CN102987333A - Compound sugar-free low-calorie sweetening agent and preparation method thereof - Google Patents
Compound sugar-free low-calorie sweetening agent and preparation method thereof Download PDFInfo
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- CN102987333A CN102987333A CN201110408011XA CN201110408011A CN102987333A CN 102987333 A CN102987333 A CN 102987333A CN 201110408011X A CN201110408011X A CN 201110408011XA CN 201110408011 A CN201110408011 A CN 201110408011A CN 102987333 A CN102987333 A CN 102987333A
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Abstract
The invention relates to a compound sugar-free low-calorie sweetening agent and a preparation method thereof. The compound sugar-free low-calorie sweetening agent comprises the following ingredients in percentage by weight: 0.83 to 5 percent of neotame, 20 to 40 percent of xylitol, 30 to 60 percent of isomaltooligosacharide and 10 to 49 percent of sorbitol. The preparation method comprises the following steps of: adding the neotame and part of the isomaltooligosacharide into a heating container respectively, adding deionized water into the heating container and mixing, and raising the temperature to dissolve the neotame and the isomaltooligosacharide; adding activated carbon into the solution respectively, filtering while the solution is hot, and collecting the filtrate into a storage tank respectively; smashing the sorbitol, the xylito and the left isomaltooligosacharide, introducing the smashed materials into a spray fluidized bed from the bottom of the spray fluidized bed by applying a positive pressure and enabling the mixture to flow in an acceleratory mode from bottom to top; applying a negative pressure to the upper part of the spray fluidized bed to ensure that the spray fluidized bed vibrates from top to bottom and the mixture boils up and down in the spray fluidized bed; and continuously spraying and dispersing the prepared neotame solution to the superfine sorbitol, xylitol and isomaltooligosacharide by using a plurality of spray guns which are arranged at the side part of the spray fluidized bed, pumping the isomaltooligosacharide solution, and continuously spraying and drying to obtain the sugar-free low-calorie sweetening agent.
Description
Technical field
The present invention relates to a kind of edible sweetener, relate in particular to the low card of a kind of composite sugar-free sweetener and preparation method thereof.
Background technology
Because of the increase with chronic metabolic disease such as the too much inferior health that brings of sugar and cardiovascular and cerebrovasculars, people's demand safety, healthy sugar-free hang down card type sweetener along with people; Reach in production procedure from raw material and put into the advanced preparation technology that one step of finished product completes; Make between sweet substance sweet sense learn from other's strong points to offset one's weaknesses, have complementary advantages on formula for a product, can play during product uses cover, the effect of synergy and lifting mouthfeel, people crave for and are satisfying under the prerequisite that sugariness is high, heat is low, easy to useization, with the low card type sweetener of cane-sugar taste safety and Health sugar-free roughly the same.
Summary of the invention
The objective of the invention is to overcome the deficiency that prior art exists, the low card of a kind of composite sugar-free sweetener and preparation method thereof is provided, adopt the scientific technology of easy operation control, the molten speed of product, mouthfeel, sugariness are all higher than the prior art optimum value.
Purpose of the present invention is achieved through the following technical solutions:
The low card of a kind of composite sugar-free sweetener, characteristics are to comprise following percentage by weight composition: knob is sweet 0.83 ~ 5%, xylitol 20 ~ 40%, oligoisomaltose 30 ~ 60%, D-sorbite 10 ~ 49%; Its preparation method comprises following processing step:
1. knob is sweet by composition proportion, part oligoisomaltose joins respectively in heating container, adds deionized water to mix;
2. be warming up to 45～100 ℃ of dissolvings, and stirring and dissolving 5-20min;
3. add respectively active carbon in the sweet solution of above-mentioned knob and oligomeric maltose solution, insulation 10～20 min filter while hot, and filtrate is pooled to respectively in the storage tank of heat tracing stand-by;
4. press composition proportion with xylitol, after pulverizing, D-sorbite and residue oligoisomaltose put in the spray-fluidized bed apparatus, xylitol, the mixed material of D-sorbite and residue oligoisomaltose enters fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and accelerates from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is first sprayed the sweet solution of the above-mentioned knob that refines continuously and is distributed on fine sugar alcohol body, pump into oligoisomaltose solution, continuous spray-drying, obtain the low card of a kind of composite sugar-free sweetener.
Further, the low card of above-mentioned a kind of composite sugar-free sweetener, wherein, knob is sweet 1.7%, xylitol 25%, oligoisomaltose 53.3%, D-sorbite 20%.
The preparation method of the low card of a kind of composite sugar-free of the present invention sweetener comprises following processing step:
1. knob is sweet by composition proportion, part oligoisomaltose joins respectively in heating container, adds deionized water to mix;
2. be warming up to 45～100 ℃ of dissolvings, and stirring and dissolving 5-20min;
3. add respectively active carbon in the sweet solution of above-mentioned knob and oligomeric maltose solution, insulation 10～20 min filter while hot, and filtrate is pooled to respectively in the storage tank of heat tracing stand-by;
4. press composition proportion with xylitol, after pulverizing, D-sorbite and residue oligoisomaltose put in the spray-fluidized bed apparatus, xylitol, the mixed material of D-sorbite and residue oligoisomaltose enters fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and accelerates from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is first sprayed the sweet solution of the above-mentioned knob that refines continuously and is distributed on fine sugar alcohol body, pump into oligoisomaltose solution, continuous spray-drying, obtain the low card of a kind of composite sugar-free sweetener.
again further, the preparation method of the low card of above-mentioned a kind of composite sugar-free sweetener, knob is sweet, part oligoisomaltose joins in container, adds respectively deionized water to mix, be warming up to respectively 45～100 ℃ of dissolvings, and stir, add respectively active carbon, be incubated 10 minutes, filter while hot, filtrate is pooled to respectively in storage tank with heat tracing, xylitol, D-sorbite and residue oligoisomaltose reach 100～120 orders through pulverizing, be sent in the spray-fluidized bed apparatus, xylitol, the mixed material of D-sorbite and residue oligoisomaltose enters fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and accelerates from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, control the fluidisation EAT at 45～120 ℃, the multiple spot spray gun of fluid bed sidepiece is first sprayed the sweet solution of the above-mentioned knob that refines continuously and is distributed on fine sugar alcohol body, after the mixing of sugar alcohol fluidisation loses surperficial moisture content, pump into oligoisomaltose solution, continuous spray drying granulation, obtain the low card of a kind of composite sugar-free sweetener.
Again further, the preparation method of the low card of above-mentioned a kind of composite sugar-free sweetener, the EAT scope of described fluidized bed with spraying is 45～120 ℃, the EAT that the sweet spraying of knob disperses is 45～95 ℃.
Again further, the preparation method of above-mentioned a kind of composite low-sugar low-calorie sweetener, within the stage of described spraying mixed fluidized bed, the Sucralose spraying is dispersed in fluidisation and smashes on fine sugar alcohol crystal body.
The substantive distinguishing features that technical solution of the present invention is outstanding and significant progressive being mainly reflected in:
The negative-pressure fluidized-bed fluidization technique of the formula of employing science, uses advanced is in conjunction with the multi-point atomizing method, and time sharing segment control appliance EAT efficiently solves Uniform Dispersion, coats the problems such as granulation, drying.Sweet in primary raw material take D-sorbite, xylitol, oligoisomaltose, knob; modify uniformly and coat by preparation method to sugariness; make product sweetness reach 50～200 times of common sucrose; products obtained therefrom does not have smell, there is no color; soluble in water; the low card of this a kind of composite sugar-free sweetener is easy to use, and its preparation process science is simple and easy to operate, is fit to very much large-scale production.
The specific embodiment
The low card of a kind of composite sugar-free of the present invention sweetener, its composition is: knob is sweet 0.83 ~ 5%, xylitol 20 ~ 40%, oligoisomaltose 30 ~ 60%, D-sorbite 10 ~ 49%.Ideal formulations is: knob is sweet 1.7%, xylitol 25%, oligoisomaltose 53.3%, D-sorbite 20%.
the preparation technology of the low card of a kind of composite sugar-free sweetener: at first, sweet and part oligoisomaltose joins respectively in heating container with knob, adds respectively deionized water to mix, be warming up to respectively 45～100 ℃ of dissolvings, and stir, add respectively active carbon in the sweet and oligoisomaltose solution of above-mentioned knob, be incubated 10～20 minutes, filtration while hot, filtrate is pooled to respectively in the storage tank of heat tracing, at last, with D-sorbite, xylitol, after pulverizing, the residue oligoisomaltose puts in the spray-fluidized bed apparatus (heating temperature control and by the sugar alcohol material the is circulated boiling of equipment positive/negative-pressure boiling technology again in fluid bed, mix that fluidisation is anhydrated and fluffy processing, passing through again following steps: mixed material → malleation material accelerates to flow from bottom to top → and negative pressure vibrates → makes material boiling up and down in fluid bed → by the fluid bed side multiple spot spray gun liquid material ejection fog-like liquid of naming a person for a particular job from top to bottom, be sprayed onto on the trickle solids mixing material of boiling), D-sorbite, xylitol, the mixed material of oligoisomaltose enters fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and accelerates from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is first sprayed the sweet solution of the above-mentioned knob that refines continuously and is distributed on trickle mixture, the EAT of controlling the sweet spraying dispersion of knob is 45～95 ℃, the sweet even spraying of knob is dispersed on the mixing sugar alcohol crystalline solid of powder, the rising EAT after fluidisation loses surface crystallization water, pumps into oligoisomaltose solution at mixing sugar alcohol, and spray drying granulation, obtain the fluffy powder granular products that even sugariness is modified continuously.
Embodiment 1:
2.3 kilograms of oligoisomaltoses are dissolved in a stainless steel heating reaction pot with 10 kilograms of deionized waters, sweet 0.83 kilogram of knob is also dissolved in another stainless steel heating reaction pot with 15 kilograms of deionized waters, in pot, material is heated to 80 ℃ by chuck, start stirring, add respectively 1 kilogram of active carbon, be incubated 10 minutes, filter while hot, filtrate collects in respectively in the storage tank of jacket heat-preservation stand-by, 25 kilograms of D-sorbites, 22 kilograms of xylitols, 49.87 kilograms of oligoisomaltoses, pulverize through pulverizer and reach 120 orders, be sent in the spray-fluidized bed apparatus, D-sorbite, xylitol, the mixed material of oligoisomaltose enters fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and accelerates from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is first sprayed the sweet solution of the above-mentioned knob that refines continuously and is distributed on fine sugar alcohol body, controlling the fluidisation EAT is 45～95 ℃, the Multipoint Uniform spraying disperses, after operation is completed, improve again EAT to 60～120 ℃, at D-sorbite, xylitol, after the mixing of oligoisomaltose fluidisation loses surface crystallization water, pump into the above-mentioned oligoisomaltose solution that refines, continuous spray drying granulation, control EAT and mist flow well, obtain the fluffy powder granular products that even sugariness is modified.
Embodiment 2:
2.8 kilograms of oligoisomaltoses are dissolved in a stainless steel heating reaction pot with 15 kilograms of deionized waters, sweet 1.7 kilograms of knob is also dissolved in another stainless steel heating reaction pot with 15 kilograms of deionized waters, in pot, material is heated to 85 ℃ by chuck, start stirring, add respectively 1 kilogram of active carbon, be incubated 10 minutes, filter while hot, filtrate collects in respectively in the storage tank of jacket heat-preservation stand-by, 20 kilograms of D-sorbites, 25 kilograms of xylitols, 50.5 kilograms of oligoisomaltoses, pulverize through pulverizer and reach 120 orders, be sent in the spray-fluidized bed apparatus, D-sorbite, xylitol, the mixed material of oligoisomaltose enters fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and accelerates from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is first sprayed the sweet solution of the above-mentioned knob that refines continuously and is distributed on fine sugar alcohol body, controlling the fluidisation EAT is 45～95 ℃, the Multipoint Uniform spraying disperses, after operation is completed, improve again EAT to 60～120 ℃, at D-sorbite, xylitol, after the mixing of oligoisomaltose fluidisation loses surface crystallization water, pump into the above-mentioned oligoisomaltose solution that refines, continuous spray drying granulation, control EAT and mist flow well, obtain the fluffy powder granular products that even sugariness is modified.
Embodiment 3:
3.5 kilograms of oligoisomaltoses are dissolved in a stainless steel heating reaction pot with 15 kilograms of deionized waters, sweet 2.49 kilograms of knob is also dissolved in another stainless steel heating reaction pot with 20 kilograms of deionized waters, in pot, material is heated to 85 ℃ by chuck, start stirring, add respectively 1 kilogram of active carbon, be incubated 10 minutes, filter while hot, filtrate collects in respectively in the storage tank of jacket heat-preservation stand-by, 18 kilograms of D-sorbites, 28 kilograms of xylitols, 48.01 kilograms of oligoisomaltoses, pulverize through pulverizer and reach 120 orders, be sent in the spray-fluidized bed apparatus, D-sorbite, xylitol, the mixed material of oligoisomaltose enters fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and accelerates from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is first sprayed the sweet solution of the above-mentioned knob that refines continuously and is distributed on fine sugar alcohol body, controlling the fluidisation EAT is 45～95 ℃, the Multipoint Uniform spraying disperses, after operation is completed, improve again EAT to 60～120 ℃, at D-sorbite, xylitol, after the mixing of oligoisomaltose fluidisation loses surface crystallization water, pump into the above-mentioned oligoisomaltose solution that refines, continuous spray drying granulation, control EAT and mist flow well, obtain the fluffy powder granular products that even sugariness is modified.
Embodiment 4:
3 kilograms of oligoisomaltoses are dissolved in a stainless steel heating reaction pot with 15 kilograms of deionized waters, sweet 3.32 kilograms of knob is also dissolved in another stainless steel heating reaction pot with 30 kilograms of deionized waters, in pot, material is heated to 85 ℃ by chuck, start stirring, add respectively 1 kilogram of active carbon, be incubated 10 minutes, filter while hot, filtrate collects in respectively in the storage tank of jacket heat-preservation stand-by, 15 kilograms of D-sorbites, 30 kilograms of xylitols, 48.68 kilograms of oligoisomaltoses, pulverize through pulverizer and reach 120 orders, be sent in the spray-fluidized bed apparatus, D-sorbite, xylitol, the mixed material of oligoisomaltose enters fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and accelerates from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is first sprayed the sweet solution of the above-mentioned knob that refines continuously and is distributed on fine sugar alcohol body, controlling the fluidisation EAT is 45～95 ℃, the Multipoint Uniform spraying disperses, after operation is completed, improve again EAT to 60～120 ℃, at D-sorbite, xylitol, after the mixing of oligoisomaltose fluidisation loses surface crystallization water, pump into the above-mentioned oligoisomaltose solution that refines, continuous spray drying granulation, control EAT and mist flow well, obtain the fluffy powder granular products that even sugariness is modified.
After testing, a kind of composite low-sugar low-calorie sweetener that adopts technical solution of the present invention to obtain, its main performance index sees Table 1.
Table 1
| Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 |
| Particle size | 40～100 orders | 40～100 orders | 40～100 orders | 40～100 orders |
| Sugariness (sucrose contrast) | 50 times | 100 times | 150 times | 200 times |
| Outward appearance | The white powder | The white powder | The white powder | The white powder |
The stability test of sweetener is to check sweetener to guarantee within a certain period of time the ability that undergoes no deterioration, and the sweetener product of the embodiment of the present invention was stored 3 years at normal temperatures, the phenomenons such as rotten and sugariness reduction occur, and stability is very superior.
The sugariness degree of modification of the low card of a kind of composite sugar-free of the present invention sweetener, will adjustment in consumption sweet in knob, usually select the common sucrose sugariness 50～200 times, relatively be fit to the use needs of food enterprise, form according to formula, in same sugariness situation, low-sugar-content and low-calorie sweetening agent is the sweet taste product of low-calorie, this sweetener can not cause blood sugar to raise, and satisfies three high crowds, the healthy people's of pursuit needs.
To sum up obviously show, the present invention adopts formula, uses advanced science and technology technique and the method for science, and products obtained therefrom does not have smell, evenly white, soluble in water, and it is very convenient that the low card of this a kind of sugar-free sweetener is used.Granularity, dissolution velocity, mouthfeel, sugariness all are much better than the prior art value, and preparation technology's simple flow of science is easily gone, and are fit to very much large-scale production, are worth wide popularization and application in the field of business.
What need to understand is: the above is only the preferred embodiment of the present invention; for those skilled in the art; under the prerequisite that does not break away from the principle of the invention, can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (5)
1. the low card of composite sugar-free sweetener is characterized in that comprising following percentage by weight composition: knob is sweet 0.83 ~ 5%, xylitol 20 ~ 40%, oligoisomaltose 30 ~ 60%, D-sorbite 10 ~ 49%; Its preparation method comprises following processing step:
1. knob is sweet by composition proportion, part oligoisomaltose joins respectively in heating container, adds deionized water to mix;
2. be warming up to 45～100 ℃ of dissolvings, and stirring and dissolving 5-20min;
3. add respectively active carbon in the sweet solution of above-mentioned knob and oligomeric maltose solution, insulation 10～20 min filter while hot, and filtrate is pooled to respectively in the storage tank of heat tracing stand-by;
4. press composition proportion with xylitol, after pulverizing, D-sorbite and residue oligoisomaltose put in the spray-fluidized bed apparatus, xylitol, the mixed material of D-sorbite and residue oligoisomaltose enters fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and accelerates from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is first sprayed the sweet solution of the above-mentioned knob that refines continuously and is distributed on fine sugar alcohol body, pump into oligoisomaltose solution, continuous spray-drying, obtain the low card of a kind of composite sugar-free sweetener.
2. the low card of a kind of composite sugar-free according to claim 1 sweetener is characterized in that its component has following percentage by weight: knob is sweet 1.7%, xylitol 25%, oligoisomaltose 53.3%, D-sorbite 20%.
3. a kind of composite sugar-free claimed in claim 1 hangs down the preparation method of card sweetener, it is characterized in that comprising following processing step:
1. knob is sweet by composition proportion, part oligoisomaltose joins respectively in heating container, adds deionized water to mix;
2. be warming up to 45～100 ℃ of dissolvings, and stirring and dissolving 5-20min;
3. add respectively active carbon in the sweet solution of above-mentioned knob and oligomeric maltose solution, insulation 10～20 min filter while hot, and filtrate is pooled to respectively in the storage tank of heat tracing stand-by;
4. press composition proportion with xylitol, after pulverizing, D-sorbite and residue oligoisomaltose put in the spray-fluidized bed apparatus, xylitol, the mixed material of D-sorbite and residue oligoisomaltose enters fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and accelerates from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is first sprayed the sweet solution of the above-mentioned knob that refines continuously and is distributed on fine sugar alcohol body, pump into oligoisomaltose solution, continuous spray-drying, obtain the low card of a kind of composite sugar-free sweetener.
4. a kind of composite sugar-free according to claim 3 hangs down the preparation method of card sweetener, and it is characterized in that: knob is sweet, part oligoisomaltose joins in container, adds respectively deionized water to mix, be warming up to respectively 45～100 ℃ of dissolvings, and stir, add respectively active carbon, be incubated 10 minutes, filter while hot, filtrate is pooled to respectively in storage tank with heat tracing, xylitol, D-sorbite and residue oligoisomaltose reach 100～120 orders through pulverizing, be sent in the spray-fluidized bed apparatus, xylitol, the mixed material of D-sorbite and residue oligoisomaltose enters fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and accelerates from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, control the fluidisation EAT at 45～120 ℃, the multiple spot spray gun of fluid bed sidepiece is first sprayed the sweet solution of the above-mentioned knob that refines continuously and is distributed on fine sugar alcohol body, after the mixing of sugar alcohol fluidisation loses surperficial moisture content, pump into oligoisomaltose solution, continuous spray drying granulation, obtain the low card of a kind of composite sugar-free sweetener.
5. a kind of composite sugar-free according to claim 4 hangs down the preparation method of card sweetener, it is characterized in that: the EAT scope of described fluidized bed with spraying is 45～120 ℃, wherein the EAT of the sweet spraying dispersion of phase I knob is 45～95 ℃, and the EAT of second stage oligoisomaltose spraying is 60～120 ℃.
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| CN104957472A (en) * | 2015-06-24 | 2015-10-07 | 陈佳伟 | Sugarless sweetening agent and preparation method thereof |
| CN106901375A (en) * | 2017-03-20 | 2017-06-30 | 禹城市恒溢生物科技有限公司 | It is a kind of compound for sugar product containing xylitol |
| CN112006263A (en) * | 2020-09-08 | 2020-12-01 | 江西福美泰生物技术有限公司 | Neotame compound sweetener and preparation method thereof |
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| CN101810305A (en) * | 2009-12-08 | 2010-08-25 | 苏州工业园区尚融科技有限公司 | Novel composite sugar-free table sweetener and production method thereof |
| CN101810298A (en) * | 2009-12-08 | 2010-08-25 | 苏州工业园区尚融科技有限公司 | Novel sugar-free table sweetening agent and preparation method thereof |
| CN101874596A (en) * | 2009-12-04 | 2010-11-03 | 苏州工业园区尚融科技有限公司 | Composite sugar-free sweetener and preparation method thereof |
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| CN101810305A (en) * | 2009-12-08 | 2010-08-25 | 苏州工业园区尚融科技有限公司 | Novel composite sugar-free table sweetener and production method thereof |
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| CN104957472A (en) * | 2015-06-24 | 2015-10-07 | 陈佳伟 | Sugarless sweetening agent and preparation method thereof |
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| CN112006263A (en) * | 2020-09-08 | 2020-12-01 | 江西福美泰生物技术有限公司 | Neotame compound sweetener and preparation method thereof |
| CN112006263B (en) * | 2020-09-08 | 2024-03-29 | 江西福美泰生物技术有限公司 | Neotame composition and preparation method thereof |
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Application publication date: 20130327 |