrate and D-sorbite enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, pump into the above-mentioned maltodextrin solution that refines again, spray-drying obtains fluffy granular composite low-sugar and low-calorie sweetener continuously.
5. the preparation method of fluffy granular composite low-sugar and low-calorie sweetener according to claim 4 is characterized in that: maltodextrin, Sucralose are joined respectively in the container, add deionized water respectively and mix; Be warming up to 60～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank that has heat tracing; Dextrose Monohydrate and D-sorbite reach 120～180 orders through pulverizing, be sent in the spray-fluidized bed apparatus, the mixed material of Dextrose Monohydrate and D-sorbite enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, control fluidized-bed layer temperature is at 35～80 ℃, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, after the mixing of sugar alcohol fluidisation loses surperficial moisture content, pump into the above-mentioned maltodextrin solution that refines again, spray drying granulation obtains fluffy granular composite low-sugar and low-calorie sweetener continuously.
6. the preparation method of fluffy granular composite low-sugar and low-calorie sweetener according to claim 5, it is characterized in that: the bed temperature scope of described fluidized bed with spraying is 35～80 ℃, wherein the bed temperature of phase I Sucralose spraying dispersion is 35～50 ℃, and the bed temperature of second stage maltodextrin mist projection granulating is 50～80 ℃.
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| CN102415547A (en) * | 2011-12-09 | 2012-04-18 | 苏州工业园区尚融科技有限公司 | Compound sweetener and preparation method thereof |
| CN102511768A (en) * | 2011-12-09 | 2012-06-27 | 苏州工业园区尚融科技有限公司 | Bulky powdery composite low-sugar and low-calorie sweetener and preparation method thereof |
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| CN102440349A (en) * | 2011-12-20 | 2012-05-09 | 苏州工业园区尚融科技有限公司 | Low-sugar table sugar and preparation method thereof |
| CN103070334A (en) * | 2013-03-13 | 2013-05-01 | 苏州工业园区尚融科技有限公司 | Low-calorie table sugar preparation method |
| CN104161214A (en) * | 2013-10-31 | 2014-11-26 | 上海新农饲料股份有限公司 | Piglet granular feed capable of high-temperature resistant storage and transportation and preparation method thereof |
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Application publication date: 20101103 |