CN101810305B - Novel composite sugar-free table sweetener and production method thereof - Google Patents
Novel composite sugar-free table sweetener and production method thereof Download PDFInfo
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- CN101810305B CN101810305B CN2009102499761A CN200910249976A CN101810305B CN 101810305 B CN101810305 B CN 101810305B CN 2009102499761 A CN2009102499761 A CN 2009102499761A CN 200910249976 A CN200910249976 A CN 200910249976A CN 101810305 B CN101810305 B CN 101810305B
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Abstract
The invention relates to a novel composite sugar-free table sweetener and a production method thereof. The sweetner comprises the following components in percentage by weight: 12 to 32 percent of xylitol, 18 to 29 percent of sorbitol, 39 to 65 percent of isomaltose hypgather, and 0.07 to 0.16 percent of neotame. The process comprises the following steps of: respectively adding 8 percent isomaltose hypgather and the neotame into heating vessels, respectively adding deionized water into the vessles for mixing, and heating the vessels to dissolve solutions; respectively adding activated carbon into solutions, filtering the solutions while the solutions are hot, and respectively collecting filtrates into a storage tank; pressing mixed materials of crushed xylitol, sorbitol and isomaltose hypgather from the bottom of a spraying fluidized bed into the bed at positive pressure, allowing the mixed materials to acceleratedly flow from the bottom to the top, and vibrating the upper part of the spraying fluidized bed from the top to the bottom by applying negative pressure to ensure the materials boil in the bed up and down; and dissipating the refined neotame solution onto superfine sugar alcohol body by continuous spray by using a multi-point spray gun on the lateral side of the fluidized bed, pumping the isomaltose hypgather solution onto the superfine sugar alcohol body, and continuously spraying and drying to prepare the sugar-free table sweetener. The preparation process is simple and easy to operate, and the sweetness of the product is 5 to 10 times that of conventional cane sugar.
Description
Technical field
The present invention relates to a kind of edible dining table sweetener, relate in particular to a kind of novel composite sugar-free table sweetener and production method thereof.
Background technology
The increase of Along with people's because of too much bringing disease with sugar, people's demand safety, healthy Sugarless type dining table sweetener; In production procedure, reach the advanced preparation technology who puts into finished product one step completion from raw material; It is learnt from other's strong points to offset one's weaknesses, has complementary advantages to make between the sugar alcohol sweet taste on the formula for a product; Can play during product uses and cover the effect that promotes mouthfeel with synergy; People thirst under the prerequisite that satisfies sugariness height, empty calory, and occupation modeization, with cane-sugar taste safety and Health Sugarless type dining table sweetener roughly the same.
Summary of the invention
The objective of the invention is to overcome the deficiency that prior art exists, a kind of fluffy granular composite sugar-free table sweetener and production method thereof are provided, adopt the scientific technology of easy operation control, the molten speed property of product, mouthfeel, sugariness all are higher than the prior art optimum value.
The object of the invention is realized through following technical scheme:
A kind of novel composite sugar-free table sweetener, characteristics are to comprise following composition (percentage by weight): xylitol 12～32%, D-sorbite 18～29%, oligoisomaltose 39～65%, knob sweet 0.07～0.16%.
Further, above-mentioned a kind of novel composite sugar-free table sweetener, wherein, xylitol 32%, D-sorbite 28%, oligoisomaltose 39.928%, knob sweet 0.072%.
A kind of production method of novel composite sugar-free table sweetener comprises following processing step:
1. with 8% sweet the joining respectively in the heating container of oligoisomaltose, knob, add deionized water respectively and mix;
2. be warming up to 52～80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned oligoisomaltose solution and the sweet solution of knob, be incubated 25～30 minutes, filter while hot, filtrating is pooled to respectively in the storage tank of heat tracing;
4. put in the spray-fluidized bed apparatus after xylitol, oligoisomaltose and D-sorbite being pulverized; The mixed material of above-mentioned various sugar alcohols is also quickened to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body; Pump into the above-mentioned oligoisomaltose solution that refines again, spray-drying obtains fluffy granular composite sugar-free table sweetener continuously.
Again further, the production method of above-mentioned a kind of novel composite sugar-free table sweetener, the oligoisomaltose with 8%, knob is sweet joins respectively in the heating container, adds deionized water respectively and mixes; Be warming up to 60～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrating is pooled to respectively in the storage tank that has heat tracing; Xylitol, oligoisomaltose and D-sorbite reach 120～180 orders through pulverizing; Be sent in the spray-fluidized bed apparatus; The mixed material of above-mentioned various sugar alcohols is also quickened to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and control fluidized-bed layer temperature is at 35～80 ℃, and the multiple spot spray gun of fluid bed sidepiece earlier will the sweet solution of the above-mentioned knob that refines be sprayed continuously and is distributed on the fine sugar alcohol body; After the mixing of sugar alcohol fluidisation loses surperficial moisture content; Pump into the above-mentioned oligoisomaltose solution that refines again, spray drying granulation obtains fluffy granular composite sugar-free table sweetener continuously.
Again further; The production method of above-mentioned a kind of novel composite sugar-free table sweetener; The bed temperature scope of said fluidized bed with spraying is 35～80 ℃; Wherein the bed temperature of the sweet spraying dispersion of phase I knob is 35～50 ℃, and the bed temperature of second stage oligoisomaltose mist projection granulating is 50～80 ℃.
Again further, the production method of above-mentioned a kind of novel composite sugar-free table sweetener, in the phase I of said Spray Mixing fluid bed, the sweet spraying of knob is dispersed in fluidisation and smashes on the fine sugar alcohol crystal body; In second stage, the oligoisomaltose spray drying granulation is on the noncrystal of mixing sugar alcohol.
Substantive distinguishing features and obvious improvement that technical scheme of the present invention is outstanding are mainly reflected in:
With xylitol, D-sorbite, oligoisomaltose, knob is sweet is primary raw material, modifies uniformly and coats through preparation method to sugariness, makes product sweetness reach 5～10 times of common sucrose.Adopt the negative pressure fluid bed fluidization technique of scientific formula, uses advanced to combine the multi-point atomizing method, time sharing segment control appliance bed temperature efficiently solves even dispersion, coats problems such as granulation, drying.Products obtained therefrom does not have smell, do not have color, and is soluble in water, and this fluffy granular composite sugar-free table sweetener is easy to use, and its preparation process science is simple and easy to operate, is fit to very much large-scale production.
Description of drawings
Below in conjunction with accompanying drawing technical scheme of the present invention is described further:
Fig. 1: process chart of the present invention.
The specific embodiment
A kind of novel composite sugar-free table sweetener, its composition is: xylitol 12～32%, D-sorbite 18～29%, oligoisomaltose 39～65%, knob sweet 0.07～0.16%.Ideal formulations is: xylitol 32%, D-sorbite 28%, oligoisomaltose 39.928%, knob sweet 0.072%.
As shown in Figure 1, a kind of preparation technology of novel composite sugar-free table sweetener: at first, the oligoisomaltose with 8%, knob is sweet joins respectively in the heating container, adds deionized water respectively and mixes; Be warming up to 52～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively in above-mentioned oligoisomaltose solution and the sweet solution of knob, be incubated 25～30 minutes, filter while hot, filtrating is pooled to respectively in the storage tank of heat tracing; Then; Put into after xylitol, oligoisomaltose and D-sorbite pulverized in the spray-fluidized bed apparatus (at heating temperature control and technological with the boiling that in fluid bed, circulates of sugar alcohol material through the positive negative pressure boiling of equipment; Mix that fluidisation is anhydrated and fluffy processing; Sugar alcohol mixtures material → malleation material quickens to flow from bottom to top → and negative pressure vibrates → makes material boiling up and down in fluid bed → by the fluid bed side multiple spot spray gun liquid material ejection fog-like liquid of naming a person for a particular job from top to bottom; Be sprayed onto on the trickle solid material body of boiling); The mixed material of xylitol, oligoisomaltose and D-sorbite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body, and the bed temperature that the sweet spraying of control knob disperses is 35～50 ℃, and the sweet even spraying of knob is dispersed on the mixing sugar alcohol crystalline solid of powder; The rising bed temperature; At mixing sugar alcohol after fluidisation loses surface crystallization water; Pump into the above-mentioned oligoisomaltose solution that refines again; Continuous spray drying granulation, the bed temperature of oligoisomaltose mist projection granulating controlled well is 50～80 ℃, the oligoisomaltose spray drying granulation is on the noncrystalline fluffy body of sugar alcohol; Obtain even sugariness and modify fluffy good shape product.
Embodiment 1:
8 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel reacting by heating pot for 25 kilograms; Knob is also dissolved in another stainless steel reacting by heating pot for 20 kilograms with deionized water for sweet 0.072 kilogram, and material is heated to 62 ℃ by chuck in the pot, starts stirring; Add 1 kilogram of active carbon respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 32 kilograms of xylitols, 31.928 kilograms of oligoisomaltoses, 28 kilograms of D-sorbites; Pulverize through pulverizer and to reach 130 orders, be sent in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols is got into the fluidized bed with spraying and quickens from bottom to top from the bottom of fluidized bed with spraying with malleation flow; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, the multiple spot spray gun of fluid bed sidepiece earlier will the sweet solution of the above-mentioned knob that refines continuously spraying be distributed on the fine sugar alcohol body, controlling the fluidized-bed layer temperature is 35～50 ℃; The multiple spot even spraying is disperseed; After operation is accomplished, improve bed temperature to 50～80 ℃ again, above-mentioned various sugar alcohols alcohol fluidisations mix lose surface crystallization water after; Pump into the above-mentioned oligoisomaltose solution that refines; Continuous spray drying granulation is controlled air quantity and mist flow well, obtains even sugariness and modifies good fluffy granular product.
Embodiment 2:
8 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel reacting by heating pot for 25 kilograms; Knob is also dissolved in another stainless steel reacting by heating pot for 20 kilograms with deionized water for sweet 0.086 kilogram, and material is heated to 62 ℃ by chuck in the pot, starts stirring; Add 1 kilogram of active carbon respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 18 kilograms of xylitols, 55.914 kilograms of oligoisomaltoses, 18 kilograms of D-sorbites; Pulverize through pulverizer and to reach 130 orders, be sent in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols is got into the fluidized bed with spraying and quickens from bottom to top from the bottom of fluidized bed with spraying with malleation flow; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, the multiple spot spray gun of fluid bed sidepiece earlier will the sweet solution of the above-mentioned knob that refines continuously spraying be distributed on the fine sugar alcohol body, controlling the fluidized-bed layer temperature is 35～50 ℃; The multiple spot even spraying is disperseed; After operation is accomplished, improve bed temperature to 50～80 ℃ again, above-mentioned various sugar alcohols alcohol fluidisations mix lose surface crystallization water after; Pump into the above-mentioned oligoisomaltose solution that refines; Continuous spray drying granulation is controlled air quantity and mist flow well, obtains even sugariness and modifies good fluffy granular product.
Embodiment 3:
8 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel reacting by heating pot for 25 kilograms; Knob is also dissolved in another stainless steel reacting by heating pot for 20 kilograms with deionized water for sweet 0.10 kilogram, and material is heated to 62 ℃ by chuck in the pot, starts stirring; Add 1 kilogram of active carbon respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 17 kilograms of xylitols, 54.90 kilograms of oligoisomaltoses, 20 kilograms of D-sorbites; Pulverize through pulverizer and to reach 130 orders, be sent in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols is got into the fluidized bed with spraying and quickens from bottom to top from the bottom of fluidized bed with spraying with malleation flow; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, the multiple spot spray gun of fluid bed sidepiece earlier will the sweet solution of the above-mentioned knob that refines continuously spraying be distributed on the fine sugar alcohol body, controlling the fluidized-bed layer temperature is 35～50 ℃; The multiple spot even spraying is disperseed; After operation is accomplished, improve bed temperature to 50～80 ℃ again, above-mentioned various sugar alcohols alcohol fluidisations mix lose surface crystallization water after; Pump into the above-mentioned oligoisomaltose solution that refines; Continuous spray drying granulation is controlled air quantity and mist flow well, obtains even sugariness and modifies good fluffy granular product.
Embodiment 4:
8 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel reacting by heating pot for 25 kilograms; Knob is also dissolved in another stainless steel reacting by heating pot for 20 kilograms with deionized water for sweet 0.12 kilogram, and material is heated to 62 ℃ by chuck in the pot, starts stirring; Add 1 kilogram of active carbon respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 12 kilograms of xylitols, 53.88 kilograms of oligoisomaltoses, 26 kilograms of D-sorbites; Pulverize through pulverizer and to reach 130 orders, be sent in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols is got into the fluidized bed with spraying and quickens from bottom to top from the bottom of fluidized bed with spraying with malleation flow; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, the multiple spot spray gun of fluid bed sidepiece earlier will the sweet solution of the above-mentioned knob that refines continuously spraying be distributed on the fine sugar alcohol body, controlling the fluidized-bed layer temperature is 35～50 ℃; The multiple spot even spraying is disperseed; After operation is accomplished, improve bed temperature to 50～80 ℃ again, above-mentioned various sugar alcohols alcohol fluidisations mix lose surface crystallization water after; Pump into the above-mentioned oligoisomaltose solution that refines; Continuous spray drying granulation is controlled air quantity and mist flow well, obtains even sugariness and modifies good fluffy granular product.
Embodiment 5:
8 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel reacting by heating pot for 25 kilograms; Knob is also dissolved in another stainless steel reacting by heating pot for 20 kilograms with deionized water for sweet 0.15 kilogram, and material is heated to 62 ℃ by chuck in the pot, starts stirring; Add 1 kilogram of active carbon respectively; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 13 kilograms of xylitols, 56.85 kilograms of oligoisomaltoses, 22 kilograms of D-sorbites; Pulverize through pulverizer and to reach 130 orders, be sent in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols is got into the fluidized bed with spraying and quickens from bottom to top from the bottom of fluidized bed with spraying with malleation flow; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, the multiple spot spray gun of fluid bed sidepiece earlier will the sweet solution of the above-mentioned knob that refines continuously spraying be distributed on the fine sugar alcohol body, controlling the fluidized-bed layer temperature is 35～50 ℃; The multiple spot even spraying is disperseed; After operation is accomplished, improve bed temperature to 50～80 ℃ again, above-mentioned various sugar alcohols alcohol fluidisations mix lose surface crystallization water after; Pump into the above-mentioned oligoisomaltose solution that refines; Continuous spray drying granulation is controlled air quantity and mist flow well, obtains even sugariness and modifies good fluffy granular product.
Through detecting, adopt the fluffy granular composite low-sugar and low-calorie sweetener of technical scheme acquisition of the present invention, its main performance index is seen table 1.
Table 1
| Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 |
| Particle size | 30～60 orders | 30～60 orders | 30～60 orders | 30～60 orders | 30～60 orders |
| Sugariness (sucrose contrast) | 5 times | 6 times | 7 times | 8 times | 10 times |
| Outward appearance | White particle | White particle | White particle | White particle | White particle |
| Bulk density (g/mm 3) | 0.60 | 0.62 | 0.62 | 0.66 | 0.66 |
The stability test of sweetener is to check sweetener to guarantee the ability that undergoes no deterioration within a certain period of time, and the dining table sweetener product of the embodiment of the invention was stored 3 years at normal temperatures, phenomenons such as rotten and sugariness reduction occur, and the stability ten minutes is superior.
The sugariness degree of modification of fluffy granular composite sugar-free table sweetener of the present invention will be according to the sweet adjustment in consumption of knob, 5～10 times of selecting the common sucrose sugariness usually for use; Relatively be fit to people's use needs, form, under same sugariness situation according to prescription; People are almost nil to the absorption of heat, and this dining table sweetener can not cause blood sugar to raise, not carious tooth; Be fit to the diabetes patient, satisfy three high crowds, pursue healthy needs of people.
Show obviously that to sum up the present invention adopts scientific formula, uses advanced science and technology technology and method, products obtained therefrom does not have smell, do not have color, and is soluble in water, and it is very convenient that this fluffy granule-shaped sugar-free dining table sweetener is used.Granularity, molten speed, mouthfeel, sugariness all are much better than the prior art value, and the scientific preparation process simple flow is prone to row, are fit to very much large-scale production, are worth wide popularization and application in the field of business.
What need understand is: the above only is a preferred implementation of the present invention; For those skilled in the art; Under the prerequisite that does not break away from the principle of the invention, can also make some improvement and retouching, these improvement and retouching also should be regarded as protection scope of the present invention.
Claims (4)
1. a composite sugar-free dining table sweetener is characterized in that comprising following percentage by weight composition: xylitol 12～32%, D-sorbite 18～29%, oligoisomaltose 39～65%, knob sweet 0.07～0.16%; Its preparation method comprises following processing step:
1. with 8% sweet the joining respectively in the heating container of oligoisomaltose, knob, add deionized water respectively and mix;
2. be warming up to 52～80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned oligoisomaltose solution and the sweet solution of knob, be incubated 25～30 minutes, filter while hot, for use in the storage tank that is pooled to heat tracing respectively of filtrating;
4. put in the spray-fluidized bed apparatus after xylitol, oligoisomaltose and D-sorbite being pulverized; The mixed material of xylitol, oligoisomaltose and D-sorbite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The bed temperature scope of fluidized bed with spraying is 35～80 ℃; Wherein the bed temperature of the sweet spraying dispersion of phase I knob is 35～50 ℃; The bed temperature of second stage oligoisomaltose mist projection granulating is 50～80 ℃, and the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the mixed material of fine xylitol, oligoisomaltose and D-sorbite, pumps into the above-mentioned oligoisomaltose solution that refines again; Spray-drying obtains fluffy granular composite sugar-free table sweetener continuously.
2. a kind of composite sugar-free dining table sweetener according to claim 1 is characterized in that its composition has following percentage by weight: xylitol 32%, D-sorbite 28%, oligoisomaltose 39.928%, knob sweet 0.072%.
3. the production method of the described a kind of composite sugar-free dining table sweetener of claim 1 is characterized in that: comprise following processing step---
1. with 8% sweet the joining respectively in the heating container of oligoisomaltose, knob, add deionized water respectively and mix;
2. be warming up to 52～80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned oligoisomaltose solution and the sweet solution of knob, be incubated 25～30 minutes, filter while hot, for use in the storage tank that is pooled to heat tracing respectively of filtrating;
4. put in the spray-fluidized bed apparatus after xylitol, oligoisomaltose and D-sorbite being pulverized; The mixed material of xylitol, oligoisomaltose and D-sorbite also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The bed temperature scope of fluidized bed with spraying is 35～80 ℃; Wherein the bed temperature of the sweet spraying dispersion of phase I knob is 35～50 ℃; The bed temperature of second stage oligoisomaltose mist projection granulating is 50～80 ℃, and the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the mixed material of fine xylitol, oligoisomaltose and D-sorbite, pumps into the above-mentioned oligoisomaltose solution that refines again; Spray-drying obtains fluffy granular composite sugar-free table sweetener continuously.
4. the production method of a kind of composite sugar-free dining table sweetener according to claim 3 is characterized in that: the oligoisomaltose with 8%, knob is sweet joins respectively in the container, adds deionized water respectively and mixes; Be warming up to 60～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrating is pooled to respectively in the storage tank that has heat tracing; Xylitol, oligoisomaltose and D-sorbite reach 120～180 orders through pulverizing; Be sent in the spray-fluidized bed apparatus; The mixed material of above-mentioned various sugar alcohols is also quickened to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and control fluidized-bed layer temperature is at 35～80 ℃, and the multiple spot spray gun of fluid bed sidepiece earlier will the sweet solution of the above-mentioned knob that refines be sprayed continuously and is distributed on the mixed material of fine xylitol, oligoisomaltose and D-sorbite; After the goods fluid mixing loses surperficial moisture content; Pump into the above-mentioned oligoisomaltose solution that refines again, spray drying granulation obtains fluffy granular composite sugar-free table sweetener continuously.
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| CN1254522A (en) * | 1999-12-09 | 2000-05-31 | 北京恒毅利科贸有限责任公司 | Method for preparing granular flavouring enriched food and its product |
| CN101181050A (en) * | 2007-12-19 | 2008-05-21 | 苏州苏克瑞甜品科技有限公司 | Sucrose succedaneum and preparation method thereof |
| CN101253968A (en) * | 2008-04-15 | 2008-09-03 | 苏州苏克瑞甜品科技有限公司 | Granular sugar-free sweetening agent and method of preparing the same |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1254522A (en) * | 1999-12-09 | 2000-05-31 | 北京恒毅利科贸有限责任公司 | Method for preparing granular flavouring enriched food and its product |
| CN101181050A (en) * | 2007-12-19 | 2008-05-21 | 苏州苏克瑞甜品科技有限公司 | Sucrose succedaneum and preparation method thereof |
| CN101253968A (en) * | 2008-04-15 | 2008-09-03 | 苏州苏克瑞甜品科技有限公司 | Granular sugar-free sweetening agent and method of preparing the same |
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