CN101874597A - Fluffy granular composite sugar-free sweetener and preparation method thereof - Google Patents
Fluffy granular composite sugar-free sweetener and preparation method thereof Download PDFInfo
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- CN101874597A CN101874597A CN2009102520368A CN200910252036A CN101874597A CN 101874597 A CN101874597 A CN 101874597A CN 2009102520368 A CN2009102520368 A CN 2009102520368A CN 200910252036 A CN200910252036 A CN 200910252036A CN 101874597 A CN101874597 A CN 101874597A
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Abstract
The invention relates to a fluffy granular composite sugar-free sweetener and a preparation method. The sweetener comprises the following components: 20-33% of erythritol, 8-20% of xylitol, 47-70% of isomaltooligosaccharide and 0.6-4.5% of neotame. The process comprises the following steps: respectively adding 10% of isomaltooligosaccharide and the neotame to a heating container and respectively adding deionized water for mixing; raising the temperature until dissolution; adding activated carbon to the solution respectively, filtering the mixture while the mixture is hot and collecting the filtrates respectively in storage tanks; and pumping the ground mixture of the erythritol, the xylitol and the isomaltooligosaccharide into a fluidized bed with spraying from the bottom of the bed under positive pressure and ensuring the mixture to flow at high speed from bottom to top, applying negative pressure to the upper part of the fluidized bed with spraying so that the bed vibrates from top to bottom to ensure the materials to boil in the bed; using a multipoint spray gun at the side of the fluidized bed to continuously spray and disperse the refined neotame solution on superfine sugar alcohols, then pumping the isomaltooligosaccharide solution and carrying out continuous spray drying, thus obtaining the sugar-free sweetener. The preparation flow is simple and convenient and easy to operate and the sweetness of the product is 50-300 times that of the common sucrose.
Description
Technical field
The present invention relates to a kind of edible sweetener, relate in particular to a kind of fluffy granular composite sugar-free sweetener and preparation method thereof.
Background technology
Along with the increase of people because of too much bringing disease, people's demand safety, health, and the sweet Sugarless type sweetener of mouthfeel with sugar; The present invention reaches in production procedure from raw material and puts into the advanced preparation technology that finished product one step finishes; It is learnt from other's strong points to offset one's weaknesses, has complementary advantages to make between the sugar alcohol sweet taste on the formula for a product, can play during product uses and cover the effect that promotes mouthfeel with synergy, people thirst under the prerequisite that satisfies sugariness height, empty calory, and occupation modeization, with cane-sugar taste roughly the same, the salubriouser safety and Health Sugarless type sweetener of mouthfeel.
Summary of the invention
The objective of the invention is to overcome the deficiency that prior art exists, a kind of fluffy granular composite sugar-free sweetener and preparation method thereof is provided, adopt the scientific technology of easy operation control, the molten speed of product, mouthfeel, local flavor, sugariness all are higher than the prior art optimum value.
Purpose of the present invention is achieved through the following technical solutions:
Fluffy granular composite sugar-free sweetener, characteristics are to comprise following composition (percentage by weight): antierythrite 20～33%, xylitol 8～20%, oligoisomaltose 47～70%, knob sweet 0.6～4.5%.
Further, above-mentioned fluffy granular composite sugar-free sweetener, wherein, antierythrite 20%, xylitol 9.28%, oligoisomaltose 70%, knob sweet 0.72%.
The preparation method of fluffy granular composite sugar-free sweetener of the present invention comprises following processing step:
1. with 10% oligoisomaltose, knob is sweet joins respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 52～80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned oligoisomaltose solution and the sweet solution of knob, be incubated 25～30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank of heat tracing;
4. with antierythrite, xylitol and oligoisomaltose are put in the spray-fluidized bed apparatus after pulverizing, with antierythrite, the mixed material of xylitol and oligoisomaltose enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body, pump into the above-mentioned oligoisomaltose solution that refines again, spray-drying obtains fluffy granular composite sugar-free sweetener continuously.
Again further, the preparation method of above-mentioned fluffy granular composite sugar-free sweetener joins 10% oligoisomaltose, Sucralose respectively in the heating container, adds deionized water respectively and mixes; Be warming up to 60～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank that has heat tracing; Antierythrite, xylitol and oligoisomaltose reach 120～180 orders through pulverizing, be sent in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, control fluidized-bed layer temperature is at 35～80 ℃, the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body, after the mixing of sugar alcohol fluidisation loses surperficial moisture content, pump into the above-mentioned oligoisomaltose solution that refines again, spray drying granulation obtains fluffy granular composite sugar-free sweetener continuously.
Again further, the preparation method of above-mentioned fluffy granular composite sugar-free sweetener, the bed temperature scope of described fluidized bed with spraying is 35～80 ℃, wherein the bed temperature of the sweet spraying dispersion of phase I knob is 35～50 ℃, and the bed temperature of second stage oligoisomaltose mist projection granulating is 50～80 ℃.
Again further, the preparation method of above-mentioned fluffy granular composite sugar-free sweetener, in the phase I of described spraying mixed fluidized bed, the sweet spraying of knob is dispersed in fluidisation and smashes on the fine sugar alcohol crystal body; In second stage, the oligoisomaltose spray drying granulation is on the noncrystal of mixing sugar alcohol.
Substantive distinguishing features and obvious improvement that technical solution of the present invention is outstanding are mainly reflected in:
The negative pressure fluid bed fluidization technique that adopts scientific formula, uses advanced is in conjunction with the multi-point atomizing method, and time sharing segment control appliance bed temperature efficiently solves even dispersion, coats problems such as granulation, drying.With antierythrite, xylitol, oligoisomaltose, knob is sweet is primary raw material; modify uniformly and coat by preparation method to sugariness; make product sweetness reach 50～300 times of common sucrose; products obtained therefrom does not have smell, does not have color; soluble in water; this fluffy granular composite sugar-free sweetener is easy to use, and its preparation process science is simple and easy to operate, is fit to very much large-scale production.
Description of drawings
Below in conjunction with accompanying drawing technical solution of the present invention is described further:
Fig. 1: process chart of the present invention.
The specific embodiment
Fluffy granular composite sugar-free sweetener of the present invention, its composition is: antierythrite 20～33%, xylitol 8～20%, oligoisomaltose 47～70%, knob sweet 0.6～4.5%.Ideal formulations is: antierythrite 20%, xylitol 9.28%, oligoisomaltose 70%, knob sweet 0.72%.
As shown in Figure 1, the preparation technology of fluffy granular composite sugar-free sweetener: at first, with 10% oligoisomaltose, knob is sweet joins respectively in the heating container, add deionized water respectively and mix; Be warming up to 52～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively in above-mentioned oligoisomaltose solution and the sweet solution of knob, be incubated 25～30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank of heat tracing; Then, with antierythrite, put into after xylitol and oligoisomaltose are pulverized in the spray-fluidized bed apparatus (heating temperature control and by the positive negative pressure boiling of equipment technology with the boiling that in fluid bed, circulates of sugar alcohol material, mix that fluidisation is anhydrated and fluffy processing, sugar alcohol mixtures material → malleation material quickens to flow from bottom to top → and negative pressure vibrates → makes material boiling up and down in fluid bed → by the fluid bed side multiple spot spray gun liquid material ejection fog-like liquid of naming a person for a particular job from top to bottom, be sprayed onto on the trickle solid material body of boiling), the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body, the bed temperature that the sweet spraying of control knob disperses is 35～50 ℃, and the sweet even spraying of knob is dispersed on the mixing sugar alcohol crystalline solid of powder; The rising bed temperature, at mixing sugar alcohol after fluidisation loses surface crystallization water, pump into the above-mentioned oligoisomaltose solution that refines again, continuous spray drying granulation, the bed temperature of oligoisomaltose mist projection granulating controlled well is 50～80 ℃, and the oligoisomaltose spray drying granulation is on the noncrystalline fluffy body of sugar alcohol; Obtain fluffy the shape product that even sugariness is modified.
Embodiment 1:
10 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel heating reaction pot for 26 kilograms, knob sweet 0.72 kilogram and deionized water are also dissolved in another stainless steel heating reaction pot for 18 kilograms, material is heated to 62 ℃ by chuck in the pot, start stirring, add 1 kilogram of active carbon respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; With 20 kilograms of antierythrites, 9.28 kilograms of xylitols, 60 kilograms of oligoisomaltoses, pulverizing reaches 130 orders through pulverizer, be sent in the spray-fluidized bed apparatus, antierythrite, the mixed material of xylitol and oligoisomaltose enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body, control fluidized-bed layer temperature is 35～50 ℃, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, at antierythrite, xylitol, after the mixing of oligoisomaltose alcohol fluidisation loses surface crystallization water, pump into the above-mentioned oligoisomaltose solution that refines, continuously spray drying granulation, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
Embodiment 2:
10 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel heating reaction pot for 26 kilograms, knob sweet 1.44 kilograms and deionized water are also dissolved in another stainless steel reaction pot for 22 kilograms, material is heated to 52 ℃ by chuck in the pot, start stirring, add 2 kilograms of active carbons respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; With 30 kilograms of antierythrites, 13.56 kilograms of xylitols, 45 kilograms of oligoisomaltoses, reach 150 orders through pulverizing, be sent to and carry out the fluidisation mixing in the spray-fluidized bed apparatus, antierythrite, the mixed material of xylitol and oligoisomaltose enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body, 35～40 ℃ of control fluidized-bed layer temperature, even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, after making above-mentioned various sugar alcohol fluidisation mixing lose surface crystallization water, pumping into the above-mentioned oligoisomaltose solution that refines, continuously spray granulating and drying, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
Embodiment 3:
10 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel heating reaction pot for 26 kilograms, knob sweet 2.16 kilograms and deionized water are also dissolved in another stainless steel heating reaction pot for 23 kilograms, material is heated to 60 ℃ by chuck in the pot, start stirring, add 2.0 kilograms of active carbons respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; With 27 kilograms of antierythrites, 17.84 kilograms of xylitols, 43 kilograms of oligoisomaltoses, pulverizing reaches 160 orders through pulverizer, be sent in the spray-fluidized bed apparatus, with antierythrite, the mixed material of xylitol and oligoisomaltose enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body, control 35～42 ℃ of fluidized-bed layer temperature well, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, after above-mentioned various sugar alcohol fluidisations mixing lose surface crystallization water, pump into the above-mentioned oligoisomaltose solution that refines, continuously spray drying granulation, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
Embodiment 4:
10 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel heating reaction pot for 26 kilograms, 27 kilograms also another dissolves in stainless steel heating reaction pot with knob sweet 2.88 kilograms and deionized water, material is heated to 80 ℃ by chuck in the pot, start stirring, add 3.0 kilograms of active carbons respectively, be incubated 35 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; With 22.12 kilograms of antierythrites, 20 kilograms of xylitols, 45 kilograms of oligoisomaltoses, pulverizing reaches 180 orders through pulverizer, be sent to fluidisation in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body, control 35～50 ℃ of fluidized-bed layer temperature well, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, after above-mentioned various sugar alcohol fluidisations lose surface crystallization water, pumping into the above-mentioned oligoisomaltose solution that refines, the combination drying granulation of spraying continuously, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is adornd.
Embodiment 5:
10 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel heating reaction pot for 26 kilograms, knob sweet 4.32 kilograms and deionized water are also dissolved in another stainless steel heating reaction pot for 28 kilograms, material is heated to 62 ℃ by chuck in the pot, start stirring, add 3 kilograms of active carbons respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; 32 kilograms of antierythrites, 15.68 kilograms of xylitols, 38 kilograms of oligoisomaltoses, pulverizing reaches 130 orders through pulverizer, be sent in the spray-fluidized bed apparatus, with antierythrite, the mixed material of xylitol and oligoisomaltose enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body, control fluidized-bed layer temperature is 35～50 ℃, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, at antierythrite, xylitol, after the mixing of oligoisomaltose alcohol fluidisation loses surface crystallization water, pump into the above-mentioned oligoisomaltose solution that refines, continuously spray drying granulation, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
After testing, the fluffy granular composite low-sugar and low-calorie sweetener that adopts technical solution of the present invention to obtain, its main performance index sees Table 1.
Table 1
| Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 |
| Particle size | 30～60 orders | 30～60 orders | 30～60 orders | 30～60 orders | 30～60 orders |
| Sugariness (sucrose contrast) | 50 times | 100 times | 150 times | 200 times | 300 times |
| Outward appearance | White particle | White particle | White particle | White particle | White particle |
| Bulk density (g/mm 3) | ??0.60 | ??0.62 | ??0.63 | ??0.66 | ??0.60 |
The stability test of sweetener is to check sweetener to guarantee the ability that undergoes no deterioration within a certain period of time, and the sweetener product of the embodiment of the invention was stored 3 years at normal temperatures, phenomenons such as rotten and sugariness reduction occur, and stability is very superior.
The sugariness degree of modification of fluffy granular composite sugar-free sweetener of the present invention, according to the sweet adjustment in consumption of knob, in use unrestricted, usually select the common sucrose sugariness for use 50～300 times, the use needs that relatively are fit to food enterprise, form according to prescription, under same sugariness situation, people are almost nil to the absorption of heat, sugar-free sweetener is the sweet taste product of low-calorie, this sweetener can not cause blood sugar to raise, and does not participate in metabolism, not carious tooth, satisfy diabetes patient, three high crowds, pursue healthy people's needs.
Show obviously that to sum up the present invention adopts scientific formula, uses advanced science and technology technology and method, products obtained therefrom does not have smell, do not have color, and is soluble in water, and it is very convenient that this fluffy granule-shaped sugar-free sweetener is used.Granularity, molten speed, mouthfeel, sugariness all are much better than the prior art value, and the scientific preparation process simple flow is easily gone, and are fit to very much large-scale production, are worth wide popularization and application in the field of business.
What need understand is: the above only is a preferred implementation of the present invention; for those skilled in the art; under the prerequisite that does not break away from the principle of the invention, can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (4)
1. fluffy granular composite sugar-free sweetener is characterized in that comprising following composition (percentage by weight): antierythrite 20～33%, xylitol 8～20%, oligoisomaltose 47～70%, knob sweet 0.6～4.5%.
2. fluffy granular composite sugar-free sweetener according to claim 1 is characterized in that its component has following percentage by weight: antierythrite 20%, xylitol 9.28%, oligoisomaltose 70%, knob sweet 0.72%.
3. the preparation method of the described fluffy granular composite sugar-free sweetener of claim 1 is characterized in that: comprise following processing step---
1. with 10% oligoisomaltose, knob is sweet joins respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 52～80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned oligoisomaltose solution and the sweet solution of knob, be incubated 25～30 minutes, filter while hot, filtrate is pooled in the storage tank of heat tracing stand-by respectively;
4. with xylitol, antierythrite and oligoisomaltose are put in the spray-fluidized bed apparatus after pulverizing, xylitol, the mixed material of antierythrite and oligoisomaltose enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body, pump into the above-mentioned oligoisomaltose solution that refines again, spray-drying obtains fluffy granular composite sugar-free sweetener continuously.
4. the preparation method of fluffy granular composite sugar-free sweetener according to claim 3 is characterized in that: with 10% oligoisomaltose, knob is sweet joins respectively in the container, add deionized water respectively and mix; Be warming up to 60～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank that has heat tracing; With antierythrite, xylitol and oligoisomaltose reach 120～180 orders through pulverizing, be sent in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, control fluidized-bed layer temperature is at 35～80 ℃, the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body, after the mixing of sugar alcohol fluidisation loses surperficial moisture content, pump into the above-mentioned oligoisomaltose solution that refines again, spray drying granulation obtains fluffy granular composite sugar-free sweetener continuously.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102550707A (en) * | 2011-12-20 | 2012-07-11 | 苏州工业园区尚融科技有限公司 | Production method of sugarless fermented whey beverage |
| CN112006263A (en) * | 2020-09-08 | 2020-12-01 | 江西福美泰生物技术有限公司 | Neotame compound sweetener and preparation method thereof |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1099846C (en) * | 1999-12-09 | 2003-01-29 | 北京恒毅利科贸有限责任公司 | Method for preparing granular flavouring enriched food and its product |
| CN101253968B (en) * | 2008-04-15 | 2011-12-28 | 苏州苏克瑞甜品科技有限公司 | Granular sugar-free sweetening agent and method of preparing the same |
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2009
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102550707A (en) * | 2011-12-20 | 2012-07-11 | 苏州工业园区尚融科技有限公司 | Production method of sugarless fermented whey beverage |
| CN112006263A (en) * | 2020-09-08 | 2020-12-01 | 江西福美泰生物技术有限公司 | Neotame compound sweetener and preparation method thereof |
| CN112006263B (en) * | 2020-09-08 | 2024-03-29 | 江西福美泰生物技术有限公司 | Neotame composition and preparation method thereof |
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