CN101897423A - Granulated composite sugar-free table sweetener and preparation method thereof - Google Patents
Granulated composite sugar-free table sweetener and preparation method thereof Download PDFInfo
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- CN101897423A CN101897423A CN2009102520457A CN200910252045A CN101897423A CN 101897423 A CN101897423 A CN 101897423A CN 2009102520457 A CN2009102520457 A CN 2009102520457A CN 200910252045 A CN200910252045 A CN 200910252045A CN 101897423 A CN101897423 A CN 101897423A
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Abstract
The invention relates to a granulated composite sugar-free table sweetener and a preparation method thereof. The granulated composite sugar-free table sweetener is prepared from the following components in percentage by weight: 20-30 percent of erythritol, 20-45 percent of sorbitol, 40-55 percent of isomaltooligosaccharide and 0.8-1.70 percent of sucralose. The process comprises the following steps of: respectively adding the 8% isomaltooligosaccharide and the sucralose to a heating container; respectively adding deionized water for mixing; increasing the temperature for dissolving; respectively adding active carbon in the solutions, filtering before cooling and respectively collecting filtrates in a storage tank; enabling the broken mixed material of the erythritol, the sorbitol and the isomaltooligosaccharide to enter a spraying fluidized bed from the bottom of the bed under positive pressure, flowing from bottom to top at an increased speed and applying negative pressure at the upper part of the spraying fluidized bed and vibrating from top to bottom so as to boil the material in the bed up and down; continuously spraying and dispersing the finely prepared sucralose solution to fine glycoside by a multi-point spray gun at one side of the fluidized bed; and pumping in the isomaltooligosaccharide solution and continuously spraying and drying to obtain the sugar-free table sweetener. The preparation flow is simple and convenient to operate.
Description
Technical field
The present invention relates to a kind of edible sweetener, relate in particular to a kind of fluffy granular composite sugar-free table sweetener and preparation method thereof.
Background technology
Along with the increase of people because of too much bringing disease, people's demand safety, health, and the sweet Sugarless type dining table sweetener of mouthfeel with sugar; The present invention reaches in production procedure from raw material and puts into the advanced preparation technology that finished product one step finishes; It is learnt from other's strong points to offset one's weaknesses, has complementary advantages to make between the sugar alcohol sweet taste on the formula for a product, can play during product uses and cover the effect that promotes mouthfeel with synergy, people thirst under the prerequisite that satisfies sugariness height, empty calory, and occupation modeization, with cane-sugar taste roughly the same, the salubriouser safety and Health Sugarless type dining table sweetener of mouthfeel.
Summary of the invention
The objective of the invention is to overcome the deficiency that prior art exists, a kind of granular composite sugar-free dining table sweetener and preparation method thereof is provided, adopt the scientific technology of easy operation control, the molten speed of product, mouthfeel, local flavor, sugariness all are higher than the prior art optimum value.
Purpose of the present invention is achieved through the following technical solutions:
Granular composite sugar-free dining table sweetener, characteristics are to comprise following composition (percentage by weight): antierythrite 20～30%, D-sorbite 20～45%, oligoisomaltose 40～55%, Sucralose 0.8～1.70%.
Further, above-mentioned granular composite sugar-free dining table sweetener, wherein, antierythrite 20%, D-sorbite 33.83%, oligoisomaltose 45%, Sucralose 1.17%.
The preparation method of granular composite sugar-free dining table sweetener of the present invention comprises following processing step:
1. 8% oligoisomaltose, Sucralose are joined respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 52～80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned oligoisomaltose solution and the sucralose solution, be incubated 25～30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank of heat tracing;
4. with antierythrite, D-sorbite and oligoisomaltose are put in the spray-fluidized bed apparatus after pulverizing, with antierythrite, the mixed material of D-sorbite and oligoisomaltose enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, pump into the above-mentioned oligoisomaltose solution that refines again, spray-drying obtains fluffy granular composite sugar-free table sweetener continuously.
Again further, the preparation method of above-mentioned granular composite sugar-free dining table sweetener joins 8% oligoisomaltose, Sucralose respectively in the heating container, adds deionized water respectively and mixes; Be warming up to 60～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank that has heat tracing; Antierythrite, D-sorbite and oligoisomaltose reach 120～180 orders through pulverizing, be sent in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, control fluidized-bed layer temperature is at 35～80 ℃, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, after the mixing of sugar alcohol fluidisation loses surperficial moisture content, pump into the above-mentioned oligoisomaltose solution that refines again, spray drying granulation obtains fluffy granular composite sugar-free table sweetener continuously.
Again further, the preparation method of above-mentioned granular composite sugar-free dining table sweetener, the bed temperature scope of described fluidized bed with spraying is 35～80 ℃, wherein the bed temperature of phase I Sucralose spraying dispersion is 35～50 ℃, and the bed temperature of second stage oligoisomaltose mist projection granulating is 50～80 ℃.
Again further, the preparation method of above-mentioned granular composite sugar-free dining table sweetener, in the phase I of described spraying mixed fluidized bed, the Sucralose spraying is dispersed in fluidisation and smashes on the fine sugar alcohol crystal body; In second stage, the oligoisomaltose spray drying granulation is on the noncrystal of mixing sugar alcohol.
Substantive distinguishing features and obvious improvement that technical solution of the present invention is outstanding are mainly reflected in:
The negative pressure fluid bed fluidization technique that adopts scientific formula, uses advanced is in conjunction with the multi-point atomizing method, and time sharing segment control appliance bed temperature efficiently solves even dispersion, coats problems such as granulation, drying.With antierythrite, D-sorbite, oligoisomaltose, Sucralose is primary raw material; modify uniformly and coat by preparation method to sugariness; make product sweetness reach 5～10 times of common sucrose; products obtained therefrom does not have smell, does not have color; soluble in water; this fluffy granular composite sugar-free table sweetener is easy to use, and its preparation process science is simple and easy to operate, is fit to very much large-scale production.
Description of drawings
Below in conjunction with accompanying drawing technical solution of the present invention is described further:
Fig. 1: process chart of the present invention.
The specific embodiment
Granular composite sugar-free dining table sweetener, its composition is: antierythrite 20～30%, D-sorbite 20～45%, oligoisomaltose 40～55%, Sucralose 0.8～1.70%.Ideal formulations is: antierythrite 20%, D-sorbite 33.83%, oligoisomaltose 45%, Sucralose 1.17%.
As shown in Figure 1, the preparation technology of granular composite sugar-free dining table sweetener: at first, 8% oligoisomaltose, Sucralose are joined respectively in the heating container, add deionized water respectively and mix; Be warming up to 52～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively in above-mentioned oligoisomaltose solution and the sucralose solution, be incubated 25～30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank of heat tracing; Then, with antierythrite, put into after D-sorbite and oligoisomaltose are pulverized in the spray-fluidized bed apparatus (heating temperature control and by the positive negative pressure boiling of equipment technology with the boiling that in fluid bed, circulates of sugar alcohol material, mix that fluidisation is anhydrated and fluffy processing, sugar alcohol mixtures material → malleation material quickens to flow from bottom to top → and negative pressure vibrates → makes material boiling up and down in fluid bed → by the fluid bed side multiple spot spray gun liquid material ejection fog-like liquid of naming a person for a particular job from top to bottom, be sprayed onto on the trickle solid material body of boiling), the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, the bed temperature that the spraying of control Sucralose disperses is 35～50 ℃, and the Sucralose even spraying is dispersed on the mixing sugar alcohol crystalline solid of powder; The rising bed temperature, at mixing sugar alcohol after fluidisation loses surface crystallization water, pump into the above-mentioned oligoisomaltose solution that refines again, continuous spray drying granulation, the bed temperature of oligoisomaltose mist projection granulating controlled well is 50～80 ℃, and the oligoisomaltose spray drying granulation is on the noncrystalline fluffy body of sugar alcohol; Obtain fluffy the shape product that even sugariness is modified.
Embodiment 1:
8 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel heating reaction pot for 20 kilograms, 0.83 kilogram of Sucralose and deionized water are also dissolved in another stainless steel heating reaction pot for 15 kilograms, material is heated to 62 ℃ by chuck in the pot, start stirring, add 1 kilogram of active carbon respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; With 24.17 kilograms of antierythrites, 25 kilograms of D-sorbites, 42 kilograms of oligoisomaltoses, pulverizing reaches 130 orders through pulverizer, be sent in the spray-fluidized bed apparatus, antierythrite, the mixed material of D-sorbite and oligoisomaltose enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, control fluidized-bed layer temperature is 35～50 ℃, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, at antierythrite, D-sorbite, after the mixing of oligoisomaltose alcohol fluidisation loses surface crystallization water, pump into the above-mentioned oligoisomaltose solution that refines, continuously spray drying granulation, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
Embodiment 2:
8 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel heating reaction pot for 20 kilograms, 1.17 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel reaction pot for 20 kilograms, material is heated to 52 ℃ by chuck in the pot, start stirring, add 2 kilograms of active carbons respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; With 20 kilograms of antierythrites, 33.83 kilograms of D-sorbites, 37 kilograms of oligoisomaltoses, reach 150 orders through pulverizing, be sent to and carry out the fluidisation mixing in the spray-fluidized bed apparatus, antierythrite, the mixed material of D-sorbite and oligoisomaltose enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, 35～40 ℃ of control fluidized-bed layer temperature, even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, after making the mixing of above-mentioned various sugar alcohol alcohol fluidisation lose surface crystallization water, pumping into the above-mentioned oligoisomaltose solution that refines, continuously spray granulating and drying, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
Embodiment 3:
8 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel heating reaction pot for 25 kilograms, 1 kilogram of Sucralose and deionized water are also dissolved in another stainless steel heating reaction pot for 20 kilograms, material is heated to 60 ℃ by chuck in the pot, start stirring, add 2.0 kilograms of active carbons respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; With 29 kilograms of antierythrites, 45 kilograms of D-sorbites, 17 kilograms of oligoisomaltoses, pulverizing reaches 160 orders through pulverizer, be sent in the spray-fluidized bed apparatus, with antierythrite, the mixed material of D-sorbite and oligoisomaltose enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, control 35～42 ℃ of fluidized-bed layer temperature well, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, after the mixing of above-mentioned various sugar alcohol alcohol fluidisations loses surface crystallization water, pump into the above-mentioned oligoisomaltose solution that refines, continuously spray drying granulation, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
Embodiment 4:
8 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel heating reaction pot for 20 kilograms, 25 kilograms also another dissolves in stainless steel heating reaction pot with 1.17 kilograms of Sucraloses and deionized water, material is heated to 80 ℃ by chuck in the pot, start stirring, add 2.0 kilograms of active carbons respectively, be incubated 35 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; With 30 kilograms of antierythrites, 28.83 kilograms of D-sorbites, 32 kilograms of oligoisomaltoses, pulverizing reaches 180 orders through pulverizer, be sent to fluidisation in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, control 35～50 ℃ of fluidized-bed layer temperature well, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, after above-mentioned various sugar alcohol alcohol fluidisations lose surface crystallization water, pumping into the above-mentioned oligoisomaltose solution that refines, the combination drying granulation of spraying continuously, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is adornd.
Embodiment 5:
8 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel heating reaction pot for 25 kilograms, 1.34 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel heating reaction pot for 20 kilograms, material is heated to 62 ℃ by chuck in the pot, start stirring, add 2 kilograms of active carbons respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; 28.66 kilograms of antierythrites, 20 kilograms of D-sorbites, 42 kilograms of oligoisomaltoses, pulverizing reaches 130 orders through pulverizer, be sent in the spray-fluidized bed apparatus, with antierythrite, the mixed material of D-sorbite and oligoisomaltose enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, control fluidized-bed layer temperature is 35～50 ℃, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, at antierythrite, D-sorbite, after the mixing of oligoisomaltose alcohol fluidisation loses surface crystallization water, pump into the above-mentioned oligoisomaltose solution that refines, continuously spray drying granulation, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
Embodiment 6:
8 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel heating reaction pot for 20 kilograms, 25 kilograms also another dissolves in stainless steel heating reaction pot with 1.66 kilograms of Sucraloses and deionized water, material is heated to 80 ℃ by chuck in the pot, start stirring, add 2.0 kilograms of active carbons respectively, be incubated 35 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; With 22 kilograms of antierythrites, 23.34 kilograms of D-sorbites, 45 kilograms of oligoisomaltoses, pulverizing reaches 180 orders through pulverizer, be sent to fluidisation in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, control 35～50 ℃ of fluidized-bed layer temperature well, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, after above-mentioned various sugar alcohol alcohol fluidisations lose surface crystallization water, pumping into the above-mentioned oligoisomaltose solution that refines, the combination drying granulation of spraying continuously, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is adornd.
After testing, the fluffy granular composite low-sugar and low-calorie sweetener that adopts technical solution of the present invention to obtain, its main performance index sees Table 1.
Table 1
| Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Embodiment 6 |
| Particle size | 30～60 orders | 30～60 orders | 30～60 orders | 30～60 orders | 30～60 orders | 30～60 orders |
| Sugariness (sucrose contrast) | 5 times | 7 times | 6 times | 7 times | 8 times | 10 times |
| Outward appearance | White particle | White particle | White particle | White particle | White particle | White particle |
| Bulk density (g/mm 3) | 0.60 | 0.62 | 0.63 | 0.66 | 0.60 | 0.64 |
The stability test of sweetener is to check sweetener to guarantee the ability that undergoes no deterioration within a certain period of time, and the sweetener product of the embodiment of the invention was stored 3 years at normal temperatures, phenomenons such as rotten and sugariness reduction occur, and stability is very superior.
The sugariness degree of modification of fluffy granular composite sugar-free table sweetener of the present invention, will be according to the adjustment of Sucralose in consumption, in use unrestricted, usually select the common sucrose sugariness for use 5～10 times, the use needs that relatively are fit to people, form according to prescription, under same sugariness situation, people are almost nil to the absorption of heat, Sugarless mensal sweetening material is the sweet taste product of low-calorie, this dining table sweetener can not cause blood sugar to raise, and does not participate in metabolism, not carious tooth, satisfy diabetes patient, three high crowds, pursue healthy people's needs.
Show obviously that to sum up the present invention adopts scientific formula, uses advanced science and technology technology and method, products obtained therefrom does not have smell, do not have color, and is soluble in water, and it is very convenient that this fluffy granule-shaped sugar-free dining table sweetener is used.Granularity, molten speed, mouthfeel, sugariness all are much better than the prior art value, and the scientific preparation process simple flow is easily gone, and are fit to very much large-scale production, are worth wide popularization and application in the field of business.
What need understand is: the above only is a preferred implementation of the present invention; for those skilled in the art; under the prerequisite that does not break away from the principle of the invention, can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (5)
1. granular composite sugar-free dining table sweetener is characterized in that comprising following composition (percentage by weight): antierythrite 20～30%, D-sorbite 20～45%, oligoisomaltose 40～55%, Sucralose 0.8～1.70%.
2. granular composite sugar-free dining table sweetener according to claim 1 is characterized in that its component has following percentage by weight: antierythrite 20%, D-sorbite 33.83%, oligoisomaltose 45%, Sucralose 1.17%.
3. the preparation method of the described granular composite sugar-free dining table sweetener of claim 1 is characterized in that: comprise following processing step---
1. 8% oligoisomaltose, Sucralose are joined respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 52～80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned maltodextrin solution and the sucralose solution, be incubated 25～30 minutes, filter while hot, filtrate is pooled in the storage tank of heat tracing stand-by respectively;
4. with antierythrite, D-sorbite and oligoisomaltose are put in the spray-fluidized bed apparatus after pulverizing, antierythrite, the mixed material of D-sorbite and oligoisomaltose enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, pump into the above-mentioned oligoisomaltose solution that refines again, spray-drying obtains fluffy granular composite sugar-free table sweetener continuously.
4. the preparation method of granular composite sugar-free dining table sweetener according to claim 3 is characterized in that: 8% oligoisomaltose, Sucralose are joined respectively in the container, add deionized water respectively and mix; Be warming up to 60～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank that has heat tracing; With antierythrite, D-sorbite and oligoisomaltose reach 120～180 orders through pulverizing, be sent in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, control fluidized-bed layer temperature is at 35～80 ℃, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, after the mixing of sugar alcohol fluidisation loses surperficial moisture content, pump into the above-mentioned oligoisomaltose solution that refines again, spray drying granulation obtains fluffy granular composite sugar-free table sweetener continuously.
5. the preparation method of granular composite sugar-free dining table sweetener according to claim 4, it is characterized in that: the bed temperature scope of described fluidized bed with spraying is 35～80 ℃, wherein the bed temperature of phase I Sucralose spraying dispersion is 35～50 ℃, and the bed temperature of second stage oligoisomaltose mist projection granulating is 50～80 ℃.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102423064A (en) * | 2011-12-15 | 2012-04-25 | 苏州工业园区尚融科技有限公司 | Composite sugar-free sweetener and preparation method thereof |
| CN102423063A (en) * | 2011-12-15 | 2012-04-25 | 苏州工业园区尚融科技有限公司 | Fluffy granular sugar-free sweetening material containing prebiotics xylooligosaccharide, and preparation method thereof |
| CN102599466A (en) * | 2012-03-09 | 2012-07-25 | 张维 | Granular sugar substitutes and preparation method thereof |
-
2009
- 2009-12-04 CN CN2009102520457A patent/CN101897423A/en active Pending
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102423064A (en) * | 2011-12-15 | 2012-04-25 | 苏州工业园区尚融科技有限公司 | Composite sugar-free sweetener and preparation method thereof |
| CN102423063A (en) * | 2011-12-15 | 2012-04-25 | 苏州工业园区尚融科技有限公司 | Fluffy granular sugar-free sweetening material containing prebiotics xylooligosaccharide, and preparation method thereof |
| CN102599466A (en) * | 2012-03-09 | 2012-07-25 | 张维 | Granular sugar substitutes and preparation method thereof |
| CN102599466B (en) * | 2012-03-09 | 2014-01-29 | 张维 | Granular sugar substitutes and preparation method thereof |
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Application publication date: 20101201 |