CN101715941A - Dinning-table sweetener and production process thereof - Google Patents

Dinning-table sweetener and production process thereof Download PDF

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Publication number
CN101715941A
CN101715941A CN200910232216A CN200910232216A CN101715941A CN 101715941 A CN101715941 A CN 101715941A CN 200910232216 A CN200910232216 A CN 200910232216A CN 200910232216 A CN200910232216 A CN 200910232216A CN 101715941 A CN101715941 A CN 101715941A
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oligoisomaltose
fluidized bed
sucralose
spraying
table sweetener
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CN101715941B (en
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历冠廷
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Suzhou Industrial Park Shangrong Technology Co Ltd
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Suzhou Industrial Park Shangrong Technology Co Ltd
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Abstract

The invention relates to a dinning-table sweetener and a production process thereof. The dinning-table sweetener comprises the following components: 11-16 percent of lower polyxylose, 35-54 percent of oligoisomaltose, 34-49 percent of erythritol and 0.83-1.68 percent of sucralose. The dinning-table sweetener is prepared by the following process of: respectively adding 8 percent oligoisomaltose and sucralose into a heating vessel, respectively adding deionized water and mixing, raising the temperature and dissolving; respectively adding active carbon in a solution, filtering while heating and collecting filtrate to a storage tank; feeding mixed material obtained by crushing the lower polyxylose, the oligoisomaltose and the erythritol from the bottom of an atomizing fluidized bed at normal pressure and accelerating to flow from bottom to top; applying negative pressure on the upper part of the atomizing fluidized bed and vibrating from top to bottom to enable the materials to boil vertically in the bed; and continuously spraying the refined sucralose solution by a multipoint spray gun at the side of the fluidized bed, dispersing the sucralose solution on a superfine sugar alcohol body, pumping an oligoisomaltose solution and continuously spraying and drying to obtain a sugar-free dinning-table sweetener. The sweetness of the dinning-table sweetener is 5-10 times of that of common sucrose.

Description

Dining table sweetener and production technology thereof
Technical field
The present invention relates to a kind of edible sweet taste material, relate in particular to a kind of low sugar dining table sweetener and production technology thereof.
Background technology
Along with the increase of people because of too much bringing disease, people's demand safety, health, and the sweet Sugarless type dining table sweetener of mouthfeel with sugar; The present invention reaches in production procedure from raw material and puts into the advanced preparation technology that finished product one step finishes; It is learnt from other's strong points to offset one's weaknesses, has complementary advantages to make between the sugar alcohol sweet taste on the formula for a product, can play during product uses and cover the effect that promotes mouthfeel with synergy, people thirst for satisfying under the low prerequisite of sugariness height, heat, and occupation modeization, with cane-sugar taste roughly the same, the salubriouser safety and Health Sugarless type dining table sweetener of mouthfeel.
Summary of the invention
The objective of the invention is to overcome the deficiency that prior art exists, a kind of dining table sweetener and production technology thereof are provided.
Purpose of the present invention is achieved through the following technical solutions:
Dining table sweetener, characteristics are to comprise following composition (percentage by weight): xylo-oligosaccharide 11~16%, oligoisomaltose 35~54%, antierythrite 34~49%, Sucralose 0.83~1.68%.
Further, above-mentioned dining table sweetener, wherein, xylo-oligosaccharide 11%, oligoisomaltose 50%, antierythrite 38.16%, Sucralose 0.84%.
The production technology of dining table sweetener comprises following processing step:
1. 8% oligoisomaltose, Sucralose are joined respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 52~80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned oligoisomaltose solution and the sucralose solution, be incubated 25~30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank of heat tracing;
4. with xylo-oligosaccharide, oligoisomaltose, antierythrite is put in the spray-fluidized bed apparatus after pulverizing, with xylo-oligosaccharide, oligoisomaltose, the mixed material of antierythrite enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, pump into the above-mentioned oligoisomaltose solution that refines again, spray-drying obtains fluffy granular composite sugar-free table sweetener continuously.
Again further, the production technology of above-mentioned dining table sweetener, the oligoisomaltose with 8%, Sucralose join respectively in the heating container, add deionized water respectively and mix; Be warming up to 60~80 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank that has heat tracing; With xylo-oligosaccharide, oligoisomaltose, antierythrite reaches 120~180 orders through pulverizing, be sent in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, control fluidized-bed layer temperature is at 35~80 ℃, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, after the mixing of sugar alcohol fluidisation loses surperficial moisture content, pump into the above-mentioned oligoisomaltose solution that refines again, spray drying granulation obtains fluffy granular composite sugar-free table sweetener continuously.
Again further, the production technology of above-mentioned dining table sweetener, the bed temperature scope of described fluidized bed with spraying is 35~80 ℃, and wherein the bed temperature of phase I Sucralose spraying dispersion is 35~50 ℃, and the bed temperature of second stage oligoisomaltose mist projection granulating is 50~80 ℃.
Again further, the production technology of above-mentioned dining table sweetener, in the phase I of described spraying mixed fluidized bed, the Sucralose spraying is dispersed in fluidisation and smashes on the fine sugar alcohol crystal body; In second stage, the oligoisomaltose spray drying granulation is on the noncrystal of mixing sugar alcohol.
Substantive distinguishing features and obvious improvement that technical solution of the present invention is outstanding are mainly reflected in:
With xylo-oligosaccharide, oligoisomaltose, antierythrite, Sucralose is primary raw material, modifies uniformly and coats by preparation method to sugariness, makes product sweetness reach 5~10 times of common sucrose, and products obtained therefrom does not have smell, do not have color, and is soluble in water.The negative pressure fluid bed fluidization technique that adopts scientific formula, uses advanced is in conjunction with the multi-point atomizing method, and time sharing segment control appliance bed temperature efficiently solves even dispersion, coats problems such as granulation, drying.This fluffy granular composite sugar-free table sweetener is easy to use, and its preparation process science is simple and easy to operate, is fit to very much large-scale production.
Description of drawings
Below in conjunction with accompanying drawing technical solution of the present invention is described further:
Fig. 1: process chart of the present invention.
The specific embodiment
Dining table sweetener, its composition is: xylo-oligosaccharide 11~16%, oligoisomaltose 35~54%, antierythrite 34~49%, Sucralose 0.83~1.68%.Ideal formulations is: xylo-oligosaccharide 11%, oligoisomaltose 50%, antierythrite 38.16%, Sucralose 0.83%.
As shown in Figure 1, the preparation technology of dining table sweetener: at first, the oligoisomaltose with 8%, Sucralose join respectively in the heating container, add deionized water respectively and mix; Be warming up to 52~80 ℃ of dissolvings respectively, and stir; Add active carbon respectively in above-mentioned oligoisomaltose solution and the sucralose solution, be incubated 25~30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank of heat tracing; Then, with xylo-oligosaccharide, oligoisomaltose, put into after antierythrite is pulverized in the spray-fluidized bed apparatus (heating temperature control and by the positive negative pressure boiling of equipment technology with the boiling that in fluid bed, circulates of sugar alcohol material, mix that fluidisation is anhydrated and fluffy processing, sugar alcohol mixtures material → malleation material quickens to flow from bottom to top → and negative pressure vibrates → makes material boiling up and down in fluid bed → by the fluid bed side multiple spot spray gun liquid material ejection fog-like liquid of naming a person for a particular job from top to bottom, be sprayed onto on the trickle solid material body of boiling), the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, the bed temperature that the spraying of control Sucralose disperses is 35~50 ℃, and the Sucralose even spraying is dispersed on the mixing sugar alcohol crystalline solid of powder; The rising bed temperature, at mixing sugar alcohol after fluidisation loses surface crystallization water, pump into the above-mentioned oligoisomaltose solution that refines again, continuous spray drying granulation, the bed temperature of oligoisomaltose mist projection granulating controlled well is 50~80 ℃, and the oligoisomaltose spray drying granulation is on the noncrystalline fluffy body of sugar alcohol; Obtain fluffy the shape product that even sugariness is modified.
Embodiment 1:
8 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel heating reaction pot for 25 kilograms, 0.84 kilogram of Sucralose and deionized water are also dissolved in another stainless steel heating reaction pot for 18 kilograms, material is heated to 62 ℃ by chuck in the pot, start stirring, add 2 kilograms of active carbons respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; With 11 kilograms of xylo-oligosaccharides, 42 kilograms of oligoisomaltoses, 38.16 kilograms of antierythrites, pulverizing reaches 130 orders through pulverizer, be sent in the spray-fluidized bed apparatus, xylo-oligosaccharide, oligoisomaltose, the mixed material of antierythrite enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, control fluidized-bed layer temperature is 35~50 ℃, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50~80 ℃ again, at xylo-oligosaccharide, oligoisomaltose, after the mixing of antierythrite alcohol fluidisation loses surface crystallization water, pump into the above-mentioned oligoisomaltose solution that refines, continuously spray drying granulation, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
Embodiment 2:
8 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel heating reaction pot for 26 kilograms, 1.0 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel reaction pot for 18 kilograms, material is heated to 52 ℃ by chuck in the pot, start stirring, add 2 kilograms of active carbons respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; With 12 kilograms of xylo-oligosaccharides, 45 kilograms of oligoisomaltoses, 34 kilograms of antierythrites, reach 150 orders through pulverizing, be sent to and carry out the fluidisation mixing in the spray-fluidized bed apparatus, xylo-oligosaccharide, oligoisomaltose, the mixed material of antierythrite enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, 35~40 ℃ of control fluidized-bed layer temperature, even spraying is disperseed, after operation is finished, improve bed temperature to 50~80 ℃ again, after making the mixing of above-mentioned various sugar alcohol alcohol fluidisation lose surface crystallization water, pumping into the above-mentioned oligoisomaltose solution that refines, continuously spray granulating and drying, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
Embodiment 3:
8 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel heating reaction pot for 27 kilograms, 1.17 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel heating reaction pot for 20 kilograms, material is heated to 60 ℃ by chuck in the pot, start stirring, add 3.0 kilograms of active carbons respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; With 13.83 kilograms of xylo-oligosaccharides, 44 kilograms of oligoisomaltoses, 33 kilograms of antierythrites, pulverizing reaches 160 orders through pulverizer, be sent in the spray-fluidized bed apparatus, with xylo-oligosaccharide, oligoisomaltose, antierythrite, mixed material enter the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quicken from bottom to top and flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, control 35~42 ℃ of fluidized-bed layer temperature well, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50~80 ℃ again, after the mixing of above-mentioned various sugar alcohol alcohol fluidisations loses surface crystallization water, pump into the above-mentioned oligoisomaltose solution that refines, continuously spray drying granulation, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
Embodiment 4:
1.17 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel heating reaction pot for 27 kilograms, 20 kilograms also another dissolves in stainless steel heating reaction pot with 1.2 kilograms of Sucraloses and deionized water, material is heated to 80 ℃ by chuck in the pot, start stirring, add 3.0 kilograms of active carbons respectively, be incubated 35 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; With 15 kilograms of xylo-oligosaccharides, 33.8 kilograms of oligoisomaltoses, 48.83 kilograms of antierythrites, pulverizing reaches 180 orders through pulverizer, be sent to fluidisation in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, control 35~50 ℃ of fluidized-bed layer temperature well, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50~80 ℃ again, after above-mentioned various sugar alcohol alcohol fluidisations lose surface crystallization water, pumping into the above-mentioned oligoisomaltose solution that refines, air quantity and mist flow are controlled in continuously spraying combination drying granulation well, obtain the fluffy granular product that even sugariness is adornd.
Embodiment 5:
8 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel heating reaction pot for 26 kilograms, 1.66 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel heating reaction pot for 20 kilograms, material is heated to 62 ℃ by chuck in the pot, start stirring, add 3 kilograms of active carbons respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; With 16 kilograms of xylo-oligosaccharides, 29 kilograms of oligoisomaltoses, 45.34 kilograms of antierythrites, pulverizing reaches 130 orders through pulverizer, be sent in the spray-fluidized bed apparatus, with xylo-oligosaccharide, oligoisomaltose, the mixed material of antierythrite enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, control fluidized-bed layer temperature is 35~50 ℃, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50~80 ℃ again, at xylo-oligosaccharide, oligoisomaltose, after the mixing of antierythrite alcohol fluidisation loses surface crystallization water, pump into the above-mentioned oligoisomaltose solution that refines, continuously spray drying granulation, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
After testing, the fluffy granular composite sugar-free sweet taste material that adopts technical solution of the present invention to obtain, its main performance index sees Table 1.
Table 1
Test item Embodiment 1 Embodiment 2 Embodiment 3 Embodiment 4 Embodiment 5
Particle size 30~60 orders 30~60 orders 30~60 orders 30~60 orders 30~60 orders
Sugariness (sucrose contrast) 5 times 6 times 7 times 7 times 10 times
Outward appearance White particle White particle White particle White particle White particle
Bulk density (g/mm 3) ??0.60 ??0.63 ??0.63 ??0.65 ??0.66
The stability test of sweetener is to check sweetener to guarantee the ability that undergoes no deterioration within a certain period of time, and the dining table sweetener product of the embodiment of the invention was stored 3 years at normal temperatures, phenomenons such as rotten and sugariness reduction occur, and stability is very superior.
The sugariness degree of modification of fluffy granular composite sugar-free table sweetener of the present invention, according to the adjustment of Sucralose in consumption, in use unrestricted, usually select the common sucrose sugariness for use 5~10 times, the use needs that relatively are fit to people, form according to prescription, under same sugariness situation, people are almost nil to the absorption of heat, the Sugarless mensal sweetening agent is noble sweet taste product, this sweet taste material can not cause that blood sugar raises, carious tooth not, is fit to the diabetes patient, satisfies three high crowds, pursues healthy people's needs.
Show obviously that to sum up the present invention adopts scientific formula, uses advanced science and technology technology and method, products obtained therefrom does not have smell, do not have color, and is soluble in water, and it is very convenient that this fluffy granule-shaped sugar-free dining table sweetener is used.Granularity, molten speed, mouthfeel, sugariness all are much better than the prior art value, and the scientific preparation process simple flow is easily gone, and are fit to very much large-scale production, are worth wide popularization and application in the field of business.
What need understand is: the above only is a preferred implementation of the present invention; for those skilled in the art; under the prerequisite that does not break away from the principle of the invention, can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.

Claims (4)

1. dining table sweetener is characterized in that comprising following composition (percentage by weight): xylo-oligosaccharide 11~16%, oligoisomaltose 35~54%, antierythrite 34~49%, Sucralose 0.83~1.68%.
2. according to the described dining table sweetener of claim 1, it is characterized in that its component has following percentage by weight: xylo-oligosaccharide 11%, oligoisomaltose 50%, antierythrite 38.16%, Sucralose 0.84%.
3. the production technology of the described dining table sweetener of claim 1 is characterized in that: comprise following processing step---
1. 8% oligoisomaltose, Sucralose are joined respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 52~80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned oligoisomaltose solution and the sucralose solution, be incubated 25~30 minutes, filter while hot, filtrate is pooled in the storage tank of heat tracing stand-by respectively;
4. with xylo-oligosaccharide, oligoisomaltose, put into after antierythrite is broken in the spray-fluidized bed apparatus, xylo-oligosaccharide, oligoisomaltose, the mixed material of antierythrite enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, pump into the above-mentioned oligoisomaltose solution that refines again, spray-drying obtains fluffy granular composite sugar-free table sweetener continuously.
4. the production technology of dining table sweetener according to claim 3, it is characterized in that: the oligoisomaltose with 8%, Sucralose join respectively in the container, add deionized water respectively and mix; Be warming up to 60~80 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank that has heat tracing; With xylo-oligosaccharide, oligoisomaltose, antierythrite reaches 120~180 orders through pulverizing, be sent in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, control fluidized-bed layer temperature is at 35~80 ℃, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, after the mixing of sugar alcohol fluidisation loses surperficial moisture content, pump into the above-mentioned oligoisomaltose solution that refines again, spray drying granulation obtains fluffy granular composite sugar-free table sweetener continuously.
CN200910232216XA 2009-12-10 2009-12-10 Dinning-table sweetener and production process thereof Expired - Fee Related CN101715941B (en)

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CN102423063A (en) * 2011-12-15 2012-04-25 苏州工业园区尚融科技有限公司 Fluffy granular sugar-free sweetening material containing prebiotics xylooligosaccharide, and preparation method thereof
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CN102342481A (en) * 2011-08-24 2012-02-08 淄博中食歌瑞生物技术有限公司 Low-heat-value phycite high sweetener
CN102511767A (en) * 2011-12-09 2012-06-27 苏州工业园区尚融科技有限公司 Composite sweetener containing xylo oligosaccharide and preparation method thereof
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CN102551024A (en) * 2011-12-09 2012-07-11 苏州工业园区尚融科技有限公司 Compound sugar-free sweetener and preparation method thereof
CN102423061A (en) * 2011-12-15 2012-04-25 苏州工业园区尚融科技有限公司 Prebiotic-containing composite sweetening material and preparation method thereof
CN102423063A (en) * 2011-12-15 2012-04-25 苏州工业园区尚融科技有限公司 Fluffy granular sugar-free sweetening material containing prebiotics xylooligosaccharide, and preparation method thereof
CN102511770A (en) * 2011-12-15 2012-06-27 苏州工业园区尚融科技有限公司 Prebiotics composite sugar-free sweetener and preparation method thereof
CN102511774A (en) * 2011-12-15 2012-06-27 苏州工业园区尚融科技有限公司 Compound sugarless sweetener for drink and preparation method for same
CN102429015A (en) * 2011-12-20 2012-05-02 苏州工业园区尚融科技有限公司 Production method of sugar-free double-protein beverage
CN104719588A (en) * 2013-12-19 2015-06-24 姜宁 Zero heat rose sugar and preparation method thereof
CN103976339A (en) * 2014-06-09 2014-08-13 天津替代医学科技有限公司 Sugar substitute and preparation method thereof

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