CN102038084B - Premix containing iron sucrose for raising pigs - Google Patents
Premix containing iron sucrose for raising pigs Download PDFInfo
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- CN102038084B CN102038084B CN2009100708508A CN200910070850A CN102038084B CN 102038084 B CN102038084 B CN 102038084B CN 2009100708508 A CN2009100708508 A CN 2009100708508A CN 200910070850 A CN200910070850 A CN 200910070850A CN 102038084 B CN102038084 B CN 102038084B
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Abstract
The invention relates to a premix containing iron sucrose for raising pigs, wherein the premix comprises the following components in parts by weight: 1-15 parts of cuprum, 20-50 parts of iron sucrose, 1-15 parts of zinc, 5-15 parts of manganese, 2-3 parts of iodine, 3-60 parts of calcium, 1- 4 parts of VA, 3-10 parts of VD3, 2-8 parts of VE, 5-8 parts of VK3, 3-9 parts of VB 1, 12-30 parts of VB2, 20-60 parts of pantothenic acid and 60-90 parts of nicotinic acid; the cuprum, the iron sucrose, the zinc, the manganese, the iodine and the calcium are stone powders; the VA, the VD3, the VE, the VK3, the VB1, the VB2, the pantothenic acid and the nicotinic acid are bran shell powders; and the premix provided by the invention can be obtained by mixing the stone powders and the bran shell powders in any proportion. The invention has the advantages of simple manufacturing process and lower cost; the survival rate of piglets can be effectively improved and the nutritional ingredients of the piglets are more balanced; and the premix containing iron sucrose for raising pigs has higher security and stability.
Description
Technical field
The invention belongs to premix field in the livestock breeding industry, especially a kind of pig that contains sucrose iron is used premix.
Background technology
Pig is mainly additional basal diet nutritional labeling deficiency with the purposes of premix, is full price property so that daily ration reaches the nutritional labeling balance; The pig that also has can enhancing body immunity with premix, promotes to grow, and increases economic efficiency; Through studying for many years in the feeding process of piglet; The picked-up of ferro element is very important, and ferro element is the necessary a kind of trace element of body, is the requisite composition of body synthetic hemoglobin; The piglet death of tool statistics about 30% is owing to iron deficiency causes; If untimely additional ferro element, also can bring following unfavorable factor to piglet: (1) can not form hemoglobin, myoglobins, cytochromes enzyme and multiple peroxidase, thereby influences the conveying of endotrophic material; (2) content of hemoglobin is low, takes oxygen, oxygen delivery capacity is low, causes biological organs depleted easily; (3) incidences of disease such as diarrhea, oedema, white muscle disease raise, poor growth, and dorsal body setae is slightly random, skin and mucosal pallor, poor appetite; (4) physiological function descends, hypoimmunity, easy infection generation secondary disease.Be applied to clinical piglet benefit iron medicine at present and be mainly iron-dextrin; Though this medicine can be effective in cure to the piglet hypoferric anemia; But have following problem for prolonged application: the synthetic of iron-dextrin is a very complicated process; Generally carry out complex reaction with ferric hydroxide and dextran molecule and make, this complex reaction is very unstable, receives the pH value and the FeCl of reaction system
3The influence of solution concentration is bigger, and product yield is lower, second-rate, and the dextran cost of raw material is higher, causes finished medicines to hold at high price, and influences clinical practice.
Summary of the invention
The objective of the invention is to overcome the deficiency of prior art, provide a kind of pig that contains sucrose iron to use premix, this premix manufacture craft is simple, cost is lower, can effectively improve the survival rate of piglet, the nutritional labeling balance more that makes piglet.
The present invention realizes through following technical scheme:
A kind of pig that contains sucrose iron is used premix, and wherein the component of this premix and ratio of weight and number thereof are:
Copper 1～15; Sucrose iron 20～50;
Zinc 1～15; Manganese 5～15;
Iodine 2～3; Calcium 30～60;
VA 1～4； VD3 3～10；
VE 2～8； VK3 5～8；
VB1 3～9； VB2 12～30；
Pantothenic acid 20～60; Nicotinic acid 60～90.
And the carrier of described copper, sucrose iron, zinc, manganese, iodine, calcium is a stone flour.
And the carrier of described VA, VD3, VE, VK3, VB1, VB2, pantothenic acid, nicotinic acid is a litter shell powder.
And the preparation method's of described sucrose iron step is:
(1) crystallization: using acetic acid is that the pH value of 50%～80% sucrose solution transfers to 1～4 with concentration, is that the iron salt solutions of 0.1mol/L～10mol/L joins and forms mixed liquor in the sucrose solution with concentration, and using concentration is 30%～50% Na
2CO
3Solution transfers to 1～3 with the pH value of this mixed liquor, stirs 20～40 minutes, and continuation adding concentration is 20%～50% Na
2CO
3The pH value that occurs muddiness and mixed liquor in solution to the mixed liquor transfers to 4～7, filters, and in the crystallization that filtration obtains, adds entry the crystallization dissolving is got final product, and obtains discus solution;
(2) complexing: with concentration is the heating of 50%～80% sucrose solution, and temperature is controlled at 90～120 ℃, and adding concentration then is that 20～40% alkali lye alkalize; PH value is controlled at 10～14, alkalizes 10～30 minutes, adds discus solution in the sucrose solution after alkalization; After the complexing 1～3 hour; In half an hour, be cooled to below 30～60 ℃, static spending the night obtains complex liquid;
(3) refining: the complex liquid after static the spending the night is filtered, and filtrating is with 2～3 times 95% precipitation with alcohol, filtration, and the sediment that obtains is soluble in water, uses precipitation with alcohol again, and sediment is dried under 50～70 ℃ of conditions, is iron sucrose bulk drug.
And the volume ratio of sucrose solution and iron salt solutions is in the described step (1): 2: 1～10: 1.
And the volume of sucrose solution and discus solution is in the described step (2): 2: 1～10: 1.
And described iron salt solutions is liquor ferri trichloridi, iron nitrate solution, ironic citrate solution, ferric acetate solution, ferric perchlorate's solution, ironic citrate ammonium salt solution, ferric ammonium nitrate solution or phosphoglycerol ferrous solution wherein a kind of.
And described alkali lye is the wherein a kind of of sodium hydroxide solution, sodium carbonate liquor, potassium hydroxide solution, Ammonia or solution of potassium carbonate.
Advantage of the present invention and beneficial effect are:
1, the pig that originally contains sucrose iron uses the sucrose iron in the premix to adopt the cheap sucrose of cost ten minutes to be raw material; Stability is better in the production, and is water-soluble higher, can absorb with molecular forms; Toxic and side effect is that the ideal that meets international standard is mended chalybeate less than traditional iron-dextrin.
2, the pig that originally contains sucrose iron uses the sucrose iron in the premix to be primary raw material with sucrose and trivalent iron salt; Through synthesis of hydroxy iron oxide iron parent nucleus; And then obtain sucrose rail injection liquid with the sucrose part complexing of alkalization, refining, preparation and sterilization; This parenteral solution can effectively improve the piglet blood content of hemoglobin, increases the body weight of piglet fast, improves the survival rate of piglet.
3, the pig that originally contains sucrose iron is improved the piglet survival rate with the interpolation of the various components of the premix nutritional labeling in can efficient balance piglet body.
4, the pig that originally contains sucrose iron uses the carrier of copper in the premix, iron, zinc, manganese, iodine, calcium to be stone flour; The carrier of VA, VD3, VE, VK3, VB1, VB2, pantothenic acid, nicotinic acid is a litter shell powder, its raw material wide material sources, and cost is lower.
5, manufacture craft of the present invention is simple, cost is lower, can effectively improve the survival rate of piglet, the nutritional labeling balance more that makes piglet, is that a kind of security and the higher pig that contains sucrose iron of stability are used premix.
The specific embodiment
The present invention further details through following examples.Need to prove: following embodiment is illustrative, is not determinate, can not limit protection scope of the present invention with following embodiment.
A kind of pig that contains sucrose iron is used premix, and wherein the component of this premix and parts by weight thereof are respectively: copper 10g, sucrose iron 30g, zinc 10g, manganese 12g; Iodine 2g, calcium 50g, VA3g, VD38g, VE6g, VK37g, VB17g, VB225g, pantothenic acid 50g, nicotinic acid 70g.The carrier of above-mentioned copper, sucrose iron, zinc, manganese, iodine, calcium is a stone flour; The carrier of VA, VD3, VE, VK3, VB1, VB2, pantothenic acid, nicotinic acid is a litter shell powder.Above-mentioned stone flour and litter shell powder arbitrary proportion mixed to obtain the pig that the present invention contains sucrose iron and use premix.
The preparation method of above-mentioned sucrose iron the steps include:
(1), crystallization: using acetic acid is that the pH value of 60% sucrose solution transfers to 1.5 with concentration; With concentration is that the iron salt solutions 50ml of 1mol/L joins in the 100ml sucrose solution and forms mixed liquor; Iron salt solutions is liquor ferri trichloridi, iron nitrate solution, ironic citrate solution, ferric acetate solution, ferric perchlorate's solution; Ironic citrate ammonium salt solution, ferric ammonium nitrate solution or phosphoglycerol ferrous solution wherein a kind of, the present embodiment iron salt solutions adopts liquor ferri trichloridi, and using concentration is 30% Na
2CO
3Solution transfers to 1.7 with the pH value of mixed liquor, stirs 30 minutes, and continuation adding concentration is 30% Na
2CO
3Just there has been the pH value of muddiness and mixed liquor to transfer to 4 in solution to the mixed liquor, filtered, obtained adding in the crystallization entry to filtration the crystallization dissolving is got final product, obtained discus solution;
(2), complexing: with concentration is the sucrose solution heating of 60%100ml, and temperature is controlled at 100 ℃, and adding concentration then is the alkalization of 20～40% alkali lye; Described alkali lye is the wherein a kind of of sodium hydroxide solution, sodium carbonate liquor, potassium hydroxide solution, Ammonia, solution of potassium carbonate; It is that 20% NaOH solution alkalizes that present embodiment adopts concentration, and the pH value control transfers to 11, and adding discus solution 50ml after 15 minutes alkalize; After the complexing 2 hours; In half an hour, be cooled to below 50 ℃, after static the spending the night, obtain complex liquid;
(3), refining: the complex liquid after static the spending the night is filtered, and filtrating is with 2 times 95% precipitation with alcohol, and filtration obtains the sediment precipitation with alcohol of using again soluble in water, and sediment is dried under 60 ℃ of conditions, is sucrose iron.
Claims (6)
1. a pig that contains sucrose iron is used premix, it is characterized in that: the component of this premix and ratio of weight and number thereof are:
Copper 1～15; Sucrose iron 20～50;
Zinc 1～15; Manganese 5～15;
Iodine 2～3; Calcium 30～60;
VA 1～4； VD3 3～10；
VE 2～8； VK3 5～8；
VB1 3～9； VB2 12～30；
Pantothenic acid 20～60; Nicotinic acid 60～90;
The carrier of described copper, sucrose iron, zinc, manganese, iodine, calcium is a stone flour;
The carrier of described VA, VD3, VE, VK3, VB1, VB2, pantothenic acid, nicotinic acid is a litter shell powder.
2. the pig that contains sucrose iron according to claim 1 is used premix, it is characterized in that: the preparation method's of described sucrose iron step is:
(1) crystallization: using acetic acid is that the pH value of 50%～80% sucrose solution transfers to 1～4 with concentration, is that the iron salt solutions of 0.1mol/L～10mol/L joins and forms mixed liquor in the sucrose solution with concentration, and use concentration is 30%～50% Na
2CO
3Solution transfers to 1～3 with the pH value of this mixed liquor, stirs 20～40 minutes, and continuation adding concentration is 20%～50% Na
2CO
3The pH value that occurs muddiness and mixed liquor in solution to the mixed liquor transfers to 4～7, filters, and in the crystallization that filtration obtains, adds entry the crystallization dissolving is got final product, and obtains discus solution;
(2) complexing: with concentration is the heating of 50%～80% sucrose solution, and temperature is controlled at 90～120 ℃, and adding concentration then is that 20～40% alkali lye alkalize; The pH value is controlled at 10～14, alkalizes 10～30 minutes, adds discus solution in the sucrose solution after alkalization; After the complexing 1～3 hour; In half an hour, be cooled to below 50 ℃, static spending the night obtains complex liquid;
(3) refining: the complex liquid after static the spending the night is filtered, and filtrating is with 2～3 times 95% precipitation with alcohol, filtration, and the sediment that obtains is soluble in water, uses precipitation with alcohol again, and sediment is dried under 50～70 ℃ of conditions, is sucrose iron.
3. the pig that contains sucrose iron according to claim 2 is used premix, it is characterized in that: the volume ratio of sucrose solution and iron salt solutions is in the described step (1): 2: 1～10: 1.
4. the pig that contains sucrose iron according to claim 2 is used premix, it is characterized in that: the volume of sucrose solution and discus solution is in the described step (2): 2: 1～10: 1.
5. the pig that contains sucrose iron according to claim 2 is used premix; It is characterized in that: described iron salt solutions is liquor ferri trichloridi, iron nitrate solution, ironic citrate solution, ferric acetate solution, ferric perchlorate's solution, ironic citrate ammonium salt solution, ferric ammonium nitrate solution or phosphoglycerol ferrous solution wherein a kind of.
6. the pig that contains sucrose iron according to claim 2 is used premix, it is characterized in that: described alkali lye is the wherein a kind of of sodium hydroxide solution, sodium carbonate liquor, potassium hydroxide solution, Ammonia or solution of potassium carbonate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009100708508A CN102038084B (en) | 2009-10-19 | 2009-10-19 | Premix containing iron sucrose for raising pigs |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009100708508A CN102038084B (en) | 2009-10-19 | 2009-10-19 | Premix containing iron sucrose for raising pigs |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102038084A CN102038084A (en) | 2011-05-04 |
| CN102038084B true CN102038084B (en) | 2012-11-28 |
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| CN2009100708508A Expired - Fee Related CN102038084B (en) | 2009-10-19 | 2009-10-19 | Premix containing iron sucrose for raising pigs |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103655683A (en) * | 2012-09-25 | 2014-03-26 | 天津瑞贝特科技发展有限公司 | Traditional Chinese medicine composition with functions of tonifying qi and nourishing blood for livestock and preparation method thereof |
| CN103798517A (en) * | 2012-11-13 | 2014-05-21 | 天津瑞贝特科技发展有限公司 | Feed additive capable of effectively supplementing nutrition required by growth of livestock and preparation method of feed additive |
| CN104206735A (en) * | 2014-09-13 | 2014-12-17 | 南宁市泽威尔饲料有限责任公司 | Microelement sucrose complex feed additive as well as preparation method and application thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101124947A (en) * | 2007-08-31 | 2008-02-20 | 北京农业职业学院 | Compound pre-mixed feed for animal and bird |
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Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101124947A (en) * | 2007-08-31 | 2008-02-20 | 北京农业职业学院 | Compound pre-mixed feed for animal and bird |
Non-Patent Citations (3)
| Title |
|---|
| 中国营养学会微量元素营养委员会.近年来我国微量元素营养研究进展.《营养学报》.1992,第14卷(第3期),311-317. * |
| 张丽萍,等.淀粉铁、蔗糖铁对铁缺乏大鼠的补铁效应.《营养学报》.1988,第10卷(第3期),220-223. * |
| 张伟，刘当慧.糖铁络合物研究进展.《饲料工业》.1998,第19卷(第10期),40-41. * |
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