CN101779785B - Xylo-oligosaccharide compounded fluffy particular sugar-free sweetener and preparation method thereof - Google Patents
Xylo-oligosaccharide compounded fluffy particular sugar-free sweetener and preparation method thereof Download PDFInfo
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Abstract
The invention relates to a xylo-oligosaccharide compounded fluffy particular sugar-free sweetener and a preparation method thereof. The xylo-oligosaccharide compounded fluffy particular sugar-free sweetener contains the following components of 8.4%-35% of trichlorosucrose, 4%-12% of xylo-oligosaccharide and 55%-87.6% of isomalto-oligosacharide. The preparation method comprises the following steps of: respectively adding the trichlorosucrose, the xylo-oligosaccharide and the isomalto-oligosacharide in a heating container, respectively adding deionized water for mixing and then heating for dissolution; respectively adding activated carbon in an isomalto-oligosacharide solution and a trichlorosucrose solution, filtering when the solutions are hot and respectively collecting filtrates to a storage tank; feeding the mixture of the xylo-oligosaccharide and the isomalto-oligosacharide to a spraying fluidized bed from the bottom of the bed in positive pressure and accelerating the flowing of the mixture from bottom to top, and applying negative pressure on the upper part of the spraying fluidized bed to vibrate from top to bottom to let the mixture boil up and down in the bed; and continuously spraying and dispersing the refined trichlorosucrose solution to superfine sugar alcohol bodies and then pumping the trichlorosucrose solution into the isomalto-oligosacharide solution by using a multi-point spray gun on the side part of the fluidized bed, and then continuously spraying and drying so that the fluffy particular sugar-free sweetener is obtained. The invention has the advantages of simple preparation process, easy operation and suitability for scale production.
Description
Technical field
The present invention relates to a kind of edible sweetener, relate in particular to a kind of Xylo-oligosaccharide compounded fluffy granule-shaped sugar-free sweetener and preparation method thereof.
Background technology
The increase of Along with people's because of too much bringing disease with sugar, people's demand safety, healthy Sugarless type non-nutritive sweetener of not participating in body metabolism; In production procedure, reach the advanced preparation technology who puts into finished product one step completion from raw material; It is learnt from other's strong points to offset one's weaknesses, has complementary advantages to make between the sugar alcohol sweet taste on the formula for a product; Can play during product uses and cover the effect that promotes mouthfeel with synergy; People thirst for satisfying under the low prerequisite of sugariness height, heat, and occupation modeization, with cane-sugar taste safety and Health Sugarless type sweetener roughly the same.
Summary of the invention
The objective of the invention is to overcome the deficiency that prior art exists, a kind of fluffy granular composite sugar-free sweetener and preparation method thereof is provided, adopt the scientific technology of easy operation control, the molten speed property of product, mouthfeel, sugariness all are higher than the prior art optimum value.
The object of the invention is realized through following technical scheme:
Xylo-oligosaccharide compounded fluffy granule-shaped sugar-free sweetener is characterized in that comprising following composition (percentage by weight): Sucralose 8.4～35%, xylo-oligosaccharide 4～12%, oligoisomaltose 55～87.6%.
Further, above-mentioned Xylo-oligosaccharide compounded fluffy granule-shaped sugar-free sweetener, Sucralose 8.5%, xylo-oligosaccharide 4%, oligoisomaltose 87.5%.
Further, above-mentioned Xylo-oligosaccharide compounded fluffy granule-shaped sugar-free sweetener, described xylo-oligosaccharide makes through following technology:
1. take by weighing straw, straw is pulverized, handle, filter, discard filtrating with hot-water soak;
2. add the NaOH aqueous solution and carry out alkali treatment, its alkali purification temp is 23～56 ℃, and the alkali treatment time is 24～36 hours;
3. centrifugal acquisition extract is used the acetic acid aqueous solution neutralising extract, to pH be 4.5～7.5;
4. centrifugal removal deposition after supernatant concentration, is used precipitation with alcohol, leaves standstill then;
5. centrifugal collecting precipitation, dry sediment is made into sediment 3～6% the aqueous solution then to remove ethanol wherein;
6. complex enzyme is carried out enzymolysis processing to the aqueous solution that 5. step makes, hydrolysis temperature is 30～45 ℃, and enzymolysis time is 24～36 hours, and 100mL handles in the aqueous solution and adds 0.05～5g complex enzyme; The component of wherein said complex enzyme is: endo-xylanase 55～85wt%, arabinofuranosidase 10～35wt%, circumscribed zytase 5～10wt%;
7. after enzymolysis finishes, enzymolysis liquid in 100～121 ℃ of deactivations 10～15 minutes, is concentrated in 40～60 ℃ of vacuum then;
8. with macroporous type absorption resin cation purifying concentrate,, obtain light yellow to white powdered granule xylo-oligosaccharide then in 45～55 ℃ of vacuum drying 14～18 hours.
The preparation method of Xylo-oligosaccharide compounded fluffy granule-shaped sugar-free sweetener comprises following processing step---
1. Sucralose, oligoisomaltose are joined respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 52～78 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned sucralose solution and the oligoisomaltose solution, be incubated 25～30 minutes, filter while hot, filtrating is pooled to respectively in the storage tank of heat tracing;
4. with putting in the spray-fluidized bed apparatus after xylo-oligosaccharide and the oligoisomaltose pulverizing; The mixed material of xylo-oligosaccharide and oligoisomaltose also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body; Pump into the above-mentioned oligoisomaltose solution that refines again, spray-drying obtains fluffy granular composite sugar-free sweetener continuously.
Again further, the preparation method of above-mentioned Xylo-oligosaccharide compounded fluffy granule-shaped sugar-free sweetener joins Sucralose, oligoisomaltose respectively in the container, adds deionized water respectively and mixes; Be warming up to 60～70 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrating is pooled to respectively in the storage tank that has heat tracing; Xylo-oligosaccharide and oligoisomaltose reach 120～180 orders through pulverizing; Be sent in the spray-fluidized bed apparatus; The mixed material of xylo-oligosaccharide and oligoisomaltose also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and control fluidized-bed layer temperature is at 35～80 ℃, and the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned sucralose solution that refines be sprayed continuously and is distributed on the fine sugar alcohol body; After the mixing of sugar alcohol fluidisation loses surperficial moisture content; Pump into the above-mentioned oligoisomaltose solution that refines again, spray drying granulation obtains fluffy granular composite sugar-free sweetener continuously.
Again further, the preparation method of above-mentioned Xylo-oligosaccharide compounded fluffy granule-shaped sugar-free sweetener, in the phase I of said Spray Mixing fluid bed, the Sucralose spraying is dispersed in fluidisation and smashes on the fine sugar alcohol crystal body; In second stage, the oligoisomaltose spray drying granulation is on the noncrystal of mixing sugar alcohol.
Substantive distinguishing features and obvious improvement that technical scheme of the present invention is outstanding are mainly reflected in:
The present invention adopts the negative pressure fluid bed fluidization technique of scientific formula, uses advanced to combine the multi-point atomizing method, and time sharing segment control appliance bed temperature efficiently solves even dispersion, coats problems such as granulation, drying.With Sucralose, xylo-oligosaccharide, oligoisomaltose is primary raw material; Modify uniformly and coat through preparation method to sugariness, make product sweetness reach 50～200 times of common sucrose, products obtained therefrom does not have smell, does not have color; Soluble in water; This fluffy granular composite sugar-free sweetener is easy to use, and its preparation process science is simple and easy to operate, is fit to very much large-scale production.
Description of drawings
Below in conjunction with accompanying drawing technical scheme of the present invention is described further:
Fig. 1: process chart of the present invention.
The specific embodiment
Fluffy granular composite sugar-free sweetener of the present invention, its composition is: Sucralose 8.4～35%, xylo-oligosaccharide 4～12%, oligoisomaltose 55～87.6%; Ideal formulations is: Sucralose 8.5%, xylo-oligosaccharide 4%, oligoisomaltose 87.5%.
Above-mentioned xylo-oligosaccharide is raw material with the straw, and through the preparation of complex enzyme zymohydrolysis technology, concrete steps are: 1. take by weighing straw, straw is pulverized, with 50～56 ℃ of hot-water soaks 6～11 hours, filter, discard filtrating; 2. add the NaOH aqueous solution and carry out alkali treatment, the concentration of the NaOH aqueous solution is 0.5～5%, uses volume 22～60 times as straw weight, and its alkali purification temp is 23～56 ℃, and the alkali treatment time is 24～36 hours; 3. centrifugal acquisition extract, using the acetic acid aqueous solution neutralising extract is 4.5～7.5 to pH, the concentration of acetic acid aqueous solution is 20～50%; 4. centrifugal removal deposition after supernatant concentration, is used precipitation with alcohol, and concentration of alcohol is 95%, leaves standstill then 6～12 hours; 5. centrifugal collecting precipitation, dry sediment is made into sediment 3～6% the aqueous solution then to remove ethanol wherein; 6. complex enzyme is carried out enzymolysis processing to the aqueous solution that 5. step makes in proportion, hydrolysis temperature is 30～45 ℃, and enzymolysis time is 24～36 hours, and 100mL handles in the aqueous solution and adds 0.05～5g complex enzyme; Wherein, the component of complex enzyme is: endo-xylanase 55～85wt%, arabinofuranosidase 10～35wt%, circumscribed zytase 5～10wt%; 7. after enzymolysis finishes, enzymolysis liquid in 100～121 ℃ of deactivations 10～15 minutes, is concentrated in 40～60 ℃ of vacuum then; 8. with macroporous type absorption resin cation purifying concentrate; Promptly earlier resin is fully moistened and rise, press the consumption of the concentrated complex enzyme hydrolysis liquid of 100g resin 200mL, 20～40 ℃ of following adsorption treatment 10～20 hours; Filter then; With 20～50% ethanolic solution wash-outs, after eluent concentrates earlier, the desalination in 24～72 hours of dialysing again; In 45～55 ℃ of vacuum drying 14～18 hours, obtain light yellow then to white powdered granule xylo-oligosaccharide.The purity of xylo-oligosaccharide is 80%～85%.
As shown in Figure 1, the preparation technology of Xylo-oligosaccharide compounded fluffy granule-shaped sugar-free sweetener: at first, Sucralose, oligoisomaltose are joined respectively in the heating container, add deionized water respectively and mix; Be warming up to 52～78 ℃ of dissolvings respectively, and stir; Add active carbon respectively in above-mentioned sucralose solution and the oligoisomaltose solution, be incubated 25～30 minutes, filter while hot, filtrating is pooled to respectively in the storage tank of heat tracing; At last; With putting in the spray-fluidized bed apparatus after xylo-oligosaccharide and the oligoisomaltose pulverizing; The mixed material of xylo-oligosaccharide and oligoisomaltose also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, and the bed temperature that the spraying of control Sucralose disperses is 35～50 ℃, and the Sucralose even spraying is dispersed on the mixing sugar alcohol crystalline solid of powder; The rising bed temperature; At mixing sugar alcohol after fluidisation loses surface crystallization water; Pump into the above-mentioned oligoisomaltose solution that refines again; Continuous spray drying granulation, the bed temperature of oligoisomaltose mist projection granulating controlled well is 50～80 ℃, the oligoisomaltose spray drying granulation is on the noncrystalline fluffy body of sugar alcohol; Obtain even sugariness and modify fluffy good shape product.
Embodiment 1:
5 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel reacting by heating pot for 25 kilograms; 8.5 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel reacting by heating pot for 25 kilograms, and material is heated to 67 ℃ by chuck in the pot, starts stirring; Add 0.5 kilogram of active carbon respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 4 kilograms of xylo-oligosaccharides, 82.5 kilograms of oligoisomaltose alcohol, pulverizing reaches 180 orders through pulverizer; Be sent in the spray-fluidized bed apparatus, the mixed material of xylo-oligosaccharide and oligoisomaltose gets into the fluidized bed with spraying from the bottom of fluidized bed with spraying and quickens from bottom to top with malleation and flows, and the top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body; Control fluidized-bed layer temperature is 35～50 ℃, and the multiple spot even spraying is disperseed, after operation is accomplished; Improve bed temperature to 50～55 ℃ again; After xylo-oligosaccharide, the mixing of oligoisomaltose alcohol fluidisation lose surface crystallization water, pump into the above-mentioned oligoisomaltose solution that refines, continuously spray drying granulation; Control air quantity and mist flow well, obtain even sugariness and modify good fluffy granular product.
Embodiment 2:
6 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel reacting by heating pot for 20 kilograms; 17.6 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel reaction pot for 30 kilograms, and material is heated to 70 ℃ by chuck in the pot, starts stirring; Add 1.5 kilograms of active carbons respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 5 kilograms of xylo-oligosaccharides, 71.4 kilograms of oligoisomaltose alcohol reach 180 orders through pulverizing; Be sent to and carry out fluidisation in the spray-fluidized bed apparatus and mix, the mixed material of xylo-oligosaccharide and oligoisomaltose gets into the fluidized bed with spraying and quickens from bottom to top from the bottom of fluidized bed with spraying with malleation and flows, and the top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom material is seethed with excitement up and down in fluid bed; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body; 35～40 ℃ of control fluidized-bed layer temperature, even spraying is disperseed, after operation is accomplished; Improve bed temperature to 50～75 ℃ again; After making xylo-oligosaccharide, the mixing of oligoisomaltose fluidisation lose surface crystallization water, pumping into the above-mentioned oligoisomaltose solution that refines, continuously spray granulating and drying; Control air quantity and mist flow well, obtain even sugariness and modify good fluffy granular product.
Embodiment 3:
7 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel reacting by heating pot for 30 kilograms; 26.4 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel reacting by heating pot for 40 kilograms, and material is heated to 65 ℃ by chuck in the pot, starts stirring; Add 3.0 kilograms of active carbons respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 6 kilograms of xylo-oligosaccharides, 60.6 kilograms of oligoisomaltoses, pulverizing reaches 170 orders through pulverizer; Be sent in the spray-fluidized bed apparatus, the mixed material of xylo-oligosaccharide and oligoisomaltose gets into the fluidized bed with spraying from the bottom of fluidized bed with spraying and quickens from bottom to top with malleation and flows, and the top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body; Control 35～42 ℃ of fluidized-bed layer temperature well, the multiple spot even spraying is disperseed, after operation is accomplished; Improve bed temperature to 50～80 ℃ again; After xylo-oligosaccharide, the mixing of oligoisomaltose fluidisation lose surface crystallization water, pump into the above-mentioned oligoisomaltose solution that refines, continuously spray drying granulation; Control air quantity and mist flow well, obtain even sugariness and modify good fluffy granular product.
Embodiment 4:
8 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel reacting by heating pot for 40 kilograms; 60 kilograms also another dissolves in stainless steel reacting by heating pot with deionized water with 33 kilograms of Sucraloses, and material is heated to 60 ℃ by chuck in the pot, starts stirring; Add 3.0 kilograms of active carbons respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 12 kilograms of xylo-oligosaccharides, 47 kilograms of oligoisomaltoses, pulverizing reaches 150 orders through pulverizer; Be sent to fluidisation in the spray-fluidized bed apparatus, the mixed material of xylo-oligosaccharide and oligoisomaltose gets into the fluidized bed with spraying from the bottom of fluidized bed with spraying and quickens from bottom to top with malleation and flows, and the top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body; Control 35～40 ℃ of fluidized-bed layer temperature well, the multiple spot even spraying is disperseed, after operation is accomplished; Improve bed temperature to 50～78 ℃ again; After xylo-oligosaccharide, oligoisomaltose fluidisation lose surface crystallization water, pumping into the above-mentioned oligoisomaltose solution that refines, continuously the Spray Mixing drying-granulating; Control air quantity and mist flow well, obtain the good fluffy granular product of even sugariness decorations.
Through detecting, adopt the fluffy granular composite sugar-free sweetener of technical scheme acquisition of the present invention, its main performance index is seen table 1.
Table 1
| Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 |
| Particle size | 30～60 orders | 30～60 orders | 30～60 orders | 30～60 orders |
| Sugariness (sucrose contrast) | 50 times | 100 times | 150 times | 200 times |
| Outward appearance | White particle | White particle | White particle | White particle |
[0041]
| Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 |
| Bulk density (g/mm 3) | 0.58 | 0.62 | 0.63 | 0.66 |
The stability test of sweetener is to check sweetener to guarantee the ability that undergoes no deterioration within a certain period of time, and the sweetener product of the embodiment of the invention was stored 3 years at normal temperatures, phenomenons such as rotten and sugariness reduction occur, and the stability ten minutes is superior.
The sugariness degree of modification of fluffy granular composite sugar-free sweetener of the present invention is with according to the adjustment of Sucralose in the food consumption adds, 50～200 times of selecting the common sucrose sugariness usually for use; Relatively be fit to the food enterprise needs; Form according to prescription, under same sugariness situation, people only are 1/50～1/200 of common sucrose to the absorption of heat; Sugar-free sweetener is the sweet taste article of low-calorie; The metabolism of this sweetener does not need insulin, can not cause blood sugar to raise, and is suitable for diabetes, three high crowds' needs.
Show obviously that to sum up the present invention adopts scientific formula, uses advanced science and technology technology and method, products obtained therefrom does not have smell, do not have color, and is soluble in water, and it is very convenient that this fluffy granule-shaped sugar-free sweetener is used.Granularity, molten speed, mouthfeel, sugariness all are much better than the prior art value, and the scientific preparation process simple flow is prone to row, are fit to very much large-scale production, are worth wide popularization and application in the field of business.
What need understand is: the above only is a preferred implementation of the present invention; For those skilled in the art; Under the prerequisite that does not break away from the principle of the invention, can also make some improvement and retouching, these improvement and retouching also should be regarded as protection scope of the present invention.
Claims (4)
1. Xylo-oligosaccharide compounded fluffy granule-shaped sugar-free sweetener is characterized in that being become to be grouped into by following percentage by weight: Sucralose 8.4～35%, xylo-oligosaccharide 4～12%, oligoisomaltose 55～87.6%; The sweetener preparation method comprises following processing step:
1. Sucralose, oligoisomaltose are joined respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 52～78 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned sucralose solution and the oligoisomaltose solution, be incubated 25～30 minutes, filter while hot, filtrating is pooled to respectively in the storage tank of heat tracing;
4. with putting in the spray-fluidized bed apparatus after xylo-oligosaccharide and the oligoisomaltose pulverizing; The mixed material of xylo-oligosaccharide and oligoisomaltose also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body; Pump into the above-mentioned oligoisomaltose solution that refines again, spray-drying obtains fluffy granular composite sugar-free sweetener continuously;
Its xylo-oligosaccharide preparation method comprises following processing step:
1. take by weighing straw, straw is pulverized, handle, filter, discard filtrating with hot-water soak;
2. add the NaOH aqueous solution and carry out alkali treatment, its alkali purification temp is 23～56 ℃, and the alkali treatment time is 24～36 hours;
3. centrifugal acquisition extract is used the acetic acid aqueous solution neutralising extract, to pH be 4.5～7.5;
4. centrifugal removal deposition after supernatant concentration, is used precipitation with alcohol, leaves standstill then;
5. centrifugal collecting precipitation, dry sediment is made into sediment 3～6% the aqueous solution then to remove ethanol wherein;
6. complex enzyme is carried out enzymolysis processing to the aqueous solution that 5. step makes, hydrolysis temperature is 30～45 ℃, and enzymolysis time is 24～36 hours, and 100mL handles in the aqueous solution and adds 0.05～5g complex enzyme; The component of wherein said complex enzyme is: endo-xylanase 55～85wt%, arabinofuranosidase 10～35wt%, circumscribed zytase 5～10wt%;
7. after enzymolysis finishes, enzymolysis liquid in 100～121 ℃ of deactivations 10～15 minutes, is concentrated in 40～60 ℃ of vacuum then;
8. with macroporous type absorption resin cation purifying concentrate,, obtain light yellow to white powdered granule xylo-oligosaccharide then in 45～55 ℃ of vacuum drying 14～18 hours.
2. Xylo-oligosaccharide compounded fluffy granule-shaped sugar-free sweetener according to claim 1 is become to be grouped into by following percentage by weight: Sucralose 8.5%, xylo-oligosaccharide 4%, oligoisomaltose 87.5%.
3. the preparation method of the described Xylo-oligosaccharide compounded fluffy granule-shaped sugar-free sweetener of claim 1 is characterized in that: comprise following processing step---
1. Sucralose, oligoisomaltose are joined respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 52～78 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned sucralose solution and the oligoisomaltose solution, be incubated 25～30 minutes, filter while hot, filtrating is pooled to respectively in the storage tank of heat tracing;
4. with putting in the spray-fluidized bed apparatus after xylo-oligosaccharide and the oligoisomaltose pulverizing; The mixed material of xylo-oligosaccharide and oligoisomaltose also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body; Pump into the above-mentioned oligoisomaltose solution that refines again, spray-drying obtains fluffy granular composite sugar-free sweetener continuously.
4. the preparation method of Xylo-oligosaccharide compounded fluffy granule-shaped sugar-free sweetener according to claim 3 is characterized in that: Sucralose, oligoisomaltose are joined respectively in the container, add deionized water respectively and mix; Be warming up to 60～70 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrating is pooled to respectively in the storage tank that has heat tracing; Xylo-oligosaccharide and oligoisomaltose reach 120～180 orders through pulverizing; Be sent in the spray-fluidized bed apparatus; The mixed material of xylo-oligosaccharide and oligoisomaltose also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and control fluidized-bed layer temperature is at 35～80 ℃, and the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned sucralose solution that refines be sprayed continuously and is distributed on the fine sugar alcohol body; After the mixing of sugar alcohol fluidisation loses surperficial moisture content; Pump into the above-mentioned oligoisomaltose solution that refines again, spray drying granulation obtains fluffy granular composite sugar-free sweetener continuously.
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1891073A (en) * | 2005-07-06 | 2007-01-10 | 王明谊 | Xylitol compound sweetener |
| CN101120768A (en) * | 2007-09-07 | 2008-02-13 | 苏州苏克瑞甜品科技有限公司 | Liquid sweetener and its preparation method |
| CN101124980A (en) * | 2007-09-25 | 2008-02-20 | 上海师范大学 | Composite sweetener containing neotame |
| CN101133822A (en) * | 2007-09-30 | 2008-03-05 | 广东省食品工业研究所 | Composite sweetening agent |
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1891073A (en) * | 2005-07-06 | 2007-01-10 | 王明谊 | Xylitol compound sweetener |
| CN101120768A (en) * | 2007-09-07 | 2008-02-13 | 苏州苏克瑞甜品科技有限公司 | Liquid sweetener and its preparation method |
| CN101124980A (en) * | 2007-09-25 | 2008-02-20 | 上海师范大学 | Composite sweetener containing neotame |
| CN101133822A (en) * | 2007-09-30 | 2008-03-05 | 广东省食品工业研究所 | Composite sweetening agent |
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