CN101874600B - Granular composite low-sugar low-calorie dining table sweetener and preparation method thereof - Google Patents
Granular composite low-sugar low-calorie dining table sweetener and preparation method thereof Download PDFInfo
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- CN101874600B CN101874600B CN200910252039A CN200910252039A CN101874600B CN 101874600 B CN101874600 B CN 101874600B CN 200910252039 A CN200910252039 A CN 200910252039A CN 200910252039 A CN200910252039 A CN 200910252039A CN 101874600 B CN101874600 B CN 101874600B
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Abstract
The invention relates to a granular composite low-sugar low-calorie dining table sweetener and a preparation method thereof. The sweetener comprises the following components in percentage by weight: 60 to 80 percent of dextrose monohydrate, 5 to 15 percent of xylitol, 4 to 18 percent of erythritol, 6 to 10 percent of maltodextrin, and 0.8 to 1.85 percent of splenda. The preparation method comprises the steps of: adding the maltodextrin and the splenda into heating containers respectively, adding deionized water into the heating containers and mixing respectively, and heating to dissolve the solution; adding activated carbon into the solution respectively, filtering the solution when the solution is hot, and collecting the filtrate in the two heating containers into a storage tank; allowing the mixed materials of crushed dextrose monohydrate, xylitol, and sorbitol to enter a spraying fluidized bed from the bottom with positive pressure and accelerating the flow from bottom to top, and applying negative pressure to the upper part of the spraying fluidized bed to vibrate from top to down, so that the materials boil up and down in the spraying fluidized bed; and continuously spraying and dispersing refined solution of splenda on superfine sugar alcohol by using a multipoint spay gun on the side of the fluidized bed, pumping solution of maltodextrin, and continuously spraying and drying to obtain the low-sugar low-calorie sweetener. The preparation process is simple and convenient, and is easy to operate.
Description
Technical field
The present invention relates to a kind of edible dining table sweetener, relate in particular to a kind of fluffy granular composite low-sugar-content and low-calorie table sweet taste material and preparation method thereof.
Background technology
The increase of Along with people's because of too much bringing disease with sugar, people's demand safety, healthy low-sugar-content and low-calorie type sweetener (dining table sweetener); In production procedure, reach the advanced preparation technology who puts into finished product one step completion from raw material; It is learnt from other's strong points to offset one's weaknesses, has complementary advantages to make between the sugar alcohol sweet taste on the formula for a product; Can play during product uses and cover the effect that promotes mouthfeel with synergy; People thirst for satisfying under the low prerequisite of sugariness height, heat, and occupation modeization, with cane-sugar taste safety and Health low-sugar-content and low-calorie type sweetener (dining table sweetener) roughly the same.
Summary of the invention
The objective of the invention is to overcome the deficiency that prior art exists; A kind of fluffy granular composite low-sugar and low-calorie sweetener (dining table sweetener) and preparation method thereof is provided; Adopt the scientific technology of easy operation control, the molten speed property of product, mouthfeel, sugariness all are higher than the prior art optimum value.
The object of the invention is realized through following technical scheme:
A kind of granular composite low-sugar-content and low-calorie table sweetening agent, characteristics are to comprise following composition (percentage by weight): Dextrose Monohydrate 60～80%, xylitol 5～15%, antierythrite 4～18%, maltodextrin 6～10%, Sucralose 0.8～1.85%.
Further, above-mentioned a kind of granular composite low-sugar-content and low-calorie table sweetening agent, wherein: Dextrose Monohydrate 80%, xylitol 6%, D-sorbite 4%, maltodextrin 8.83%, Sucralose 1.17%.
Further, above-mentioned a kind of granular composite low-sugar-content and low-calorie table sweetening agent, said maltodextrin DE value is 10～20.
The preparation method of fluffy granular composite low-sugar-content and low-calorie table sweet taste material of the present invention comprises following processing step:
1. maltodextrin, Sucralose are joined respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 52～80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned maltodextrin solution and the sucralose solution, be incubated 25～30 minutes, filter while hot, filtrating is pooled to respectively in the storage tank of heat tracing;
4. put in the spray-fluidized bed apparatus after Dextrose Monohydrate, xylitol and antierythrite being pulverized; The mixed material of Dextrose Monohydrate, xylitol and antierythrite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body; Pump into the above-mentioned maltodextrin solution that refines again, spray-drying obtains fluffy granular composite low-sugar and low-calorie sweetener (dining table sweetener) continuously.
Again further, the preparation method of above-mentioned a kind of granular composite low-sugar-content and low-calorie table sweetening agent joins maltodextrin, Sucralose respectively in the heating container, adds deionized water respectively and mixes; Be warming up to 60～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrating is pooled to respectively in the storage tank that has heat tracing; Dextrose Monohydrate, xylitol and antierythrite reach 120～180 orders through pulverizing; Be sent in the spray-fluidized bed apparatus; The mixed material of Dextrose Monohydrate, xylitol and antierythrite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and control fluidized-bed layer temperature is at 35～80 ℃, and the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned sucralose solution that refines be sprayed continuously and is distributed on the fine sugar alcohol body; After above-mentioned various sugar alcohol fluidisations mixing lose surperficial moisture content; Pump into the above-mentioned maltodextrin solution that refines again, spray drying granulation obtains fluffy granular composite low-sugar-content and low-calorie table sweet taste material continuously.
Again further; The preparation method of above-mentioned a kind of granular composite low-sugar-content and low-calorie table sweetening agent; The bed temperature scope of said fluidized bed with spraying is 35～80 ℃; Wherein the bed temperature of phase I Sucralose spraying dispersion is 35～50 ℃, and the bed temperature of second stage maltodextrin mist projection granulating is 50～80 ℃.
Again further, the preparation method of above-mentioned a kind of granular composite low-sugar-content and low-calorie table sweetening agent, in the phase I of said Spray Mixing fluid bed, the Sucralose spraying is dispersed in fluidisation and smashes on the fine sugar alcohol crystal body; In second stage, the maltodextrin spray drying granulation is on the noncrystal of mixing sugar alcohol.
Substantive distinguishing features and obvious improvement that technical scheme of the present invention is outstanding are mainly reflected in:
Adopt the negative pressure fluid bed fluidization technique of scientific formula, uses advanced to combine the multi-point atomizing method, time sharing segment control appliance bed temperature efficiently solves even dispersion, coats problems such as granulation, drying.With Dextrose Monohydrate, xylitol, antierythrite, Sucralose is primary raw material; Modify uniformly and coat through preparation method to sugariness, make product sweetness reach 5～11 times of common sucrose, products obtained therefrom does not have smell, does not have color; Soluble in water; This fluffy granular composite low-sugar and low-calorie sweetener is easy to use, and its preparation process science is simple and easy to operate, is fit to very much large-scale production.
Description of drawings
Below in conjunction with accompanying drawing technical scheme of the present invention is described further:
Fig. 1: process chart of the present invention.
The specific embodiment
A kind of granular composite low-sugar-content and low-calorie table sweetening agent, its composition is: Dextrose Monohydrate 60～80%, xylitol 5～15%, antierythrite 4～18%, maltodextrin 6～10%, Sucralose 0.8～1.85%.Ideal formulations is:: Dextrose Monohydrate 80%, xylitol 6%, D-sorbite 4%, maltodextrin 8.83%, Sucralose 1.17%.
As shown in Figure 1, a kind of preparation technology of granular composite low-sugar-content and low-calorie table sweetening agent: at first, maltodextrin, Sucralose are joined respectively in the heating container, add deionized water respectively and mix; Be warming up to 52～80 ℃ of dissolvings respectively, and stir; Add active carbon in above-mentioned maltodextrin solution and the sucralose solution respectively, be incubated 25～30 minutes, filter while hot, filtrating is pooled to respectively in the storage tank of heat tracing; Then; Put into after Dextrose Monohydrate, xylitol and antierythrite pulverized in the spray-fluidized bed apparatus (at heating temperature control and technological with the boiling that in fluid bed, circulates of sugar alcohol material through the positive negative pressure boiling of equipment; Mix that fluidisation is anhydrated and fluffy processing; Sugar alcohol mixtures material → malleation material quickens to flow from bottom to top → and negative pressure vibrates → makes material boiling up and down in fluid bed → by the fluid bed side multiple spot spray gun liquid material ejection fog-like liquid of naming a person for a particular job from top to bottom; Be sprayed onto on the trickle solid material body of boiling); The mixed material of Dextrose Monohydrate, xylitol and antierythrite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, and the bed temperature that the spraying of control Sucralose disperses is 35～50 ℃, and the Sucralose even spraying is dispersed on the mixing sugar alcohol crystalline solid of powder; The rising bed temperature; At mixing sugar alcohol after fluidisation loses surface crystallization water; Pump into the above-mentioned maltodextrin solution that refines again; Continuous spray drying granulation, the bed temperature of maltodextrin mist projection granulating controlled well is 50～80 ℃, the maltodextrin spray drying granulation is on the noncrystalline fluffy body of sugar alcohol; Obtain even sugariness and modify fluffy good shape product.
Embodiment 1:
Maltodextrin 9.16 and deionized water are dissolved in a stainless steel reacting by heating pot for 30 kilograms; 0.84 kilogram of Sucralose and deionized water are also dissolved in another stainless steel reacting by heating pot for 15 kilograms, and material is heated to 62 ℃ by chuck in the pot, starts stirring; Add 2 kilograms of active carbons respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 77 kilograms of Dextrose Monohydrates, 5 kilograms of xylitols, 8 kilograms of antierythrites; Pulverizing reaches 130 orders through pulverizer, is sent in the spray-fluidized bed apparatus, and the mixed material of Dextrose Monohydrate, xylitol and D-sorbite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned sucralose solution that refines continuously spraying be distributed on the fine sugar alcohol body, controlling the fluidized-bed layer temperature is 35～50 ℃; The multiple spot even spraying is disperseed; After operation is accomplished, improve bed temperature to 50～80 ℃ again, Dextrose Monohydrate, xylitol, antierythrite fluidisation mix lose surface crystallization water after; Pump into the above-mentioned maltodextrin solution that refines; Continuous spray drying granulation is controlled air quantity and mist flow well, obtains even sugariness and modifies good fluffy granular product.
Embodiment 2:
8.83 kilograms of maltodextrins and deionized water are dissolved in a stainless steel reacting by heating pot for 30 kilograms; 1.17 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel reaction pot for 20 kilograms, and material is heated to 52 ℃ by chuck in the pot, starts stirring; Add 2 kilograms of active carbons respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 80 kilograms of Dextrose Monohydrates, 6 kilograms of xylitols, 4 kilograms of antierythrites; Reach 150 orders through pulverizing, be sent to and carry out the fluidisation mixing in the spray-fluidized bed apparatus, the mixed material of Dextrose Monohydrate, xylitol and antierythrite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned sucralose solution that refines continuously spraying be distributed on the fine sugar alcohol body, control 35～40 ℃ of fluidized-bed layer temperature; Even spraying is disperseed; After operation is accomplished, improve bed temperature to 50～80 ℃ again, after Dextrose Monohydrate, xylitol, antierythrite fluidisation being mixed lose surface crystallization water; Pumping into the above-mentioned maltodextrin solution that refines; Continuous spray granulating and drying is controlled air quantity and mist flow well, obtains even sugariness and modifies good fluffy granular product.
Embodiment 3:
6 kilograms of maltodextrins and deionized water are dissolved in a stainless steel reacting by heating pot for 25 kilograms; 1 kilogram of Sucralose and deionized water are also dissolved in another stainless steel reacting by heating pot for 20 kilograms, and material is heated to 60 ℃ by chuck in the pot, starts stirring; Add 2.0 kilograms of active carbons respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 78 kilograms of Dextrose Monohydrates, 8 kilograms of xylitols, 7 kilograms of antierythrites; Pulverizing reaches 160 orders through pulverizer, is sent in the spray-fluidized bed apparatus, and the mixed material of Dextrose Monohydrate, xylitol and antierythrite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned sucralose solution that refines be sprayed continuously and is distributed on the fine sugar alcohol body, controls 35～42 ℃ of fluidized-bed layer temperature well; The multiple spot even spraying is disperseed; After operation is accomplished, improve bed temperature to 50～80 ℃ again, Dextrose Monohydrate, xylitol, antierythrite fluidisation mix lose surface crystallization water after; Pump into the above-mentioned maltodextrin solution that refines; Continuous spray drying granulation is controlled air quantity and mist flow well, obtains even sugariness and modifies good fluffy granular product.
Embodiment 4:
6 kilograms of maltodextrins and deionized water are dissolved in a stainless steel reacting by heating pot for 25 kilograms; 25 kilograms also another dissolves in stainless steel reacting by heating pot with deionized water with 1.17 kilograms of Sucraloses, and material is heated to 80 ℃ by chuck in the pot, starts stirring; Add 3.0 kilograms of active carbons respectively; Be incubated 35 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 73.83 kilograms of Dextrose Monohydrates, 9 kilograms of xylitols, 10 kilograms of antierythrites; Pulverizing reaches 180 orders through pulverizer, is sent to fluidisation in the spray-fluidized bed apparatus, and the mixed material of Dextrose Monohydrate, xylitol and antierythrite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned sucralose solution that refines be sprayed continuously and is distributed on the fine sugar alcohol body, controls 35～50 ℃ of fluidized-bed layer temperature well; The multiple spot even spraying is disperseed; After operation is accomplished, improve bed temperature to 50～80 ℃ again, after Dextrose Monohydrate, xylitol, antierythrite fluidisation lose surface crystallization water; Pumping into the above-mentioned maltodextrin solution that refines; Continuous Spray Mixing drying-granulating is controlled air quantity and mist flow well, obtains the good fluffy granular product of even sugariness decorations.
Embodiment 5:
Maltodextrin 7.66 and deionized water are dissolved in a stainless steel reacting by heating pot for 25 kilograms; 1.34 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel reacting by heating pot for 20 kilograms, and material is heated to 62 ℃ by chuck in the pot, starts stirring; Add 1 kilogram of active carbon respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 66 kilograms of Dextrose Monohydrates, 11 kilograms of xylitols, 14 kilograms of antierythrites; Pulverizing reaches 130 orders through pulverizer, is sent in the spray-fluidized bed apparatus, and the mixed material of Dextrose Monohydrate, xylitol and antierythrite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned sucralose solution that refines continuously spraying be distributed on the fine sugar alcohol body, controlling the fluidized-bed layer temperature is 35～50 ℃; The multiple spot even spraying is disperseed; After operation is accomplished, improve bed temperature to 50～80 ℃ again, Dextrose Monohydrate, xylitol, antierythrite fluidisation mix lose surface crystallization water after; Pump into the above-mentioned maltodextrin solution that refines; Continuous spray drying granulation is controlled air quantity and mist flow well, obtains even sugariness and modifies good fluffy granular product.
Embodiment 6:
6.34 kilograms of maltodextrin public affairs and deionized water are dissolved in a stainless steel reacting by heating pot for 25 kilograms; 1.66 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel reaction pot for 20 kilograms, and material is heated to 52 ℃ by chuck in the pot, starts stirring; Add 2 kilograms of active carbons respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 72 kilograms of Dextrose Monohydrates, 7 kilograms of xylitols, 13 kilograms of antierythrites; Reach 150 orders through pulverizing, be sent to and carry out the fluidisation mixing in the spray-fluidized bed apparatus, the mixed material of Dextrose Monohydrate, xylitol and D-sorbite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned sucralose solution that refines continuously spraying be distributed on the fine sugar alcohol body, control 35～40 ℃ of fluidized-bed layer temperature; Even spraying is disperseed; After operation is accomplished, improve bed temperature to 50～80 ℃ again, after Dextrose Monohydrate, xylitol, antierythrite fluidisation being mixed lose surface crystallization water; Pumping into the above-mentioned maltodextrin solution that refines; Continuous spray granulating and drying is controlled air quantity and mist flow well, obtains even sugariness and modifies good fluffy granular product.
Embodiment 7:
7.16 kilograms of maltodextrins and deionized water are dissolved in a stainless steel reacting by heating pot for 25 kilograms; 1.84 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel reacting by heating pot for 20 kilograms, and material is heated to 60 ℃ by chuck in the pot, starts stirring; Add 2.0 kilograms of active carbons respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 61 kilograms of Dextrose Monohydrates, 12 kilograms of xylitols, 18 kilograms of antierythrites; Pulverizing reaches 160 orders through pulverizer, is sent in the spray-fluidized bed apparatus, and the mixed material of Dextrose Monohydrate, xylitol and antierythrite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned sucralose solution that refines be sprayed continuously and is distributed on the fine sugar alcohol body, controls 35～42 ℃ of fluidized-bed layer temperature well; The multiple spot even spraying is disperseed; After operation is accomplished, improve bed temperature to 50～80 ℃ again, Dextrose Monohydrate, xylitol, antierythrite fluidisation mix lose surface crystallization water after; Pump into the above-mentioned maltodextrin solution that refines; Continuous spray drying granulation is controlled air quantity and mist flow well, obtains even sugariness and modifies good fluffy granular product.
Through detecting, adopt the fluffy granular composite low-sugar and low-calorie sweetener (dining table sweetener) of technical scheme acquisition of the present invention, its main performance index is seen table 1.
Table 1
| Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Embodiment 6 | Embodiment 7 |
| Particle size | 30～60 orders | 30～60 orders | 30～60 orders | 30～60 orders | 30～60 orders | 30～60 orders | 30～60 orders |
| Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Embodiment 6 | Embodiment 7 |
| Sugariness (sucrose contrast) | 5 times | 7 times | 6 times | 7 times | 8 times | 10 times | 11 times |
| Outward appearance | White particle | White particle | White particle | White particle | White particle | White particle | White particle |
| Bulk density (g/mm 3) | 0.60 | 0.62 | 0.63 | 0.66 | 0.60 | 0.62 | 0.63 |
The stability test of sweetener is to check sweetener to guarantee the ability that undergoes no deterioration within a certain period of time, and the dining table sweetener product of the embodiment of the invention was stored 3 years at normal temperatures, phenomenons such as rotten and sugariness reduction occur, and the stability ten minutes is superior.
The sugariness degree of modification of fluffy granular composite low-sugar and low-calorie sweetener of the present invention (dining table sweetener); Will be according to the adjustment of Sucralose in consumption, select the common sucrose sugariness usually for use 5～11 times, relatively be fit to people's use needs; Form according to prescription; Under same sugariness situation, people only are 1/5～1/11 of common sucrose to the absorption of heat, and low-sugar-content and low-calorie sweetening agent is the sweet taste article of low-calorie; This sweetener (dining table sweetener) can not cause blood sugar to raise, and satisfies three high crowds, pursues healthy needs of people.
Show obviously that to sum up the present invention adopts scientific formula, uses advanced science and technology technology and method, products obtained therefrom does not have smell, do not have color, and is soluble in water, and it is very convenient that this fluffy granular low-sugar-content and low-calorie sweetening agent is used.Granularity, molten speed, mouthfeel, sugariness all are much better than the prior art value, and the scientific preparation process simple flow is prone to row, are fit to very much large-scale production, are worth wide popularization and application in the field of business.
What need understand is: the above only is a preferred implementation of the present invention; For those skilled in the art; Under the prerequisite that does not break away from the principle of the invention, can also make some improvement and retouching, these improvement and retouching also should be regarded as protection scope of the present invention.
Claims (5)
1. a granular composite low-sugar-content and low-calorie table sweetening agent is characterized in that comprising following percentage by weight composition: Dextrose Monohydrate 60～80%, xylitol 5～15%, antierythrite 4～18%, maltodextrin 6～10%, Sucralose 0.8～1.85%; Its preparation method comprises following processing step:
1. maltodextrin, Sucralose are joined respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 52～80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned maltodextrin solution and the sucralose solution, be incubated 25～30 minutes, filter while hot, for use in the storage tank that is pooled to heat tracing respectively of filtrating;
4. put in the spray-fluidized bed apparatus after Dextrose Monohydrate, xylitol and antierythrite being pulverized; The mixed material of Dextrose Monohydrate, xylitol and antierythrite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body; Pump into the above-mentioned maltodextrin solution that refines again, spray-drying obtains fluffy granular composite low-sugar-content and low-calorie table sweet taste material continuously.
2. a kind of granular composite low-sugar-content and low-calorie table sweetening agent according to claim 1 is characterized in that: said maltodextrin DE value is 10～20.
3. the preparation method of the described a kind of granular composite low-sugar-content and low-calorie table sweetening agent of claim 1 is characterized in that: comprise following processing step---
1. maltodextrin, Sucralose are joined respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 52～80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned maltodextrin solution and the sucralose solution, be incubated 25～30 minutes, filter while hot, for use in the storage tank that is pooled to heat tracing respectively of filtrating;
4. put in the spray-fluidized bed apparatus after Dextrose Monohydrate, xylitol and antierythrite being pulverized; The mixed material of Dextrose Monohydrate, xylitol and antierythrite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body; Pump into the above-mentioned maltodextrin solution that refines again, spray-drying obtains fluffy granular composite low-sugar-content and low-calorie table sweet taste material continuously.
4. the preparation method of a kind of granular composite low-sugar-content and low-calorie table sweetening agent according to claim 3 is characterized in that: maltodextrin, Sucralose are joined respectively in the container, add deionized water respectively and mix; Be warming up to 60～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrating is pooled to respectively in the storage tank that has heat tracing; Dextrose Monohydrate, xylitol and antierythrite reach 120～180 orders through pulverizing; Be sent in the spray-fluidized bed apparatus; The mixed material of Dextrose Monohydrate, xylitol and antierythrite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and control fluidized-bed layer temperature is at 35～80 ℃, and the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned sucralose solution that refines be sprayed continuously and is distributed on the fine sugar alcohol body; After the mixing of sugar alcohol fluidisation loses surperficial moisture content; Pump into the above-mentioned maltodextrin solution that refines again, spray drying granulation obtains the fluffy granular composite low-sugar and low-calorie sweetener dining table sweetener continuously.
5. the preparation method of a kind of granular composite low-sugar-content and low-calorie table sweetening agent according to claim 4; It is characterized in that: the bed temperature scope of said fluidized bed with spraying is 35～80 ℃; Wherein the bed temperature of phase I Sucralose spraying dispersion is 35～50 ℃, and the bed temperature of second stage maltodextrin mist projection granulating is 50～80 ℃.
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| CN102524633A (en) * | 2010-12-16 | 2012-07-04 | 苏州工业园区尚融科技有限公司 | Dining table sugar containing xylooligosaccharide, and preparation method thereof |
| CN102524632A (en) * | 2010-12-16 | 2012-07-04 | 苏州工业园区尚融科技有限公司 | Dining table sugar containing xylooligosaccharide and sucralose, and preparation method thereof |
| CN103211200A (en) * | 2012-11-30 | 2013-07-24 | 苏州工业园区尚融科技有限公司 | High-intensity composite sweetener containing xylitol and preparation method thereof |
| CN102960687A (en) * | 2012-11-30 | 2013-03-13 | 苏州工业园区尚融科技有限公司 | Xylitol compound sweetener and preparation method thereof |
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| CN101120768A (en) * | 2007-09-07 | 2008-02-13 | 苏州苏克瑞甜品科技有限公司 | Liquid sweetener and its preparation method |
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| CN101534661A (en) * | 2006-09-18 | 2009-09-16 | 麦克内尔营养有限公司 | Cohesive non-free flowing sweetener compositions containing a hygroscopic gluing agent and a desiccant |
| CN101120768A (en) * | 2007-09-07 | 2008-02-13 | 苏州苏克瑞甜品科技有限公司 | Liquid sweetener and its preparation method |
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