CN101810298B - Novel sugar-free table sweetening agent and preparation method thereof - Google Patents
Novel sugar-free table sweetening agent and preparation method thereof Download PDFInfo
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- CN101810298B CN101810298B CN2009102499691A CN200910249969A CN101810298B CN 101810298 B CN101810298 B CN 101810298B CN 2009102499691 A CN2009102499691 A CN 2009102499691A CN 200910249969 A CN200910249969 A CN 200910249969A CN 101810298 B CN101810298 B CN 101810298B
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Abstract
The invention relates to a novel sugar-free table sweetening agent and a preparation method thereof. The novel sugar-free table sweetening agent comprises the following components: 12 to 20 percent of xylitol, 12 to 25 percent of erythritol, 20 to 45 percent of sorbitol, 25 to 50 percent of isomaltooligosaccharide and 0.072 to 0.16 percent of neotame; and a process for preparing the sweetening agent comprises the following steps of: adding 9 percent of the xylitol and the neotame into a heating container respectively, adding deionized water into the xylitol and the neotame respectively and mixing, and raising the temperature and dissolving the mixture; adding activated carbon into solution respectively, filtering the mixture while hot, and collecting filtrate into a storage tank; and allowing a mixed material of the pulverized xylitol, sorbitol and dextrose monohydrate to enter a spray fluidized bed from the bottom thereof by positive pressure and accelerating the flow of the mixed material from bottom to top, applying negative pressure to the upper part of the spray fluidized bed to vibrate the fluidized bed from top to bottom, so that the material boils inside the bed up and down, continuously spraying and dispersing the refined neotame solution on microfine sugar alcohol by using a multipoint spray gun on the side part of the fluidized bed, pumping the maltodextrin solution, and continuously spraying and drying to obtain the low-sugar low-calorie sweetening agent. The saccharinity of a product is 5 to 10 times that of common saccharose.
Description
Technical field
The present invention relates to a kind of edible dining table sweetener, relate in particular to a kind of novel sugar-free table sweetening agent and production method thereof.
Background technology
The increase of Along with people's because of too much bringing disease with sugar, people's demand safety, healthy Sugarless type dining table sweetener; In production procedure, reach the Advanced Manufacturing Technology of putting into finished product one step completion from raw material; It is learnt from other's strong points to offset one's weaknesses, has complementary advantages to make between the sugar alcohol sweet taste on the formula for a product; Can play during product uses and cover the effect that promotes mouthfeel with synergy; People thirst under the prerequisite that satisfies sugariness height, empty calory, and occupation modeization, with cane-sugar taste safety and Health Sugarless type dining table sweetener roughly the same.
Summary of the invention
The objective of the invention is to overcome the deficiency that prior art exists, a kind of novel sugar-free table sweetening agent and production method thereof are provided.
The object of the invention is realized through following technical scheme:
A kind of novel sugar-free table sweetening agent, characteristics are to comprise following composition (percentage by weight): xylitol 12～20%, antierythrite 12～25%, D-sorbite 20～45%, oligoisomaltose 25～50%, knob sweet 0.072～0.16%.
Further, above-mentioned a kind of novel sugar-free table sweetening agent, wherein, xylitol 20%, antierythrite 20%, D-sorbite 20%, oligoisomaltose 39.928%, knob sweet 0.072%.
The production method of a kind of novel sugar-free table sweetening agent of the present invention comprises following processing step:
1. with 9% sweet the joining respectively in the heating container of xylitol, knob, add deionized water respectively and mix;
2. be warming up to 52～80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned xylitol solution and the sweet solution of knob, be incubated 25～30 minutes, filter while hot, filtrating is pooled to respectively in the storage tank of heat tracing;
4. put in the spray-fluidized bed apparatus after xylitol, antierythrite, oligoisomaltose and D-sorbite being pulverized; The mixed material of above-mentioned various sugar alcohols is also quickened to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body; Pump into the above-mentioned xylitol solution that refines again, spray-drying obtains fluffy granular composite sugar-free table sweetener continuously.
Again further, the production method of above-mentioned a kind of novel sugar-free table sweetening agent, the xylitol with 9%, knob is sweet joins respectively in the heating container, adds deionized water respectively and mixes; Be warming up to 60～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrating is pooled to respectively in the storage tank that has heat tracing; Xylitol, antierythrite, oligoisomaltose and D-sorbite reach 120～180 orders through pulverizing; Be sent in the spray-fluidized bed apparatus; The mixed material of above-mentioned various sugar alcohols is also quickened to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and control fluidized-bed layer temperature is at 35～80 ℃, and the multiple spot spray gun of fluid bed sidepiece earlier will the sweet solution of the above-mentioned knob that refines be sprayed continuously and is distributed on the fine sugar alcohol body; After the mixing of sugar alcohol fluidisation loses surperficial moisture content; Pump into the above-mentioned xylitol solution that refines again, spray drying granulation obtains fluffy granular composite sugar-free table sweetener continuously.
Again further; The production method of above-mentioned a kind of novel sugar-free table sweetening agent; The bed temperature scope of said fluidized bed with spraying is 35～80 ℃, and wherein the bed temperature of the sweet spraying dispersion of phase I knob is 35～50 ℃, and the bed temperature of second stage xylitol mist projection granulating is 50～80 ℃.
Again further, the production method of above-mentioned a kind of novel sugar-free table sweetening agent, in the phase I of said Spray Mixing fluid bed, the sweet spraying of knob is dispersed in fluidisation and smashes on the fine sugar alcohol crystal body; In second stage, the xylitol spray drying granulation is on the noncrystal of mixing sugar alcohol.
Substantive distinguishing features and obvious improvement that technical scheme of the present invention is outstanding are mainly reflected in:
With xylitol, antierythrite, D-sorbite, oligoisomaltose, knob is sweet is primary raw material; Modify uniformly and coat through preparation method to sugariness; Make product sweetness reach 5～10 times of common sucrose, products obtained therefrom does not have smell, do not have color, and is soluble in water.Adopt the negative pressure fluid bed fluidization technique of scientific formula, uses advanced to combine the multi-point atomizing method, time sharing segment control appliance bed temperature efficiently solves even dispersion, coats problems such as granulation, drying.This fluffy granular composite sugar-free table sweetener is easy to use, and its process for making science is simple and easy to operate, is fit to very much large-scale production.
Description of drawings
Below in conjunction with accompanying drawing technical scheme of the present invention is described further:
Fig. 1: process chart of the present invention.
The specific embodiment
A kind of novel sugar-free table sweetening agent, its composition is: xylitol 12～20%, antierythrite 12～25%, D-sorbite 20～45%, oligoisomaltose 25～50%, knob sweet 0.072～0.16%.Ideal formulations is: xylitol 20%, antierythrite 20%, D-sorbite 20%, oligoisomaltose 39.928%, knob sweet 0.072%.
As shown in Figure 1, a kind of manufacturing process of novel sugar-free table sweetening agent: at first, the xylitol with 9%, knob is sweet joins respectively in the heating container, adds deionized water respectively and mixes; Be warming up to 52～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively in the sweet solution of above-mentioned xylitol solution and knob, be incubated 25～30 minutes, filter while hot, filtrating is pooled to respectively in the storage tank of heat tracing; At last; Put into after xylitol, antierythrite, oligoisomaltose and D-sorbite pulverized in the spray-fluidized bed apparatus (at heating temperature control and technological with the boiling that in fluid bed, circulates of sugar alcohol material through the positive negative pressure boiling of equipment; Mix that fluidisation is anhydrated and fluffy processing; Sugar alcohol mixtures material → malleation material quickens to flow from bottom to top → and negative pressure vibrates → makes material boiling up and down in fluid bed → by the fluid bed side multiple spot spray gun liquid material ejection fog-like liquid of naming a person for a particular job from top to bottom; Be sprayed onto on the trickle solid material body of boiling); The mixed material of xylitol, antierythrite, oligoisomaltose and D-sorbite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body, and the bed temperature that the sweet spraying of control knob disperses is 35～50 ℃, and the sweet even spraying of knob is dispersed on the mixing sugar alcohol crystalline solid of powder; The rising bed temperature; After fluidisation loses surface crystallization water, pump into the above-mentioned xylitol solution that refines at mixing sugar alcohol again, continuously spray drying granulation; The bed temperature of xylitol mist projection granulating controlled well is 50～80 ℃, and the xylitol spray drying granulation is on the noncrystalline fluffy body of sugar alcohol; Obtain even sugariness and modify fluffy good shape product.
Embodiment 1:
9 kilograms of xylitols and deionized water are dissolved in a stainless steel reacting by heating pot for 25 kilograms; Knob is also dissolved in another stainless steel reacting by heating pot for 20 kilograms with deionized water for sweet 0.072 kilogram, and material is heated to 62 ℃ by chuck in the pot, starts stirring; Add 1 kilogram of active carbon respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 11 kilograms of xylitols, 20 kilograms of antierythrites, 39.928 kilograms of oligoisomaltoses; 20 kilograms of D-sorbites, pulverizing reaches 130 orders through pulverizer, is sent in the spray-fluidized bed apparatus; The mixed material of above-mentioned various sugar alcohols got into the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and the multiple spot spray gun of fluid bed sidepiece earlier will the sweet solution of the above-mentioned knob that refines be sprayed continuously and is distributed on the fine sugar alcohol body; Control fluidized-bed layer temperature is 35～50 ℃, and the multiple spot even spraying is disperseed, after operation is accomplished; Improve bed temperature to 50～80 ℃ again; After the mixing of above-mentioned various sugar alcohol alcohol fluidisations loses surface crystallization water, pump into the above-mentioned xylitol solution that refines, continuously spray drying granulation; Control air quantity and mist flow well, obtain even sugariness and modify good fluffy granular product.
Embodiment 2:
9 kilograms of xylitols and deionized water are dissolved in a stainless steel reacting by heating pot for 26 kilograms; Knob is also dissolved in another stainless steel reaction pot for 21 kilograms with deionized water for sweet 0.086 kilogram, and material is heated to 52 ℃ by chuck in the pot, starts stirring; Add 2 kilograms of active carbons respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 6 kilograms of xylitols, 20 kilograms of antierythrites, 35 kilograms of oligoisomaltoses; 29.914 kilograms of D-sorbites reach 150 orders through pulverizing, and are sent to carry out the fluidisation mixing in the spray-fluidized bed apparatus; The mixed material of above-mentioned various sugar alcohols got into the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and the multiple spot spray gun of fluid bed sidepiece earlier will the sweet solution of the above-mentioned knob that refines be sprayed continuously and is distributed on the fine sugar alcohol body; 35～40 ℃ of control fluidized-bed layer temperature, even spraying is disperseed, after operation is accomplished; Improve bed temperature to 50～80 ℃ again; After making the mixing of above-mentioned various sugar alcohol alcohol fluidisation lose surface crystallization water, pumping into the above-mentioned xylitol solution that refines, continuously spray granulating and drying; Control air quantity and mist flow well, obtain even sugariness and modify good fluffy granular product.
Embodiment 3:
9 kilograms of xylitols and deionized water are dissolved in a stainless steel reacting by heating pot for 28 kilograms; Knob is also dissolved in another stainless steel reacting by heating pot for 20 kilograms with deionized water for sweet 0.10 kilogram, and material is heated to 60 ℃ by chuck in the pot, starts stirring; Add 3.0 kilograms of active carbons respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 9 kilograms of xylitols, 12 kilograms of antierythrites, 25 kilograms of oligoisomaltoses; 44.90 kilograms of D-sorbites, pulverizing reaches 160 orders through pulverizer, is sent in the spray-fluidized bed apparatus; The mixed material of above-mentioned various sugar alcohols got into the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and the multiple spot spray gun of fluid bed sidepiece earlier will the sweet solution of the above-mentioned knob that refines be sprayed continuously and is distributed on the fine sugar alcohol body; Control 35～42 ℃ of fluidized-bed layer temperature well, the multiple spot even spraying is disperseed, after operation is accomplished; Improve bed temperature to 50～80 ℃ again; After the mixing of above-mentioned various sugar alcohol alcohol fluidisations loses surface crystallization water, pump into the above-mentioned xylitol solution that refines, continuously spray drying granulation; Control air quantity and mist flow well, obtain even sugariness and modify good fluffy granular product.
Embodiment 4:
9 kilograms of xylitols and deionized water are dissolved in a stainless steel reacting by heating pot for 30 kilograms; With knob sweet 0.12 kilogram with deionized water 20 kilograms also another dissolves in stainless steel reacting by heating pot, the pot in material be heated to 80 ℃ by chuck, start stirring; Add 3.0 kilograms of active carbons respectively; Be incubated 35 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 4 kilograms of xylitols, 17 kilograms of antierythrites, 50 kilograms of oligoisomaltoses; 19.88 kilograms of D-sorbites, pulverizing reaches 180 orders through pulverizer, is sent to fluidisation in the spray-fluidized bed apparatus; The mixed material of above-mentioned various sugar alcohols got into the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and the multiple spot spray gun of fluid bed sidepiece earlier will the sweet solution of the above-mentioned knob that refines be sprayed continuously and is distributed on the fine sugar alcohol body; Control 35～50 ℃ of fluidized-bed layer temperature well, the multiple spot even spraying is disperseed, after operation is accomplished; Improve bed temperature to 50～80 ℃ again; After above-mentioned various sugar alcohol alcohol fluidisations lose surface crystallization water, pumping into the above-mentioned xylitol solution that refines, continuously the Spray Mixing drying-granulating; Control air quantity and mist flow well, obtain the good fluffy granular product of even sugariness decorations.
Through detecting, adopt the fluffy granular composite low-sugar and low-calorie sweetener of technical scheme acquisition of the present invention, its main performance index is seen table 1.
Table 1
| Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 4 |
| Particle size | 30～60 orders | 30～60 orders | 30～60 orders | 30～60 orders | 30～60 orders |
| Sugariness (sucrose contrast) | 5 times | 6 times | 7 times | 8 times | 10 times |
| Outward appearance | White particle | White particle | White particle | White particle | White particle |
| Bulk density (g/mm 3) | 0.60 | 0.62 | 0.64 | 0.65 | 0.66 |
The stability test of sweetener is to check sweetener to guarantee the ability that undergoes no deterioration within a certain period of time, and the dining table sweetener product of the embodiment of the invention was stored 3 years at normal temperatures, phenomenons such as rotten and sugariness reduction occur, and the stability ten minutes is superior.
The sugariness degree of modification of fluffy granular composite sugar-free table sweetener of the present invention will be according to the sweet adjustment in consumption of knob, 5～10 times of selecting the common sucrose sugariness usually for use; Relatively be fit to people's use needs, form, under same sugariness situation according to prescription; People are almost nil to the absorption of heat, and this dining table sweetener can not cause blood sugar to raise, not carious tooth; Be fit to the diabetes patient, satisfy three high crowds, pursue healthy needs of people.
Show obviously that to sum up the present invention adopts scientific formula, uses advanced science and technology technology and method, products obtained therefrom does not have smell, do not have color, and is soluble in water, and it is very convenient that this fluffy granule-shaped sugar-free dining table sweetener is used.Granularity, molten speed, mouthfeel, sugariness all are much better than the prior art value, and the manufacturing process flow of science is simple and easy to do, are fit to very much large-scale production, are worth wide popularization and application in the field of business.
What need understand is: the above only is a preferred implementation of the present invention; For those skilled in the art; Under the prerequisite that does not break away from the principle of the invention, can also make some improvement and retouching, these improvement and retouching also should be regarded as protection scope of the present invention.
Claims (4)
1. a Sugarless mensal sweetening material is characterized in that comprising following percentage by weight composition: xylitol 12～20%, antierythrite 12～25%, D-sorbite 20～45%, oligoisomaltose 25～50%, knob sweet 0.072～0.16%; Its preparation method comprises following processing step:
1. with 9% sweet the joining respectively in the heating container of xylitol, knob, add deionized water respectively and mix;
2. be warming up to 52～80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned xylitol solution and the sweet solution of knob, be incubated 25～30 minutes, filter while hot, for use in the storage tank that is pooled to heat tracing respectively of filtrating;
4. put in the spray-fluidized bed apparatus after xylitol, antierythrite, oligoisomaltose and D-sorbite being pulverized; The mixed material of xylitol, antierythrite, oligoisomaltose and D-sorbite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The bed temperature scope of fluidized bed with spraying is 35～80 ℃; Wherein the bed temperature of the sweet spraying dispersion of phase I knob is 35～50 ℃; The bed temperature of second stage xylitol mist projection granulating is 50～80 ℃, and the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the mixed material of fine xylitol, antierythrite, oligoisomaltose and D-sorbite, pumps into the above-mentioned xylitol solution that refines again; Spray-drying obtains fluffy granular composite sugar-free table sweetener continuously.
2. a kind of Sugarless mensal sweetening material according to claim 1 is characterized in that its composition has following percentage by weight: xylitol 20%, antierythrite 20%, D-sorbite 20%, oligoisomaltose 39.928%, knob sweet 0.072%.
3. the production method of the described a kind of Sugarless mensal sweetening material of claim 1 is characterized in that: comprise following processing step---
1. with 9% sweet the joining respectively in the heating container of xylitol, knob, add deionized water respectively and mix;
2. be warming up to 52～80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned xylitol solution and the sweet solution of knob, be incubated 25～30 minutes, filter while hot, for use in the storage tank that is pooled to heat tracing respectively of filtrating;
4. put in the spray-fluidized bed apparatus after xylitol, antierythrite, oligoisomaltose and D-sorbite being pulverized; The mixed material of xylitol, antierythrite, oligoisomaltose and D-sorbite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The bed temperature scope of fluidized bed with spraying is 35～80 ℃; Wherein the bed temperature of the sweet spraying dispersion of phase I knob is 35～50 ℃; The bed temperature of second stage xylitol mist projection granulating is 50～80 ℃, and the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the mixed material of fine xylitol, antierythrite, oligoisomaltose and D-sorbite, pumps into the above-mentioned xylitol solution that refines again; Spray-drying obtains fluffy granular composite sugar-free table sweetener continuously.
4. the production method of a kind of Sugarless mensal sweetening material according to claim 3 is characterized in that: the xylitol with 9%, knob is sweet joins respectively in the container, adds deionized water respectively and mixes; Be warming up to 60～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrating is pooled to respectively in the storage tank that has heat tracing; Xylitol, antierythrite, oligoisomaltose and D-sorbite reach 120～180 orders through pulverizing; Be sent in the spray-fluidized bed apparatus; The mixed material of above-mentioned various sugar alcohols is also quickened to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and control fluidized-bed layer temperature is at 35～80 ℃, and the multiple spot spray gun of fluid bed sidepiece earlier will the sweet solution of the above-mentioned knob that refines be sprayed continuously and is distributed on the mixed material of fine xylitol, antierythrite, oligoisomaltose and D-sorbite; After the goods fluid mixing loses surperficial moisture content; Pump into the above-mentioned xylitol solution that refines again, spray drying granulation obtains fluffy granular composite sugar-free table sweetener continuously.
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| CN106579294A (en) * | 2016-12-12 | 2017-04-26 | 南昌泰康食品科技有限公司 | Dining-table sugar substitute product and preparation method thereof |
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|---|---|---|---|---|
| CN1254522A (en) * | 1999-12-09 | 2000-05-31 | 北京恒毅利科贸有限责任公司 | Method for preparing granular flavouring enriched food and its product |
| CN101181050A (en) * | 2007-12-19 | 2008-05-21 | 苏州苏克瑞甜品科技有限公司 | Sucrose succedaneum and preparation method thereof |
| CN101253968A (en) * | 2008-04-15 | 2008-09-03 | 苏州苏克瑞甜品科技有限公司 | Granular sugar-free sweetening agent and method of preparing the same |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1254522A (en) * | 1999-12-09 | 2000-05-31 | 北京恒毅利科贸有限责任公司 | Method for preparing granular flavouring enriched food and its product |
| CN101181050A (en) * | 2007-12-19 | 2008-05-21 | 苏州苏克瑞甜品科技有限公司 | Sucrose succedaneum and preparation method thereof |
| CN101253968A (en) * | 2008-04-15 | 2008-09-03 | 苏州苏克瑞甜品科技有限公司 | Granular sugar-free sweetening agent and method of preparing the same |
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