CN101874601B - Granular composite low-sugar low-calorie table sweetner and preparation method thereof - Google Patents
Granular composite low-sugar low-calorie table sweetner and preparation method thereof Download PDFInfo
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- CN101874601B CN101874601B CN2009102520476A CN200910252047A CN101874601B CN 101874601 B CN101874601 B CN 101874601B CN 2009102520476 A CN2009102520476 A CN 2009102520476A CN 200910252047 A CN200910252047 A CN 200910252047A CN 101874601 B CN101874601 B CN 101874601B
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Abstract
The invention relates to a granular composite low-sugar low-calorie table sweetner and a preparation method thereof. The sweetner comprises the following components: 55-77 percent of dextrose monohydrate, 9-18 percent of xylitol, 11-20 percent of sorbitol, 3-5 percent of maltodextrin and 0.8-1.85 percent of trichlorosucrose. The process comprises the following steps of: respectively adding the maltodextrin and the trichlorosucrose to heating containers, respectively adding deionized water for mixing, and heating to dissolve the maltodextrin and the trichlorosucrose; respectively adding activated carbon to solutions, filtering while the solutions are hot, and respectively collecting filter liquor to storage tanks; making the crushed mixture of the dextrose monohydrate, the xylitol and the sorbitol enter into a bed from the bottom of an atomizing fluidized bed by positive pressure and accelerating the mixture to flow from bottom up; applying negative pressure to the upper part of the atomizing fluidized bed to vibrate from top to bottom to make mixture boiled up and down in the bed; and continuously spraying and dispersing a refined trichlorosucrose solution to superfine sugar-alcohol bodies by a multipoint spray gun on the side of the fluidized bed, then pumping into with a monohydrate solution and carrying out continuous spraying and drying to obtain the low-sugar low-calorie table sweetner. The sweetness of the low-sugar low-calorie table sweetner is 5-11 times of the sweetness of common cane sugar.
Description
Technical field
The present invention relates to a kind of edible dining table sweetener, relate in particular to a kind of granular composite low-sugar-content and low-calorie table sweetening agent and preparation method thereof.
Background technology
The increase of Along with people's because of too much bringing disease with sugar, people's demand safety, healthy low-sugar-content and low-calorie type dining table sweetener; In production procedure, reach the advanced preparation technology who puts into finished product one step completion from raw material; It is learnt from other's strong points to offset one's weaknesses, has complementary advantages to make between the sugar alcohol sweet taste on the formula for a product; Can play during product uses and cover the effect that promotes mouthfeel with synergy; People thirst for satisfying under the low prerequisite of sugariness height, heat, and occupation modeization, with cane-sugar taste safety and Health low-sugar-content and low-calorie type dining table sweetener roughly the same.
Summary of the invention
The objective of the invention is to overcome the deficiency that prior art exists; A kind of fluffy granular composite low-sugar-content and low-calorie table sweet taste material and preparation method thereof is provided; Adopt the scientific technology of easy operation control, the molten speed property of product, mouthfeel, sugariness all are higher than the prior art optimum value.
The object of the invention is realized through following technical scheme:
Granular composite low-sugar-content and low-calorie table sweetening agent, characteristics are to comprise following composition (percentage by weight): Dextrose Monohydrate 55～77%, xylitol 9～18%, D-sorbite 11～20%, maltodextrin 3～5%, Sucralose 0.8～1.85%.
Further, above-mentioned granular composite low-sugar-content and low-calorie table sweetening agent, wherein, Dextrose Monohydrate 65%, xylitol 11%, D-sorbite 19%, maltodextrin 3.83%, Sucralose 1.17%.
Further, above-mentioned granular composite low-sugar-content and low-calorie table sweetening agent, said maltodextrin DE value is 10～20.
The preparation method of granular composite low-sugar-content and low-calorie table sweetening agent of the present invention comprises following processing step:
1. maltodextrin, Sucralose are joined respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 52～80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned maltodextrin solution and the sucralose solution, be incubated 25～30 minutes, filter while hot, filtrating is pooled to respectively in the storage tank of heat tracing;
4. put in the spray-fluidized bed apparatus after Dextrose Monohydrate, xylitol and D-sorbite being pulverized; The mixed material of Dextrose Monohydrate, xylitol and D-sorbite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body; Pump into the above-mentioned maltodextrin solution that refines again, spray-drying obtains fluffy granular composite low-sugar-content and low-calorie table sweet taste material continuously.
Again further, the preparation method of above-mentioned granular composite low-sugar-content and low-calorie table sweetening agent joins maltodextrin, Sucralose respectively in the heating container, adds deionized water respectively and mixes; Be warming up to 60～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrating is pooled to respectively in the storage tank that has heat tracing; Dextrose Monohydrate, xylitol and D-sorbite reach 120～180 orders through pulverizing; Be sent in the spray-fluidized bed apparatus; The mixed material of Dextrose Monohydrate, xylitol and D-sorbite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and control fluidized-bed layer temperature is at 35～80 ℃, and the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned sucralose solution that refines be sprayed continuously and is distributed on the fine sugar alcohol body; After above-mentioned various sugar alcohol fluidisations mixing lose surperficial moisture content; Pump into the above-mentioned maltodextrin solution that refines again, spray drying granulation obtains fluffy granular composite low-sugar-content and low-calorie table sweet taste material continuously.
Again further; The preparation method of above-mentioned granular composite low-sugar-content and low-calorie table sweetening agent; The bed temperature scope of said fluidized bed with spraying is 35～80 ℃; Wherein the bed temperature of phase I Sucralose spraying dispersion is 35～50 ℃, and the bed temperature of second stage maltodextrin mist projection granulating is 50～80 ℃.
Again further, the preparation method of above-mentioned granular composite low-sugar-content and low-calorie table sweetening agent, in the phase I of said Spray Mixing fluid bed, the Sucralose spraying is dispersed in fluidisation and smashes on the fine sugar alcohol crystal body; In second stage, the maltodextrin spray drying granulation is on the noncrystal of mixing sugar alcohol.
Substantive distinguishing features and obvious improvement that technical scheme of the present invention is outstanding are mainly reflected in:
Adopt the negative pressure fluid bed fluidization technique of scientific formula, uses advanced to combine the multi-point atomizing method, time sharing segment control appliance bed temperature efficiently solves even dispersion, coats problems such as granulation, drying.With Dextrose Monohydrate, xylitol, D-sorbite, Sucralose is primary raw material; Modify uniformly and coat through preparation method to sugariness, make product sweetness reach 5～11 times of common sucrose, products obtained therefrom does not have smell, does not have color; Soluble in water; This fluffy granular composite low-sugar and low-calorie sweetener is easy to use, and its preparation process science is simple and easy to operate, is fit to very much large-scale production.
Description of drawings
Below in conjunction with accompanying drawing technical scheme of the present invention is described further:
Fig. 1: process chart of the present invention.
The specific embodiment
Granular composite low-sugar-content and low-calorie table sweetening agent, its composition is: Dextrose Monohydrate 55～77%, xylitol 9～18%, D-sorbite 11～20%, maltodextrin 3～5%, Sucralose 0.8～1.85%.Ideal formulations is: Dextrose Monohydrate 65%, xylitol 11%, D-sorbite 19%, maltodextrin 3.83%, Sucralose 1.17%.
As shown in Figure 1, the preparation technology of granular composite low-sugar-content and low-calorie table sweetening agent: at first, maltodextrin, Sucralose are joined respectively in the heating container, add deionized water respectively and mix; Be warming up to 52～80 ℃ of dissolvings respectively, and stir; Add active carbon in above-mentioned maltodextrin solution and the sucralose solution respectively, be incubated 25～30 minutes, filter while hot, filtrating is pooled to respectively in the storage tank of heat tracing; Then; Put into after Dextrose Monohydrate, xylitol and D-sorbite pulverized in the spray-fluidized bed apparatus (at heating temperature control and technological with the boiling that in fluid bed, circulates of sugar alcohol material through the positive negative pressure boiling of equipment; Mix that fluidisation is anhydrated and fluffy processing; Sugar alcohol mixtures material → malleation material quickens to flow from bottom to top → and negative pressure vibrates → makes material boiling up and down in fluid bed → by the fluid bed side multiple spot spray gun liquid material ejection fog-like liquid of naming a person for a particular job from top to bottom; Be sprayed onto on the trickle solid material body of boiling); The mixed material of Dextrose Monohydrate, xylitol and D-sorbite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, and the bed temperature that the spraying of control Sucralose disperses is 35～50 ℃, and the Sucralose even spraying is dispersed on the mixing sugar alcohol crystalline solid of powder; The rising bed temperature; At mixing sugar alcohol after fluidisation loses surface crystallization water; Pump into the above-mentioned maltodextrin solution that refines again; Continuous spray drying granulation, the bed temperature of maltodextrin mist projection granulating controlled well is 50～80 ℃, the maltodextrin spray drying granulation is on the noncrystalline fluffy body of sugar alcohol; Obtain even sugariness and modify fluffy good shape product.
Embodiment 1:
Maltodextrin 2.16 and deionized water are dissolved in a stainless steel reacting by heating pot for 20 kilograms; 0.84 kilogram of Sucralose and deionized water are also dissolved in another stainless steel reacting by heating pot for 20 kilograms, and material is heated to 62 ℃ by chuck in the pot, starts stirring; Add 1 kilogram of active carbon respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 77 kilograms of Dextrose Monohydrates, 9 kilograms of xylitols, 11 kilograms of D-sorbites; Pulverizing reaches 130 orders through pulverizer, is sent in the spray-fluidized bed apparatus, and the mixed material of Dextrose Monohydrate, xylitol and D-sorbite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned sucralose solution that refines continuously spraying be distributed on the fine sugar alcohol body, controlling the fluidized-bed layer temperature is 35～50 ℃; The multiple spot even spraying is disperseed; After operation is accomplished, improve bed temperature to 50～80 ℃ again, Dextrose Monohydrate, xylitol, the stupid fluidisation of sorbose mix lose surface crystallization water after; Pump into the above-mentioned maltodextrin solution that refines; Continuous spray drying granulation is controlled air quantity and mist flow well, obtains even sugariness and modifies good fluffy granular product.
Embodiment 2:
3.83 kilograms of maltodextrins and deionized water are dissolved in a stainless steel reacting by heating pot for 25 kilograms; 1.17 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel reaction pot for 20 kilograms, and material is heated to 52 ℃ by chuck in the pot, starts stirring; Add 2 kilograms of active carbons respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 65 kilograms of Dextrose Monohydrates, xylitol 11%, 19 kilograms of D-sorbites; Reach 150 orders through pulverizing, be sent to and carry out the fluidisation mixing in the spray-fluidized bed apparatus, the mixed material of Dextrose Monohydrate, xylitol and D-sorbite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned sucralose solution that refines continuously spraying be distributed on the fine sugar alcohol body, control 35～40 ℃ of fluidized-bed layer temperature; Even spraying is disperseed; After operation is accomplished, improve bed temperature to 50～80 ℃ again, after Dextrose Monohydrate, xylitol, the stupid fluidisation of sorbose being mixed lose surface crystallization water; Pumping into the above-mentioned maltodextrin solution that refines; Continuous spray granulating and drying is controlled air quantity and mist flow well, obtains even sugariness and modifies good fluffy granular product.
Embodiment 3:
4 kilograms of maltodextrins and deionized water are dissolved in a stainless steel reacting by heating pot for 25 kilograms; 1 kilogram of Sucralose and deionized water are also dissolved in another stainless steel reacting by heating pot for 20 kilograms, and material is heated to 60 ℃ by chuck in the pot, starts stirring; Add 2.0 kilograms of active carbons respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 66 kilograms of Dextrose Monohydrates, 13 kilograms of xylitols, 16 kilograms of D-sorbites; Pulverizing reaches 160 orders through pulverizer, is sent in the spray-fluidized bed apparatus, and the mixed material of Dextrose Monohydrate, xylitol and D-sorbite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned sucralose solution that refines be sprayed continuously and is distributed on the fine sugar alcohol body, controls 35～42 ℃ of fluidized-bed layer temperature well; The multiple spot even spraying is disperseed; After operation is accomplished, improve bed temperature to 50～80 ℃ again, Dextrose Monohydrate, xylitol, the stupid fluidisation of sorbose mix lose surface crystallization water after; Pump into the above-mentioned maltodextrin solution that refines; Continuous spray drying granulation is controlled air quantity and mist flow well, obtains even sugariness and modifies good fluffy granular product.
Embodiment 4:
4.5 kilograms of maltodextrins and deionized water are dissolved in a stainless steel reacting by heating pot for 25 kilograms; 25 kilograms also another dissolves in stainless steel reacting by heating pot with deionized water with 1.17 kilograms of Sucraloses, and material is heated to 80 ℃ by chuck in the pot, starts stirring; Add 3.0 kilograms of active carbons respectively; Be incubated 35 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 68.83 kilograms of Dextrose Monohydrates, 10 kilograms of xylitols, 15.5 kilograms of D-sorbites; Pulverizing reaches 180 orders through pulverizer, is sent to fluidisation in the spray-fluidized bed apparatus, and the mixed material of Dextrose Monohydrate, xylitol and D-sorbite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned sucralose solution that refines be sprayed continuously and is distributed on the fine sugar alcohol body, controls 35～50 ℃ of fluidized-bed layer temperature well; The multiple spot even spraying is disperseed; After operation is accomplished, improve bed temperature to 50～80 ℃ again, after Dextrose Monohydrate, xylitol, the stupid fluidisation of sorbose lose surface crystallization water; Pumping into the above-mentioned maltodextrin solution that refines; Continuous Spray Mixing drying-granulating is controlled air quantity and mist flow well, obtains the good fluffy granular product of even sugariness decorations.
Embodiment 5:
Maltodextrin 4.66 and deionized water are dissolved in a stainless steel reacting by heating pot for 25 kilograms; 1.34 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel reacting by heating pot for 20 kilograms, and material is heated to 62 ℃ by chuck in the pot, starts stirring; Add 1 kilogram of active carbon respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 64 kilograms of Dextrose Monohydrates, 12 kilograms of xylitols, 18 kilograms of D-sorbites; Pulverizing reaches 130 orders through pulverizer, is sent in the spray-fluidized bed apparatus, and the mixed material of Dextrose Monohydrate, xylitol and D-sorbite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned sucralose solution that refines continuously spraying be distributed on the fine sugar alcohol body, controlling the fluidized-bed layer temperature is 35～50 ℃; The multiple spot even spraying is disperseed; After operation is accomplished, improve bed temperature to 50～80 ℃ again, Dextrose Monohydrate, xylitol, the stupid fluidisation of sorbose mix lose surface crystallization water after; Pump into the above-mentioned maltodextrin solution that refines; Continuous spray drying granulation is controlled air quantity and mist flow well, obtains even sugariness and modifies good fluffy granular product.
Embodiment 6:
3 kilograms of maltodextrins and deionized water are dissolved in a stainless steel reacting by heating pot for 25 kilograms; 1.66 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel reaction pot for 20 kilograms, and material is heated to 52 ℃ by chuck in the pot, starts stirring; Add 2 kilograms of active carbons respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 66.34 kilograms of Dextrose Monohydrates, 15 kilograms of xylitols, 14 kilograms of D-sorbites; Reach 150 orders through pulverizing, be sent to and carry out the fluidisation mixing in the spray-fluidized bed apparatus, the mixed material of Dextrose Monohydrate, xylitol and D-sorbite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned sucralose solution that refines continuously spraying be distributed on the fine sugar alcohol body, control 35～40 ℃ of fluidized-bed layer temperature; Even spraying is disperseed; After operation is accomplished, improve bed temperature to 50～80 ℃ again, after Dextrose Monohydrate, xylitol, the stupid fluidisation of sorbose being mixed lose surface crystallization water; Pumping into the above-mentioned maltodextrin solution that refines; Continuous spray granulating and drying is controlled air quantity and mist flow well, obtains even sugariness and modifies good fluffy granular product.
Embodiment 7:
5 kilograms of maltodextrins and deionized water are dissolved in a stainless steel reacting by heating pot for 25 kilograms; 1.84 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel reacting by heating pot for 20 kilograms, and material is heated to 60 ℃ by chuck in the pot, starts stirring; Add 2.0 kilograms of active carbons respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 58.16 kilograms of Dextrose Monohydrates, 16 kilograms of xylitols, 19 kilograms of D-sorbites; Pulverizing reaches 160 orders through pulverizer, is sent in the spray-fluidized bed apparatus, and the mixed material of Dextrose Monohydrate, xylitol and D-sorbite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned sucralose solution that refines be sprayed continuously and is distributed on the fine sugar alcohol body, controls 35～42 ℃ of fluidized-bed layer temperature well; The multiple spot even spraying is disperseed; After operation is accomplished, improve bed temperature to 50～80 ℃ again, Dextrose Monohydrate, xylitol, the stupid fluidisation of sorbose mix lose surface crystallization water after; Pump into the above-mentioned maltodextrin solution that refines; Continuous spray drying granulation is controlled air quantity and mist flow well, obtains even sugariness and modifies good fluffy granular product.
Through detecting, adopt the fluffy granular composite low-sugar-content and low-calorie table sweet taste material of technical scheme acquisition of the present invention, its main performance index is seen table 1.
Table 1
| Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Embodiment 6 | Embodiment 4 |
| Particle size | 30～60 orders | 30～60 orders | 30～60 orders | 30～60 orders | 30～60 orders | 30～60 orders | 30～60 orders |
| Sugariness (sucrose contrast) | 5 times | 7 times | 6 times | 7 times | 8 times | 10 times | 11 times |
| Outward appearance | White particle | White particle | White particle | White particle | White particle | White particle | White particle |
| Bulk density (g/mm 3) | 0.60 | 0.62 | 0.63 | 0.66 | 0.60 | 0.62 | 0.66 |
The stability test of sweetener is to check sweetener to guarantee the ability that undergoes no deterioration within a certain period of time, and sweetener (dining table sweetener) product of the embodiment of the invention was stored 3 years at normal temperatures, phenomenons such as rotten and sugariness reduction occur, and the stability ten minutes is superior.
The sugariness degree of modification of fluffy granular composite low-sugar-content and low-calorie table sweet taste material of the present invention; Will be according to the adjustment of Sucralose in consumption, select the common sucrose sugariness usually for use 5～11 times, relatively be fit to people's use needs; Form according to prescription; Under same sugariness situation, people only are 1/5～1/11 of common sucrose to the absorption of heat, and low-sugar-content and low-calorie sweetening agent is the sweet taste article of low-calorie; This dining table sweetener can not cause blood sugar to raise, and satisfies three high crowds, pursues healthy needs of people.
Show obviously that to sum up the present invention adopts scientific formula, uses advanced science and technology technology and method, products obtained therefrom does not have smell, do not have color, and is soluble in water, and it is very convenient that this fluffy granular low-sugar-content and low-calorie sweetening agent is used.Granularity, molten speed, mouthfeel, sugariness all are much better than the prior art value, and the scientific preparation process simple flow is prone to row, are fit to very much large-scale production, are worth wide popularization and application in the field of business.
What need understand is: the above only is a preferred implementation of the present invention; For those skilled in the art; Under the prerequisite that does not break away from the principle of the invention, can also make some improvement and retouching, these improvement and retouching also should be regarded as protection scope of the present invention.
Claims (5)
1. granular composite low-sugar-content and low-calorie table sweetening agent; It is characterized in that becoming to be grouped into: Dextrose Monohydrate 55～77% by following percentage by weight; Xylitol 9～18%, D-sorbite 11～20%, maltodextrin 3～5%; Sucralose 0.8～1.85%, above-mentioned each substance weight percentage sum is 100%; Its preparation method comprises following processing step:
1. maltodextrin, Sucralose are joined respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 52～80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned maltodextrin solution and the sucralose solution, be incubated 25～30 minutes, filter while hot, for use in the storage tank that is pooled to heat tracing respectively of filtrating;
4. put in the spray-fluidized bed apparatus after Dextrose Monohydrate, xylitol and D-sorbite being pulverized; The mixed material of Dextrose Monohydrate, xylitol and D-sorbite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The bed temperature scope of fluidized bed with spraying is 35～80 ℃; Wherein the bed temperature of phase I Sucralose spraying dispersion is 35～50 ℃; The bed temperature of second stage maltodextrin mist projection granulating is 50～80 ℃, and the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, pumps into the above-mentioned maltodextrin solution that refines again; Spray-drying obtains fluffy granular composite low-sugar-content and low-calorie table sweet taste material continuously.
2. granular composite low-sugar-content and low-calorie table sweetening agent according to claim 1 is characterized in that being become to be grouped into by following percentage by weight: Dextrose Monohydrate 65%, xylitol 11%, D-sorbite 19%, maltodextrin 3.83%, Sucralose 1.17%.
3. granular composite low-sugar-content and low-calorie table sweetening agent according to claim 1 and 2 is characterized in that: said maltodextrin DE value is 10～20.
4. the preparation method of the described granular composite low-sugar-content and low-calorie table sweetening agent of claim 1 is characterized in that: comprise following processing step---
1. maltodextrin, Sucralose are joined respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 52～80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned maltodextrin solution and the sucralose solution, be incubated 25～30 minutes, filter while hot, for use in the storage tank that is pooled to heat tracing respectively of filtrating;
4. put in the spray-fluidized bed apparatus after Dextrose Monohydrate, xylitol and D-sorbite being pulverized; The mixed material of Dextrose Monohydrate, xylitol and D-sorbite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The bed temperature scope of fluidized bed with spraying is 35～80 ℃; Wherein the bed temperature of phase I Sucralose spraying dispersion is 35～50 ℃; The bed temperature of second stage maltodextrin mist projection granulating is 50～80 ℃, and the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, pumps into the above-mentioned maltodextrin solution that refines again; Spray-drying obtains fluffy granular composite low-sugar-content and low-calorie table sweet taste material continuously.
5. the preparation method of granular composite low-sugar-content and low-calorie table sweetening agent according to claim 4 is characterized in that: maltodextrin, Sucralose are joined respectively in the container, add deionized water respectively and mix; Be warming up to 60～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrating is pooled to respectively in the storage tank that has heat tracing; Dextrose Monohydrate, xylitol and D-sorbite reach 120～180 orders through pulverizing; Be sent in the spray-fluidized bed apparatus; The mixed material of Dextrose Monohydrate, xylitol and D-sorbite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and control fluidized-bed layer temperature is at 35～80 ℃, and the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned sucralose solution that refines be sprayed continuously and is distributed on the fine sugar alcohol body; After the mixing of sugar alcohol fluidisation loses surperficial moisture content; Pump into the above-mentioned maltodextrin solution that refines again, spray drying granulation obtains fluffy granular composite low-sugar-content and low-calorie table sweet taste material continuously.
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1713825A (en) * | 2002-12-18 | 2005-12-28 | 株式会社上野制药应用研究所 | Food containing sweetener mixture |
| CN101299929A (en) * | 2005-09-13 | 2008-11-05 | 麦克内尔营养有限公司 | Methods and compositions to improve the palatability of foods |
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2009
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1713825A (en) * | 2002-12-18 | 2005-12-28 | 株式会社上野制药应用研究所 | Food containing sweetener mixture |
| CN101299929A (en) * | 2005-09-13 | 2008-11-05 | 麦克内尔营养有限公司 | Methods and compositions to improve the palatability of foods |
Non-Patent Citations (1)
| Title |
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| 王建国."甜味剂的现状与发展".《江西化工》.2008,(第4期),第82-84页. |
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| CN101874601A (en) | 2010-11-03 |
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