CN102415548A - Fluffy powder particle composite low-sugar and low-calorie sweetener and preparation method thereof - Google Patents
Fluffy powder particle composite low-sugar and low-calorie sweetener and preparation method thereof Download PDFInfo
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- CN102415548A CN102415548A CN201110407995XA CN201110407995A CN102415548A CN 102415548 A CN102415548 A CN 102415548A CN 201110407995X A CN201110407995X A CN 201110407995XA CN 201110407995 A CN201110407995 A CN 201110407995A CN 102415548 A CN102415548 A CN 102415548A
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Abstract
The invention relates to a fluffy powder particle composite low-sugar and low-calorie sweetener and a preparation method thereof. The fluffy powder particle composite low-sugar and low-calorie sweetener comprises the following ingredients: 50-86% of dextrose monohydrate, 10-46% of maltodextrin, 0.664-2.666% of neotame and 1.666-6.8% of sucralose. The preparation method comprises the following steps of: respectively adding the sucralose and the neotame into a heating container; adding deionized water to mix; heating and dissolving; respectively collecting the hot solution into a storage tank; enabling the mixed material comprising the smashed dextrose monohydrate and maltodextrin to enter a bed from the bottom of a spraying fluidized bed at the positive pressure, and quickening the mixed material to flow from bottom to top; applying negative pressure to the upper part of the spraying fluidized bed to vibrate from top to bottom to cause materials to vertically boil in the bed; continuously spraying and dispersing the refined sucralose solution to a superfine sugar alcohol body by a multi-point spray gun on the side part of the fluidized bed; pumping in the neotame solution; and continuously spraying and drying to obtain the composite sugar-free sweetener. The preparation flow is simple and easy to operate, and the product sweetness is 50-200 times that of the common cane sugar.
Description
Technical field
The present invention relates to a kind of edible sweetener, relate in particular to a kind of fluffy powder shape composite low-sugar low-calorie sweetener and preparation method thereof.
Background technology
The increase of Along with people's because of too much bringing disease with sugar, people's demand safety, healthy low-sugar-content and low-calorie sweetening agent; In production procedure, reach the advanced preparation technology who puts into finished product one step completion from raw material; It is learnt from other's strong points to offset one's weaknesses, has complementary advantages to make between sweetener and the sugar alcohol sweet taste on the formula for a product; Can play during product uses and cover the effect that promotes mouthfeel with synergy; People thirst for satisfying under the low prerequisite of sugariness height, heat, and occupation modeization, with cane-sugar taste safety and Health low-sugar-content and low-calorie sweetening agent roughly the same.
Summary of the invention
The objective of the invention is to overcome the deficiency that prior art exists, a kind of fluffy powder shape composite low-sugar low-calorie sweetener and preparation method thereof is provided, adopt the scientific technology of easy operation control, the molten speed property of product, mouthfeel, sugariness all are higher than the prior art optimum value.
The object of the invention is realized through following technical scheme:
Fluffy powder shape composite low-sugar low-calorie sweetener, characteristics are to comprise following percentage by weight composition: Dextrose Monohydrate 50～86%, and maltodextrin 10～46%, knob is sweet 0.664～2.666%, Sucralose 1.666～6.8%.
Further, above-mentioned fluffy powder shape composite low-sugar low-calorie sweetener, wherein, and Dextrose Monohydrate 60%, maltodextrin 35.34%, knob is sweet 1.328%, Sucralose 3.332%.
The preparation method of the fluffy powder shape of the present invention composite low-sugar low-calorie sweetener comprises following processing step:
1. knob is sweet, Sucralose joins respectively in the heating container, adds deionized water respectively and mixes;
2. be warming up to 50～100 ℃ of dissolvings respectively, and stir;
3. the sweet solution of above-mentioned knob and sucralose solution insulation 10～20 minutes is pooled in the storage tank of heat tracing for use while hot respectively;
4. with putting in the spray-fluidized bed apparatus after Dextrose Monohydrate and the maltodextrin pulverizing; The mixed material of Dextrose Monohydrate and maltodextrin also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body; Pump into the sweet solution of the above-mentioned knob that refines again, spray-drying obtains fluffy powder shape composite low-sugar low-calorie sweetener continuously.
Again further, the preparation method of above-mentioned fluffy powder shape composite low-sugar low-calorie sweetener, knob is sweet, Sucralose joins respectively in the container, adds deionized water respectively and mixes; Be warming up to 50～100 ℃ of dissolvings respectively, and stir; Be incubated 10 minutes, be pooled to respectively in the storage tank that has heat tracing; Dextrose Monohydrate and maltodextrin reach 100～120 orders through pulverizing; Be sent in the spray-fluidized bed apparatus; The mixed material of Dextrose Monohydrate and maltodextrin also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and control fluidisation EAT is at 50～120 ℃, and the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned sucralose solution that refines be sprayed continuously and is distributed on the fine sugar alcohol body; After the mixing of sugar alcohol fluidisation loses surperficial moisture content; Pump into the sweet solution of the above-mentioned knob that refines again, spray-drying obtains fluffy powder shape composite low-sugar low-calorie sweetener continuously.
Again further; The preparation method of above-mentioned fluffy powder shape composite low-sugar low-calorie sweetener; The EAT scope of said fluidized bed with spraying is 50～120 ℃; Wherein the bed temperature of phase I Sucralose spraying dispersion is 50～80 ℃, and the bed temperature of the sweet mist projection granulating of second stage knob is 60～120 ℃.
Again further, the preparation method of above-mentioned fluffy powder shape composite low-sugar low-calorie sweetener, in the phase I of said Spray Mixing fluid bed, the Sucralose spraying is dispersed in fluidisation and smashes on the fine sugar alcohol crystal body; In second stage, the sweet spray drying granulation of knob is on the noncrystal of mixing sugar alcohol.
Substantive distinguishing features and obvious improvement that technical scheme of the present invention is outstanding are mainly reflected in:
Adopt the negative pressure fluid bed fluidization technique of scientific formula, uses advanced to combine the multi-point atomizing method, time sharing segment control appliance EAT efficiently solves even dispersion, coats problems such as granulation, drying.With Dextrose Monohydrate, maltodextrin, Sucralose, knob is sweet is primary raw material; Modify uniformly and coat through preparation method to sugariness, make product sweetness reach 50～200 times of common sucrose, products obtained therefrom does not have smell, does not have color; Soluble in water; This fluffy powder shape composite sugar-free sweetener is easy to use, and its preparation process science is simple and easy to operate, is fit to very much large-scale production.
The specific embodiment
The fluffy powder shape of the present invention composite low-sugar low-calorie sweetener, its composition is: Dextrose Monohydrate 50～86%, maltodextrin 10～46%, knob is sweet 0.664～2.666%, Sucralose 1.666～6.8%.Ideal formulations is: Dextrose Monohydrate 60%, and maltodextrin 35.34%, knob is sweet 1.328%, Sucralose 3.332%.
The preparation technology of fluffy powder shape composite low-sugar low-calorie sweetener: at first, knob is sweet, Sucralose joins respectively in the heating container, adds deionized water respectively and mixes; Be warming up to 50～100 ℃ of dissolvings respectively, and stir; Add active carbon respectively in sweet solution of above-mentioned knob and the sucralose solution, be incubated 10～20 minutes, be pooled in the storage tank of heat tracing while hot respectively; At last; Put into after antierythrite and oligoisomaltose pulverized in the spray-fluidized bed apparatus (at heating temperature control and technological with the boiling that in fluid bed, circulates of sugar alcohol material through the positive negative pressure boiling of equipment; Mix that fluidisation is anhydrated and fluffy processing; Sugar alcohol mixtures material → malleation material quickens to flow from bottom to top → and negative pressure vibrates → makes material boiling up and down in fluid bed → by the fluid bed side multiple spot spray gun liquid material ejection fog-like liquid of naming a person for a particular job from top to bottom; Be sprayed onto on the trickle solid material body of boiling); The mixed material of Dextrose Monohydrate and maltodextrin also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, and the EAT that the spraying of control Sucralose disperses is 50～100 ℃, and the Sucralose even spraying is dispersed on the mixing sugar alcohol crystalline solid of powder; The rising bed temperature; After fluidisation loses surface crystallization water, pump into the sweet solution of the above-mentioned knob that refines at mixing sugar alcohol again, continuously spray drying granulation; The EAT of the sweet mist projection granulating of knob controlled well is 60～120 ℃, and the sweet spray drying granulation of knob is on the noncrystalline fluffy body of sugar alcohol; Obtain even sugariness and modify good fluffy powder granular products.
Embodiment 1:
Knob is dissolved in a stainless steel reacting by heating pot for 5 kilograms with deionized water for sweet 0.666 kilogram; 1.7 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel reacting by heating pot for 10 kilograms; Material is heated to 75 ℃ by chuck in the pot; Start stirring, be incubated 10 minutes, collect in the storage tank of chuck insulation for use while hot respectively; 65 kilograms of Dextrose Monohydrates, 32.634 kilograms of maltodextrins, pulverizing reaches 120 orders through pulverizer; Be sent in the spray-fluidized bed apparatus, the mixed material of Dextrose Monohydrate and maltodextrin gets into the fluidized bed with spraying from the bottom of fluidized bed with spraying and quickens from bottom to top with malleation and flows, and the top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body; Control fluidisation EAT is 50～100 ℃, and the multiple spot even spraying is disperseed, after operation is accomplished; Improve EAT to 60～120 ℃ again; After Dextrose Monohydrate, the mixing of maltodextrin sugar alcohol fluidisation lose surface crystallization water, pump into the sweet solution of the above-mentioned knob that refines, continuously spray-drying; Control air quantity and mist flow well, obtain even sugariness and modify good fluffy room pelletized product.
Embodiment 2:
Knob is dissolved in a stainless steel reacting by heating pot for 10 kilograms with deionized water for sweet 1.332 kilograms; 3.4 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel reaction pot for 10 kilograms; Material is heated to 80 ℃ by chuck in the pot; Start stirring, be incubated 10 minutes, collect in the storage tank of chuck insulation for use while hot respectively; 60 kilograms of Dextrose Monohydrates, 35.268 kilograms of maltodextrins reach 120 orders through pulverizing; Be sent to and carry out fluidisation in the spray-fluidized bed apparatus and mix, the mixed material of Dextrose Monohydrate and maltodextrin gets into the fluidized bed with spraying and quickens from bottom to top from the bottom of fluidized bed with spraying with malleation and flows, and the top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom material is seethed with excitement up and down in fluid bed; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body; 50～100 ℃ of control fluidisation EATs, even spraying is disperseed, after operation is accomplished; Improve EAT to 60～120 ℃ again; After making Dextrose Monohydrate, the mixing of maltodextrin fluidisation lose surface crystallization water, pumping into the sweet solution of the above-mentioned knob that refines, continuously spray granulating and drying; Control air quantity and mist flow well, obtain even sugariness and modify fluffy good pelletized product.
Embodiment 3:
Knob is dissolved in a stainless steel reacting by heating pot for 10 kilograms with deionized water for sweet 1.328 kilograms; 3.332 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel reacting by heating pot for 15 kilograms; Material is heated to 85 ℃ by chuck in the pot; Start stirring, be incubated 10 minutes, collect in the storage tank of chuck insulation for use while hot respectively; 60 kilograms of Dextrose Monohydrates, 35.34 kilograms of maltodextrins, pulverizing reaches 120 orders through pulverizer; The mixed material that is sent to spray-fluidized bed apparatus mesoerythrit and oligoisomaltose also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned sucralose solution that refines be sprayed continuously and is distributed on the fine sugar alcohol body, controls 50～100 ℃ of fluidized-bed layer temperature well; The multiple spot even spraying is disperseed; Operation improves 60～120 ℃ of bed temperatures after accomplishing again, after Dextrose Monohydrate, the mixing of maltodextrin fluidisation lose surface crystallization water; Pump into the sweet solution of the above-mentioned knob that refines; Continuous spray-drying is controlled air quantity and mist flow well, obtains even sugariness and modifies good fluffy powder granular products.
Embodiment 4:
Knob is dissolved in a stainless steel reacting by heating pot for 15 kilograms with deionized water for sweet 2.664 kilograms; 15 kilograms also another dissolves in stainless steel reacting by heating pot with deionized water with 6.8 kilograms of Sucraloses; Material is heated to 85 ℃ by chuck in the pot; Start stirring, be incubated 15 minutes, collect in the storage tank of chuck insulation for use while hot respectively; 75 kilograms of Dextrose Monohydrates, 15.536 kilograms of maltodextrins, pulverizing reaches 120 orders through pulverizer; Be sent to fluidisation in the spray-fluidized bed apparatus, the mixed material of Dextrose Monohydrate and maltodextrin gets into the fluidized bed with spraying from the bottom of fluidized bed with spraying and quickens from bottom to top with malleation and flows, and the top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body; Control 50～100 ℃ of fluidisation EATs well, the multiple spot even spraying is disperseed, after operation is accomplished; Improve EAT to 60～120 ℃ again; After Dextrose Monohydrate, maltodextrin fluidisation lose surface crystallization water, pumping into the sweet solution of the above-mentioned knob that refines, Spray Mixing is dry continuously; Control air quantity and mist flow well, obtain the good fluffy powder granular products of even sugariness decorations.
Through detecting, adopt the fluffy powder shape composite low-sugar low-calorie sweetener of technical scheme acquisition of the present invention, its main performance index is seen table 1.
Table 1
| Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 |
| Particle size | 50～100 orders | 50～100 orders | 50～100 orders | 50～100 orders |
| Sugariness (sucrose contrast) | 50 times | 100 times | 150 times | 200 times |
| Outward appearance | The white powder | The white powder | The white powder | The white powder |
The stability test of sweetener is to check sweetener to guarantee the ability that undergoes no deterioration within a certain period of time, and the composite sweetener product of the embodiment of the invention was stored 3 years at normal temperatures, phenomenons such as rotten and sugariness reduction occur, and the stability ten minutes is superior.
The sugariness degree of modification of the fluffy powder shape of the present invention composite sweetener will be according to, the adjustment of the sweet Sucralose of knob in consumption, 50～200 times of selecting the common sucrose sugariness usually for use; The use needs that relatively are fit to food enterprise; Form according to prescription, under same sugariness situation, people are to the sweet taste article of the absorption low-calorie of heat; This sweetener can not cause blood sugar to raise, and satisfies three high crowds, pursues healthy needs of people.
Show obviously that to sum up the present invention adopts scientific formula, uses advanced science and technology technology and method, products obtained therefrom does not have smell, do not have color, and is soluble in water, and it is very convenient that this fluffy powder shape low-sugar-content and low-calorie sweetening agent is used.Granularity, molten speed, mouthfeel, sugariness all are much better than the prior art value, and the scientific preparation process simple flow is prone to row, are fit to very much large-scale production, are worth wide popularization and application in the field of business.
What need understand is: the above only is a preferred implementation of the present invention; For those skilled in the art; Under the prerequisite that does not break away from the principle of the invention, can also make some improvement and retouching, these improvement and retouching also should be regarded as protection scope of the present invention.
Claims (5)
1. fluffy powder shape composite low-sugar low-calorie sweetener is characterized in that comprising following percentage by weight composition: Dextrose Monohydrate 50～86%, and maltodextrin 10～46%, knob is sweet 0.664～2.666%, Sucralose 1.666～6.8%.
2. fluffy powder shape composite low-sugar low-calorie sweetener according to claim 1 is characterized in that its component has following percentage by weight: Dextrose Monohydrate 60%, and maltodextrin 35.34%, knob is sweet 1.328%, Sucralose 3.332%.
3. the preparation method of the described fluffy powder shape composite low-sugar low-calorie sweetener of claim 1 is characterized in that comprising following processing step:
1. knob is sweet, Sucralose joins respectively in the heating container, adds deionized water respectively and mixes;
2. be warming up to 50～100 ℃ of dissolvings respectively, and stir;
3. the sweet solution of above-mentioned knob and sucralose solution insulation 10～20 minutes is pooled in the storage tank of heat tracing for use while hot respectively;
4. with putting in the spray-fluidized bed apparatus after Dextrose Monohydrate and the maltodextrin pulverizing; The mixed material of Dextrose Monohydrate and maltodextrin also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body; Pump into the sweet solution of the above-mentioned knob that refines again, spray-drying obtains fluffy powder shape composite low-sugar low-calorie sweetener continuously.
4. the preparation method of fluffy powder shape composite low-sugar low-calorie sweetener according to claim 3 is characterized in that: knob is sweet, Sucralose joins respectively in the container, adds deionized water respectively and mixes; Be warming up to 50～100 ℃ of dissolvings respectively, and stir; Be incubated 10 minutes, be pooled to respectively in the storage tank that has heat tracing; Dextrose Monohydrate and maltodextrin reach 100～120 orders through pulverizing; Be sent in the spray-fluidized bed apparatus; The mixed material of Dextrose Monohydrate and maltodextrin also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and control fluidisation EAT is at 50～120 ℃, and the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned sucralose solution that refines be sprayed continuously and is distributed on the fine sugar alcohol body; After the mixing of sugar alcohol fluidisation loses surperficial moisture content; Pump into the sweet solution of the above-mentioned knob that refines again, spray-drying obtains fluffy powder shape composite low-sugar low-calorie sweetener continuously.
5. the preparation method of fluffy powder shape composite low-sugar low-calorie sweetener according to claim 4; It is characterized in that: the EAT scope of said fluidized bed with spraying is 50～120 ℃; Wherein the bed temperature of phase I Sucralose spraying dispersion is 50～80 ℃, and the bed temperature of the sweet mist projection granulating of second stage knob is 60～120 ℃.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106072423A (en) * | 2016-06-21 | 2016-11-09 | 厦门华高食品科技有限公司 | A kind of low in calories or empty calory high sugariness compound sweetener and preparation method thereof |
| CN110506922A (en) * | 2019-09-24 | 2019-11-29 | 湖南艾达伦科技有限公司 | A kind of Siraitia grosvenorii compound sweetener and preparation method thereof for stabilizing blood glucose |
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| CN101810302A (en) * | 2009-12-08 | 2010-08-25 | 苏州工业园区尚融科技有限公司 | Novel fluffy granular composite low-sugar low-calorie sweetening agent and preparing method thereof |
| CN101874591A (en) * | 2009-11-24 | 2010-11-03 | 苏州工业园区尚融科技有限公司 | Fluffy granular composite low-sugar and low-calorie sweetener and preparation method thereof |
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Patent Citations (2)
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| CN101874591A (en) * | 2009-11-24 | 2010-11-03 | 苏州工业园区尚融科技有限公司 | Fluffy granular composite low-sugar and low-calorie sweetener and preparation method thereof |
| CN101810302A (en) * | 2009-12-08 | 2010-08-25 | 苏州工业园区尚融科技有限公司 | Novel fluffy granular composite low-sugar low-calorie sweetening agent and preparing method thereof |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106072423A (en) * | 2016-06-21 | 2016-11-09 | 厦门华高食品科技有限公司 | A kind of low in calories or empty calory high sugariness compound sweetener and preparation method thereof |
| CN110477353A (en) * | 2016-06-21 | 2019-11-22 | 赵西南 | High sugariness compound sweetener of a kind of low in calories or empty calory and preparation method thereof |
| CN110506922A (en) * | 2019-09-24 | 2019-11-29 | 湖南艾达伦科技有限公司 | A kind of Siraitia grosvenorii compound sweetener and preparation method thereof for stabilizing blood glucose |
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Application publication date: 20120418 |