CN101120768A - Liquid sweetener and its preparation method - Google Patents
Liquid sweetener and its preparation method Download PDFInfo
- Publication number
- CN101120768A CN101120768A CNA2007101320261A CN200710132026A CN101120768A CN 101120768 A CN101120768 A CN 101120768A CN A2007101320261 A CNA2007101320261 A CN A2007101320261A CN 200710132026 A CN200710132026 A CN 200710132026A CN 101120768 A CN101120768 A CN 101120768A
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- CN
- China
- Prior art keywords
- liquid sweetener
- agent
- add
- added
- liquid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 239000007788 liquid Substances 0.000 title claims abstract description 31
- 235000003599 food sweetener Nutrition 0.000 title claims description 38
- 239000003765 sweetening agent Substances 0.000 title claims description 38
- 238000002360 preparation method Methods 0.000 title claims description 10
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 31
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000003963 antioxidant agent Substances 0.000 claims abstract description 11
- 235000006708 antioxidants Nutrition 0.000 claims abstract description 11
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 11
- 239000003085 diluting agent Substances 0.000 claims abstract description 11
- 239000002562 thickening agent Substances 0.000 claims abstract description 11
- 239000000203 mixture Substances 0.000 claims abstract description 4
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 27
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims description 22
- 238000003756 stirring Methods 0.000 claims description 20
- 239000004376 Sucralose Substances 0.000 claims description 17
- BAQAVOSOZGMPRM-QBMZZYIRSA-N sucralose Chemical compound O[C@@H]1[C@@H](O)[C@@H](Cl)[C@@H](CO)O[C@@H]1O[C@@]1(CCl)[C@@H](O)[C@H](O)[C@@H](CCl)O1 BAQAVOSOZGMPRM-QBMZZYIRSA-N 0.000 claims description 16
- 235000019408 sucralose Nutrition 0.000 claims description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 16
- 239000000243 solution Substances 0.000 claims description 12
- CHHHXKFHOYLYRE-UHFFFAOYSA-M 2,4-Hexadienoic acid, potassium salt (1:1), (2E,4E)- Chemical group [K+].CC=CC=CC([O-])=O CHHHXKFHOYLYRE-UHFFFAOYSA-M 0.000 claims description 11
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 claims description 11
- 229930003268 Vitamin C Natural products 0.000 claims description 11
- 239000004302 potassium sorbate Substances 0.000 claims description 11
- 235000010241 potassium sorbate Nutrition 0.000 claims description 11
- 229940069338 potassium sorbate Drugs 0.000 claims description 11
- 235000019154 vitamin C Nutrition 0.000 claims description 11
- 239000011718 vitamin C Substances 0.000 claims description 11
- 229920002907 Guar gum Polymers 0.000 claims description 10
- 239000000665 guar gum Substances 0.000 claims description 10
- 229960002154 guar gum Drugs 0.000 claims description 10
- 235000010417 guar gum Nutrition 0.000 claims description 10
- 238000010792 warming Methods 0.000 claims description 10
- 230000003078 antioxidant effect Effects 0.000 claims description 9
- 239000007853 buffer solution Substances 0.000 claims description 9
- 238000005374 membrane filtration Methods 0.000 claims description 9
- 229920001817 Agar Polymers 0.000 claims description 6
- 239000008272 agar Substances 0.000 claims description 6
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 5
- 239000003651 drinking water Substances 0.000 claims description 5
- 235000020188 drinking water Nutrition 0.000 claims description 5
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical group CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 claims description 5
- 229910052708 sodium Inorganic materials 0.000 claims description 5
- 239000011734 sodium Substances 0.000 claims description 5
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 claims description 5
- 235000010234 sodium benzoate Nutrition 0.000 claims description 5
- 239000004299 sodium benzoate Substances 0.000 claims description 5
- 150000001413 amino acids Chemical class 0.000 claims description 4
- -1 amino-acid salt Chemical class 0.000 claims description 4
- CEYULKASIQJZGP-UHFFFAOYSA-L disodium;2-(carboxymethyl)-2-hydroxybutanedioate Chemical compound [Na+].[Na+].[O-]C(=O)CC(O)(C(=O)O)CC([O-])=O CEYULKASIQJZGP-UHFFFAOYSA-L 0.000 claims description 4
- 239000001508 potassium citrate Substances 0.000 claims description 4
- 229960002635 potassium citrate Drugs 0.000 claims description 4
- QEEAPRPFLLJWCF-UHFFFAOYSA-K potassium citrate (anhydrous) Chemical compound [K+].[K+].[K+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O QEEAPRPFLLJWCF-UHFFFAOYSA-K 0.000 claims description 4
- 235000011082 potassium citrates Nutrition 0.000 claims description 4
- 229960004106 citric acid Drugs 0.000 claims description 2
- 235000015165 citric acid Nutrition 0.000 claims description 2
- 229930006000 Sucrose Natural products 0.000 abstract description 5
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 abstract description 5
- 238000004519 manufacturing process Methods 0.000 abstract description 5
- 239000005720 sucrose Substances 0.000 abstract description 5
- 239000004599 antimicrobial Substances 0.000 abstract 2
- 230000003301 hydrolyzing effect Effects 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 230000009967 tasteless effect Effects 0.000 abstract 1
- 238000003860 storage Methods 0.000 description 4
- 230000007062 hydrolysis Effects 0.000 description 3
- 238000006460 hydrolysis reaction Methods 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000013112 stability test Methods 0.000 description 1
Abstract
The present invention provides a liquid sweeting agent and the manufacturing method. The compositions of the present invention are: sucrose trichloride 10-28%, diluent 58-89.93%, antiseptic agents 0.01-3.0%, acidity buffer 0.01-3.0%, anti-oxidants 0.01-2.0%, anti-crystallizing agents 0.02-3.0%, thickening agent 0.02-3.0%. The manufacturing method is as following. Firstly, the diluent is added into the container and is heated to 35 centigrade to 55 centigrade. Secondly, sucrose trichloride is added in and stirred up to make the sucrose trichloride dissolve. Thirdly, the active carbon is added in. The mixed liquid is filtered after 15-25 minutes, and then the solution is transfered into another container. After the temperature of the solution is reduced to room temperature, and antiseptic agent, acidity buffer, anti-oxidants, anti-crystallizing agents and thickening agent are added in. Finally, the mixture is mixed evenly. The present invention used scientific formula, advanced modulation method. The produced liquid sweeting agent is tasteless and colorless. Under the normal temperature, the products can be stored two years long without denaturalization phenomenon of color changing or hydrolyzing and so on. The production has moderate sugariness, simple manufacturing technology and is convenient to prepare.
Description
Technical field
The present invention relates to a kind of edible sweetener, relate in particular to prescription of liquid sweetener and preparation method thereof.
Background technology
In daily life, sweetener more and more is widely used, sweetener particularly of new generation---Sucralose because security, pure taste, no calorie, sugariness height, the edible advantage such as carious tooth that can not cause, has been familiar with by people and has been accepted use.
But sweetener product is that solid forms, sugariness are 600 times of sucrose, and during use, metering is extremely inconvenient; Make liquid form, have " stability " problem.
Therefore, the new liquid sweetener of the moderate good stability of a kind of sugariness will be the technical task that is significant that is worth research.
Summary of the invention
The purpose of this invention is to provide moderate liquid sweetener of a kind of sugariness and preparation method thereof, be intended to effectively solve technical problems such as liquid sweetener storage colour-change, hydrolysis, significantly improve storage stability, the ease of use of sweetener.
Purpose of the present invention is achieved through the following technical solutions:
A kind of liquid sweetener, it is characterized in that comprising following composition (percentage by weight): Sucralose 10～28%, diluent 58～89.93%, anticorrisive agent 0.01～3.0%, acid buffer agent 0.01～3.0%, antioxidant 0.01～2.0%, anti-crystallizing agent 0.02～3.0%, thickener 0.02～3.0%.
Further, above-mentioned liquid sweetener, wherein said diluent are condensed water or membrane filtration water or drinking water; Described anticorrisive agent is potassium sorbate or Sodium Benzoate; Described antioxidant is vitamin C or sodium iso-vc; Described acid buffer agent is at least a in potassium citrate, natrium citricum, citric acid, amino acid, the amino-acid salt; Described anti-crystallizing agent is propane diols or sorbierite; Described thickener is guar gum or agar.
Further, above-mentioned liquid sweetener, wherein Sucralose 20%, membrane filtration water 75%, potassium sorbate 1.25%, citric acid 1.25%, vitamin C 0.5%, sorbierite 1.0%, guar gum 1.0%.
Again further, a kind of preparation method of liquid sweetener is characterized in that: earlier diluent is added in the container, be warming up to 35 ℃～55 ℃, add Sucralose, stirring is dissolved it, adds active carbon again, filters after 15～25 minutes, shift solution to another container, reduce to room temperature, add anticorrisive agent, acid buffer agent, antioxidant, anti-crystallizing agent and thickener again, stir.
Again further, the preparation method of above-mentioned a kind of liquid sweetener adds membrane filtration water in the container earlier, is warming up to 45 ℃, add Sucralose, stirring is dissolved it, adds active carbon again, filters after 20 minutes, shift solution to another container, reduce to room temperature, add potassium sorbate, citric acid, vitamin C, sorbierite and guar gum again, stir.
The outstanding substantive distinguishing features and the obvious improvement of technical solution of the present invention is mainly reflected in:
The present invention adopts the modulator approach of scientific formula, uses advanced, and the liquid sweetener that is obtained does not have smell, do not have color, and normal temperature was stored 2 years down, and variable color, hydrolysis iso-metamorphism phenomenon do not appear in sweetener, and stability better.Liquid sweetener uses without limits, and sugariness can be adjusted arbitrarily by adding pure water, and it is very convenient to use.Compared with prior art, its sugariness is that raw material is easy to get with more than 60 times of weight sucrose, preparation technology simple, preparation is convenient, and storage stability is superior, has extensive market prospects.
The specific embodiment
The prescription of liquid sweetener of the present invention (percentage by weight): Sucralose 10～28%, diluent 58～89.93%, anticorrisive agent 0.01～3.0%, acid buffer agent 0.01～3.0%, antioxidant 0.01～2.0%, anti-crystallizing agent 0.02～3.0%, thickener 0.02～3.0%.Diluent is condensed water or membrane filtration water or drinking water; Anticorrisive agent is potassium sorbate or Sodium Benzoate; Antioxidant is vitamin C or sodium iso-vc; Acid buffer agent is at least a in potassium citrate, natrium citricum, citric acid, amino acid, the amino-acid salt; Anti-crystallizing agent is propane diols or sorbierite; Thickener is guar gum or agar.
The prescription of desirable liquid sweetener preferred (percentage by weight): Sucralose 20%, membrane filtration water 75%, potassium sorbate 1.25%, citric acid 1.25%, vitamin C 0.5%, sorbierite 1.0%, guar gum 1.0%.
The manufacturing process of liquid sweetener: earlier diluent is added in the container, be warming up to 35 ℃～55 ℃, add Sucralose, stirring is dissolved it, adds active carbon again, filters after 15～25 minutes, shift solution to another container, reduce to room temperature, add anticorrisive agent, acid buffer agent, antioxidant, anti-crystallizing agent and thickener again, stir.
Embodiment 1:
Earlier the 73.0kg condensed water is added in the container, be warming up to 50 ℃, add the 18kg Sucralose, stirring is dissolved it, adds the 1.1kg active carbon again, filter after 18 minutes, shift solution to another container, reduce to room temperature, add 2.0kg potassium sorbate, 2.0kg amino-acid salt, 1.0kg vitamin C, 2.0kg sorbierite again, 2.0kg agar stirs.
Embodiment 2:
Earlier the 89.93kg drinking water is added in the container, be warming up to 55 ℃, add the 10kg Sucralose, stirring is dissolved it, adds the 1.0kg active carbon again, filter after 25 minutes, shift solution to another container, reduce to room temperature, add 0.01kg Sodium Benzoate, 0.01kg potassium citrate, 0.01kg sodium iso-vc, 0.02kg propane diols again, 0.02kg agar stirs.
Embodiment 3:
Earlier the 79.7kg drinking water is added in the container, be warming up to 40 ℃, add the 15kg Sucralose, stirring is dissolved it, adds the 1.3kg active carbon again, filter after 17 minutes, shift solution to another container, reduce to room temperature, add 1.0kg Sodium Benzoate, 1.0kg natrium citricum, 0.6kg sodium iso-vc, 1.2kg propane diols again, 1.5kg guar gum stirs.
Embodiment 4:
Earlier 75kg membrane filtration water is added in the container, be warming up to 45 ℃, add the 20kg Sucralose, stirring is dissolved it, adds the 1.2kg active carbon again, filter after 20 minutes, shift solution to another container, reduce to room temperature, add 1.25kg potassium sorbate, 1.25kg citric acid, 0.5kg vitamin C, 1.0kg sorbierite again, 1.0kg guar gum stirs.
Embodiment 5:
Earlier the 58kg condensed water is added in the container, be warming up to 35 ℃, add the 28kg Sucralose, stirring is dissolved it, adds the 1.5kg active carbon again, filter after 15 minutes, shift solution to another container, reduce to room temperature, add 3.0kg potassium sorbate, 3.0kg amino acid, 2.0kg vitamin C, 3.0kg sorbierite again, 3.0kg agar stirs.
The stability test of sweetener is that the check sweetener guarantees the stay-in-grade ability within a certain period of time, and the sweetener of the above embodiment of the present invention was stored 2 years at normal temperatures, and denaturalization phenomenon does not appear in sweetener, and stability is superior.
Can show obviously that to sum up the present invention adopts the modulator approach of scientific formula, uses advanced, effectively solve technical problems such as sweetener storage colour-change, hydrolysis; Products obtained therefrom does not have smell, does not have color.Its sugariness is comparatively moderate, and liquid sweetener uses without limits, and sugariness can be adjusted arbitrarily by adding pure water, and it is very convenient to use.
Below only be concrete exemplary applications of the present invention, protection scope of the present invention is not constituted any limitation.All employing equivalents or equivalence are replaced and the technical scheme of formation, all drop within the rights protection scope of the present invention.
Claims (10)
1. liquid sweetener, it is characterized in that comprising following composition (percentage by weight): Sucralose 10～28%, diluent 58～89.93%, anticorrisive agent 0.01～3.0%, acid buffer agent 0.01～3.0%, antioxidant 0.01～2.0%, anti-crystallizing agent 0.02～3.0%, thickener 0.02～3.0%.
2. a kind of liquid sweetener according to claim 1 is characterized in that: described diluent is condensed water or membrane filtration water or drinking water.
3. a kind of liquid sweetener according to claim 1 is characterized in that: described anticorrisive agent is potassium sorbate or Sodium Benzoate.
4. a kind of liquid sweetener according to claim 1 is characterized in that: described antioxidant is vitamin C or sodium iso-vc.
5. a kind of liquid sweetener according to claim 1 is characterized in that: described acid buffer agent is at least a in potassium citrate, natrium citricum, citric acid, amino acid, the amino-acid salt.
6. a kind of liquid sweetener according to claim 1 is characterized in that: described anti-crystallizing agent is propane diols or sorbierite.
7. a kind of liquid sweetener according to claim 1 is characterized in that: described thickener is guar gum or agar.
8. a kind of liquid sweetener according to claim 1 is characterized in that its component has following percentage by weight: Sucralose 20%, membrane filtration water 75%, potassium sorbate 1.25%, citric acid 1.25%, vitamin C 0.5%, sorbierite 1.0%, guar gum 1.0%.
9. the preparation method of the described a kind of liquid sweetener of claim 1, it is characterized in that: earlier diluent is added in the container, be warming up to 35 ℃～55 ℃, add Sucralose, stirring is dissolved it, add active carbon again, filter after 15～25 minutes, shift solution, reduce to room temperature to another container, add anticorrisive agent, acid buffer agent, antioxidant, anti-crystallizing agent and thickener again, stir.
10. the preparation method of a kind of liquid sweetener according to claim 9, it is characterized in that: earlier membrane filtration water is added in the container, be warming up to 45 ℃, add Sucralose, stirring is dissolved it, add active carbon again, filter after 20 minutes, shift solution, reduce to room temperature to another container, add potassium sorbate, citric acid, vitamin C, sorbierite and guar gum again, stir.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2007101320261A CN101120768B (en) | 2007-09-07 | 2007-09-07 | Liquid sweetener and its preparation method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2007101320261A CN101120768B (en) | 2007-09-07 | 2007-09-07 | Liquid sweetener and its preparation method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101120768A true CN101120768A (en) | 2008-02-13 |
| CN101120768B CN101120768B (en) | 2011-08-31 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2007101320261A Expired - Fee Related CN101120768B (en) | 2007-09-07 | 2007-09-07 | Liquid sweetener and its preparation method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101120768B (en) |
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101779785A (en) * | 2010-03-22 | 2010-07-21 | 苏州工业园区尚融科技有限公司 | Xylo-oligosaccharide compounded fluffy particular sugar-free sweetener and preparation method thereof |
| CN101791105A (en) * | 2010-03-22 | 2010-08-04 | 苏州工业园区尚融科技有限公司 | Fluffy granule-shaped sugar-free sweetener compounded with xylooligosaccharide and preparation method thereof |
| WO2011085645A1 (en) * | 2010-01-18 | 2011-07-21 | 浙江杭州鑫富药业股份有限公司 | Sucralose solution and preparation method thereof |
| CN102224920A (en) * | 2011-05-11 | 2011-10-26 | 深圳市纽全德生物科技有限公司 | Liquid table sweetener and preparation method thereof |
| CN101874599B (en) * | 2009-12-04 | 2012-04-25 | 苏州工业园区尚融科技有限公司 | Composite low-sugar low-calorie dining-table sweetener and preparation method thereof |
| CN101874607B (en) * | 2009-12-04 | 2012-04-25 | 苏州工业园区尚融科技有限公司 | Granular composite low-sugar low-calorie sweetener and preparation method thereof |
| CN102524644A (en) * | 2012-01-18 | 2012-07-04 | 常州市牛塘化工厂有限公司 | Liquid trichlorosucrose |
| CN102599465A (en) * | 2012-03-09 | 2012-07-25 | 张维 | Low-calorie low-cost syrup and making method thereof |
| CN101874600B (en) * | 2009-12-04 | 2012-09-05 | 苏州工业园区尚融科技有限公司 | Granular composite low-sugar low-calorie dining table sweetener and preparation method thereof |
| CN101897425B (en) * | 2009-12-04 | 2012-09-12 | 苏州工业园区尚融科技有限公司 | Fluffy granular composite low-sugar low-calorie table sweetener and preparation method thereof |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20040185093A1 (en) * | 2003-03-18 | 2004-09-23 | Szymczak Christopher E. | Compositions containing sucralose |
| CN1221188C (en) * | 2003-05-30 | 2005-10-05 | 北京威德生物科技有限公司 | Inulin drink composition |
| CN1911114B (en) * | 2006-08-25 | 2012-08-15 | 李罡 | Beverage containing trichloro-saccharose |
-
2007
- 2007-09-07 CN CN2007101320261A patent/CN101120768B/en not_active Expired - Fee Related
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101874599B (en) * | 2009-12-04 | 2012-04-25 | 苏州工业园区尚融科技有限公司 | Composite low-sugar low-calorie dining-table sweetener and preparation method thereof |
| CN101874607B (en) * | 2009-12-04 | 2012-04-25 | 苏州工业园区尚融科技有限公司 | Granular composite low-sugar low-calorie sweetener and preparation method thereof |
| CN101874600B (en) * | 2009-12-04 | 2012-09-05 | 苏州工业园区尚融科技有限公司 | Granular composite low-sugar low-calorie dining table sweetener and preparation method thereof |
| CN101897425B (en) * | 2009-12-04 | 2012-09-12 | 苏州工业园区尚融科技有限公司 | Fluffy granular composite low-sugar low-calorie table sweetener and preparation method thereof |
| WO2011085645A1 (en) * | 2010-01-18 | 2011-07-21 | 浙江杭州鑫富药业股份有限公司 | Sucralose solution and preparation method thereof |
| CN101779785A (en) * | 2010-03-22 | 2010-07-21 | 苏州工业园区尚融科技有限公司 | Xylo-oligosaccharide compounded fluffy particular sugar-free sweetener and preparation method thereof |
| CN101791105A (en) * | 2010-03-22 | 2010-08-04 | 苏州工业园区尚融科技有限公司 | Fluffy granule-shaped sugar-free sweetener compounded with xylooligosaccharide and preparation method thereof |
| CN101779785B (en) * | 2010-03-22 | 2012-09-05 | 苏州工业园区尚融科技有限公司 | Xylo-oligosaccharide compounded fluffy particular sugar-free sweetener and preparation method thereof |
| CN101791105B (en) * | 2010-03-22 | 2012-12-12 | 苏州工业园区尚融科技有限公司 | Fluffy granule-shaped sugar-free sweetener compounded with xylooligosaccharide and preparation method thereof |
| CN102224920A (en) * | 2011-05-11 | 2011-10-26 | 深圳市纽全德生物科技有限公司 | Liquid table sweetener and preparation method thereof |
| CN102524644A (en) * | 2012-01-18 | 2012-07-04 | 常州市牛塘化工厂有限公司 | Liquid trichlorosucrose |
| CN102599465A (en) * | 2012-03-09 | 2012-07-25 | 张维 | Low-calorie low-cost syrup and making method thereof |
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| Publication number | Publication date |
|---|---|
| CN101120768B (en) | 2011-08-31 |
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