CN101715941B - Dinning-table sweetener and production process thereof - Google Patents
Dinning-table sweetener and production process thereof Download PDFInfo
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- CN101715941B CN101715941B CN200910232216XA CN200910232216A CN101715941B CN 101715941 B CN101715941 B CN 101715941B CN 200910232216X A CN200910232216X A CN 200910232216XA CN 200910232216 A CN200910232216 A CN 200910232216A CN 101715941 B CN101715941 B CN 101715941B
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Abstract
The invention relates to a dinning-table sweetener and a production process thereof. The dinning-table sweetener comprises the following components: 11-16 percent of lower polyxylose, 35-54 percent of oligoisomaltose, 34-49 percent of erythritol and 0.83-1.68 percent of sucralose. The dinning-table sweetener is prepared by the following process of: respectively adding 8 percent oligoisomaltose and sucralose into a heating vessel, respectively adding deionized water and mixing, raising the temperature and dissolving; respectively adding active carbon in a solution, filtering while heating and collecting filtrate to a storage tank; feeding mixed material obtained by crushing the lower polyxylose, the oligoisomaltose and the erythritol from the bottom of an atomizing fluidized bed at normal pressure and accelerating to flow from bottom to top; applying negative pressure on the upper part of the atomizing fluidized bed and vibrating from top to bottom to enable the materials to boil vertically in the bed; and continuously spraying the refined sucralose solution by a multipoint spray gun at the side of the fluidized bed, dispersing the sucralose solution on a superfine sugar alcohol body, pumping an oligoisomaltose solution and continuously spraying and drying to obtain a sugar-free dinning-table sweetener. The sweetness of the dinning-table sweetener is 5-10 times of that of common sucrose.
Description
Technical field
The present invention relates to a kind of edible sweet taste material, relate in particular to a kind of low sugar dining table sweetener and production technology thereof.
Background technology
The increase of Along with people's because of too much bringing disease with sugar, people's demand safety, health, and the sweet Sugarless type dining table sweetener of mouthfeel; The present invention reaches the advanced preparation technology who puts into finished product one step completion from raw material in production procedure; It is learnt from other's strong points to offset one's weaknesses, has complementary advantages to make between the sugar alcohol sweet taste on the formula for a product; Can play during product uses and cover the effect that promotes mouthfeel with synergy; People thirst for satisfying under the low prerequisite of sugariness height, heat, and occupation modeization, with cane-sugar taste roughly the same, the salubriouser safety and Health Sugarless type dining table sweetener of mouthfeel.
Summary of the invention
The objective of the invention is to overcome the deficiency that prior art exists, a kind of dining table sweetener and production technology thereof are provided.
The object of the invention is realized through following technical scheme:
Dining table sweetener, characteristics are to comprise following composition (percentage by weight): xylo-oligosaccharide 11～16%, oligoisomaltose 35～54%, antierythrite 34～49%, Sucralose 0.83～1.68%.
Further, above-mentioned dining table sweetener, wherein, xylo-oligosaccharide 11%, oligoisomaltose 50%, antierythrite 38.16%, Sucralose 0.84%.
The production technology of dining table sweetener comprises following processing step:
1. 8% oligoisomaltose, Sucralose are joined respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 52～80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned oligoisomaltose solution and the sucralose solution, be incubated 25～30 minutes, filter while hot, filtrating is pooled to respectively in the storage tank of heat tracing;
4. xylo-oligosaccharide, oligoisomaltose, antierythrite are put in the spray-fluidized bed apparatus after pulverizing; The mixed material of xylo-oligosaccharide, oligoisomaltose, antierythrite is also quickened to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body; Pump into the above-mentioned oligoisomaltose solution that refines again, spray-drying obtains fluffy granular composite sugar-free table sweetener continuously.
Again further, the production technology of above-mentioned dining table sweetener, the oligoisomaltose with 8%, Sucralose join respectively in the heating container, add deionized water respectively and mix; Be warming up to 60～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrating is pooled to respectively in the storage tank that has heat tracing; Xylo-oligosaccharide, oligoisomaltose, antierythrite are reached 120～180 orders through pulverizing; Be sent in the spray-fluidized bed apparatus; The mixed material of above-mentioned various sugar alcohols is also quickened to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and control fluidized-bed layer temperature is at 35～80 ℃, and the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned sucralose solution that refines be sprayed continuously and is distributed on the fine sugar alcohol body; After the mixing of sugar alcohol fluidisation loses surperficial moisture content; Pump into the above-mentioned oligoisomaltose solution that refines again, spray drying granulation obtains fluffy granular composite sugar-free table sweetener continuously.
Again further; The production technology of above-mentioned dining table sweetener; The bed temperature scope of said fluidized bed with spraying is 35～80 ℃, and wherein the bed temperature of phase I Sucralose spraying dispersion is 35～50 ℃, and the bed temperature of second stage oligoisomaltose mist projection granulating is 50～80 ℃.
Again further, the production technology of above-mentioned dining table sweetener, in the phase I of said Spray Mixing fluid bed, the Sucralose spraying is dispersed in fluidisation and smashes on the fine sugar alcohol crystal body; In second stage, the oligoisomaltose spray drying granulation is on the noncrystal of mixing sugar alcohol.
Substantive distinguishing features and obvious improvement that technical scheme of the present invention is outstanding are mainly reflected in:
With xylo-oligosaccharide, oligoisomaltose, antierythrite, Sucralose is primary raw material, modifies uniformly and coats through preparation method to sugariness, makes product sweetness reach 5～10 times of common sucrose, and products obtained therefrom does not have smell, do not have color, and is soluble in water.Adopt the negative pressure fluid bed fluidization technique of scientific formula, uses advanced to combine the multi-point atomizing method, time sharing segment control appliance bed temperature efficiently solves even dispersion, coats problems such as granulation, drying.This fluffy granular composite sugar-free table sweetener is easy to use, and its preparation process science is simple and easy to operate, is fit to very much large-scale production.
Description of drawings
Below in conjunction with accompanying drawing technical scheme of the present invention is described further:
Fig. 1: process chart of the present invention.
The specific embodiment
Dining table sweetener, its composition is: xylo-oligosaccharide 11～16%, oligoisomaltose 35～54%, antierythrite 34～49%, Sucralose 0.83～1.68%.Ideal formulations is: xylo-oligosaccharide 11%, oligoisomaltose 50%, antierythrite 38.16%, Sucralose 0.83%.
As shown in Figure 1, the preparation technology of dining table sweetener: at first, the oligoisomaltose with 8%, Sucralose join respectively in the heating container, add deionized water respectively and mix; Be warming up to 52～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively in above-mentioned oligoisomaltose solution and the sucralose solution, be incubated 25～30 minutes, filter while hot, filtrating is pooled to respectively in the storage tank of heat tracing; Then; Put into after xylo-oligosaccharide, oligoisomaltose, antierythrite pulverized in the spray-fluidized bed apparatus (at heating temperature control and technological with the boiling that in fluid bed, circulates of sugar alcohol material through the positive negative pressure boiling of equipment; Mix that fluidisation is anhydrated and fluffy processing; Sugar alcohol mixtures material → malleation material quickens to flow from bottom to top → and negative pressure vibrates → makes material boiling up and down in fluid bed → by the fluid bed side multiple spot spray gun liquid material ejection fog-like liquid of naming a person for a particular job from top to bottom; Be sprayed onto on the trickle solid material body of boiling); The mixed material of above-mentioned various sugar alcohols is also quickened to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, and the bed temperature that the spraying of control Sucralose disperses is 35～50 ℃, and the Sucralose even spraying is dispersed on the mixing sugar alcohol crystalline solid of powder; The rising bed temperature; At mixing sugar alcohol after fluidisation loses surface crystallization water; Pump into the above-mentioned oligoisomaltose solution that refines again; Continuous spray drying granulation, the bed temperature of oligoisomaltose mist projection granulating controlled well is 50～80 ℃, the oligoisomaltose spray drying granulation is on the noncrystalline fluffy body of sugar alcohol; Obtain even sugariness and modify fluffy good shape product.
Embodiment 1:
8 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel reacting by heating pot for 25 kilograms; 0.84 kilogram of Sucralose and deionized water are also dissolved in another stainless steel reacting by heating pot for 18 kilograms, and material is heated to 62 ℃ by chuck in the pot, starts stirring; Add 2 kilograms of active carbons respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; With 11 kilograms of xylo-oligosaccharides, 42 kilograms of oligoisomaltoses, 38.16 kilograms of antierythrites; Pulverizing reaches 130 orders through pulverizer, is sent in the spray-fluidized bed apparatus, and the mixed material of xylo-oligosaccharide, oligoisomaltose, antierythrite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned sucralose solution that refines continuously spraying be distributed on the fine sugar alcohol body, controlling the fluidized-bed layer temperature is 35～50 ℃; The multiple spot even spraying is disperseed; After operation is accomplished, improve bed temperature to 50～80 ℃ again, xylo-oligosaccharide, oligoisomaltose, antierythrite alcohol fluidisation mix lose surface crystallization water after; Pump into the above-mentioned oligoisomaltose solution that refines; Continuous spray drying granulation is controlled air quantity and mist flow well, obtains even sugariness and modifies good fluffy granular product.
Embodiment 2:
8 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel reacting by heating pot for 26 kilograms; 1.0 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel reaction pot for 18 kilograms, and material is heated to 52 ℃ by chuck in the pot, starts stirring; Add 2 kilograms of active carbons respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; With 12 kilograms of xylo-oligosaccharides, 45 kilograms of oligoisomaltoses, 34 kilograms of antierythrites; Reach 150 orders through pulverizing, be sent to and carry out the fluidisation mixing in the spray-fluidized bed apparatus, the mixed material of xylo-oligosaccharide, oligoisomaltose, antierythrite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned sucralose solution that refines continuously spraying be distributed on the fine sugar alcohol body, control 35～40 ℃ of fluidized-bed layer temperature; Even spraying is disperseed; After operation is accomplished, improve bed temperature to 50～80 ℃ again, after above-mentioned various sugar alcohol alcohol fluidisation being mixed lose surface crystallization water; Pumping into the above-mentioned oligoisomaltose solution that refines; Continuous spray granulating and drying is controlled air quantity and mist flow well, obtains even sugariness and modifies good fluffy granular product.
Embodiment 3:
8 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel reacting by heating pot for 27 kilograms; 1.17 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel reacting by heating pot for 20 kilograms, and material is heated to 60 ℃ by chuck in the pot, starts stirring; Add 3.0 kilograms of active carbons respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; With 13.83 kilograms of xylo-oligosaccharides, 44 kilograms of oligoisomaltoses, 33 kilograms of antierythrites; Pulverize through pulverizer and to reach 160 orders, be sent in the spray-fluidized bed apparatus, with xylo-oligosaccharide, oligoisomaltose, antierythrite, mixed material get into the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation and flow; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned sucralose solution that refines be sprayed continuously and is distributed on the fine sugar alcohol body, controls 35～42 ℃ of fluidized-bed layer temperature well; The multiple spot even spraying is disperseed; After operation is accomplished, improve bed temperature to 50～80 ℃ again, above-mentioned various sugar alcohols alcohol fluidisations mix lose surface crystallization water after; Pump into the above-mentioned oligoisomaltose solution that refines; Continuous spray drying granulation is controlled air quantity and mist flow well, obtains even sugariness and modifies good fluffy granular product.
Embodiment 4:
1.17 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel reacting by heating pot for 27 kilograms; 20 kilograms also another dissolves in stainless steel reacting by heating pot with deionized water with 1.2 kilograms of Sucraloses, and material is heated to 80 ℃ by chuck in the pot, starts stirring; Add 3.0 kilograms of active carbons respectively; Be incubated 35 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; With 15 kilograms of xylo-oligosaccharides, 33.8 kilograms of oligoisomaltoses, 48.83 kilograms of antierythrites, process pulverizer are pulverized and are reached 180 orders; Be sent to fluidisation in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols got into the fluidized bed with spraying and quickens from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body; Control 35～50 ℃ of fluidized-bed layer temperature well, the multiple spot even spraying is disperseed, after operation is accomplished; Improve bed temperature to 50～80 ℃ again; After above-mentioned various sugar alcohol alcohol fluidisations lose surface crystallization water, pumping into the above-mentioned oligoisomaltose solution that refines, continuously the Spray Mixing drying-granulating; Control air quantity and mist flow well, obtain the good fluffy granular product of even sugariness decorations.
Embodiment 5:
8 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel reacting by heating pot for 26 kilograms; 1.66 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel reacting by heating pot for 20 kilograms, and material is heated to 62 ℃ by chuck in the pot, starts stirring; Add 3 kilograms of active carbons respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; With 16 kilograms of xylo-oligosaccharides, 29 kilograms of oligoisomaltoses, 45.34 kilograms of antierythrites; Pulverize through pulverizer and to reach 130 orders, be sent in the spray-fluidized bed apparatus, the mixed material of xylo-oligosaccharide, oligoisomaltose, antierythrite is got into the fluidized bed with spraying and quickens from bottom to top from the bottom of fluidized bed with spraying with malleation flow; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned sucralose solution that refines continuously spraying be distributed on the fine sugar alcohol body, controlling the fluidized-bed layer temperature is 35～50 ℃; The multiple spot even spraying is disperseed; After operation is accomplished, improve bed temperature to 50～80 ℃ again, xylo-oligosaccharide, oligoisomaltose, antierythrite alcohol fluidisation mix lose surface crystallization water after; Pump into the above-mentioned oligoisomaltose solution that refines; Continuous spray drying granulation is controlled air quantity and mist flow well, obtains even sugariness and modifies good fluffy granular product.
Through detecting, adopt the fluffy granular composite sugar-free sweet taste material of technical scheme acquisition of the present invention, its main performance index is seen table 1.
Table 1
| Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 |
| Particle size | 30～60 orders | 30～60 orders | 30～60 orders | 30～60 orders | 30～60 orders |
| Sugariness (sucrose contrast) | 5 times | 6 times | 7 times | 7 times | 10 times |
| Outward appearance | White particle | White particle | White particle | White particle | White particle |
| Bulk density (g/mm 3) | 0.60 | 0.63 | 0.63 | 0.65 | 0.66 |
The stability test of sweetener is to check sweetener to guarantee the ability that undergoes no deterioration within a certain period of time, and the dining table sweetener product of the embodiment of the invention was stored 3 years at normal temperatures, phenomenons such as rotten and sugariness reduction occur, and the stability ten minutes is superior.
The sugariness degree of modification of fluffy granular composite sugar-free table sweetener of the present invention, according to the adjustment of Sucralose in consumption, in use unrestricted; Usually select the common sucrose sugariness for use 5～10 times; Relatively be fit to people's use needs, form, under same sugariness situation according to prescription; People are almost nil to the absorption of heat; The Sugarless mensal sweetening agent is noble sweet taste article, and this sweet taste material can not cause that blood sugar raises, carious tooth not, is fit to diabetes patient, satisfied three high crowds, pursues healthy needs of people.
Show obviously that to sum up the present invention adopts scientific formula, uses advanced science and technology technology and method, products obtained therefrom does not have smell, do not have color, and is soluble in water, and it is very convenient that this fluffy granule-shaped sugar-free dining table sweetener is used.Granularity, molten speed, mouthfeel, sugariness all are much better than the prior art value, and the scientific preparation process simple flow is prone to row, are fit to very much large-scale production, are worth wide popularization and application in the field of business.
What need understand is: the above only is a preferred implementation of the present invention; For those skilled in the art; Under the prerequisite that does not break away from the principle of the invention, can also make some improvement and retouching, these improvement and retouching also should be regarded as protection scope of the present invention.
Claims (2)
1. the production technology of dining table sweetener; Dining table sweetener comprises following percentage by weight composition: xylo-oligosaccharide 11～16%, oligoisomaltose 35～54%, antierythrite 34～49%; Sucralose 0.83～1.68% is characterized in that: comprise following processing step---
1. 8% oligoisomaltose, Sucralose are joined respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 52～80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned oligoisomaltose solution and the sucralose solution, be incubated 25～30 minutes, filter while hot, for use in the storage tank that is pooled to heat tracing respectively of filtrating;
4. xylo-oligosaccharide, oligoisomaltose, antierythrite are put in the spray-fluidized bed apparatus after broken; The mixed material of xylo-oligosaccharide, oligoisomaltose, antierythrite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body; Pump into the above-mentioned oligoisomaltose solution that refines again, spray-drying obtains fluffy granular composite sugar-free table sweetener continuously.
2. the production technology of dining table sweetener according to claim 1, it is characterized in that: the oligoisomaltose with 8%, Sucralose join respectively in the container, add deionized water respectively and mix; Be warming up to 60～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrating is pooled to respectively in the storage tank that has heat tracing; Xylo-oligosaccharide, oligoisomaltose, antierythrite are reached 120～180 orders through pulverizing; Be sent in the spray-fluidized bed apparatus; The mixed material of above-mentioned various sugar alcohols is also quickened to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and control fluidized-bed layer temperature is at 35～80 ℃, and the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned sucralose solution that refines be sprayed continuously and is distributed on the fine sugar alcohol body; After the mixing of sugar alcohol fluidisation loses surperficial moisture content; Pump into the above-mentioned oligoisomaltose solution that refines again, spray drying granulation obtains fluffy granular composite sugar-free table sweetener continuously.
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| CN102342481A (en) * | 2011-08-24 | 2012-02-08 | 淄博中食歌瑞生物技术有限公司 | Low-heat-value phycite high sweetener |
| CN102551024A (en) * | 2011-12-09 | 2012-07-11 | 苏州工业园区尚融科技有限公司 | Compound sugar-free sweetener and preparation method thereof |
| CN102511767A (en) * | 2011-12-09 | 2012-06-27 | 苏州工业园区尚融科技有限公司 | Composite sweetener containing xylo oligosaccharide and preparation method thereof |
| CN102511765A (en) * | 2011-12-09 | 2012-06-27 | 苏州工业园区尚融科技有限公司 | Fluffy powdery composite sugar-free sweetener and its preparation method |
| CN102511770A (en) * | 2011-12-15 | 2012-06-27 | 苏州工业园区尚融科技有限公司 | Prebiotics composite sugar-free sweetener and preparation method thereof |
| CN102423063A (en) * | 2011-12-15 | 2012-04-25 | 苏州工业园区尚融科技有限公司 | Fluffy granular sugar-free sweetening material containing prebiotics xylooligosaccharide, and preparation method thereof |
| CN102423061A (en) * | 2011-12-15 | 2012-04-25 | 苏州工业园区尚融科技有限公司 | Prebiotic-containing composite sweetening material and preparation method thereof |
| CN102511774A (en) * | 2011-12-15 | 2012-06-27 | 苏州工业园区尚融科技有限公司 | Compound sugarless sweetener for drink and preparation method for same |
| CN102429015A (en) * | 2011-12-20 | 2012-05-02 | 苏州工业园区尚融科技有限公司 | Production method of sugar-free double-protein beverage |
| CN104719588A (en) * | 2013-12-19 | 2015-06-24 | 姜宁 | Zero heat rose sugar and preparation method thereof |
| CN103976339A (en) * | 2014-06-09 | 2014-08-13 | 天津替代医学科技有限公司 | Sugar substitute and preparation method thereof |
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| CN1254522A (en) * | 1999-12-09 | 2000-05-31 | 北京恒毅利科贸有限责任公司 | Method for preparing granular flavouring enriched food and its product |
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| CN1254522A (en) * | 1999-12-09 | 2000-05-31 | 北京恒毅利科贸有限责任公司 | Method for preparing granular flavouring enriched food and its product |
| CN1806685A (en) * | 2006-02-08 | 2006-07-26 | 江南大学 | Method for preparing thermal reaction type shrimp tasted seasoning by utilizing shrimp or shrimp leftovers as raw materials |
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