CN101874594B - Fluffy granular composite sugar-free sweetener and preparation method thereof - Google Patents
Fluffy granular composite sugar-free sweetener and preparation method thereof Download PDFInfo
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- CN101874594B CN101874594B CN2009102345994A CN200910234599A CN101874594B CN 101874594 B CN101874594 B CN 101874594B CN 2009102345994 A CN2009102345994 A CN 2009102345994A CN 200910234599 A CN200910234599 A CN 200910234599A CN 101874594 B CN101874594 B CN 101874594B
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Abstract
The invention relates to a fluffy granular composite sugar-free sweetener and a preparation method. The sweetener comprises the following components: 40-60% of xylitol, 20-28% of isomaltooligosaccharide, 3-5% of maltodextrin and 8-35.5% of sucralose. The process comprises the following steps: respectively adding the maltodextrin and the sucralose to a heating container and respectively adding deionized water for mixing; raising the temperature until dissolution; adding activated carbon to the solution respectively, filtering the mixture while the mixture is hot and collecting the filtrates respectively in storage tanks; and pumping the ground mixture of the xylitol and the isomaltooligosaccharide into a fluidized bed with spraying from the bottom of the bed under positive pressure and ensuring the mixture to flow at high speed from bottom to top, applying negative pressure to the upper part of the fluidized bed with spraying so that the bed vibrates from top to bottom to ensure the materials to boil in the bed; using a multipoint spray gun at the side of the fluidized bed to continuously spray and disperse the refined sucralose solution on superfine sugar alcohols, then pumping the maltodextrin solution and carrying out continuous spray drying, thus obtaining the fluffy granular composite sugar-free sweetener. The preparation flow is simple and convenient and easy to operate and is suitable for scale production.
Description
Technical field
The present invention relates to a kind of edible sweetener, relate in particular to a kind of fluffy granular composite sugar-free sweetener and preparation method thereof.
Background technology
The increase of Along with people's because of too much bringing disease with sugar, people's demand safety, healthy Sugarless type non-nutritive sweetener of not participating in body metabolism; In production procedure, reach the advanced preparation technology who puts into finished product one step completion from raw material; It is learnt from other's strong points to offset one's weaknesses, has complementary advantages to make between the sugar alcohol sweet taste on the formula for a product; Can play during product uses and cover the effect that promotes mouthfeel with synergy; People thirst for satisfying under the low prerequisite of sugariness height, heat, and occupation modeization, with cane-sugar taste safety and Health Sugarless type sweetener roughly the same.
Summary of the invention
The objective of the invention is to overcome the deficiency that prior art exists, a kind of fluffy granular composite sugar-free sweetener and preparation method thereof is provided, adopt the scientific technology of easy operation control, the molten speed property of product, mouthfeel, sugariness all are higher than the prior art optimum value.
The object of the invention is realized through following technical scheme:
Fluffy granular composite sugar-free sweetener, characteristics are to comprise following composition (percentage by weight): xylitol 40～60%, oligoisomaltose 20～28%, maltodextrin 3～5%, Sucralose 8～35.5%.
Further, above-mentioned fluffy granular composite sugar-free sweetener, wherein, xylitol 41%, oligoisomaltose 20%, maltodextrin 4%, Sucralose 35%.
Further, above-mentioned fluffy granular composite sugar-free sweetener, said maltodextrin DE value is 10～20.
The preparation method of fluffy granular composite sugar-free sweetener of the present invention comprises following processing step:
1. maltodextrin, Sucralose are joined respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 52～78 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned maltodextrin solution and the sucralose solution, be incubated 25～30 minutes, filter while hot, for use in the storage tank that is pooled to heat tracing respectively of filtrating;
4. with putting in the spray-fluidized bed apparatus after xylitol and the oligoisomaltose pulverizing; The mixed material of xylitol and oligoisomaltose also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body; Pump into the above-mentioned maltodextrin solution that refines again, spray-drying obtains fluffy granular composite sugar-free sweetener continuously.
Again further, the preparation method of above-mentioned fluffy granular composite sugar-free sweetener joins maltodextrin, Sucralose respectively in the container, adds deionized water respectively and mixes; Be warming up to 60～70 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrating is pooled to respectively in the storage tank that has heat tracing; Xylitol and oligoisomaltose reach 120～180 orders through pulverizing; Be sent in the spray-fluidized bed apparatus; The mixed material of xylitol and oligoisomaltose also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and control fluidized-bed layer temperature is at 35～80 ℃, and the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned sucralose solution that refines be sprayed continuously and is distributed on the fine sugar alcohol body; After the mixing of sugar alcohol fluidisation loses surperficial moisture content; Pump into the above-mentioned maltodextrin solution that refines again, spray drying granulation obtains fluffy granular composite sugar-free sweetener continuously.
Again further; The preparation method of above-mentioned fluffy granular composite sugar-free sweetener; The bed temperature scope of said fluidized bed with spraying is 35～80 ℃; Wherein the bed temperature of phase I Sucralose spraying dispersion is 35～50 ℃, and the bed temperature of second stage maltodextrin mist projection granulating is 50～80 ℃.
Again further, the preparation method of above-mentioned fluffy granular composite sugar-free sweetener, in the phase I of said Spray Mixing fluid bed, the Sucralose spraying is dispersed in fluidisation and smashes on the fine sugar alcohol crystal body; In second stage, the maltodextrin spray drying granulation is on the noncrystal of mixing sugar alcohol.
Substantive distinguishing features and obvious improvement that technical scheme of the present invention is outstanding are mainly reflected in:
The present invention adopts the negative pressure fluid bed fluidization technique of scientific formula, uses advanced to combine the multi-point atomizing method, and time sharing segment control appliance bed temperature efficiently solves even dispersion, coats problems such as granulation, drying.With xylitol, oligoisomaltose, Sucralose is primary raw material; Modify uniformly and coat through preparation method to sugariness, make product sweetness reach 50～200 times of common sucrose, products obtained therefrom does not have smell, does not have color; Soluble in water; This fluffy granular composite sugar-free sweetener is easy to use, and its preparation process science is simple and easy to operate, is fit to very much large-scale production.
Description of drawings
Below in conjunction with accompanying drawing technical scheme of the present invention is described further:
Fig. 1: process chart of the present invention.
The specific embodiment
Fluffy granular composite sugar-free sweetener of the present invention, its composition is: xylitol 40～60%, oligoisomaltose 20～28%, maltodextrin 3～5%, Sucralose 8～35.5%.Ideal formulations is: xylitol 41%, oligoisomaltose 20%, maltodextrin 4%, Sucralose 35%.Wherein, maltodextrin DE value is 10～20.
As shown in Figure 1, the preparation technology of fluffy granular composite sugar-free sweetener: at first, maltodextrin, Sucralose are joined respectively in the heating container, add deionized water respectively and mix; Be warming up to 52～78 ℃ of dissolvings respectively, and stir; Add active carbon in above-mentioned maltodextrin solution and the sucralose solution respectively, be incubated 25～30 minutes, filter while hot, filtrating is pooled to respectively in the storage tank of heat tracing; At last; Put into after xylitol and oligoisomaltose pulverized in the spray-fluidized bed apparatus (at heating temperature control and technological with the boiling that in fluid bed, circulates of sugar alcohol material through the positive negative pressure boiling of equipment; Mix that fluidisation is anhydrated and fluffy processing; Sugar alcohol mixtures material → malleation material quickens to flow from bottom to top → and negative pressure vibrates → makes material boiling up and down in fluid bed → by the fluid bed side multiple spot spray gun liquid material ejection fog-like liquid of naming a person for a particular job from top to bottom; Be sprayed onto on the trickle solid material body of boiling); The mixed material of xylitol and oligoisomaltose also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, and the bed temperature that the spraying of control Sucralose disperses is 35～50 ℃, and the Sucralose even spraying is dispersed on the mixing sugar alcohol crystalline solid of powder; The rising bed temperature; At mixing sugar alcohol after fluidisation loses surface crystallization water; Pump into the above-mentioned maltodextrin solution that refines again; Continuous spray drying granulation, the bed temperature of maltodextrin mist projection granulating controlled well is 50～80 ℃, the maltodextrin spray drying granulation is on the noncrystalline fluffy body of sugar alcohol; Obtain even sugariness and modify fluffy good shape product.
Embodiment 1:
3.2 kilograms of maltodextrins and deionized water are dissolved in a stainless steel reacting by heating pot for 25 kilograms; 8.8 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel reacting by heating pot for 25 kilograms, and material is heated to 67 ℃ by chuck in the pot, starts stirring; Add 0.5 kilogram of active carbon respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 60 kilograms of xylitols, 28 kilograms of oligoisomaltose alcohol, pulverizing reaches 180 orders through pulverizer; Be sent in the spray-fluidized bed apparatus, the mixed material of xylitol and oligoisomaltose gets into the fluidized bed with spraying from the bottom of fluidized bed with spraying and quickens from bottom to top with malleation and flows, and the top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body; Control fluidized-bed layer temperature is 35～50 ℃, and the multiple spot even spraying is disperseed, after operation is accomplished; Improve bed temperature to 50～55 ℃ again; After xylitol, the mixing of oligoisomaltose alcohol fluidisation lose surface crystallization water, pump into the above-mentioned maltodextrin solution that refines, continuously spray drying granulation; Control air quantity and mist flow well, obtain even sugariness and modify good fluffy granular product.
Embodiment 2:
4.5 kilograms of maltodextrins and deionized water are dissolved in a stainless steel reacting by heating pot for 20 kilograms; 17.5 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel reaction pot for 30 kilograms, and material is heated to 70 ℃ by chuck in the pot, starts stirring; Add 1.5 kilograms of active carbons respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 54 kilograms of xylitols, 24 kilograms of oligoisomaltose alcohol reach 180 orders through pulverizing; Be sent to and carry out fluidisation in the spray-fluidized bed apparatus and mix, the mixed material of xylitol and oligoisomaltose gets into the fluidized bed with spraying and quickens from bottom to top from the bottom of fluidized bed with spraying with malleation and flows, and the top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom material is seethed with excitement up and down in fluid bed; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body; 35～40 ℃ of control fluidized-bed layer temperature, even spraying is disperseed, after operation is accomplished; Improve bed temperature to 50～75 ℃ again; After making xylitol, the mixing of oligoisomaltose alcohol fluidisation lose surface crystallization water, pumping into the above-mentioned maltodextrin solution that refines, continuously spray granulating and drying; Control air quantity and mist flow well, obtain even sugariness and modify good fluffy granular product.
Embodiment 3:
3.5 kilograms of maltodextrins and deionized water are dissolved in a stainless steel reacting by heating pot for 30 kilograms; 26.5 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel reacting by heating pot for 40 kilograms, and material is heated to 65 ℃ by chuck in the pot, starts stirring; Add 3.0 kilograms of active carbons respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 50 kilograms of xylitols, 20 kilograms of oligoisomaltoses, pulverizing reaches 170 orders through pulverizer; Be sent in the spray-fluidized bed apparatus, the mixed material of xylitol and oligoisomaltose gets into the fluidized bed with spraying from the bottom of fluidized bed with spraying and quickens from bottom to top with malleation and flows, and the top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body; Control 35～42 ℃ of fluidized-bed layer temperature well, the multiple spot even spraying is disperseed, after operation is accomplished; Improve bed temperature to 50～80 ℃ again; After xylitol, the mixing of oligoisomaltose fluidisation lose surface crystallization water, pump into the above-mentioned maltodextrin solution that refines, continuously spray drying granulation; Control air quantity and mist flow well, obtain even sugariness and modify good fluffy granular product.
Embodiment 4:
4 kilograms of maltodextrins and deionized water are dissolved in a stainless steel reacting by heating pot for 40 kilograms; 60 kilograms also another dissolves in stainless steel reacting by heating pot with deionized water with 35 kilograms of Sucraloses, and material is heated to 60 ℃ by chuck in the pot, starts stirring; Add 3.0 kilograms of active carbons respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 41 kilograms of xylitols, 20 kilograms of oligoisomaltose alcohol, pulverizing reaches 150 orders through pulverizer; Be sent to fluidisation in the spray-fluidized bed apparatus, the mixed material of xylitol and oligoisomaltose gets into the fluidized bed with spraying from the bottom of fluidized bed with spraying and quickens from bottom to top with malleation and flows, and the top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body; Control 35～40 ℃ of fluidized-bed layer temperature well, the multiple spot even spraying is disperseed, after operation is accomplished; Improve bed temperature to 50～78 ℃ again; After xylitol, oligoisomaltose fluidisation lose surface crystallization water, pumping into the above-mentioned maltodextrin solution that refines, continuously the Spray Mixing drying-granulating; Control air quantity and mist flow well, obtain the good fluffy granular product of even sugariness decorations.
Through detecting, adopt the fluffy granular composite sugar-free sweetener of technical scheme acquisition of the present invention, its main performance index is seen table 1.
Table 1
| Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 |
| Particle size | 30～60 orders | 30～60 orders | 30～60 orders | 30～60 orders |
| Sugariness (sucrose contrast) | 50 times | 100 times | 150 times | 200 times |
| Outward appearance | White particle | White particle | White particle | White particle |
| Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 |
| Bulk density (g/mm 3) | 0.58 | 0.62 | 0.63 | 0.66 |
The stability test of sweetener is to check sweetener to guarantee the ability that undergoes no deterioration within a certain period of time, and the sweetener product of the embodiment of the invention was stored 3 years at normal temperatures, phenomenons such as rotten and sugariness reduction occur, and the stability ten minutes is superior.
The sugariness degree of modification of fluffy granular composite sugar-free sweetener of the present invention is with according to the adjustment of Sucralose in the food consumption adds, 50～200 times of selecting the common sucrose sugariness usually for use; Relatively be fit to the food enterprise needs; Form according to prescription, under same sugariness situation, people only are 1/50～1/200 of common sucrose to the absorption of heat; Sugar-free sweetener is the sweet taste article of low-calorie; The metabolism of this sweetener does not need insulin, can not cause blood sugar to raise, and is suitable for diabetes, three high crowds' needs.
Show obviously that to sum up the present invention adopts scientific formula, uses advanced science and technology technology and method, products obtained therefrom does not have smell, do not have color, and is soluble in water, and it is very convenient that this fluffy granule-shaped sugar-free sweetener is used.Granularity, molten speed, mouthfeel, sugariness all are much better than the prior art value, and the scientific preparation process simple flow is prone to row, are fit to very much large-scale production, are worth wide popularization and application in the field of business.
What need understand is: the above only is a preferred implementation of the present invention; For those skilled in the art; Under the prerequisite that does not break away from the principle of the invention, can also make some improvement and retouching, these improvement and retouching also should be regarded as protection scope of the present invention.
Claims (4)
1. fluffy granular composite sugar-free sweetener is characterized in that comprising following percentage by weight composition: antierythrite 20～33%, xylitol 8～20%, oligoisomaltose 47～70%, knob sweet 0.6～4.5%; Its preparation method comprises following processing step:
1. with 10% oligoisomaltose, knob is sweet joins respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 52～80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned oligoisomaltose solution and the sweet solution of knob, be incubated 25～30 minutes, filter while hot, for use in the storage tank that is pooled to heat tracing respectively of filtrating;
4. put in the spray-fluidized bed apparatus after xylitol, antierythrite and oligoisomaltose being pulverized; The mixed material of xylitol, antierythrite and oligoisomaltose also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The bed temperature scope of fluidized bed with spraying is 35～80 ℃; Wherein the bed temperature of the sweet spraying dispersion of phase I knob is 35～50 ℃; The bed temperature of second stage oligoisomaltose mist projection granulating is 50～80 ℃, and the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the mixed material of fine xylitol, antierythrite and oligoisomaltose, pumps into the above-mentioned oligoisomaltose solution that refines again; Spray-drying obtains fluffy granular composite sugar-free sweetener continuously.
2. fluffy granular composite sugar-free sweetener according to claim 1 is characterized in that its composition has following percentage by weight: antierythrite 20%, xylitol 9.28%, oligoisomaltose 70%, knob sweet 0.72%.
3. the preparation method of the described fluffy granular composite sugar-free sweetener of claim 1 is characterized in that: comprise following processing step---
1. with 10% oligoisomaltose, knob is sweet joins respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 52～80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned oligoisomaltose solution and the sweet solution of knob, be incubated 25～30 minutes, filter while hot, for use in the storage tank that is pooled to heat tracing respectively of filtrating;
4. put in the spray-fluidized bed apparatus after xylitol, antierythrite and oligoisomaltose being pulverized; The mixed material of xylitol, antierythrite and oligoisomaltose also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The bed temperature scope of fluidized bed with spraying is 35～80 ℃; Wherein the bed temperature of the sweet spraying dispersion of phase I knob is 35～50 ℃; The bed temperature of second stage oligoisomaltose mist projection granulating is 50～80 ℃, and the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the mixed material of fine xylitol, antierythrite and oligoisomaltose, pumps into the above-mentioned oligoisomaltose solution that refines again; Spray-drying obtains fluffy granular composite sugar-free sweetener continuously.
4. the preparation method of fluffy granular composite sugar-free sweetener according to claim 3 is characterized in that: with 10% oligoisomaltose, knob is sweet joins respectively in the container, add deionized water respectively and mix; Be warming up to 60～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrating is pooled to respectively in the storage tank that has heat tracing; Antierythrite, xylitol and oligoisomaltose are reached 120～180 orders through pulverizing; Be sent in the spray-fluidized bed apparatus; The mixed material of above-mentioned various sugar alcohols is also quickened to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and control fluidized-bed layer temperature is at 35～80 ℃, and the multiple spot spray gun of fluid bed sidepiece earlier will the sweet solution of the above-mentioned knob that refines be sprayed continuously and is distributed on the mixed material of fine xylitol, antierythrite and oligoisomaltose; After the goods fluid mixing loses surperficial moisture content; Pump into the above-mentioned oligoisomaltose solution that refines again, spray drying granulation obtains fluffy granular composite sugar-free sweetener continuously.
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| CN102415549A (en) * | 2011-12-15 | 2012-04-18 | 苏州工业园区尚融科技有限公司 | Compound sugar-free sweetener and preparation method thereof |
| CN102429205A (en) * | 2011-12-20 | 2012-05-02 | 苏州工业园区尚融科技有限公司 | Compound low-sugar sweetener and preparation method thereof |
| CN102960694A (en) * | 2012-11-30 | 2013-03-13 | 苏州工业园区尚融科技有限公司 | Compound sweetening agent applicable to coffee and preparation method thereof |
| CN103766697A (en) * | 2014-01-07 | 2014-05-07 | 长春禾甜科技有限责任公司 | Sugar-free sweetener and preparation method thereof |
| CN111084384A (en) * | 2019-12-30 | 2020-05-01 | 湖南点道生物科技有限公司 | Compound carbohydrate component and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1254522A (en) * | 1999-12-09 | 2000-05-31 | 北京恒毅利科贸有限责任公司 | Method for preparing granular flavouring enriched food and its product |
| CN101181050A (en) * | 2007-12-19 | 2008-05-21 | 苏州苏克瑞甜品科技有限公司 | Sucrose succedaneum and preparation method thereof |
| CN101253968A (en) * | 2008-04-15 | 2008-09-03 | 苏州苏克瑞甜品科技有限公司 | Granular sugar-free sweetening agent and method of preparing the same |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1254522A (en) * | 1999-12-09 | 2000-05-31 | 北京恒毅利科贸有限责任公司 | Method for preparing granular flavouring enriched food and its product |
| CN101181050A (en) * | 2007-12-19 | 2008-05-21 | 苏州苏克瑞甜品科技有限公司 | Sucrose succedaneum and preparation method thereof |
| CN101253968A (en) * | 2008-04-15 | 2008-09-03 | 苏州苏克瑞甜品科技有限公司 | Granular sugar-free sweetening agent and method of preparing the same |
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