CN102511767A - Composite sweetener containing xylo oligosaccharide and preparation method thereof - Google Patents
Composite sweetener containing xylo oligosaccharide and preparation method thereof Download PDFInfo
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- CN102511767A CN102511767A CN2011104079803A CN201110407980A CN102511767A CN 102511767 A CN102511767 A CN 102511767A CN 2011104079803 A CN2011104079803 A CN 2011104079803A CN 201110407980 A CN201110407980 A CN 201110407980A CN 102511767 A CN102511767 A CN 102511767A
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Abstract
The invention relates to a composite sweetener containing xylo oligosaccharide and a preparation method thereof. The composite sweetener contains the following components of: by weight, 60-83% of erythritol, 3-20% of xylo oligosaccharide, 7.5-15% of stevioside and 5.833-11.70% of sucralose. The technology contains the following steps of: respectively adding sucralose and stevioside into a heating container, adding deionized water for mixing, heating to dissolve, respectively collecting the solution into a storage tank while the solution is hot, allowing a mixed material of crushed erythritol and xylo oligosaccharide to enter from to bottom of a spray fluidized bed into the bed and quickly flow from bottom to top by positive pressure, applying negative pressure on the upper portion of the spray fluidized bed to make the spray fluidized bed vibrate from top to bottom so as to make the material boil up and down, continuously and dispersely spraying the refined sucralose solution on the fine sugar alcohol body by the use of a multi-point spray gun at the side portion of the fluidized bed, pumping a stevioside solution, and continuously carrying out spray drying to obtain the composite sugar-free sweetener. The preparation flow is simple and easy to operate, and sweetness of the product is 50-100 times than that of common cane sugar.
Description
Technical field
The present invention relates to a kind of edible sweetener, relate in particular to a kind of Xylo-oligosaccharide compounded sweetener and preparation method thereof that contains.
Background technology
The increase of Along with people's because of too much bringing disease with sugar, people's demand safety, healthy sugar-free sweetener; In production procedure, reach the advanced preparation technology who puts into finished product one step completion from raw material; It is learnt from other's strong points to offset one's weaknesses, has complementary advantages to make between sweetener and the sugar alcohol sweet taste on the formula for a product; Can play during product uses and cover the effect that promotes mouthfeel with synergy; People thirst for satisfying under the low prerequisite of sugariness height, heat, and occupation modeization, with cane-sugar taste safety and Health sugar-free sweetener roughly the same.
Summary of the invention
The objective of the invention is to overcome the deficiency that prior art exists, a kind of Xylo-oligosaccharide compounded sweetener and preparation method thereof that contains is provided, adopt the scientific technology of easy operation control, the molten speed property of product, mouthfeel, sugariness all are higher than the prior art optimum value.
The object of the invention is realized through following technical scheme:
A kind ofly contain Xylo-oligosaccharide compounded sweetener, characteristics are to comprise following percentage by weight composition: antierythrite 60～83%, xylo-oligosaccharide 3～20%, steviol glycoside 7.5～15%, Sucralose 5.833～11.70%.
Further, above-mentioned a kind of Xylo-oligosaccharide compounded sweetener that contains, wherein, antierythrite 68.3%, xylo-oligosaccharide 5%, steviol glycoside 15%, Sucralose 11.70%.
The preparation method of the fluffy powder shape of the present invention composite sugar-free sweetener comprises following processing step:
1. steviol glycoside, Sucralose are joined respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 50～100 ℃ of dissolvings respectively, and stir;
3. above-mentioned steviol glycoside solution and sucralose solution insulation 10～20 minutes is pooled in the storage tank of heat tracing for use while hot respectively;
4. with putting in the spray-fluidized bed apparatus after antierythrite and the xylo-oligosaccharide pulverizing; The mixed material of antierythrite and xylo-oligosaccharide also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body; Pump into the above-mentioned steviol glycoside solution that refines again, spray-drying obtains fluffy powder shape composite sugar-free sweetener continuously.
Again further, above-mentioned a kind of preparation method who contains Xylo-oligosaccharide compounded sweetener joins steviol glycoside, Sucralose respectively in the heating container, adds deionized water respectively and mixes; Be warming up to 50～100 ℃ of dissolvings respectively, and stir; Be incubated 10 minutes, be pooled in the storage tank that has heat tracing while hot respectively; Antierythrite and xylo-oligosaccharide reach 100～120 orders through pulverizing; Be sent in the spray-fluidized bed apparatus; The mixed material of antierythrite and xylo-oligosaccharide also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and control fluidized-bed layer temperature is at 50～120 ℃, and the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned sucralose solution that refines be sprayed continuously and is distributed on the fine sugar alcohol body; After the mixing of sugar alcohol fluidisation loses surperficial moisture content; Pump into the above-mentioned steviol glycoside solution that refines again, spray drying granulation obtains fluffy powder shape composite sugar-free sweetener continuously.
Again further; Above-mentioned a kind of preparation method who contains Xylo-oligosaccharide compounded sweetener; The EAT scope of said fluidized bed with spraying is 50～120 ℃; Wherein the bed temperature of phase I Sucralose spraying dispersion is 50～80 ℃, and the bed temperature of the sweet mist projection granulating of second stage knob is 60～120 ℃.
Again further, above-mentioned a kind of preparation method who contains Xylo-oligosaccharide compounded sweetener, in the phase I of said Spray Mixing fluid bed, the Sucralose spraying is dispersed in fluidisation and smashes on the fine sugar alcohol crystal body; In second stage, the steviol glycoside spray drying granulation is on the noncrystal of mixing sugar alcohol.
Substantive distinguishing features and obvious improvement that technical scheme of the present invention is outstanding are mainly reflected in:
Adopt the negative pressure fluid bed fluidization technique of scientific formula, uses advanced to combine the multi-point atomizing method, time sharing segment control appliance EAT efficiently solves even dispersion, coats problems such as granulation, drying.With antierythrite, xylo-oligosaccharide, Sucralose, steviol glycoside is primary raw material; Modify uniformly and coat through preparation method to sugariness, make product sweetness reach 50～100 times of common sucrose, products obtained therefrom does not have smell, does not have color; Soluble in water; This fluffy powder shape composite sugar-free sweetener is easy to use, and its preparation process science is simple and easy to operate, is fit to very much large-scale production.
The specific embodiment
The present invention is a kind of to contain Xylo-oligosaccharide compounded sweetener, and its composition is: antierythrite 60～83%, xylo-oligosaccharide 3～20%, steviol glycoside 7.5～15%, Sucralose 5.833～11.70%.Ideal formulations is: antierythrite 68.3%, xylo-oligosaccharide 5%, steviol glycoside 15%, Sucralose 11.70%.
A kind of preparation technology who contains Xylo-oligosaccharide compounded sweetener: at first, steviol glycoside, Sucralose are joined respectively in the heating container, add deionized water respectively and mix; Be warming up to 50～100 ℃ of dissolvings respectively, and stir; Add active carbon respectively in above-mentioned steviol glycoside solution and the sucralose solution, be incubated 10～20 minutes, be pooled in the storage tank of heat tracing while hot respectively; At last; Put into after antierythrite and xylo-oligosaccharide pulverized in the spray-fluidized bed apparatus (at heating temperature control and technological with the boiling that in fluid bed, circulates of sugar alcohol material through the positive negative pressure boiling of equipment; Mix that fluidisation is anhydrated and fluffy processing; Sugar alcohol mixtures material → malleation material quickens to flow from bottom to top → and negative pressure vibrates → makes material boiling up and down in fluid bed → by the fluid bed side multiple spot spray gun liquid material ejection fog-like liquid of naming a person for a particular job from top to bottom; Be sprayed onto on the trickle solid material body of boiling); The mixed material of antierythrite and xylo-oligosaccharide also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, and the EAT that the spraying of control Sucralose disperses is 50～100 ℃, and the Sucralose even spraying is dispersed on the mixing sugar alcohol crystalline solid of powder; The rising bed temperature; After fluidisation loses surface crystallization water, pump into the above-mentioned steviol glycoside solution that refines at mixing sugar alcohol again, continuously spray drying granulation; The EAT of the sweet mist projection granulating of knob controlled well is 60～120 ℃, and the sweet spray drying granulation of knob is on the noncrystalline fluffy body of sugar alcohol; Obtain even sugariness and modify good fluffy powder granular products.
Embodiment 1:
7.5 kilograms of steviol glycosides and deionized water are dissolved in a stainless steel reacting by heating pot for 10 kilograms; 5.833 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel reacting by heating pot for 10 kilograms; Material is heated to 75 ℃ by chuck in the pot; Start stirring, be incubated 10 minutes, collect in the storage tank of chuck insulation for use while hot respectively; 76.667 kilograms of antierythrites, 10 kilograms of xylo-oligosaccharides, pulverizing reaches 120 orders through pulverizer; Be sent in the spray-fluidized bed apparatus, the mixed material of antierythrite and xylo-oligosaccharide gets into the fluidized bed with spraying from the bottom of fluidized bed with spraying and quickens from bottom to top with malleation and flows, and the top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body; Control fluidisation EAT is 50～100 ℃, and the multiple spot even spraying is disperseed, after operation is accomplished; Improve EAT to 60～120 ℃ again; After antierythrite, the mixing of xylo-oligosaccharide sugar alcohol fluidisation lose surface crystallization water, pump into the above-mentioned steviol glycoside solution that refines, continuously spray-drying; Control air quantity and mist flow well, obtain even sugariness and modify good fluffy room pelletized product.
Embodiment 2:
15 kilograms of steviol glycosides and deionized water are dissolved in a stainless steel reacting by heating pot for 20 kilograms; 11.70 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel reaction pot for 15 kilograms; Material is heated to 80 ℃ by chuck in the pot; Start stirring, be incubated 10 minutes, collect in the storage tank of chuck insulation for use while hot respectively; 68.30 kilograms of antierythrites, 5 kilograms of xylo-oligosaccharides reach 120 orders through pulverizing; Be sent to and carry out fluidisation in the spray-fluidized bed apparatus and mix, the mixed material of antierythrite and xylo-oligosaccharide gets into the fluidized bed with spraying and quickens from bottom to top from the bottom of fluidized bed with spraying with malleation and flows, and the top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom material is seethed with excitement up and down in fluid bed; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body; 50～100 ℃ of control fluidisation EATs, even spraying is disperseed, after operation is accomplished; Improve EAT to 60～120 ℃ again; After making antierythrite, the mixing of xylo-oligosaccharide fluidisation lose surface crystallization water, pumping into the above-mentioned steviol glycoside solution that refines, continuously spray granulating and drying; Control air quantity and mist flow well, obtain even sugariness and modify fluffy good pelletized product.
The stability test of sweetener is to check sweetener to guarantee the ability that undergoes no deterioration within a certain period of time, and the composite sweetener product of the embodiment of the invention was stored 3 years at normal temperatures, phenomenons such as rotten and sugariness reduction occur, and the stability ten minutes is superior.
The sugariness degree of modification of the fluffy powder shape of the present invention composite sugar-free sweetener will be according to, the adjustment of the sweet Sucralose of knob in consumption, 50～100 times of selecting the common sucrose sugariness usually for use; The use needs that relatively are fit to food enterprise; Form according to prescription, under same sugariness situation, people are to the sweet taste article of the absorption low-calorie of heat; This sweetener can not cause blood sugar to raise, and satisfies three high crowds, pursues healthy needs of people.
Show obviously that to sum up the present invention adopts scientific formula, uses advanced science and technology technology and method, products obtained therefrom does not have smell, do not have color, and is soluble in water, and it is very convenient that this fluffy powder shape sugar-free sweetener is used.Granularity, molten speed, mouthfeel, sugariness all are much better than the prior art value, and the scientific preparation process simple flow is prone to row, are fit to very much large-scale production, are worth wide popularization and application in the field of business.
What need understand is: the above only is a preferred implementation of the present invention; For those skilled in the art; Under the prerequisite that does not break away from the principle of the invention, can also make some improvement and retouching, these improvement and retouching also should be regarded as protection scope of the present invention.
Claims (5)
1. one kind contains Xylo-oligosaccharide compounded sweetener, it is characterized in that comprising following percentage by weight composition: antierythrite 60～83%, xylo-oligosaccharide 3～20%, steviol glycoside 7.5～15%, Sucralose 5.833～11.70%.
2. a kind of Xylo-oligosaccharide compounded sweetener that contains according to claim 1 is characterized in that its component has following percentage by weight: antierythrite 68.3%, xylo-oligosaccharide 5%, steviol glycoside 15%, Sucralose 11.70%.
3. the described a kind of preparation method who contains Xylo-oligosaccharide compounded sweetener of claim 1 is characterized in that comprising following processing step:
1. steviol glycoside, Sucralose are joined respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 50～100 ℃ of dissolvings respectively, and stir;
3. above-mentioned steviol glycoside solution and sucralose solution insulation 10～20 minutes is pooled in the storage tank of heat tracing for use while hot respectively;
4. with putting in the spray-fluidized bed apparatus after antierythrite and the xylo-oligosaccharide pulverizing; The mixed material of antierythrite and xylo-oligosaccharide also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body; Pump into the above-mentioned steviol glycoside solution that refines again, spray-drying obtains fluffy powder shape composite sugar-free sweetener continuously.
4. a kind of preparation method who contains Xylo-oligosaccharide compounded sweetener according to claim 3 is characterized in that: steviol glycoside, Sucralose are joined respectively in the container, add deionized water respectively and mix; Be warming up to 50～100 ℃ of dissolvings respectively, and stir; Be incubated 10 minutes, be pooled to respectively in the storage tank that has heat tracing; Antierythrite and xylo-oligosaccharide reach 100～120 orders through pulverizing; Be sent in the spray-fluidized bed apparatus; The mixed material of antierythrite and xylo-oligosaccharide also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and control fluidisation EAT is at 50～120 ℃, and the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned sucralose solution that refines be sprayed continuously and is distributed on the fine sugar alcohol body; After the mixing of sugar alcohol fluidisation loses surperficial moisture content; Pump into the above-mentioned steviol glycoside solution that refines again, spray-drying obtains fluffy powder shape composite sugar-free sweetener continuously.
5. a kind of preparation method who contains Xylo-oligosaccharide compounded sweetener according to claim 4; It is characterized in that: the EAT scope of said fluidized bed with spraying is 50～120 ℃; Wherein the bed temperature of phase I Sucralose spraying dispersion is 50～80 ℃, and the bed temperature of the sweet mist projection granulating of second stage knob is 60～120 ℃.
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| CN2011104079803A CN102511767A (en) | 2011-12-09 | 2011-12-09 | Composite sweetener containing xylo oligosaccharide and preparation method thereof |
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| CN2011104079803A CN102511767A (en) | 2011-12-09 | 2011-12-09 | Composite sweetener containing xylo oligosaccharide and preparation method thereof |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102960695A (en) * | 2012-11-30 | 2013-03-13 | 苏州工业园区尚融科技有限公司 | Compound sweetening agent applicable to solid milk tea and preparation method thereof |
| CN102960686A (en) * | 2012-11-30 | 2013-03-13 | 苏州工业园区尚融科技有限公司 | Compound sweetener applied to solid milky tea and preparation method of sweetener |
| CN103704554A (en) * | 2012-10-06 | 2014-04-09 | 杜志坚 | Sugar-free granulated sugar, and preparation method thereof |
| CN103976339A (en) * | 2014-06-09 | 2014-08-13 | 天津替代医学科技有限公司 | Sugar substitute and preparation method thereof |
| CN104687176A (en) * | 2015-02-10 | 2015-06-10 | 叶节和 | Plant beverage and preparation method thereof |
| CN106820069A (en) * | 2016-12-28 | 2017-06-13 | 山东龙力生物科技股份有限公司 | A kind of natural built-up sweetener with regulating intestinal canal function and preparation method thereof |
| CN109329864A (en) * | 2018-10-31 | 2019-02-15 | 郑书旺 | A kind of composite sweetener and preparation method |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101715941A (en) * | 2009-12-10 | 2010-06-02 | 苏州工业园区尚融科技有限公司 | Dinning-table sweetener and production process thereof |
| CN102224920A (en) * | 2011-05-11 | 2011-10-26 | 深圳市纽全德生物科技有限公司 | Liquid table sweetener and preparation method thereof |
-
2011
- 2011-12-09 CN CN2011104079803A patent/CN102511767A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101715941A (en) * | 2009-12-10 | 2010-06-02 | 苏州工业园区尚融科技有限公司 | Dinning-table sweetener and production process thereof |
| CN102224920A (en) * | 2011-05-11 | 2011-10-26 | 深圳市纽全德生物科技有限公司 | Liquid table sweetener and preparation method thereof |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103704554A (en) * | 2012-10-06 | 2014-04-09 | 杜志坚 | Sugar-free granulated sugar, and preparation method thereof |
| CN102960695A (en) * | 2012-11-30 | 2013-03-13 | 苏州工业园区尚融科技有限公司 | Compound sweetening agent applicable to solid milk tea and preparation method thereof |
| CN102960686A (en) * | 2012-11-30 | 2013-03-13 | 苏州工业园区尚融科技有限公司 | Compound sweetener applied to solid milky tea and preparation method of sweetener |
| CN103976339A (en) * | 2014-06-09 | 2014-08-13 | 天津替代医学科技有限公司 | Sugar substitute and preparation method thereof |
| CN104687176A (en) * | 2015-02-10 | 2015-06-10 | 叶节和 | Plant beverage and preparation method thereof |
| CN106820069A (en) * | 2016-12-28 | 2017-06-13 | 山东龙力生物科技股份有限公司 | A kind of natural built-up sweetener with regulating intestinal canal function and preparation method thereof |
| CN109329864A (en) * | 2018-10-31 | 2019-02-15 | 郑书旺 | A kind of composite sweetener and preparation method |
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Application publication date: 20120627 |