CN101874594A - Fluffy granular composite sugar-free sweetener and preparation method thereof - Google Patents
Fluffy granular composite sugar-free sweetener and preparation method thereof Download PDFInfo
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- CN101874594A CN101874594A CN2009102345994A CN200910234599A CN101874594A CN 101874594 A CN101874594 A CN 101874594A CN 2009102345994 A CN2009102345994 A CN 2009102345994A CN 200910234599 A CN200910234599 A CN 200910234599A CN 101874594 A CN101874594 A CN 101874594A
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- maltodextrin
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- fluidized bed
- sucralose
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- 235000003599 food sweetener Nutrition 0.000 title claims abstract description 37
- 239000003765 sweetening agent Substances 0.000 title claims abstract description 37
- 239000002131 composite material Substances 0.000 title claims abstract description 28
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 238000005507 spraying Methods 0.000 claims abstract description 42
- 229920002774 Maltodextrin Polymers 0.000 claims abstract description 38
- 235000019408 sucralose Nutrition 0.000 claims abstract description 37
- 239000005913 Maltodextrin Substances 0.000 claims abstract description 34
- 229940035034 maltodextrin Drugs 0.000 claims abstract description 34
- 239000004376 Sucralose Substances 0.000 claims abstract description 33
- BAQAVOSOZGMPRM-QBMZZYIRSA-N sucralose Chemical compound O[C@@H]1[C@@H](O)[C@@H](Cl)[C@@H](CO)O[C@@H]1O[C@@]1(CCl)[C@@H](O)[C@H](O)[C@@H](CCl)O1 BAQAVOSOZGMPRM-QBMZZYIRSA-N 0.000 claims abstract description 33
- 235000010447 xylitol Nutrition 0.000 claims abstract description 31
- TVXBFESIOXBWNM-UHFFFAOYSA-N Xylitol Natural products OCCC(O)C(O)C(O)CCO TVXBFESIOXBWNM-UHFFFAOYSA-N 0.000 claims abstract description 27
- 239000000463 material Substances 0.000 claims abstract description 27
- HEBKCHPVOIAQTA-UHFFFAOYSA-N meso ribitol Natural products OCC(O)C(O)C(O)CO HEBKCHPVOIAQTA-UHFFFAOYSA-N 0.000 claims abstract description 27
- 239000000811 xylitol Substances 0.000 claims abstract description 27
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 claims abstract description 27
- 229960002675 xylitol Drugs 0.000 claims abstract description 27
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 21
- 150000005846 sugar alcohols Chemical class 0.000 claims abstract description 20
- 239000008367 deionised water Substances 0.000 claims abstract description 14
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 14
- 239000000203 mixture Substances 0.000 claims abstract description 14
- 239000007921 spray Substances 0.000 claims abstract description 13
- 238000010438 heat treatment Methods 0.000 claims abstract description 12
- 239000000706 filtrate Substances 0.000 claims abstract description 10
- 238000002156 mixing Methods 0.000 claims abstract description 10
- 238000001694 spray drying Methods 0.000 claims abstract description 10
- 238000003860 storage Methods 0.000 claims abstract description 10
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000012530 fluid Substances 0.000 claims description 22
- 238000009835 boiling Methods 0.000 claims description 13
- 238000005243 fluidization Methods 0.000 claims description 12
- 238000005469 granulation Methods 0.000 claims description 9
- 230000003179 granulation Effects 0.000 claims description 9
- 238000003756 stirring Methods 0.000 claims description 9
- 238000010298 pulverizing process Methods 0.000 claims description 8
- 239000003595 mist Substances 0.000 claims description 7
- 229910052799 carbon Inorganic materials 0.000 claims description 6
- 238000010792 warming Methods 0.000 claims description 5
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- DLRVVLDZNNYCBX-RTPHMHGBSA-N isomaltose Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1OC[C@@H]1[C@@H](O)[C@H](O)[C@@H](O)C(O)O1 DLRVVLDZNNYCBX-RTPHMHGBSA-N 0.000 abstract 2
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- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 5
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 5
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Abstract
The invention relates to a fluffy granular composite sugar-free sweetener and a preparation method. The sweetener comprises the following components: 40-60% of xylitol, 20-28% of isomaltooligosaccharide, 3-5% of maltodextrin and 8-35.5% of sucralose. The process comprises the following steps: respectively adding the maltodextrin and the sucralose to a heating container and respectively adding deionized water for mixing; raising the temperature until dissolution; adding activated carbon to the solution respectively, filtering the mixture while the mixture is hot and collecting the filtrates respectively in storage tanks; and pumping the ground mixture of the xylitol and the isomaltooligosaccharide into a fluidized bed with spraying from the bottom of the bed under positive pressure and ensuring the mixture to flow at high speed from bottom to top, applying negative pressure to the upper part of the fluidized bed with spraying so that the bed vibrates from top to bottom to ensure the materials to boil in the bed; using a multipoint spray gun at the side of the fluidized bed to continuously spray and disperse the refined sucralose solution on superfine sugar alcohols, then pumping the maltodextrin solution and carrying out continuous spray drying, thus obtaining the fluffy granular composite sugar-free sweetener. The preparation flow is simple and convenient and easy to operate and is suitable for scale production.
Description
Technical field
The present invention relates to a kind of edible sweetener, relate in particular to a kind of fluffy granular composite sugar-free sweetener and preparation method thereof.
Background technology
Along with the increase of people because of too much bringing disease with sugar, people's demand safety, the healthy Sugarless type non-nutritive sweetener that does not participate in body metabolism; In production procedure, reach from raw material and put into the advanced preparation technology that finished product one step finishes; It is learnt from other's strong points to offset one's weaknesses, has complementary advantages to make between the sugar alcohol sweet taste on the formula for a product, can play during product uses and cover the effect that promotes mouthfeel with synergy, people thirst for satisfying under the low prerequisite of sugariness height, heat, and occupation modeization, with cane-sugar taste safety and Health Sugarless type sweetener roughly the same.
Summary of the invention
The objective of the invention is to overcome the deficiency that prior art exists, a kind of fluffy granular composite sugar-free sweetener and preparation method thereof is provided, adopt the scientific technology of easy operation control, the molten speed of product, mouthfeel, sugariness all are higher than the prior art optimum value.
Purpose of the present invention is achieved through the following technical solutions:
Fluffy granular composite sugar-free sweetener, characteristics are to comprise following composition (percentage by weight): xylitol 40～60%, oligoisomaltose 20～28%, maltodextrin 3～5%, Sucralose 8～35.5%.
Further, above-mentioned fluffy granular composite sugar-free sweetener, wherein, xylitol 41%, oligoisomaltose 20%, maltodextrin 4%, Sucralose 35%.
Further, above-mentioned fluffy granular composite sugar-free sweetener, described maltodextrin DE value is 10～20.
The preparation method of fluffy granular composite sugar-free sweetener of the present invention comprises following processing step:
1. maltodextrin, Sucralose are joined respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 52～78 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned maltodextrin solution and the sucralose solution, be incubated 25～30 minutes, filter while hot, filtrate is pooled in the storage tank of heat tracing stand-by respectively;
4. will put in the spray-fluidized bed apparatus after xylitol and the oligoisomaltose pulverizing, the mixed material of xylitol and oligoisomaltose enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, pump into the above-mentioned maltodextrin solution that refines again, spray-drying obtains fluffy granular composite sugar-free sweetener continuously.
Again further, the preparation method of above-mentioned fluffy granular composite sugar-free sweetener joins maltodextrin, Sucralose respectively in the container, adds deionized water respectively and mixes; Be warming up to 60～70 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank that has heat tracing; Xylitol and oligoisomaltose reach 120～180 orders through pulverizing, be sent in the spray-fluidized bed apparatus, the mixed material of xylitol and oligoisomaltose enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, control fluidized-bed layer temperature is at 35～80 ℃, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, after the mixing of sugar alcohol fluidisation loses surperficial moisture content, pump into the above-mentioned maltodextrin solution that refines again, spray drying granulation obtains fluffy granular composite sugar-free sweetener continuously.
Again further, the preparation method of above-mentioned fluffy granular composite sugar-free sweetener, the bed temperature scope of described fluidized bed with spraying is 35～80 ℃, wherein the bed temperature of phase I Sucralose spraying dispersion is 35～50 ℃, and the bed temperature of second stage maltodextrin mist projection granulating is 50～80 ℃.
Again further, the preparation method of above-mentioned fluffy granular composite sugar-free sweetener, in the phase I of described spraying mixed fluidized bed, the Sucralose spraying is dispersed in fluidisation and smashes on the fine sugar alcohol crystal body; In second stage, the maltodextrin spray drying granulation is on the noncrystal of mixing sugar alcohol.
Substantive distinguishing features and obvious improvement that technical solution of the present invention is outstanding are mainly reflected in:
The present invention adopts the negative pressure fluid bed fluidization technique of scientific formula, uses advanced in conjunction with the multi-point atomizing method, and time sharing segment control appliance bed temperature efficiently solves even dispersion, coats problems such as granulation, drying.With xylitol, oligoisomaltose, Sucralose is primary raw material; modify uniformly and coat by preparation method to sugariness; make product sweetness reach 50～200 times of common sucrose; products obtained therefrom does not have smell, does not have color; soluble in water; this fluffy granular composite sugar-free sweetener is easy to use, and its preparation process science is simple and easy to operate, is fit to very much large-scale production.
Description of drawings
Below in conjunction with accompanying drawing technical solution of the present invention is described further:
Fig. 1: process chart of the present invention.
The specific embodiment
Fluffy granular composite sugar-free sweetener of the present invention, its composition is: xylitol 40～60%, oligoisomaltose 20～28%, maltodextrin 3～5%, Sucralose 8～35.5%.Ideal formulations is: xylitol 41%, oligoisomaltose 20%, maltodextrin 4%, Sucralose 35%.Wherein, maltodextrin DE value is 10～20.
As shown in Figure 1, the preparation technology of fluffy granular composite sugar-free sweetener: at first, maltodextrin, Sucralose are joined respectively in the heating container, add deionized water respectively and mix; Be warming up to 52～78 ℃ of dissolvings respectively, and stir; Add active carbon in above-mentioned maltodextrin solution and the sucralose solution respectively, be incubated 25～30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank of heat tracing; At last, put into after xylitol and oligoisomaltose pulverized in the spray-fluidized bed apparatus (heating temperature control and by the positive negative pressure boiling of equipment technology with the boiling that in fluid bed, circulates of sugar alcohol material, mix that fluidisation is anhydrated and fluffy processing, sugar alcohol mixtures material → malleation material quickens to flow from bottom to top → and negative pressure vibrates → makes material boiling up and down in fluid bed → by the fluid bed side multiple spot spray gun liquid material ejection fog-like liquid of naming a person for a particular job from top to bottom, be sprayed onto on the trickle solid material body of boiling), the mixed material of xylitol and oligoisomaltose enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, the bed temperature that the spraying of control Sucralose disperses is 35～50 ℃, and the Sucralose even spraying is dispersed on the mixing sugar alcohol crystalline solid of powder; The rising bed temperature, at mixing sugar alcohol after fluidisation loses surface crystallization water, pump into the above-mentioned maltodextrin solution that refines again, continuous spray drying granulation, the bed temperature of maltodextrin mist projection granulating controlled well is 50～80 ℃, and the maltodextrin spray drying granulation is on the noncrystalline fluffy body of sugar alcohol; Obtain fluffy the shape product that even sugariness is modified.
Embodiment 1:
3.2 kilograms of maltodextrins and deionized water are dissolved in a stainless steel heating reaction pot for 25 kilograms, 8.8 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel heating reaction pot for 25 kilograms, material is heated to 67 ℃ by chuck in the pot, start stirring, add 0.5 kilogram of active carbon respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; 60 kilograms of xylitols, 28 kilograms of oligoisomaltose alcohol, pulverizing reaches 180 orders through pulverizer, be sent in the spray-fluidized bed apparatus, the mixed material of xylitol and oligoisomaltose enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, control fluidized-bed layer temperature is 35～50 ℃, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50～55 ℃ again, at xylitol, after the mixing of oligoisomaltose alcohol fluidisation loses surface crystallization water, pump into the above-mentioned maltodextrin solution that refines, continuous spray drying granulation is controlled air quantity and mist flow well, obtains the fluffy granular product that even sugariness is modified.
Embodiment 2:
4.5 kilograms of maltodextrins and deionized water are dissolved in a stainless steel heating reaction pot for 20 kilograms, 17.5 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel reaction pot for 30 kilograms, material is heated to 70 ℃ by chuck in the pot, start stirring, add 1.5 kilograms of active carbons respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; 54 kilograms of xylitols, 24 kilograms of oligoisomaltose alcohol, reach 180 orders through pulverizing, be sent to and carry out the fluidisation mixing in the spray-fluidized bed apparatus, the mixed material of xylitol and oligoisomaltose enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, 35～40 ℃ of control fluidized-bed layer temperature, even spraying is disperseed, after operation is finished, improve bed temperature to 50～75 ℃ again, make xylitol, after the mixing of oligoisomaltose alcohol fluidisation loses surface crystallization water, pumping into the above-mentioned maltodextrin solution that refines, continuous spray granulating and drying is controlled air quantity and mist flow well, obtains the fluffy granular product that even sugariness is modified.
Embodiment 3:
3.5 kilograms of maltodextrins and deionized water are dissolved in a stainless steel heating reaction pot for 30 kilograms, 26.5 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel heating reaction pot for 40 kilograms, material is heated to 65 ℃ by chuck in the pot, start stirring, add 3.0 kilograms of active carbons respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; 50 kilograms of xylitols, 20 kilograms of oligoisomaltoses, pulverizing reaches 170 orders through pulverizer, be sent in the spray-fluidized bed apparatus, the mixed material of xylitol and oligoisomaltose enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, control 35～42 ℃ of fluidized-bed layer temperature well, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, at xylitol, after the mixing of oligoisomaltose fluidisation loses surface crystallization water, pump into the above-mentioned maltodextrin solution that refines, continuous spray drying granulation is controlled air quantity and mist flow well, obtains the fluffy granular product that even sugariness is modified.
Embodiment 4:
4 kilograms of maltodextrins and deionized water are dissolved in a stainless steel heating reaction pot for 40 kilograms, 60 kilograms also another dissolves in stainless steel heating reaction pot with 35 kilograms of Sucraloses and deionized water, material is heated to 60 ℃ by chuck in the pot, start stirring, add 3.0 kilograms of active carbons respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; 41 kilograms of xylitols, 20 kilograms of oligoisomaltose alcohol, pulverizing reaches 150 orders through pulverizer, be sent to fluidisation in the spray-fluidized bed apparatus, the mixed material of xylitol and oligoisomaltose enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, control 35～40 ℃ of fluidized-bed layer temperature well, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50～78 ℃ again, at xylitol, after the oligoisomaltose fluidisation loses surface crystallization water, pumping into the above-mentioned maltodextrin solution that refines, air quantity and mist flow are controlled in continuously spraying combination drying granulation well, obtain the fluffy granular product that even sugariness is adornd.
After testing, the fluffy granular composite sugar-free sweetener that adopts technical solution of the present invention to obtain, its main performance index sees Table 1.
Table 1
| Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 |
| Particle size | 30～60 orders | 30～60 orders | 30～60 orders | 30～60 orders |
| Sugariness (sucrose contrast) | 50 times | 100 times | 150 times | 200 times |
| Outward appearance | White particle | White particle | White particle | White particle |
| Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 |
| Bulk density (g/mm 3) | ??0.58 | ??0.62 | ??0.63 | ??0.66 |
The stability test of sweetener is to check sweetener to guarantee the ability that undergoes no deterioration within a certain period of time, and the sweetener product of the embodiment of the invention was stored 3 years at normal temperatures, phenomenons such as rotten and sugariness reduction occur, and stability is very superior.
The sugariness degree of modification of fluffy granular composite sugar-free sweetener of the present invention, with according to the adjustment of Sucralose in the food consumption adds, usually select the common sucrose sugariness for use 50～200 times, relatively be fit to the food enterprise needs, form according to prescription, under same sugariness situation, people only are 1/50～1/200 of common sucrose to the absorption of heat, sugar-free sweetener is the sweet taste product of low-calorie, the metabolism of this sweetener does not need insulin, can not cause blood sugar to raise, be suitable for diabetes, three high crowds' needs.
Show obviously that to sum up the present invention adopts scientific formula, uses advanced science and technology technology and method, products obtained therefrom does not have smell, do not have color, and is soluble in water, and it is very convenient that this fluffy granule-shaped sugar-free sweetener is used.Granularity, molten speed, mouthfeel, sugariness all are much better than the prior art value, and the scientific preparation process simple flow is easily gone, and are fit to very much large-scale production, are worth wide popularization and application in the field of business.
What need understand is: the above only is a preferred implementation of the present invention; for those skilled in the art; under the prerequisite that does not break away from the principle of the invention, can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (6)
1. fluffy granular composite sugar-free sweetener is characterized in that comprising following composition (percentage by weight): xylitol 40～60%, oligoisomaltose 20～28%, maltodextrin 3～5%, Sucralose 8～35.5%.
2. fluffy granular composite sugar-free sweetener according to claim 1 is characterized in that its component has following percentage by weight: xylitol 41%, oligoisomaltose 20%, maltodextrin 4%, Sucralose 35%.
3. fluffy granular composite sugar-free sweetener according to claim 1 and 2 is characterized in that: described maltodextrin DE value is 10～20.
4. the preparation method of the described fluffy granular composite sugar-free sweetener of claim 1 is characterized in that: comprise following processing step---
1. maltodextrin, Sucralose are joined respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 52～78 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned maltodextrin solution and the sucralose solution, be incubated 25～30 minutes, filter while hot, filtrate is pooled in the storage tank of heat tracing stand-by respectively;
4. will put in the spray-fluidized bed apparatus after xylitol and the oligoisomaltose pulverizing, the mixed material of xylitol and oligoisomaltose enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, pump into the above-mentioned maltodextrin solution that refines again, spray-drying obtains fluffy granular composite sugar-free sweetener continuously.
5. the preparation method of fluffy granular composite sugar-free sweetener according to claim 4 is characterized in that: maltodextrin, Sucralose are joined respectively in the container, add deionized water respectively and mix; Be warming up to 60～70 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank that has heat tracing; Xylitol and oligoisomaltose reach 120～180 orders through pulverizing, be sent in the spray-fluidized bed apparatus, the mixed material of xylitol and oligoisomaltose enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, control fluidized-bed layer temperature is at 35～80 ℃, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, after the mixing of sugar alcohol fluidisation loses surperficial moisture content, pump into the above-mentioned maltodextrin solution that refines again, spray drying granulation obtains fluffy granular composite sugar-free sweetener continuously.
6. the preparation method of fluffy granular composite sugar-free sweetener according to claim 5, it is characterized in that: the bed temperature scope of described fluidized bed with spraying is 35～80 ℃, wherein the bed temperature of phase I Sucralose spraying dispersion is 35～50 ℃, and the bed temperature of second stage maltodextrin mist projection granulating is 50～80 ℃.
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102415549A (en) * | 2011-12-15 | 2012-04-18 | 苏州工业园区尚融科技有限公司 | Compound sugar-free sweetener and preparation method thereof |
| CN102429205A (en) * | 2011-12-20 | 2012-05-02 | 苏州工业园区尚融科技有限公司 | Compound low-sugar sweetener and preparation method thereof |
| CN102960694A (en) * | 2012-11-30 | 2013-03-13 | 苏州工业园区尚融科技有限公司 | Compound sweetening agent applicable to coffee and preparation method thereof |
| CN103766697A (en) * | 2014-01-07 | 2014-05-07 | 长春禾甜科技有限责任公司 | Sugar-free sweetener and preparation method thereof |
| CN111084384A (en) * | 2019-12-30 | 2020-05-01 | 湖南点道生物科技有限公司 | Compound carbohydrate component and preparation method thereof |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1099846C (en) * | 1999-12-09 | 2003-01-29 | 北京恒毅利科贸有限责任公司 | Method for preparing granular flavouring enriched food and its product |
| CN101181050B (en) * | 2007-12-19 | 2011-12-28 | 苏州苏克瑞甜品科技有限公司 | Sucrose succedaneum and preparation method thereof |
| CN101253968B (en) * | 2008-04-15 | 2011-12-28 | 苏州苏克瑞甜品科技有限公司 | Granular sugar-free sweetening agent and method of preparing the same |
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2009
- 2009-11-24 CN CN2009102345994A patent/CN101874594B/en not_active Expired - Fee Related
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102415549A (en) * | 2011-12-15 | 2012-04-18 | 苏州工业园区尚融科技有限公司 | Compound sugar-free sweetener and preparation method thereof |
| CN102429205A (en) * | 2011-12-20 | 2012-05-02 | 苏州工业园区尚融科技有限公司 | Compound low-sugar sweetener and preparation method thereof |
| CN102960694A (en) * | 2012-11-30 | 2013-03-13 | 苏州工业园区尚融科技有限公司 | Compound sweetening agent applicable to coffee and preparation method thereof |
| CN103766697A (en) * | 2014-01-07 | 2014-05-07 | 长春禾甜科技有限责任公司 | Sugar-free sweetener and preparation method thereof |
| CN111084384A (en) * | 2019-12-30 | 2020-05-01 | 湖南点道生物科技有限公司 | Compound carbohydrate component and preparation method thereof |
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