CN101810299A - Composite sugar-free low-calorie sweetener and manufacturing method thereof - Google Patents
Composite sugar-free low-calorie sweetener and manufacturing method thereof Download PDFInfo
- Publication number
- CN101810299A CN101810299A CN200910249970A CN200910249970A CN101810299A CN 101810299 A CN101810299 A CN 101810299A CN 200910249970 A CN200910249970 A CN 200910249970A CN 200910249970 A CN200910249970 A CN 200910249970A CN 101810299 A CN101810299 A CN 101810299A
- Authority
- CN
- China
- Prior art keywords
- sugar
- spraying
- fluidized bed
- bed
- maltodextrin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000002131 composite material Substances 0.000 title claims abstract description 26
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 16
- 235000013615 non-nutritive sweetener Nutrition 0.000 title claims abstract description 11
- 238000005507 spraying Methods 0.000 claims abstract description 48
- 239000000463 material Substances 0.000 claims abstract description 38
- 229920002774 Maltodextrin Polymers 0.000 claims abstract description 35
- 239000005913 Maltodextrin Substances 0.000 claims abstract description 32
- 229940035034 maltodextrin Drugs 0.000 claims abstract description 32
- SPFMQWBKVUQXJV-BTVCFUMJSA-N (2r,3s,4r,5r)-2,3,4,5,6-pentahydroxyhexanal;hydrate Chemical compound O.OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C=O SPFMQWBKVUQXJV-BTVCFUMJSA-N 0.000 claims abstract description 28
- 150000005846 sugar alcohols Chemical class 0.000 claims abstract description 28
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 24
- 229960000673 dextrose monohydrate Drugs 0.000 claims abstract description 21
- 238000000034 method Methods 0.000 claims abstract description 17
- 239000008367 deionised water Substances 0.000 claims abstract description 16
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 16
- 238000010438 heat treatment Methods 0.000 claims abstract description 15
- 239000007921 spray Substances 0.000 claims abstract description 14
- 239000000706 filtrate Substances 0.000 claims abstract description 11
- 238000002156 mixing Methods 0.000 claims abstract description 11
- 238000003860 storage Methods 0.000 claims abstract description 11
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 7
- 235000009508 confectionery Nutrition 0.000 claims description 37
- 239000012530 fluid Substances 0.000 claims description 24
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 claims description 20
- 235000003599 food sweetener Nutrition 0.000 claims description 18
- 239000003765 sweetening agent Substances 0.000 claims description 18
- 238000009835 boiling Methods 0.000 claims description 14
- 238000005243 fluidization Methods 0.000 claims description 13
- 238000005469 granulation Methods 0.000 claims description 10
- 230000003179 granulation Effects 0.000 claims description 10
- 239000000203 mixture Substances 0.000 claims description 10
- 238000001694 spray drying Methods 0.000 claims description 10
- 238000003756 stirring Methods 0.000 claims description 10
- 238000010298 pulverizing process Methods 0.000 claims description 9
- 239000003595 mist Substances 0.000 claims description 8
- 238000010792 warming Methods 0.000 claims description 5
- 239000006185 dispersion Substances 0.000 claims description 3
- 239000000047 product Substances 0.000 abstract description 16
- 229930006000 Sucrose Natural products 0.000 abstract description 6
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 abstract description 6
- 229960004793 sucrose Drugs 0.000 abstract description 6
- 238000001035 drying Methods 0.000 abstract description 4
- 238000005086 pumping Methods 0.000 abstract description 3
- 230000000630 rising effect Effects 0.000 abstract description 2
- 239000004384 Neotame Substances 0.000 abstract 3
- HLIAVLHNDJUHFG-HOTGVXAUSA-N neotame Chemical compound CC(C)(C)CCN[C@@H](CC(O)=O)C(=O)N[C@H](C(=O)OC)CC1=CC=CC=C1 HLIAVLHNDJUHFG-HOTGVXAUSA-N 0.000 abstract 3
- 235000019412 neotame Nutrition 0.000 abstract 3
- 108010070257 neotame Proteins 0.000 abstract 3
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 abstract 2
- AYRXSINWFIIFAE-SCLMCMATSA-N Isomaltose Natural products OC[C@H]1O[C@H](OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C=O)[C@@H](O)[C@@H](O)[C@@H]1O AYRXSINWFIIFAE-SCLMCMATSA-N 0.000 abstract 2
- DLRVVLDZNNYCBX-RTPHMHGBSA-N isomaltose Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1OC[C@@H]1[C@@H](O)[C@H](O)[C@@H](O)C(O)O1 DLRVVLDZNNYCBX-RTPHMHGBSA-N 0.000 abstract 2
- 239000000600 sorbitol Substances 0.000 abstract 2
- 238000001914 filtration Methods 0.000 abstract 1
- 239000004615 ingredient Substances 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 description 10
- 229910001220 stainless steel Inorganic materials 0.000 description 10
- 239000010935 stainless steel Substances 0.000 description 10
- 235000019605 sweet taste sensations Nutrition 0.000 description 9
- 238000002425 crystallisation Methods 0.000 description 6
- 230000008025 crystallization Effects 0.000 description 6
- 238000005516 engineering process Methods 0.000 description 6
- 239000002245 particle Substances 0.000 description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 5
- 238000009413 insulation Methods 0.000 description 5
- 239000005720 sucrose Substances 0.000 description 4
- 230000006872 improvement Effects 0.000 description 3
- 230000004048 modification Effects 0.000 description 3
- 238000012986 modification Methods 0.000 description 3
- 230000036541 health Effects 0.000 description 2
- 238000011031 large-scale manufacturing process Methods 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- TVXBFESIOXBWNM-UHFFFAOYSA-N Xylitol Natural products OCCC(O)C(O)C(O)CCO TVXBFESIOXBWNM-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 230000000295 complement effect Effects 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000011344 liquid material Substances 0.000 description 1
- HEBKCHPVOIAQTA-UHFFFAOYSA-N meso ribitol Natural products OCC(O)C(O)C(O)CO HEBKCHPVOIAQTA-UHFFFAOYSA-N 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000011343 solid material Substances 0.000 description 1
- 238000013112 stability test Methods 0.000 description 1
- 230000035922 thirst Effects 0.000 description 1
- 235000010447 xylitol Nutrition 0.000 description 1
- 239000000811 xylitol Substances 0.000 description 1
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 description 1
- 229960002675 xylitol Drugs 0.000 description 1
Images
Landscapes
- Seasonings (AREA)
Abstract
The invention relates to a composite sugar-free low-calorie sweetener and a manufacturing method thereof. The composite sugar-free low-calorie sweetener comprises the following ingredients by weight percent: 50-69 percent of dextrose monohydrate, 15-30 percent of sorbitol, 5-13 percent of isomaltose hypgather, 4-8 percent of maltodextrin and 0.7-4.32 percent of neotame. The technique comprises the following steps: respectively adding the maltodextrin and the neotame into a heating container, respectively adding deionized water for mixing, and rising temperature for dissolving; respectively adding active carbon into the solution, filtering with heat, and respectively collecting the filtrate into a storage tank; leading the mixed material after crushing the dextrose monohydrate, the sorbitol and the isomaltose hypgather to enter a bed from the bottom part of the spray fluidized bed by positive pressure and to flow from bottom to top in a speed-increasing manner, applying negative pressure on the upper part of the spraying fluidized bed to lead the spraying fluidized bed to vibrate from top to bottom so as to lead the material to boil from top to bottom in the bed, firstly spraying and dispersing the refined neotame solution continuously on fine sugar alcohol bodies by a multi-point spray gun of the side part of the fluidized bed, then pumping into the maltodextrin solution, continuously spraying and drying to obtain the sugar-free low-calorie sweetener. The sweetness of a product is 50-300 times of that of a common cane sugar.
Description
Technical field
The present invention relates to a kind of edible sweet taste material, relate in particular to a kind of composite sugar-free low-calorie sweetener and manufacture method thereof.
Background technology
Along with the increase of people because of too much bringing disease, people's demand safety, health, and the sweet low-sugar-content and low-calorie type sweet taste material of mouthfeel with sugar; The present invention reaches in production procedure from raw material and puts into the Advanced Manufacturing Technology that finished product one step finishes; It is learnt from other's strong points to offset one's weaknesses, has complementary advantages to make between the sugar alcohol sweet taste on the formula for a product, can play during product uses and cover the effect that promotes mouthfeel with synergy, people thirst for satisfying under the low prerequisite of sugariness height, heat, and occupation modeization, with cane-sugar taste roughly the same, the salubriouser safety and Health low-sugar-content and low-calorie type sweet taste material of mouthfeel.
Summary of the invention
The objective of the invention is to overcome the deficiency that prior art exists, a kind of composite low-sugar low-calorie sweetening agent and manufacture method thereof are provided, adopt the scientific technology of easy operation control, the molten speed of product, mouthfeel, local flavor, sugariness all are higher than the prior art optimum value.
Purpose of the present invention is achieved through the following technical solutions:
A kind of composite low-sugar low-calorie sweetening agent, characteristics are to comprise following composition (percentage by weight): Dextrose Monohydrate 50～69%, D-sorbite 15～30%, oligoisomaltose 5～13%, maltodextrin 4～8%, knob sweet 0.7～4.32%.
Further, above-mentioned a kind of composite sugar-free low-calorie sweetener, wherein, Dextrose Monohydrate 64.28%, D-sorbite 25%, oligoisomaltose 5%, maltodextrin 5%, knob sweet 0.72%.
The manufacture method of composite low-sugar low-calorie sweetening agent of the present invention comprises following processing step:
1. with maltodextrin, knob is sweet joins respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 50～80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned maltodextrin solution and the sweet solution of knob, be incubated 25～30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank of heat tracing;
4. with Dextrose Monohydrate, D-sorbite and oligoisomaltose are put in the spray-fluidized bed apparatus after pulverizing, with Dextrose Monohydrate, the mixed material of D-sorbite and oligoisomaltose enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body, pump into the above-mentioned maltodextrin solution that refines again, spray-drying obtains fluffy granular composite low-sugar low-calorie sweetening agent continuously.
Again further, the manufacture method of above-mentioned a kind of composite low-sugar low-calorie sweetening agent with maltodextrin, knob is sweet joins respectively in the heating container, adds deionized water respectively and mixes; Be warming up to 60～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank that has heat tracing; With Dextrose Monohydrate, D-sorbite and oligoisomaltose reach 120～180 orders through pulverizing, be sent in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, control fluidized-bed layer temperature is at 35～80 ℃, the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body, after the mixing of sugar alcohol fluidisation loses surperficial moisture content, pump into the above-mentioned maltodextrin solution that refines again, spray drying granulation obtains fluffy granular composite low-sugar low-calorie sweetening agent continuously.
Again further, the manufacture method of above-mentioned a kind of composite low-sugar low-calorie sweetening agent, the bed temperature scope of described fluidized bed with spraying is 35～80 ℃, wherein the bed temperature of the sweet spraying dispersion of phase I knob is 35～50 ℃, and the bed temperature of second stage maltodextrin mist projection granulating is 50～80 ℃.
Again further, the manufacture method of above-mentioned a kind of composite low-sugar low-calorie sweetening agent, in the phase I of described spraying mixed fluidized bed, the sweet spraying of knob is dispersed in fluidisation and smashes on the fine sugar alcohol crystal body; In second stage, the maltodextrin spray drying granulation is on the noncrystal of mixing sugar alcohol.
Substantive distinguishing features and obvious improvement that technical solution of the present invention is outstanding are mainly reflected in:
With Dextrose Monohydrate, D-sorbite, oligoisomaltose, knob is sweet is primary raw material, modifies uniformly and coats by preparation method to sugariness, makes product sweetness reach 50～300 times of common sucrose, products obtained therefrom does not have smell, do not have color, and is soluble in water.The negative pressure fluid bed fluidization technique that adopts scientific formula, uses advanced is in conjunction with the multi-point atomizing method, and time sharing segment control appliance bed temperature efficiently solves even dispersion, coats problems such as granulation, drying.This fluffy granular composite low-sugar low-calorie sweetening agent is easy to use, and its process for making science is simple and easy to operate, is fit to very much large-scale production.
Description of drawings
Below in conjunction with accompanying drawing technical solution of the present invention is described further:
Fig. 1: process chart of the present invention.
The specific embodiment
A kind of composite low-sugar low-calorie sweetening agent, its composition is: Dextrose Monohydrate 50～69%, D-sorbite 15～30%, oligoisomaltose 5～13%, maltodextrin 4～8%, knob sweet 0.7～4.32%.Ideal formulations is: Dextrose Monohydrate 64.28%, D-sorbite 25%, oligoisomaltose 5%, maltodextrin 5%, knob sweet 0.72%.
As shown in Figure 1, a kind of manufacturing process of composite low-sugar low-calorie sweetening agent: at first, with maltodextrin, knob is sweet joins respectively in the heating container, add deionized water respectively and mix; Be warming up to 50～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively in the sweet solution of above-mentioned maltodextrin solution and knob, be incubated 25～30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank of heat tracing; Then, with Dextrose Monohydrate, put into after D-sorbite and oligoisomaltose are pulverized in the spray-fluidized bed apparatus (heating temperature control and by the positive negative pressure boiling of equipment technology with the boiling that in fluid bed, circulates of sugar alcohol material, mix that fluidisation is anhydrated and fluffy processing, sugar alcohol mixtures material → malleation material quickens to flow from bottom to top → and negative pressure vibrates → makes material boiling up and down in fluid bed → by the fluid bed side multiple spot spray gun liquid material ejection fog-like liquid of naming a person for a particular job from top to bottom, be sprayed onto on the trickle solid material body of boiling), the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body, the bed temperature that the sweet spraying of control knob disperses is 35～50 ℃, and the sweet even spraying of knob is dispersed on the mixing sugar alcohol crystalline solid of powder; The rising bed temperature, at mixing sugar alcohol after fluidisation loses surface crystallization water, pump into the above-mentioned maltodextrin solution that refines again, continuous spray drying granulation, the bed temperature of maltodextrin mist projection granulating controlled well is 50～80 ℃, and the maltodextrin spray drying granulation is on the noncrystalline fluffy body of sugar alcohol; Obtain fluffy the shape product that even sugariness is modified.
Embodiment 1:
5 kilograms of maltodextrins and deionized water are dissolved in a stainless steel heating reaction pot for 20 kilograms, knob sweet 0.72 kilogram and deionized water are also dissolved in another stainless steel heating reaction pot for 20 kilograms, material is heated to 62 ℃ by chuck in the pot, start stirring, add 1 kilogram of active carbon respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; With 64.28 kilograms of Dextrose Monohydrates, 25 kilograms of D-sorbites, 5 kilograms of oligoisomaltoses, pulverizing reaches 130 orders through pulverizer, be sent in the spray-fluidized bed apparatus, Dextrose Monohydrate, the mixed material of D-sorbite and oligoisomaltose enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body, control fluidized-bed layer temperature is 35～50 ℃, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, at Dextrose Monohydrate, D-sorbite, after the mixing of oligoisomaltose alcohol fluidisation loses surface crystallization water, pump into the above-mentioned maltodextrin solution that refines, continuously spray drying granulation, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
Embodiment 2:
6 kilograms of maltodextrins and deionized water are dissolved in a stainless steel heating reaction pot for 21 kilograms, knob sweet 1.45 kilograms and deionized water are also dissolved in another stainless steel reaction pot for 24 kilograms, material is heated to 52 ℃ by chuck in the pot, start stirring, add 2 kilograms of active carbons respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; With 69 kilograms of Dextrose Monohydrates, 15 kilograms of D-sorbites, 8.55 kilograms of oligoisomaltoses, reach 150 orders through pulverizing, be sent to and carry out the fluidisation mixing in the spray-fluidized bed apparatus, Dextrose Monohydrate, the mixed material of D-sorbite and oligoisomaltose enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body, 35～40 ℃ of control fluidized-bed layer temperature, even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, after making the mixing of above-mentioned various sugar alcohol alcohol fluidisation lose surface crystallization water, pumping into the above-mentioned maltodextrin solution that refines, continuously spray granulating and drying, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
Embodiment 3:
7 kilograms of maltodextrins and deionized water are dissolved in a stainless steel heating reaction pot for 22 kilograms, knob sweet 2.16 kilograms and deionized water are also dissolved in another stainless steel heating reaction pot for 25 kilograms, material is heated to 60 ℃ by chuck in the pot, start stirring, add 3.0 kilograms of active carbons respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; With 63 kilograms of Dextrose Monohydrates, 20 kilograms of D-sorbites, 7.84 kilograms of oligoisomaltoses, pulverizing reaches 160 orders through pulverizer, be sent in the spray-fluidized bed apparatus, with Dextrose Monohydrate, the mixed material of D-sorbite and oligoisomaltose enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body, control 35～42 ℃ of fluidized-bed layer temperature well, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, after the mixing of above-mentioned various sugar alcohol alcohol fluidisations loses surface crystallization water, pump into the above-mentioned maltodextrin solution that refines, continuously spray drying granulation, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
Embodiment 4:
4 kilograms of Dextrose Monohydrates and deionized water are dissolved in a stainless steel heating reaction pot for 20 kilograms, 25 kilograms also another dissolves in stainless steel heating reaction pot with knob sweet 2.88 kilograms and deionized water, material is heated to 80 ℃ by chuck in the pot, start stirring, add 3.0 kilograms of active carbons respectively, be incubated 35 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; With 52 kilograms of Dextrose Monohydrates, 29 kilograms of D-sorbites, 12.12 kilograms of oligoisomaltoses, pulverizing reaches 180 orders through pulverizer, be sent to fluidisation in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body, control 35～50 ℃ of fluidized-bed layer temperature well, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, after above-mentioned various sugar alcohol alcohol fluidisations lose surface crystallization water, pumping into the above-mentioned maltodextrin solution that refines, the combination drying granulation of spraying continuously, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is adornd.
Embodiment 5:
8 kilograms of Dextrose Monohydrates and deionized water are dissolved in a stainless steel heating reaction pot for 25 kilograms, knob sweet 4.32 kilograms and deionized water are also dissolved in another stainless steel heating reaction pot for 29 kilograms, material is heated to 62 ℃ by chuck in the pot, start stirring, add 3 kilograms of active carbons respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; With 50 kilograms of Dextrose Monohydrates, 25.68 kilograms of D-sorbites, 12 kilograms of oligoisomaltoses, pulverizing reaches 130 orders through pulverizer, be sent in the spray-fluidized bed apparatus, with Dextrose Monohydrate, the mixed material of D-sorbite and oligoisomaltose enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body, control fluidized-bed layer temperature is 35～50 ℃, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, at xylitol, D-sorbite, after the mixing of oligoisomaltose alcohol fluidisation loses surface crystallization water, pump into the above-mentioned maltodextrin solution that refines, continuously spray drying granulation, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
After testing, the fluffy granular composite low-sugar low-calorie sweetening agent that adopts technical solution of the present invention to obtain, its main performance index sees Table 1.
Table 1
| Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 |
| Particle size | 30～60 orders | 30～60 orders | 30～60 orders | 30～60 orders | 30～60 orders |
| Sugariness (sucrose contrast) | 50 times | 100 times | 150 times | 200 times | 300 times |
| Outward appearance | White particle | White particle | White particle | White particle | White particle |
| Bulk density (g/mm 3) | ??0.60 | ??0.62 | ??0.63 | ??0.65 | ??0.66 |
The stability test of sweet taste material is to check the sweet taste material to guarantee the ability that undergoes no deterioration within a certain period of time, and the sweet taste material product of the embodiment of the invention was stored 3 years at normal temperatures, phenomenons such as rotten and sugariness reduction occur, and stability is very superior.
The sugariness degree of modification of fluffy granular composite low-sugar low-calorie sweetening agent of the present invention, according to the sweet adjustment in consumption of knob, in use unrestricted, usually select the common sucrose sugariness for use 50～300 times, the use needs that relatively are fit to food enterprise, form according to prescription, under same sugariness situation, people only are 1/50,1/300 of sucrose to the absorption of heat, low-sugar low-calorie sweetening agent is the sweet taste product of low-calorie, and this sweet taste material can not cause blood sugar to raise, satisfy three high crowds, the healthy people's of pursuit needs.
Show obviously that to sum up the present invention adopts scientific formula, uses advanced science and technology technology and method, products obtained therefrom does not have smell, do not have color, and is soluble in water, and it is very convenient that this fluffy granular low-sugar low-calorie sweetening agent is used.Granularity, molten speed, mouthfeel, sugariness all are much better than the prior art value, and the manufacturing process flow of science is simple and easy to do, are fit to very much large-scale production, are worth wide popularization and application in the field of business.
What need understand is: the above only is a preferred implementation of the present invention; for those skilled in the art; under the prerequisite that does not break away from the principle of the invention, can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (5)
1. a composite sugar-free low-calorie sweetener is characterized in that comprising following composition (percentage by weight): Dextrose Monohydrate 50～69%, D-sorbite 15～30%, oligoisomaltose 5～13%, maltodextrin 4～8%, knob sweet 0.7～4.32%.
2. a kind of composite sugar-free low-calorie sweetener according to claim 1 is characterized in that its component has following percentage by weight: Dextrose Monohydrate 64.28%, D-sorbite 25%, oligoisomaltose 5%, maltodextrin 5%, knob sweet 0.72%.
3. the manufacture method of the described a kind of composite sugar-free low-calorie sweetener of claim 1 is characterized in that: comprise following processing step---
1. with maltodextrin, knob is sweet joins respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 50～80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned maltodextrin solution and the sweet solution of knob, be incubated 25～30 minutes, filter while hot, filtrate is pooled in the storage tank of heat tracing stand-by respectively;
4. with Dextrose Monohydrate, D-sorbite and oligoisomaltose are put in the spray-fluidized bed apparatus after pulverizing, Dextrose Monohydrate, the mixed material of D-sorbite and oligoisomaltose enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body, pump into the above-mentioned maltodextrin solution that refines again, spray-drying obtains fluffy granular composite low-sugar low-calorie sweetening agent continuously.
4. the manufacture method of a kind of composite sugar-free low-calorie sweetener according to claim 3 is characterized in that: with maltodextrin, knob is sweet joins respectively in the container, add deionized water respectively and mix; Be warming up to 60～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank that has heat tracing; With Dextrose Monohydrate, D-sorbite and oligoisomaltose reach 120～180 orders through pulverizing, be sent in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, control fluidized-bed layer temperature is at 35～80 ℃, the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body, after the mixing of sugar alcohol fluidisation loses surperficial moisture content, pump into the above-mentioned maltodextrin solution that refines again, spray drying granulation obtains fluffy granular composite low-sugar low-calorie sweetening agent continuously.
5. the manufacture method of a kind of composite low-sugar low-calorie sweetening agent according to claim 4, it is characterized in that: the bed temperature scope of described fluidized bed with spraying is 35～80 ℃, wherein the bed temperature of the sweet spraying dispersion of phase I knob is 35～50 ℃, and the bed temperature of second stage maltodextrin mist projection granulating is 50～80 ℃.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200910249970A CN101810299B (en) | 2009-12-08 | 2009-12-08 | Composite sugar-free low-calorie sweetener and manufacturing method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200910249970A CN101810299B (en) | 2009-12-08 | 2009-12-08 | Composite sugar-free low-calorie sweetener and manufacturing method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101810299A true CN101810299A (en) | 2010-08-25 |
| CN101810299B CN101810299B (en) | 2012-09-05 |
Family
ID=42617790
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN200910249970A Expired - Fee Related CN101810299B (en) | 2009-12-08 | 2009-12-08 | Composite sugar-free low-calorie sweetener and manufacturing method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101810299B (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102424777A (en) * | 2011-12-20 | 2012-04-25 | 苏州工业园区尚融科技有限公司 | Production method for low-sugar grain alcohol fermentation beverage |
| EP2568816A4 (en) * | 2010-05-12 | 2015-09-16 | Cargill Inc | Sweetener compositions with reduced bitter off taste and methods of preparing |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20050208190A1 (en) * | 2004-03-16 | 2005-09-22 | Kraft Foods Holdings, Inc. | Method for drying neotame with co-agents |
| US20080069936A1 (en) * | 2006-09-18 | 2008-03-20 | ISON Renny | Cohesive non-free flowing sweeetener compositions containing a hygroscopic gluing agent and a desiccant |
-
2009
- 2009-12-08 CN CN200910249970A patent/CN101810299B/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2568816A4 (en) * | 2010-05-12 | 2015-09-16 | Cargill Inc | Sweetener compositions with reduced bitter off taste and methods of preparing |
| CN102424777A (en) * | 2011-12-20 | 2012-04-25 | 苏州工业园区尚融科技有限公司 | Production method for low-sugar grain alcohol fermentation beverage |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101810299B (en) | 2012-09-05 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101874599B (en) | Composite low-sugar low-calorie dining-table sweetener and preparation method thereof | |
| CN101897422A (en) | Fluffy granular compound low-sugar low-calorie sweetening agent and preparation method thereof | |
| CN101874591A (en) | Fluffy granular composite low-sugar and low-calorie sweetener and preparation method thereof | |
| CN101874592A (en) | Fluffy granular composite low-sugar and low-calorie table sweetener and preparation method thereof | |
| CN101874606A (en) | Fluffy granular composite sugar-free table sweetener and preparation method thereof | |
| CN101720911A (en) | Low-calorie dining table sweetener and production method thereof | |
| CN101874607B (en) | Granular composite low-sugar low-calorie sweetener and preparation method thereof | |
| CN101874596A (en) | Composite sugar-free sweetener and preparation method thereof | |
| CN101810302B (en) | Novel fluffy granular composite low-sugar low-calorie sweetening agent and preparing method thereof | |
| CN101874594A (en) | Fluffy granular composite sugar-free sweetener and preparation method thereof | |
| CN101874600B (en) | Granular composite low-sugar low-calorie dining table sweetener and preparation method thereof | |
| CN101874593A (en) | Fluffy granular composite sugar-free table sweetener and preparation method thereof | |
| CN101874604B (en) | Fluffy granular composite low-sugar and low-calorie sweetener and preparation method thereof | |
| CN101874602B (en) | Fluffy granular composite low-sugar and low-calorie table sweetener and preparation method thereof | |
| CN101810299B (en) | Composite sugar-free low-calorie sweetener and manufacturing method thereof | |
| CN101810309B (en) | Novel composite low-sugar low-calorie sweetener for dining table and manufacturing process thereof | |
| CN101874601B (en) | Granular composite low-sugar low-calorie table sweetner and preparation method thereof | |
| CN101810310B (en) | Table sweetener and manufacturing process thereof | |
| CN101897423A (en) | Granulated composite sugar-free table sweetener and preparation method thereof | |
| CN101810300B (en) | Composite low-sugar-content and low-calorie sweetening agent and manufacture method thereof | |
| CN101874605B (en) | Granular composite low-sugar low-calorie sweetner and preparation method thereof | |
| CN101810304A (en) | Novel low-sugar low-calorie table sweetener and manufacturing method thereof | |
| CN101810308B (en) | Low-sugar low-calorie table sweetener and manufacturing process thereof | |
| CN101897425B (en) | Fluffy granular composite low-sugar low-calorie table sweetener and preparation method thereof | |
| CN102415548A (en) | Fluffy powder particle composite low-sugar and low-calorie sweetener and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20120905 |