CN101810299B - Composite sugar-free low-calorie sweetener and manufacturing method thereof - Google Patents
Composite sugar-free low-calorie sweetener and manufacturing method thereof Download PDFInfo
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- CN101810299B CN101810299B CN200910249970A CN200910249970A CN101810299B CN 101810299 B CN101810299 B CN 101810299B CN 200910249970 A CN200910249970 A CN 200910249970A CN 200910249970 A CN200910249970 A CN 200910249970A CN 101810299 B CN101810299 B CN 101810299B
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- 239000002131 composite material Substances 0.000 title abstract description 18
- 238000005507 spraying Methods 0.000 claims abstract description 52
- 239000000463 material Substances 0.000 claims abstract description 43
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- 229960000673 dextrose monohydrate Drugs 0.000 claims abstract description 24
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- 238000010438 heat treatment Methods 0.000 claims abstract description 16
- 238000003860 storage Methods 0.000 claims abstract description 12
- 238000002156 mixing Methods 0.000 claims abstract description 9
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 8
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 8
- 235000009508 confectionery Nutrition 0.000 claims description 40
- 239000012530 fluid Substances 0.000 claims description 28
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 claims description 23
- 238000009835 boiling Methods 0.000 claims description 15
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- 150000005846 sugar alcohols Chemical class 0.000 abstract description 24
- 238000000034 method Methods 0.000 abstract description 7
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- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 abstract description 6
- 229960004793 sucrose Drugs 0.000 abstract description 6
- 238000001035 drying Methods 0.000 abstract description 3
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- 239000004384 Neotame Substances 0.000 abstract 3
- HLIAVLHNDJUHFG-HOTGVXAUSA-N neotame Chemical compound CC(C)(C)CCN[C@@H](CC(O)=O)C(=O)N[C@H](C(=O)OC)CC1=CC=CC=C1 HLIAVLHNDJUHFG-HOTGVXAUSA-N 0.000 abstract 3
- 235000019412 neotame Nutrition 0.000 abstract 3
- 108010070257 neotame Proteins 0.000 abstract 3
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 abstract 2
- AYRXSINWFIIFAE-SCLMCMATSA-N Isomaltose Natural products OC[C@H]1O[C@H](OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C=O)[C@@H](O)[C@@H](O)[C@@H]1O AYRXSINWFIIFAE-SCLMCMATSA-N 0.000 abstract 2
- DLRVVLDZNNYCBX-RTPHMHGBSA-N isomaltose Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1OC[C@@H]1[C@@H](O)[C@H](O)[C@@H](O)C(O)O1 DLRVVLDZNNYCBX-RTPHMHGBSA-N 0.000 abstract 2
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- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 5
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- TVXBFESIOXBWNM-UHFFFAOYSA-N Xylitol Natural products OCCC(O)C(O)C(O)CCO TVXBFESIOXBWNM-UHFFFAOYSA-N 0.000 description 1
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- HEBKCHPVOIAQTA-UHFFFAOYSA-N meso ribitol Natural products OCC(O)C(O)C(O)CO HEBKCHPVOIAQTA-UHFFFAOYSA-N 0.000 description 1
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- 229960002675 xylitol Drugs 0.000 description 1
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Abstract
The invention relates to a composite low sugar low-calorie sweetener and a manufacturing method thereof. The composite low sugar low-calorie sweetener comprises the following ingredients by weight percent: 50-69 percent of dextrose monohydrate, 15-30 percent of sorbitol, 5-13 percent of isomaltose hypgather, 4-8 percent of maltodextrin and 0.7-4.32 percent of neotame. The technique comprises the following steps: respectively adding the maltodextrin and the neotame into a heating container, respectively adding deionized water for mixing, and rising temperature for dissolving; respectively adding active carbon into the solution, filtering with heat, and respectively collecting the filtrate into a storage tank; leading the mixed material after crushing the dextrose monohydrate, the sorbitol and the isomaltose hypgather to enter a bed from the bottom part of the spray fluidized bed by positive pressure and to flow from bottom to top in a speed-increasing manner, applying negative pressure on the upper part of the spraying fluidized bed to lead the spraying fluidized bed to vibrate from top to bottom so as to lead the material to boil from top to bottom in the bed, firstly spraying and dispersing the refined neotame solution continuously on fine sugar alcohol bodies by a multi-point spray gun of the side part of the fluidized bed, then pumping into the maltodextrin solution, continuously spraying and drying to obtain the low sugar low-calorie sweetener. The sweetness of a product is 50-300 times of that of a common cane sugar.
Description
Technical field
The present invention relates to a kind of edible sweet taste material, relate in particular to a kind of composite sugar-free low-calorie sweetener and manufacturing approach thereof.
Background technology
The increase of Along with people's because of too much bringing disease with sugar, people's demand safety, health, and the sweet low-sugar-content and low-calorie type sweet taste material of mouthfeel; The present invention reaches the Advanced Manufacturing Technology of putting into finished product one step completion from raw material in production procedure; It is learnt from other's strong points to offset one's weaknesses, has complementary advantages to make between the sugar alcohol sweet taste on the formula for a product; Can play during product uses and cover the effect that promotes mouthfeel with synergy; People thirst for satisfying under the low prerequisite of sugariness height, heat, and occupation modeization, with cane-sugar taste roughly the same, the salubriouser safety and Health low-sugar-content and low-calorie type sweet taste material of mouthfeel.
Summary of the invention
The objective of the invention is to overcome the deficiency that prior art exists, a kind of composite low-sugar low-calorie sweetening agent and manufacturing approach thereof are provided, adopt the scientific technology of easy operation control, the molten speed property of product, mouthfeel, local flavor, sugariness all are higher than the prior art optimum value.
The object of the invention is realized through following technical scheme:
A kind of composite low-sugar low-calorie sweetening agent, characteristics are to comprise following composition (percentage by weight): Dextrose Monohydrate 50～69%, D-sorbite 15～30%, oligoisomaltose 5～13%, maltodextrin 4～8%, knob sweet 0.7～4.32%.
Further, above-mentioned a kind of composite sugar-free low-calorie sweetener, wherein, Dextrose Monohydrate 64.28%, D-sorbite 25%, oligoisomaltose 5%, maltodextrin 5%, knob sweet 0.72%.
The manufacturing approach of composite low-sugar low-calorie sweetening agent of the present invention comprises following processing step:
1. with maltodextrin, knob is sweet joins respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 50～80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned maltodextrin solution and the sweet solution of knob, be incubated 25～30 minutes, filter while hot, filtrating is pooled to respectively in the storage tank of heat tracing;
4. put in the spray-fluidized bed apparatus after Dextrose Monohydrate, D-sorbite and oligoisomaltose being pulverized; The mixed material of Dextrose Monohydrate, D-sorbite and oligoisomaltose is also quickened to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body; Pump into the above-mentioned maltodextrin solution that refines again, spray-drying obtains fluffy granular composite low-sugar low-calorie sweetening agent continuously.
Again further, the manufacturing approach of above-mentioned a kind of composite low-sugar low-calorie sweetening agent with maltodextrin, knob is sweet joins respectively in the heating container, adds deionized water respectively and mixes; Be warming up to 60～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrating is pooled to respectively in the storage tank that has heat tracing; Dextrose Monohydrate, D-sorbite and oligoisomaltose are reached 120～180 orders through pulverizing; Be sent in the spray-fluidized bed apparatus; The mixed material of above-mentioned various sugar alcohols is also quickened to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and control fluidized-bed layer temperature is at 35～80 ℃, and the multiple spot spray gun of fluid bed sidepiece earlier will the sweet solution of the above-mentioned knob that refines be sprayed continuously and is distributed on the fine sugar alcohol body; After the mixing of sugar alcohol fluidisation loses surperficial moisture content; Pump into the above-mentioned maltodextrin solution that refines again, spray drying granulation obtains fluffy granular composite low-sugar low-calorie sweetening agent continuously.
Again further; The manufacturing approach of above-mentioned a kind of composite low-sugar low-calorie sweetening agent; The bed temperature scope of said fluidized bed with spraying is 35～80 ℃; Wherein the bed temperature of the sweet spraying dispersion of phase I knob is 35～50 ℃, and the bed temperature of second stage maltodextrin mist projection granulating is 50～80 ℃.
Again further, the manufacturing approach of above-mentioned a kind of composite low-sugar low-calorie sweetening agent, in the phase I of said Spray Mixing fluid bed, the sweet spraying of knob is dispersed in fluidisation and smashes on the fine sugar alcohol crystal body; In second stage, the maltodextrin spray drying granulation is on the noncrystal of mixing sugar alcohol.
Substantive distinguishing features and obvious improvement that technical scheme of the present invention is outstanding are mainly reflected in:
With Dextrose Monohydrate, D-sorbite, oligoisomaltose, knob is sweet is primary raw material, modifies uniformly and coats through preparation method to sugariness, makes product sweetness reach 50～300 times of common sucrose, products obtained therefrom does not have smell, do not have color, and is soluble in water.Adopt the negative pressure fluid bed fluidization technique of scientific formula, uses advanced to combine the multi-point atomizing method, time sharing segment control appliance bed temperature efficiently solves even dispersion, coats problems such as granulation, drying.This fluffy granular composite low-sugar low-calorie sweetening agent is easy to use, and its process for making science is simple and easy to operate, is fit to very much large-scale production.
Description of drawings
Below in conjunction with accompanying drawing technical scheme of the present invention is described further:
Fig. 1: process chart of the present invention.
The specific embodiment
A kind of composite low-sugar low-calorie sweetening agent, its composition is: Dextrose Monohydrate 50～69%, D-sorbite 15～30%, oligoisomaltose 5～13%, maltodextrin 4～8%, knob sweet 0.7～4.32%.Ideal formulations is: Dextrose Monohydrate 64.28%, D-sorbite 25%, oligoisomaltose 5%, maltodextrin 5%, knob sweet 0.72%.
As shown in Figure 1, a kind of manufacturing process of composite low-sugar low-calorie sweetening agent: at first, with maltodextrin, knob is sweet joins respectively in the heating container, add deionized water respectively and mix; Be warming up to 50～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively in the sweet solution of above-mentioned maltodextrin solution and knob, be incubated 25～30 minutes, filter while hot, filtrating is pooled to respectively in the storage tank of heat tracing; Then; Put into after Dextrose Monohydrate, D-sorbite and oligoisomaltose pulverized in the spray-fluidized bed apparatus (at heating temperature control and technological with the boiling that in fluid bed, circulates of sugar alcohol material through the positive negative pressure boiling of equipment; Mix that fluidisation is anhydrated and fluffy processing; Sugar alcohol mixtures material → malleation material quickens to flow from bottom to top → and negative pressure vibrates → makes material boiling up and down in fluid bed → by the fluid bed side multiple spot spray gun liquid material ejection fog-like liquid of naming a person for a particular job from top to bottom; Be sprayed onto on the trickle solid material body of boiling); The mixed material of above-mentioned various sugar alcohols is also quickened to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body, and the bed temperature that the sweet spraying of control knob disperses is 35～50 ℃, and the sweet even spraying of knob is dispersed on the mixing sugar alcohol crystalline solid of powder; The rising bed temperature; At mixing sugar alcohol after fluidisation loses surface crystallization water; Pump into the above-mentioned maltodextrin solution that refines again; Continuous spray drying granulation, the bed temperature of maltodextrin mist projection granulating controlled well is 50～80 ℃, the maltodextrin spray drying granulation is on the noncrystalline fluffy body of sugar alcohol; Obtain even sugariness and modify fluffy good shape product.
Embodiment 1:
5 kilograms of maltodextrins and deionized water are dissolved in a stainless steel reacting by heating pot for 20 kilograms; Knob is also dissolved in another stainless steel reacting by heating pot for 20 kilograms with deionized water for sweet 0.72 kilogram, and material is heated to 62 ℃ by chuck in the pot, starts stirring; Add 1 kilogram of active carbon respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; With 64.28 kilograms of Dextrose Monohydrates, 25 kilograms of D-sorbites, 5 kilograms of oligoisomaltoses; Pulverizing reaches 130 orders through pulverizer, is sent in the spray-fluidized bed apparatus, and the mixed material of Dextrose Monohydrate, D-sorbite and oligoisomaltose also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, the multiple spot spray gun of fluid bed sidepiece earlier will the sweet solution of the above-mentioned knob that refines continuously spraying be distributed on the fine sugar alcohol body, controlling the fluidized-bed layer temperature is 35～50 ℃; The multiple spot even spraying is disperseed; After operation is accomplished, improve bed temperature to 50～80 ℃ again, Dextrose Monohydrate, D-sorbite, oligoisomaltose alcohol fluidisation mix lose surface crystallization water after; Pump into the above-mentioned maltodextrin solution that refines; Continuous spray drying granulation is controlled air quantity and mist flow well, obtains even sugariness and modifies good fluffy granular product.
Embodiment 2:
6 kilograms of maltodextrins and deionized water are dissolved in a stainless steel reacting by heating pot for 21 kilograms; Knob is also dissolved in another stainless steel reaction pot for 24 kilograms with deionized water for sweet 1.45 kilograms, and material is heated to 52 ℃ by chuck in the pot, starts stirring; Add 2 kilograms of active carbons respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; With 69 kilograms of Dextrose Monohydrates, 15 kilograms of D-sorbites, 8.55 kilograms of oligoisomaltoses; Reach 150 orders through pulverizing, be sent to and carry out the fluidisation mixing in the spray-fluidized bed apparatus, the mixed material of Dextrose Monohydrate, D-sorbite and oligoisomaltose also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, the multiple spot spray gun of fluid bed sidepiece earlier will the sweet solution of the above-mentioned knob that refines continuously spraying be distributed on the fine sugar alcohol body, control 35～40 ℃ of fluidized-bed layer temperature; Even spraying is disperseed; After operation is accomplished, improve bed temperature to 50～80 ℃ again, after above-mentioned various sugar alcohol alcohol fluidisation being mixed lose surface crystallization water; Pumping into the above-mentioned maltodextrin solution that refines; Continuous spray granulating and drying is controlled air quantity and mist flow well, obtains even sugariness and modifies good fluffy granular product.
Embodiment 3:
7 kilograms of maltodextrins and deionized water are dissolved in a stainless steel reacting by heating pot for 22 kilograms; Knob is also dissolved in another stainless steel reacting by heating pot for 25 kilograms with deionized water for sweet 2.16 kilograms, and material is heated to 60 ℃ by chuck in the pot, starts stirring; Add 3.0 kilograms of active carbons respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; With 63 kilograms of Dextrose Monohydrates, 20 kilograms of D-sorbites, 7.84 kilograms of oligoisomaltoses; Pulverize through pulverizer and to reach 160 orders, be sent in the spray-fluidized bed apparatus, the mixed material of Dextrose Monohydrate, D-sorbite and oligoisomaltose is got into the fluidized bed with spraying and quickens from bottom to top from the bottom of fluidized bed with spraying with malleation flow; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and the multiple spot spray gun of fluid bed sidepiece earlier will the sweet solution of the above-mentioned knob that refines be sprayed continuously and is distributed on the fine sugar alcohol body, controls 35～42 ℃ of fluidized-bed layer temperature well; The multiple spot even spraying is disperseed; After operation is accomplished, improve bed temperature to 50～80 ℃ again, above-mentioned various sugar alcohols alcohol fluidisations mix lose surface crystallization water after; Pump into the above-mentioned maltodextrin solution that refines; Continuous spray drying granulation is controlled air quantity and mist flow well, obtains even sugariness and modifies good fluffy granular product.
Embodiment 4:
4 kilograms of Dextrose Monohydrates and deionized water are dissolved in a stainless steel reacting by heating pot for 20 kilograms; With knob sweet 2.88 kilograms with deionized water 25 kilograms also another dissolves in stainless steel reacting by heating pot, the pot in material be heated to 80 ℃ by chuck, start stirring; Add 3.0 kilograms of active carbons respectively; Be incubated 35 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; With 52 kilograms of Dextrose Monohydrates, 29 kilograms of D-sorbites, 12.12 kilograms of oligoisomaltoses; Pulverize through pulverizer and to reach 180 orders, be sent to fluidisation in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols is got into the fluidized bed with spraying and quickens from bottom to top from the bottom of fluidized bed with spraying with malleation flow; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and the multiple spot spray gun of fluid bed sidepiece earlier will the sweet solution of the above-mentioned knob that refines be sprayed continuously and is distributed on the fine sugar alcohol body, controls 35～50 ℃ of fluidized-bed layer temperature well; The multiple spot even spraying is disperseed; After operation is accomplished, improve bed temperature to 50～80 ℃ again, after above-mentioned various sugar alcohols alcohol fluidisations lose surface crystallization water; Pumping into the above-mentioned maltodextrin solution that refines; Continuous Spray Mixing drying-granulating is controlled air quantity and mist flow well, obtains the good fluffy granular product of even sugariness decorations.
Embodiment 5:
8 kilograms of Dextrose Monohydrates and deionized water are dissolved in a stainless steel reacting by heating pot for 25 kilograms; Knob is also dissolved in another stainless steel reacting by heating pot for 29 kilograms with deionized water for sweet 4.32 kilograms, and material is heated to 62 ℃ by chuck in the pot, starts stirring; Add 3 kilograms of active carbons respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; With 50 kilograms of Dextrose Monohydrates, 25.68 kilograms of D-sorbites, 12 kilograms of oligoisomaltoses; Pulverize through pulverizer and to reach 130 orders, be sent in the spray-fluidized bed apparatus, the mixed material of Dextrose Monohydrate, D-sorbite and oligoisomaltose is got into the fluidized bed with spraying and quickens from bottom to top from the bottom of fluidized bed with spraying with malleation flow; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, the multiple spot spray gun of fluid bed sidepiece earlier will the sweet solution of the above-mentioned knob that refines continuously spraying be distributed on the fine sugar alcohol body, controlling the fluidized-bed layer temperature is 35～50 ℃; The multiple spot even spraying is disperseed; After operation is accomplished, improve bed temperature to 50～80 ℃ again, xylitol, D-sorbite, oligoisomaltose alcohol fluidisation mix lose surface crystallization water after; Pump into the above-mentioned maltodextrin solution that refines; Continuous spray drying granulation is controlled air quantity and mist flow well, obtains even sugariness and modifies good fluffy granular product.
Through detecting, adopt the fluffy granular composite low-sugar low-calorie sweetening agent of technical scheme acquisition of the present invention, its main performance index is seen table 1.
Table 1
| Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 |
| Particle size | 30～60 orders | 30～60 orders | 30～60 orders | 30～60 orders | 30～60 orders |
| Sugariness (sucrose contrast) | 50 times | 100 times | 150 times | 200 times | 300 times |
| Outward appearance | White particle | White particle | White particle | White particle | White particle |
| Bulk density (g/mm 3) | 0.60 | 0.62 | 0.63 | 0.65 | 0.66 |
The stability test of sweet taste material is to check the sweet taste material to guarantee the ability that undergoes no deterioration within a certain period of time, and the sweet taste material product of the embodiment of the invention was stored 3 years at normal temperatures, phenomenons such as rotten and sugariness reduction occur, and the stability ten minutes is superior.
The sugariness degree of modification of fluffy granular composite low-sugar low-calorie sweetening agent of the present invention; According to the sweet adjustment in consumption of knob, in use unrestricted, select the common sucrose sugariness usually for use 50～300 times; The use needs that relatively are fit to food enterprise; Form according to prescription, under same sugariness situation, people only are 1/50,1/300 of sucrose to the absorption of heat; Low-sugar low-calorie sweetening agent is the sweet taste article of low-calorie, and this sweet taste material can not cause blood sugar to raise, satisfies three high crowds, pursue healthy needs of people.
Show obviously that to sum up the present invention adopts scientific formula, uses advanced science and technology technology and method, products obtained therefrom does not have smell, do not have color, and is soluble in water, and it is very convenient that this fluffy granular low-sugar low-calorie sweetening agent is used.Granularity, molten speed, mouthfeel, sugariness all are much better than the prior art value, and the manufacturing process flow of science is simple and easy to do, are fit to very much large-scale production, are worth wide popularization and application in the field of business.
What need understand is: the above only is a preferred implementation of the present invention; For those skilled in the art; Under the prerequisite that does not break away from the principle of the invention, can also make some improvement and retouching, these improvement and retouching also should be regarded as protection scope of the present invention.
Claims (5)
1. a compound low-calorie sweetener is characterized in that its component and percentage by weight thereof are: Dextrose Monohydrate 50～69%, D-sorbite 15～30%, oligoisomaltose 5～13%, maltodextrin 4～8%, knob sweet 0.7～4.32%; Its preparation method comprises following processing step:
1. with maltodextrin, knob is sweet joins respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 50～80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned maltodextrin solution and the sweet solution of knob, be incubated 25～30 minutes, filter while hot, for use in the storage tank that is pooled to heat tracing respectively of filtrating;
4. put in the spray-fluidized bed apparatus after Dextrose Monohydrate, D-sorbite and oligoisomaltose being pulverized; The mixed material of Dextrose Monohydrate, D-sorbite and oligoisomaltose also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine mixed material; Pump into the above-mentioned maltodextrin solution that refines again, spray-drying obtains the compound low-calorie sweetener of fluffy granular continuously.
2. a kind of compound low-calorie sweetener according to claim 1 is characterized in that its component has following percentage by weight: Dextrose Monohydrate 64.28%, D-sorbite 25%, oligoisomaltose 5%, maltodextrin 5%, knob sweet 0.72%.
3. the manufacturing approach of the described a kind of compound low-calorie sweetener of claim 1 is characterized in that: comprise following processing step---
1. with maltodextrin, knob is sweet joins respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 50～80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned maltodextrin solution and the sweet solution of knob, be incubated 25～30 minutes, filter while hot, for use in the storage tank that is pooled to heat tracing respectively of filtrating;
4. put in the spray-fluidized bed apparatus after Dextrose Monohydrate, D-sorbite and oligoisomaltose being pulverized; The mixed material of Dextrose Monohydrate, D-sorbite and oligoisomaltose also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine mixed material; Pump into the above-mentioned maltodextrin solution that refines again, spray-drying obtains the compound low-calorie sweetener of fluffy granular continuously.
4. the manufacturing approach of a kind of compound low-calorie sweetener according to claim 3 is characterized in that: with maltodextrin, knob is sweet joins respectively in the container, add deionized water respectively and mix; Be warming up to 60～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrating is pooled to respectively in the storage tank that has heat tracing; Dextrose Monohydrate, D-sorbite and oligoisomaltose are reached 120～180 orders through pulverizing; Be sent in the spray-fluidized bed apparatus; Dextrose Monohydrate, D-sorbite and oligoisomaltose mixed material also quicken to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and control fluidized-bed layer temperature is at 35～80 ℃, and the multiple spot spray gun of fluid bed sidepiece earlier will the sweet solution of the above-mentioned knob that refines be sprayed continuously and is distributed on the fine mixed material; After the goods fluid mixing loses surperficial moisture content; Pump into the above-mentioned maltodextrin solution that refines again, spray drying granulation obtains the compound low-calorie sweetener of fluffy granular continuously.
5. the manufacturing approach of a kind of compound low-calorie sweetener according to claim 4; It is characterized in that: the bed temperature scope of said fluidized bed with spraying is 35～80 ℃; Wherein the bed temperature of the sweet spraying dispersion of phase I knob is 35～50 ℃, and the bed temperature of second stage maltodextrin mist projection granulating is 50～80 ℃.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1833542A (en) * | 2004-03-16 | 2006-09-20 | 卡夫食品集团公司 | Improved method for drying neotame with co-agents |
| CN101534661A (en) * | 2006-09-18 | 2009-09-16 | 麦克内尔营养有限公司 | Cohesive non-free flowing sweetener compositions containing a hygroscopic gluing agent and a desiccant |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1833542A (en) * | 2004-03-16 | 2006-09-20 | 卡夫食品集团公司 | Improved method for drying neotame with co-agents |
| CN101534661A (en) * | 2006-09-18 | 2009-09-16 | 麦克内尔营养有限公司 | Cohesive non-free flowing sweetener compositions containing a hygroscopic gluing agent and a desiccant |
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| JP特开2002-27942A 2002.01.29 |
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