CN102960694A - Compound sweetening agent applicable to coffee and preparation method thereof - Google Patents
Compound sweetening agent applicable to coffee and preparation method thereof Download PDFInfo
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- CN102960694A CN102960694A CN2012105011732A CN201210501173A CN102960694A CN 102960694 A CN102960694 A CN 102960694A CN 2012105011732 A CN2012105011732 A CN 2012105011732A CN 201210501173 A CN201210501173 A CN 201210501173A CN 102960694 A CN102960694 A CN 102960694A
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Abstract
The invention relates to a compound sweetening agent applicable to coffee and a preparation method thereof. The compound sweetening agent comprises the following components: 13.33-25% of sucralose, 25-45% of erythritol, and 35-53% of modified starch. The process comprises the following steps: putting the sucralose, the erythritol and the modified starch accounting for 40-60% of the total amount into a multi-dimensional mixing machine for mixing at the speed of 800-1000rpm for 20-50 minutes to obtain mixed materials; dissolving the rest modified starch into deionized water to obtain a modified starch water solution; causing the mixed materials to enter a spray fluidized bed from the bottom of the fluidized bed at a positive pressure and flow from bottom to top at an accelerating speed, and applying a negative pressure on the upper part of the spray fluidized bed, so as to generate vibration from top to bottom, so that the mixed materials boil up and down in the fluidized bed to form fine sugar alcohol particles; and continuously spraying and dispersing a glucose water solution onto the fine sugar alcohol particles in the fluidized bed through a multipoint spray gun, and drying with hot air to obtain the compound sweetening agent.
Description
Technical field
The present invention relates to a kind of food additives, be specifically related to applicable composite sweetener of a kind of coffee and preparation method thereof.
Background technology
In the last few years, raising along with expanding economy and people's lives wealth, obesity, hypertension, diabetes, carious tooth etc. become the height morbidity among the crowd, and the generation of these high morbidities is considered to especially with the sucrose Excessive Intake substantial connection is arranged with eating habit and diet structure.Therefore, as the sweetener of food additives, one of its development priority is exactly safe, without nutritive value, empty calory or functional high sweetener extremely low in calories.The characteristics of functional high sweetener are use safe, and consumption is few, and sugariness is high, and use cost is generally all far below sucrose, and this also is the power place that Food Science man continually develops novel high-intensity sweetener.At present, about 20 kinds of the granted high sweetener in countries in the world obtains that kind that the majority state approval allows to use mainly contains that saccharin sodium, honey element, 3,4-Dihydro-6-methyl-1,2,3-oxathiazin-4-one 2,2-dioxide potassium salt, Aspartame, Sucralose, alitame, knob are sweet, glycyrrhizin, stevioside, Momordica grosvenori is sweet and Talin etc.These high sweeteners have plenty of artificial synthetic, and are sweet etc. such as Aspartame, Sucralose, knob; What have then is natural extract, sweet etc. such as sky chrysanthemum glycosides and arhat.No matter be artificial synthesis edulcorant or natural extraction sweetener, at sugariness, sweet taste, stable aspects its pluses and minuses arranged respectively all, therefore, want to give full play to the optimal efficacy of these sweeteners, reduce cost, the most frequently used means are exactly compound at present.By carrying out various sweeteners or sweet substance compound, bring into play may exist between the various sweeteners synergistic function, in the hope of as far as possible approaching or satisfy the requirement of desirable sweetener: safety non-toxic, sweet taste is pure similar to sucrose (this is to be popular generally accepted sweet tastes), high sugariness, low heat value or without calorific value, stable height, unlikely dental caries, reduction cost.
In the prior art, the major defect that the composite sweetener take Sucralose as main sweetening material exists when being applied in the coffee is: mouthfeel is compared in addition different with sucrose, and is front sweet slow, rear sweet heavy; When using as the generation sugar of white granulated sugar, coffee is thinned out and bitter sense increases the weight of, make the mouthfeel of coffee beverage bad, do not liked by the consumer.
Composite sweetener take Sucralose as main sweetening material in the prior art, can process by method or the spray-dired method of substep of simple blend, the composite sweetener that the simple blend method makes is with low cost, but be difficult to guarantee that main sweetening material Sucralose can be uniformly dispersed, and this point can affect the quality of composite sweetener product to a great extent.The spray-dired method of substep is that substep is dissolved in main sweetening material and each auxiliary sweetening material in the deionized water in batches, then the method by the wet spray drying is coated on each composition material on the granular sweetener by spraying respectively, the composite sweetener product sweetness that this method makes is uniformly dispersed, instant capacity is good, quality is better than the composite sweetener product that additive method makes, but its shortcoming is: material loss, the loss of especially main sweetening material is larger, machinery equipment power consumption is too high, the cost of product is significantly increased, and therefore this method also has been subject to certain restriction in implementation process.
Summary of the invention
The objective of the invention is to overcome the deficiency that prior art exists, applicable composite sweetener of a kind of coffee with low cost, that sugariness is uniformly dispersed and mouthfeel is better and preparation method thereof is provided.
Purpose of the present invention is achieved through the following technical solutions:
The composite sweetener that a kind of coffee is applicable comprises following percentage by weight composition: Sucralose 13.33～25%, antierythrite 25 ~ 45%, converted starch 35 ~ 53%; Its preparation method comprises following processing step:
1. Sucralose, antierythrite and the converted starch that accounts for total amount 40 ~ 60% are dropped in the Multidimensionblender, progression with 800 ~ 1000rpm mixed 20 ~ 50 minutes, the granularity of control mixed material obtains the mixed material of Sucralose, antierythrite and converted starch at 80 ~ 130 orders;
2. the converted starch with surplus is dissolved in the deionized water, obtains the converted starch aqueous solution;
3. with step 1. the mixed material of gained put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with step 2. the prepared converted starch aqueous solution continuously spraying be distributed on the sugar alcohol granule in the fluid bed, by heated-air drying, obtain described composite sweetener again.
The preparation method of the composite sweetener that a kind of coffee of the present invention is applicable comprises following processing step:
1. Sucralose, antierythrite and the converted starch that accounts for total amount 40 ~ 60% are dropped in the Multidimensionblender, progression with 800 ~ 1000rpm mixed 20 ~ 50 minutes, the granularity of control mixed material obtains the mixed material of Sucralose, antierythrite and converted starch at 80 ~ 130 orders;
2. the converted starch with surplus is dissolved in the deionized water, obtains the converted starch aqueous solution;
3. with step 1. the mixed material of gained put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with step 2. the prepared converted starch aqueous solution continuously spraying be distributed on the sugar alcohol granule in the fluid bed, by heated-air drying, obtain described composite sweetener again.
Further, the preparation method of the composite sweetener that above-mentioned a kind of coffee is applicable, step 3. in, the EAT of fluid bed is controlled at 60 ~ 105 ℃.
Again further, the preparation method of the composite sweetener that above-mentioned a kind of coffee is applicable, step 3. in, when the spraying of the converted starch aqueous solution disperseed, the EAT of control fluid bed was at 60 ~ 80 ℃, the EAT of control fluid bed is at 80 ~ 105 ℃ during heated-air drying
The substantive distinguishing features that technical solution of the present invention is outstanding and significant progressive being mainly reflected in:
The present invention utilizes the synergy of converted starch and antierythrite, by adjusting and optimize the per distribution ratio of each component, can effectively cover and alleviate front sweet slow, the rear sweet heavy problem of Sucralose composite sweetener, especially when being applied to coffee or have in the bitter beverage of feeling of coffee, can also remedy the problem that replaces white granulated sugar that mouthfeel is thinned out owing to the use composite sweetener in the beverage, make the taste flavor of beverage more near consumer demand.
The present invention will carry out tentatively mixing in composite sweetener master sweetening material and the auxiliary sweetening material input of the part Multidimensionblender first, then remaining auxiliary sweetening material is dissolved into the aqueous solution, and disperse dry by the disposable wet spray of advanced negative-pressure fluidized bed apparatus, make it to be coated on just mixed mixed material surface, obtain the Fluffy powder grain compound sweetener product.The present invention compares with the method for prior art simple blend, and the product instant capacity that obtains, sugariness dispersiveness etc. have significantly lifting, have good quality; And with prior art in batches spray-dired method compare, can greatly shorten the process-cycle again, reduce the loss of the especially main sweetening material of raw material, the amount of saving energy has reduced production cost.
The specific embodiment
Composite sweetener of the present invention, its composition is: Sucralose 13.33～25%, antierythrite 25 ~ 45%, converted starch 35 ~ 53%; Ideal formulations is: Sucralose 18.33%, antierythrite 35%, converted starch 46.67%.
Among the present invention, employed converted starch mainly is the converted starch of thickening class, the STAR-DRI 5 MALTODEXTRIN type products that the converted starch that specifically uses among the embodiment is produced as A.E. Staley Manufacturing Company.
The preparation technology of this composite sweetener: first Sucralose, antierythrite and the converted starch that accounts for total amount 40 ~ 60% are dropped in the Multidimensionblender, progression with 800 ~ 1000rpm mixed 20 ~ 50 minutes, the granularity of control mixed material obtains the mixed material of Sucralose, antierythrite and converted starch at 80 ~ 130 orders; Converted starch with surplus is dissolved in the deionized water again, obtains the converted starch aqueous solution; The mixed material of gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, the EAT of fluid bed is controlled at 60 ~ 105 ℃, forms tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with prepared D/W continuously spraying be distributed on the sugar alcohol granule in the fluid bed, when the spraying of the converted starch aqueous solution disperses, the EAT of control fluid bed is at 60 ~ 80 ℃, pass through again heated-air drying, the EAT of control fluid bed obtains described composite sweetener at 80 ~ 105 ℃ during heated-air drying.
Multidimensionblender used in the present invention adopts commercial 200 feather weight Multidimensionblenders, rotating speed level journey is 200 ~ 1800rpm, barrel is two taper, middle column, and during work, this Multidimensionblender can make the material in the barrel collide, pulverize and mix from a plurality of angles.
Embodiment 1:
(1) gets in 13.33 kilograms of Sucraloses, 33.67 kilograms of antierythrites, 27 kilograms of inputs of the converted starch Multidimensionblender, the progression of control Multidimensionblender is 1000rpm, mixed 35 minutes, obtain the mixed material of Sucralose, antierythrite and converted starch, granularity is between 80 ~ 130 orders;
(2) 26 kilograms of remaining converted starches are mixed with deionized water, the intensification stirring and dissolving obtains the converted starch aqueous solution;
(3) mixed material of step (1) gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece is distributed to the continuous spraying of the prepared converted starch aqueous solution of step (2) on the interior sugar alcohol granule of fluid bed, the EAT of control fluid bed is between 60 ~ 80 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the EAT of fluid bed between 80 ~ 105 ℃, carry out heated-air drying, last discharging obtains Fluffy powder grain compound sweetener.
Embodiment 2:
(1) gets in 15.83 kilograms of Sucraloses, 34.5 kilograms of antierythrites, 25.67 kilograms of inputs of the converted starch Multidimensionblender, the progression of control Multidimensionblender is 1000rpm, mixed 35 minutes, obtain the mixed material of Sucralose, antierythrite and converted starch, granularity is between 80 ~ 130 orders;
(2) 24 kilograms of remaining converted starches are mixed with deionized water, the intensification stirring and dissolving obtains the converted starch aqueous solution;
(3) mixed material of step (1) gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece is distributed to the continuous spraying of the prepared converted starch aqueous solution of step (2) on the interior sugar alcohol granule of fluid bed, the EAT of control fluid bed is between 60 ~ 80 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the EAT of fluid bed between 80 ~ 105 ℃, carry out heated-air drying, last discharging obtains Fluffy powder grain compound sweetener.
Embodiment 3:
(1) gets in 18.33 kilograms of Sucraloses, 35 kilograms of antierythrites, 23.67 kilograms of inputs of the converted starch Multidimensionblender, the progression of control Multidimensionblender is 1000rpm, mixed 35 minutes, obtain the mixed material of Sucralose, antierythrite and converted starch, granularity is between 80 ~ 130 orders;
(2) 23 kilograms of remaining converted starches are mixed with deionized water, the intensification stirring and dissolving obtains the converted starch aqueous solution;
(3) mixed material of step (1) gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece is distributed to the continuous spraying of the prepared converted starch aqueous solution of step (2) on the interior sugar alcohol granule of fluid bed, the EAT of control fluid bed is between 60 ~ 80 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the EAT of fluid bed between 80 ~ 105 ℃, carry out heated-air drying, last discharging obtains Fluffy powder grain compound sweetener.
Embodiment 4:
(1) gets in 21.67 kilograms of Sucraloses, 36 kilograms of antierythrites, 22.33 kilograms of inputs of the converted starch Multidimensionblender, the progression of control Multidimensionblender is 1000rpm, mixed 40 minutes, obtain the mixed material of Sucralose, antierythrite and converted starch, granularity is between 80 ~ 130 orders;
(2) 20 kilograms of remaining converted starches are mixed with deionized water, the intensification stirring and dissolving obtains the converted starch aqueous solution;
(3) mixed material of step (1) gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece is distributed to the continuous spraying of the prepared converted starch aqueous solution of step (2) on the interior sugar alcohol granule of fluid bed, the EAT of control fluid bed is between 60 ~ 80 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the EAT of fluid bed between 80 ~ 105 ℃, carry out heated-air drying, last discharging obtains Fluffy powder grain compound sweetener.
Embodiment 5:
(1) gets in 25 kilograms of Sucraloses, 38 kilograms of antierythrites, 19 kilograms of inputs of the converted starch Multidimensionblender, the progression of control Multidimensionblender is 1000rpm, mixed 40 minutes, and obtained the mixed material of Sucralose, antierythrite and converted starch, granularity is between 80 ~ 130 orders;
(2) 18 kilograms of remaining converted starches are mixed with deionized water, the intensification stirring and dissolving obtains the converted starch aqueous solution;
(3) mixed material of step (1) gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece is distributed to the continuous spraying of the prepared converted starch aqueous solution of step (2) on the interior sugar alcohol granule of fluid bed, the EAT of control fluid bed is between 60 ~ 80 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the EAT of fluid bed between 80 ~ 105 ℃, carry out heated-air drying, last discharging obtains Fluffy powder grain compound sweetener.
The composite sweetener that adopts technical solution of the present invention to obtain, its main performance index sees Table 1.
Table 1
The molten speed of composite sweetener product of the present invention, mouthfeel, the sugariness uniformity are all very good, can effectively cover and alleviate front sweet slow, the rear sweet heavy problem of Sucralose composite sweetener, when being applied to coffee or have in the bitter beverage of feeling of coffee, can coordinate mutually with the drink taste, make the taste flavor of beverage more near consumer demand.
The present invention will carry out tentatively mixing in composite sweetener master sweetening material and the auxiliary sweetening material input of the part Multidimensionblender first, then remaining auxiliary sweetening material is dissolved into the aqueous solution, and disperse dry by the disposable wet spray of advanced negative-pressure fluidized bed apparatus, make it to be coated on just mixed mixed material surface, obtain the Fluffy powder grain compound sweetener product.The present invention compares with the method for prior art simple blend, and the product instant capacity that obtains, sugariness dispersiveness etc. have significantly lifting, have good quality; And with prior art in batches spray-dired method compare, can greatly shorten the process-cycle again, reduce the loss of the especially main sweetening material of raw material, the amount of saving energy, reduced production cost (about 60 ~ 80 minutes of product manufacturing cycle of the present invention, and about 2 ~ 3 hours of the manufacturing cycle of spray drying process in batches, and the present invention just the mixed power consumption that uses Multidimensionblender be approximately fluidized bed with spraying electricity consumption of equipment amount 1/24).
The sugariness degree of modification of composite sweetener of the present invention can be adjusted by the consumption of Sucralose according to actual needs, and the present invention is fit to the composite sweetener of 80～150 times of sucrose sweetness of preparation usually.
What need to understand is: the above only is preferred embodiment of the present invention; for those skilled in the art; under the prerequisite that does not break away from the principle of the invention, can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (4)
1. the applicable composite sweetener of coffee is characterized in that comprising following percentage by weight composition: Sucralose 13.33～25%, antierythrite 25 ~ 45%, converted starch 35 ~ 53%; Its preparation method comprises following processing step:
1. Sucralose, antierythrite and the converted starch that accounts for total amount 40 ~ 60% are dropped in the Multidimensionblender, progression with 800 ~ 1000rpm mixed 20 ~ 50 minutes, the granularity of control mixed material obtains the mixed material of Sucralose, antierythrite and converted starch at 80 ~ 130 orders;
2. the converted starch with surplus is dissolved in the deionized water, obtains the converted starch aqueous solution;
3. with step 1. the mixed material of gained put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with step 2. the prepared converted starch aqueous solution continuously spraying be distributed on the sugar alcohol granule in the fluid bed, by heated-air drying, obtain described composite sweetener again.
2. the preparation method of the applicable composite sweetener of coffee claimed in claim 1 is characterized in that comprising following processing step:
1. Sucralose, antierythrite and the converted starch that accounts for total amount 40 ~ 60% are dropped in the Multidimensionblender, progression with 800 ~ 1000rpm mixed 20 ~ 50 minutes, the granularity of control mixed material obtains the mixed material of Sucralose, antierythrite and converted starch at 80 ~ 130 orders;
2. the converted starch with surplus is dissolved in the deionized water, obtains the converted starch aqueous solution;
3. with step 1. the mixed material of gained put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with step 2. the prepared converted starch aqueous solution continuously spraying be distributed on the sugar alcohol granule in the fluid bed, by heated-air drying, obtain described composite sweetener again.
3. the preparation method of the applicable composite sweetener of coffee according to claim 2 is characterized in that: step 3. in, the EAT of fluid bed is controlled at 60 ~ 105 ℃.
4. the preparation method of the applicable composite sweetener of coffee according to claim 3, it is characterized in that: step 3. in, when the spraying of the converted starch aqueous solution disperseed, the EAT of control fluid bed was at 60 ~ 80 ℃, and the EAT of control fluid bed is at 80 ~ 105 ℃ during heated-air drying.
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| CN101897425A (en) * | 2009-12-04 | 2010-12-01 | 苏州工业园区尚融科技有限公司 | Fluffy granular composite low-sugar low-calorie table sweetener and preparation method thereof |
| CN102578448A (en) * | 2011-01-05 | 2012-07-18 | 湖北益泰药业有限公司 | Sucralose effervescent granules and preparation method thereof |
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- 2012-11-30 CN CN2012105011732A patent/CN102960694A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101874594A (en) * | 2009-11-24 | 2010-11-03 | 苏州工业园区尚融科技有限公司 | Fluffy granular composite sugar-free sweetener and preparation method thereof |
| CN101874604A (en) * | 2009-12-04 | 2010-11-03 | 苏州工业园区尚融科技有限公司 | Fluffy granular composite low-sugar and low-calorie sweetener and preparation method thereof |
| CN101897425A (en) * | 2009-12-04 | 2010-12-01 | 苏州工业园区尚融科技有限公司 | Fluffy granular composite low-sugar low-calorie table sweetener and preparation method thereof |
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Application publication date: 20130313 |