CN101810313A - Dessert sweetener and production process - Google Patents
Dessert sweetener and production process Download PDFInfo
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- CN101810313A CN101810313A CN200910250390A CN200910250390A CN101810313A CN 101810313 A CN101810313 A CN 101810313A CN 200910250390 A CN200910250390 A CN 200910250390A CN 200910250390 A CN200910250390 A CN 200910250390A CN 101810313 A CN101810313 A CN 101810313A
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Abstract
The invention relates to a dessert sweetener and a production process. The dessert sweetener comprises the following components: 18-22 percent of xylitol, 0.037-0.045 percent of sucralose, 37-41.99 percent of sorbitol and 37-42 percent of erythritol. The process comprises the following steps of: respectively adding 5% xylitol and sucralose to a heating container, respectively adding deionized water and mixing, increasing the temperature to dissolve; respectively adding active carbon to the solution; filtering before cooling and respectively converging filtrate to a storage tank; enabling the crushed mixture of the xylitol, the sorbitol and the erythritol to enter the bed from the bottom of a spraying fluidized bed under positive pressure and flow at a high speed from bottom to top; applying negative pressure at the upper part of the spraying fluidized bed to vibrate from top to bottom so that materials are vertically boiled in the bed; continuously spraying and dispersing the refined sucralose solution to superfine sugar alcohol bodies by a multi-point spray gun at one side of the fluidized bed; and then; pumping the xylitol solution in, continuously spraying and drying to obtain a sugarless dessert sweetening agent. The preparation flows are simple and easy to operate, and the sweetness of the product is 0.70-0.74 times that of common sugar.
Description
Technical field
The present invention relates to a kind of edible dining table sweetener, relate in particular to a kind of fluffy granular composite sugar-free dessert sweetener and production technology thereof.
Background technology
Along with the increase of people because of too much bringing disease, people's demand safety, healthy Sugarless type dining table sweetener with sugar; In production procedure, reach from raw material and put into the advanced preparation technology that finished product one step finishes; It is learnt from other's strong points to offset one's weaknesses, has complementary advantages to make between the sugar alcohol sweet taste on the formula for a product, can play during product uses and cover the effect that promotes mouthfeel with synergy, people thirst under the prerequisite that satisfies sugariness height, empty calory, and occupation modeization, with cane-sugar taste safety and Health Sugarless type dessert sweetener roughly the same.
Summary of the invention
The objective of the invention is to overcome the deficiency that prior art exists, a kind of fluffy granular composite sugar-free dessert sweetener and production technology thereof are provided, adopt the scientific technology of easy operation control, the molten speed of product, mouthfeel, sugariness all are higher than the prior art optimum value.
Purpose of the present invention is achieved through the following technical solutions:
Dessert sweetener, characteristics are to comprise following composition (percentage by weight): xylitol 18～22%, Sucralose 0.037～0.045%, D-sorbite 37～41.99%, antierythrite 37～42%.
Further, above-mentioned dessert sweetener, wherein, xylitol 18%, Sucralose 0.0374%, D-sorbite 41.9626%, antierythrite 40%.
The production technology of dessert sweetener of the present invention comprises following processing step:
1. with 5% xylitol, Sucralose joins respectively in the heating container, adds deionized water respectively and mixes;
2. be warming up to 52～80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned xylitol solution and the sucralose solution, be incubated 25～30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank of heat tracing;
4. with xylitol, antierythrite and D-sorbite are put in the spray-fluidized bed apparatus after pulverizing, the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, pump into the above-mentioned xylitol solution that refines again, spray-drying obtains the fluffy granular composite sugar-free dessert sweetener continuously.
Again further, the production technology of above-mentioned dessert sweetener, the xylitol with 5%, Sucralose join respectively in the heating container, add deionized water respectively and mix; Be warming up to 60～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank that has heat tracing; Xylitol, antierythrite and D-sorbite reach 120～180 orders through pulverizing, be sent in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, control fluidized-bed layer temperature is at 35～80 ℃, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, after the mixing of sugar alcohol fluidisation loses surperficial moisture content, pump into the above-mentioned xylitol solution that refines again, spray drying granulation obtains the fluffy granular composite sugar-free dessert sweetener continuously.
Again further, the production technology of above-mentioned dessert sweetener, the bed temperature scope of described fluidized bed with spraying is 35～80 ℃, and wherein the bed temperature of phase I Sucralose spraying dispersion is 35～50 ℃, and the bed temperature of second stage xylitol mist projection granulating is 50～80 ℃.
Again further, the production technology of above-mentioned dessert sweetener, in the phase I of described spraying mixed fluidized bed, the Sucralose spraying is dispersed in fluidisation and smashes on the fine sugar alcohol crystal body; In second stage, the xylitol spray drying granulation is on the noncrystal of mixing sugar alcohol.
Substantive distinguishing features and obvious improvement that technical solution of the present invention is outstanding are mainly reflected in:
The negative pressure fluid bed fluidization technique that adopts scientific formula, uses advanced is in conjunction with the multi-point atomizing method, and time sharing segment control appliance bed temperature efficiently solves even dispersion, coats problems such as granulation, drying.With xylitol, D-sorbite, antierythrite is primary raw material; modify uniformly and coat by preparation method to sugariness; make product sweetness reach 0.70～0.74 times of common sucrose; products obtained therefrom does not have smell, does not have color; soluble in water; this fluffy granular composite sugar-free dessert sweetener is easy to use, and its preparation process science is simple and easy to operate, is fit to very much large-scale production.
Description of drawings
Below in conjunction with accompanying drawing technical solution of the present invention is described further:
Fig. 1: process chart of the present invention.
The specific embodiment
Dessert sweetener, its composition is: xylitol 18～22%, Sucralose 0.037～0.045%, D-sorbite 37～41.99%, antierythrite 37～42%.Ideal formulations is: xylitol 18%, Sucralose 0.0374%, D-sorbite 41.9626%, antierythrite 40%.
As shown in Figure 1, the preparation technology of dessert sweetener: at first, the xylitol with 5%, Sucralose join respectively in the heating container, add deionized water respectively and mix; Be warming up to 52～80 ℃ of dissolvings respectively, and stir; Add active carbon in above-mentioned xylitol solution and the sucralose solution respectively, be incubated 25～30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank of heat tracing; Then, with xylitol, put into after antierythrite and D-sorbite are pulverized in the spray-fluidized bed apparatus (heating temperature control and by the positive negative pressure boiling of equipment technology with the boiling that in fluid bed, circulates of sugar alcohol material, mix that fluidisation is anhydrated and fluffy processing, sugar alcohol mixtures material → malleation material quickens to flow from bottom to top → and negative pressure vibrates → makes material boiling up and down in fluid bed → by the fluid bed side multiple spot spray gun liquid material ejection fog-like liquid of naming a person for a particular job from top to bottom, be sprayed onto on the trickle solid material body of boiling), xylitol, the mixed material of antierythrite and D-sorbite enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, the bed temperature that the spraying of control Sucralose disperses is 35～50 ℃, and the Sucralose even spraying is dispersed on the mixing sugar alcohol crystalline solid of powder; The rising bed temperature, after fluidisation loses surface crystallization water, pump into the above-mentioned xylitol solution that refines at mixing sugar alcohol again, continuously spray drying granulation, the bed temperature of xylitol mist projection granulating controlled well is 50～80 ℃, and the xylitol spray drying granulation is on the noncrystalline fluffy body of sugar alcohol; Obtain fluffy the shape product that even sugariness is modified.
Embodiment 1:
6 kilograms of xylitols and deionized water are dissolved in a stainless steel heating reaction pot for 21 kilograms, 0.0374 kilogram of Sucralose and deionized water are also dissolved in another stainless steel heating reaction pot for 22 kilograms, material is heated to 62 ℃ by chuck in the pot, start stirring, add 1 kilogram of active carbon respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; 18 kilograms of xylitols, 40 kilograms of antierythrites, 41.9626 kilograms of D-sorbites, pulverizing reaches 130 orders through pulverizer, be sent in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, control fluidized-bed layer temperature is 35～50 ℃, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, after the mixing of above-mentioned various sugar alcohol alcohol fluidisations loses surface crystallization water, pump into the above-mentioned xylitol solution that refines, continuously spray drying granulation, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
Embodiment 2:
6 kilograms of xylitols and deionized water are dissolved in a stainless steel heating reaction pot for 25 kilograms, 0.0391 kilogram of Sucralose and deionized water are also dissolved in another stainless steel reaction pot for 20 kilograms, material is heated to 52 ℃ by chuck in the pot, start stirring, add 2 kilograms of active carbons respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; 19 kilograms of xylitols, 41.9609 kilograms of antierythrites, 40 kilograms of D-sorbites, reach 150 orders through pulverizing, be sent to and carry out the fluidisation mixing in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, 35～40 ℃ of control fluidized-bed layer temperature, even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, after making the mixing of above-mentioned various sugar alcohol alcohol fluidisation lose surface crystallization water, pumping into the above-mentioned xylitol solution that refines, continuously spray granulating and drying, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
Embodiment 3:
6 kilograms of xylitols and deionized water are dissolved in a stainless steel heating reaction pot for 26 kilograms, 0.0408 kilogram of Sucralose and deionized water are also dissolved in another stainless steel heating reaction pot for 20 kilograms, material is heated to 60 ℃ by chuck in the pot, start stirring, add 3.0 kilograms of active carbons respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; 20 kilograms of xylitols, 42 kilograms of antierythrites, 37.9592 kilograms of D-sorbites, pulverizing reaches 160 orders through pulverizer, be sent in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, control 35～42 ℃ of fluidized-bed layer temperature well, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, after the mixing of above-mentioned various sugar alcohol alcohol fluidisations loses surface crystallization water, pump into the above-mentioned xylitol solution that refines, continuously spray drying granulation, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
Embodiment 4:
6 kilograms of xylitols and deionized water are dissolved in a stainless steel heating reaction pot for 25 kilograms, 20 kilograms also another dissolves in stainless steel heating reaction pot with 0.0425 kilogram of Sucralose and deionized water, material is heated to 80 ℃ by chuck in the pot, start stirring, add 3.0 kilograms of active carbons respectively, be incubated 35 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; 21 kilograms of xylitols, 39.95975 kilograms of antierythrites, 40 kilograms of D-sorbites, pulverizing reaches 180 orders through pulverizer, be sent to fluidisation in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, control 35～50 ℃ of fluidized-bed layer temperature well, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, after above-mentioned various sugar alcohol alcohol fluidisations lose surface crystallization water, pumping into the above-mentioned xylitol solution that refines, the combination drying granulation of spraying continuously, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is adornd.
Embodiment 5:
6 kilograms of xylitols and deionized water are dissolved in a stainless steel heating reaction pot for 24 kilograms, 20 kilograms also another dissolves in stainless steel heating reaction pot with 0.0442 kilogram of Sucralose and deionized water, material is heated to 80 ℃ by chuck in the pot, start stirring, add 3.0 kilograms of active carbons respectively, be incubated 35 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; 22 kilograms of xylitols, 38 kilograms of antierythrites, 39.9558 kilograms of D-sorbites, pulverizing reaches 180 orders through pulverizer, be sent to fluidisation in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, control 35～50 ℃ of fluidized-bed layer temperature well, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, after above-mentioned various sugar alcohol alcohol fluidisations lose surface crystallization water, pumping into the above-mentioned xylitol solution that refines, the combination drying granulation of spraying continuously, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is adornd.
After testing, the fluffy granular composite sugar-free dessert sweetener that adopts technical solution of the present invention to obtain, its main performance index sees Table 1.
Table 1
| Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 |
| Particle size | 30～60 orders | 30～60 orders | 30～60 orders | 30～60 orders | 30～60 orders |
| Sugariness (sucrose contrast) | 0.70 doubly | 0.71 doubly | 0.72 doubly | 0.73 doubly | 0.74 doubly |
| Outward appearance | White particle | White particle | White particle | White particle | White particle |
| Bulk density (g/mm 3) | ??0.60 | ??0.62 | ??0.63 | ??0.66 | ??0.66 |
The stability test of sweetener is to check sweetener to guarantee the ability that undergoes no deterioration within a certain period of time, and the dessert sweetener product of the embodiment of the invention was stored 3 years at normal temperatures, phenomenons such as rotten and sugariness reduction occur, and stability is very superior.
The sugariness degree of modification of fluffy granular composite sugar-free dessert sweetener of the present invention, will be according to the adjustment of Sucralose in consumption, usually select the common sucrose sugariness for use 0.70～0.74 times, relatively be fit to use needs of food enterprise dessert, according to the prescription composition, under same sugariness situation, people are almost nil to the absorption of heat, and this composite sugar-free dessert sweetener can not cause blood sugar to raise, not carious tooth, be fit to the diabetes patient, satisfy three high crowds, the healthy people's of pursuit needs.
Show obviously that to sum up the present invention adopts scientific formula, uses advanced science and technology technology and method, products obtained therefrom does not have smell, do not have color, and is soluble in water, and it is very convenient that this fluffy granule-shaped sugar-free dessert sweetener is used.Granularity, molten speed, mouthfeel, sugariness all are much better than the prior art value, and the scientific preparation process simple flow is easily gone, and are fit to very much large-scale production, are worth wide popularization and application in the field of business.
What need understand is: the above only is a preferred implementation of the present invention; for those skilled in the art; under the prerequisite that does not break away from the principle of the invention, can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (5)
1. dessert sweetener is characterized in that comprising following composition (percentage by weight): xylitol 18～22%, Sucralose 0.037～0.045%, D-sorbite 37～41.99%, antierythrite 37～42%.
2. dessert sweetener according to claim 1 is characterized in that its component has following percentage by weight: xylitol 18%, Sucralose 0.0374%, D-sorbite 41.9626%, antierythrite 40%.
3. the production technology of the described dessert sweetener of claim 1 is characterized in that: comprise following processing step---
1. with 6% xylitol, Sucralose joins respectively in the heating container, adds deionized water respectively and mixes;
2. be warming up to 52～80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned xylitol solution and the sucralose solution, be incubated 25～30 minutes, filter while hot, filtrate is pooled in the storage tank of heat tracing stand-by respectively;
4. with xylitol, antierythrite and D-sorbite are put in the spray-fluidized bed apparatus after pulverizing, xylitol, the mixed material of antierythrite and D-sorbite enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, pump into the above-mentioned xylitol solution that refines again, spray-drying obtains the fluffy granular composite sugar-free dessert sweetener continuously.
4. the production technology of dessert sweetener according to claim 3, it is characterized in that: the xylitol with 6%, Sucralose join respectively in the container, add deionized water respectively and mix; Be warming up to 60～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank that has heat tracing; Xylitol, antierythrite and D-sorbite reach 120～180 orders through pulverizing, be sent in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, control fluidized-bed layer temperature is at 35～80 ℃, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, after the mixing of sugar alcohol fluidisation loses surperficial moisture content, pump into the above-mentioned xylitol solution that refines again, spray drying granulation obtains the fluffy granular composite sugar-free dessert sweetener continuously.
5. the production technology of dessert sweetener according to claim 4, it is characterized in that: the bed temperature scope of described fluidized bed with spraying is 35～80 ℃, wherein the bed temperature of phase I Sucralose spraying dispersion is 35～50 ℃, and the bed temperature of second stage xylitol mist projection granulating is 50～80 ℃.
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| CN2009102503907A CN101810313B (en) | 2009-12-07 | 2009-12-07 | Dessert sweetener and production process |
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| CN2009102503907A CN101810313B (en) | 2009-12-07 | 2009-12-07 | Dessert sweetener and production process |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102960823A (en) * | 2012-11-30 | 2013-03-13 | 苏州工业园区尚融科技有限公司 | Compound sweetener suitable for sour drinks and preparation method of sweetener |
| CN102960824A (en) * | 2012-11-30 | 2013-03-13 | 苏州工业园区尚融科技有限公司 | Compound sweetener applied sour beverages and preparation method of sweetener |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1099846C (en) * | 1999-12-09 | 2003-01-29 | 北京恒毅利科贸有限责任公司 | Method for preparing granular flavouring enriched food and its product |
| CN101181050B (en) * | 2007-12-19 | 2011-12-28 | 苏州苏克瑞甜品科技有限公司 | Sucrose succedaneum and preparation method thereof |
| CN101253968B (en) * | 2008-04-15 | 2011-12-28 | 苏州苏克瑞甜品科技有限公司 | Granular sugar-free sweetening agent and method of preparing the same |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102960823A (en) * | 2012-11-30 | 2013-03-13 | 苏州工业园区尚融科技有限公司 | Compound sweetener suitable for sour drinks and preparation method of sweetener |
| CN102960824A (en) * | 2012-11-30 | 2013-03-13 | 苏州工业园区尚融科技有限公司 | Compound sweetener applied sour beverages and preparation method of sweetener |
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