CN102960821A - Compound sweetener suitable for dietary fiber beverage and preparation method thereof - Google Patents

Compound sweetener suitable for dietary fiber beverage and preparation method thereof Download PDF

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Publication number
CN102960821A
CN102960821A CN2012105007050A CN201210500705A CN102960821A CN 102960821 A CN102960821 A CN 102960821A CN 2012105007050 A CN2012105007050 A CN 2012105007050A CN 201210500705 A CN201210500705 A CN 201210500705A CN 102960821 A CN102960821 A CN 102960821A
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dietary fiber
fluid bed
isomalt
fluidized bed
mixed material
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历冠廷
马力量
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Suzhou Industrial Park Shangrong Technology Co Ltd
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Suzhou Industrial Park Shangrong Technology Co Ltd
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Abstract

The invention relates to a compound sweetener suitable for dietary fiber beverage and a preparation method thereof. The compound sweetener comprises the components of 3.33-8.33% of sucralose, 5-15% of erythritol, 25-30% of isomaltitol, and 46.67-66.67% of soluble dietary fiber. The preparation process comprises the steps of: feeding the erythritol, the soluble dietary fiber and the isomaltitol which is 40-60% of total weight into a multi-dimensional mixer; primarily mixing the materials, then dissolving the sucralose and residual isomaltitol into deionized water to obtain mixed aqueous solution; feeding the mixed materials into a fluidized bed from the bottom part of a spray fluidized bed by positive pressure and accelerating flow from bottom to top; exerting negative pressure to the upper part of the spray fluidized bed, and vibrating the mixed materials from top to bottom, so that the mixed materials boil up and down inside the fluidized bed and form fine sugar alcohol granules; and continuously spraying and dispersing the mixed aqueous solution on the sugar alcohol granules inside the fluidized bed through a multi-point spray gun at the side part of the fluidized bed to obtain the compound sweetener.

Description

A kind of composite sweetener of using in the dietary fiber drink and preparation method thereof that is adapted at
Technical field
The present invention relates to a kind of food additives, be specifically related to a kind of composite sweetener of using in the dietary fiber drink and preparation method thereof that is adapted at.
Background technology
In the last few years, raising along with expanding economy and people's lives wealth, obesity, hypertension, diabetes, carious tooth etc. become the height morbidity among the crowd, and the generation of these high morbidities is considered to especially with the sucrose Excessive Intake substantial connection is arranged with eating habit and diet structure.Therefore, as the sweetener of food additives, one of its development priority is exactly safe, without nutritive value, empty calory or functional high sweetener extremely low in calories.The characteristics of functional high sweetener are use safe, and consumption is few, and sugariness is high, and use cost is generally all far below sucrose, and this also is the power place that Food Science man continually develops novel high-intensity sweetener.At present, about 20 kinds of the granted high sweetener in countries in the world obtains that kind that the majority state approval allows to use mainly contains that saccharin sodium, honey element, 3,4-Dihydro-6-methyl-1,2,3-oxathiazin-4-one 2,2-dioxide potassium salt, Aspartame, Sucralose, alitame, knob are sweet, glycyrrhizin, stevioside, Momordica grosvenori is sweet and Talin etc.These high sweeteners have plenty of artificial synthetic, and are sweet etc. such as Aspartame, Sucralose, knob; What have then is natural extract, sweet etc. such as sky chrysanthemum glycosides and arhat.No matter be artificial synthesis edulcorant or natural extraction sweetener, at sugariness, sweet taste, stable aspects its pluses and minuses arranged respectively all, therefore, want to give full play to the optimal efficacy of these sweeteners, reduce cost, the most frequently used means are exactly compound at present.By carrying out various sweeteners or sweet substance compound, bring into play may exist between the various sweeteners synergistic function, in the hope of as far as possible approaching or satisfy the requirement of desirable sweetener: safety non-toxic, sweet taste is pure similar to sucrose (this is to be popular generally accepted sweet tastes), high sugariness, low heat value or without calorific value, stable height, unlikely dental caries, reduction cost.
In the prior art, the major defect that the composite sweetener take Sucralose as main sweetening material exists is: mouthfeel has been compared different with sucrose, and is front sweet slow, rear sweet heavy; Especially when in the functional beverage that is applied to dietary fiber drink etc. and has denseer thick mouthfeel, this composite sweetener as generation sugar be difficult to reach the taste that traditional white granulated sugar can bring in drink so that the mouthfeel of drink is undesirable.
Composite sweetener take Sucralose as main sweetening material in the prior art, can process by method or the spray-dired method of substep of simple blend, the composite sweetener that the simple blend method makes is with low cost, but be difficult to guarantee that main sweetening material Sucralose can be uniformly dispersed, and this point can affect the quality of composite sweetener product to a great extent.The spray-dired method of substep is that substep is dissolved in main sweetening material and each auxiliary sweetening material in the deionized water in batches, then the method by the wet spray drying is coated on each composition material on the granular sweetener by spraying respectively, the composite sweetener product sweetness that this method makes is uniformly dispersed, instant capacity is good, quality is better than the composite sweetener product that additive method makes, but its shortcoming is: material loss, the loss of especially main sweetening material is larger, machinery equipment power consumption is too high, the cost of product is significantly increased, and therefore this method also has been subject to certain restriction in implementation process.
Summary of the invention
The objective of the invention is to overcome the deficiency that prior art exists, provide that a kind of mouthfeel is good, with low cost, sugariness is uniformly dispersed and be adapted at composite sweetener that uses in the dietary fiber drink and preparation method thereof.
Purpose of the present invention is achieved through the following technical solutions:
A kind of composite sweetener of using in the dietary fiber drink of being adapted at comprises following percentage by weight composition: Sucralose 3.33~8.33%, antierythrite 5~15%, isomalt 25~30%, soluble dietary fiber 46.67~66.67%; Its preparation method comprises following processing step:
1. just antierythrite, soluble dietary fiber and the isomalt that accounts for total amount 40 ~ 60% drop in the Multidimensionblender, progression with 600 ~ 1000rpm mixed 20 ~ 50 minutes, the granularity of control mixed material obtains the mixed material of antierythrite, soluble dietary fiber and isomalt at 80 ~ 130 orders;
2. the isomalt with Sucralose and surplus is dissolved in the deionized water, obtains the mixed aqueous solution of Sucralose and isomalt;
3. with step 1. the mixed material of gained put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with step 2. prepared mixed aqueous solution continuously spraying be distributed on the sugar alcohol granule in the fluid bed, by heated-air drying, obtain described composite sweetener again.
Further, above-mentioned a kind of composite sweetener of using in the dietary fiber drink of being adapted at, described soluble dietary fiber is konjaku flour or soybean polyoses.
The present invention is a kind of to be adapted at the preparation method of the composite sweetener that uses in the dietary fiber drink, comprises following processing step:
1. just antierythrite, soluble dietary fiber and the isomalt that accounts for total amount 40 ~ 60% drop in the Multidimensionblender, progression with 600 ~ 1000rpm mixed 20 ~ 50 minutes, the granularity of control mixed material obtains the mixed material of antierythrite, soluble dietary fiber and isomalt at 80 ~ 130 orders;
2. the isomalt with Sucralose and surplus is dissolved in the deionized water, obtains the mixed aqueous solution of Sucralose and isomalt;
3. with step 1. the mixed material of gained put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with step 2. prepared mixed aqueous solution continuously spraying be distributed on the sugar alcohol granule in the fluid bed, by heated-air drying, obtain described composite sweetener again.
Further, above-mentioned a kind of preparation method who is adapted at the composite sweetener that uses in the dietary fiber drink, step 3. in, the EAT of fluid bed is controlled at 50 ~ 110 ℃.
Again further, above-mentioned a kind of preparation method who is adapted at the composite sweetener that uses in the dietary fiber drink, step 3. in, when the mixed aqueous solution spraying disperses, the EAT of control fluid bed is between 50 ~ 80 ℃, and the EAT of control fluid bed is at 80 ~ 110 ℃ during heated-air drying.
The substantive distinguishing features that technical solution of the present invention is outstanding and significant progressive being mainly reflected in:
The present invention adds soluble dietary fiber and cooperates with antierythrite, isomalt etc. in composition of raw materials, by adjusting and optimize the per distribution ratio of each component, can effectively cover and alleviate front sweet slow, the rear sweet heavy problem of Sucralose composite sweetener, especially when in the functional beverage that is applied to dietary fiber drink etc. and has denseer thick mouthfeel, composite sweetener of the present invention can be coordinated mutually with the drink mouthfeel, when substituting traditional white granulated sugar the drink mouthfeel is thinned out.
The present invention drops into the auxiliary sweetening material of the part of composite sweetener in the Multidimensionblender first and carries out tentatively mixing, then main sweetening material and remaining auxiliary sweetening material are dissolved into mixed aqueous solution, and disperse dry by the disposable spraying of advanced negative-pressure fluidized bed apparatus, make it to be coated on just mixed mixed material surface, obtain the Fluffy powder grain compound sweetener product.The present invention compares with the method for prior art simple blend, and the product instant capacity that obtains, sugariness dispersiveness etc. have significantly lifting, have good quality; And with prior art in batches spray-dired method compare, can greatly shorten the process-cycle again, the amount of saving energy has reduced production cost (about 60 ~ 90 minutes of product manufacturing cycle of the present invention, and in batches about 2 ~ 3 hours of the manufacturing cycle of spray drying process).
The specific embodiment
Composite sweetener of the present invention, its composition is: Sucralose 3.33~8.33%, antierythrite 5~15%, isomalt 25~30%, soluble dietary fiber 46.67~66.67%.
The preparation technology of composite sweetener: first antierythrite, soluble dietary fiber and the isomalt that accounts for total amount 40 ~ 60% are dropped in the Multidimensionblender, progression with 600 ~ 1000rpm mixed 20 ~ 50 minutes, the granularity of control mixed material obtains the mixed material of antierythrite, soluble dietary fiber and isomalt at 80 ~ 130 orders; Isomalt with Sucralose and surplus is dissolved in the deionized water again, obtains the mixed aqueous solution of Sucralose and isomalt; Then mixed material is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, the EAT of fluid bed is controlled at 50 ~ 110 ℃, forms tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with prepared mixed aqueous solution continuously spraying be distributed on the sugar alcohol granule in the fluid bed, when the mixed aqueous solution spraying disperses, the EAT of control fluid bed is between 50 ~ 80 ℃, pass through again heated-air drying, the EAT of control fluid bed obtains described composite sweetener at 80 ~ 110 ℃ during heated-air drying.
Multidimensionblender used in the present invention adopts commercial 200 feather weight Multidimensionblenders, rotating speed level journey is 200 ~ 1800rpm, barrel is two taper, middle column, and during work, this Multidimensionblender can make the material in the barrel collide, pulverize and mix from a plurality of angles.
Embodiment 1:
(1) gets in 6.5 kilograms of antierythrites, 65.17 kilograms of konjaku flours, 13.5 kilograms of inputs of the isomalt Multidimensionblender, the progression of control Multidimensionblender is 1000rpm, mixed 40 minutes, obtain the mixed material of antierythrite, konjaku flour and isomalt, granularity is between 80 ~ 130 orders;
(2) 11.5 kilograms of 3.33 kilograms of Sucraloses, remaining isomalt are mixed with deionized water, the intensification stirring and dissolving obtains the mixed aqueous solution of Sucralose and isomalt;
(3) mixed material of step (1) gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece is distributed to the continuous spraying of the prepared mixed aqueous solution of step (2) on the interior sugar alcohol granule of fluid bed, the EAT of control fluid bed is between 50 ~ 80 ℃, when spraying finishes substantially after 25 ~ 30 minutes, control again the EAT of fluid bed between 80 ~ 110 ℃, carry out heated-air drying, last discharging obtains Fluffy powder grain compound sweetener.
Embodiment 2:
(1) gets in 8 kilograms of antierythrites, 61 kilograms of konjaku flours, 14 kilograms of inputs of the isomalt Multidimensionblender, the progression of control Multidimensionblender is 1000rpm, mixed 40 minutes, and obtained the mixed material of antierythrite, konjaku flour and isomalt, granularity is between 80 ~ 130 orders;
(2) 12 kilograms of 5 kilograms of Sucraloses, remaining isomalt are mixed with deionized water, the intensification stirring and dissolving obtains the mixed aqueous solution of Sucralose and isomalt;
(3) mixed material of step (1) gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece is distributed to the continuous spraying of the prepared mixed aqueous solution of step (2) on the interior sugar alcohol granule of fluid bed, the EAT of control fluid bed is between 50 ~ 80 ℃, when spraying finishes substantially after 30 ~ 35 minutes, control again the EAT of fluid bed between 80 ~ 110 ℃, carry out heated-air drying, last discharging obtains Fluffy powder grain compound sweetener.。
Embodiment 3:
(1) gets in 10 kilograms of antierythrites, 55.33 kilograms of soybean polyoses, 15 kilograms of inputs of the isomalt Multidimensionblender, the progression of control Multidimensionblender is 800rpm, mixed 40 minutes, obtain the mixed material of antierythrite, soybean polyoses and isomalt, granularity is between 80 ~ 130 orders;
(2) 13 kilograms of 6.67 kilograms of Sucraloses, remaining isomalt are mixed with deionized water, the intensification stirring and dissolving obtains the mixed aqueous solution of Sucralose and isomalt;
(3) mixed material of step (1) gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece is distributed to the continuous spraying of the prepared mixed aqueous solution of step (2) on the interior sugar alcohol granule of fluid bed, the EAT of control fluid bed is between 50 ~ 80 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the EAT of fluid bed between 80 ~ 110 ℃, carry out heated-air drying, last discharging obtains Fluffy powder grain compound sweetener.
Embodiment 4:
(1) gets in 12 kilograms of antierythrites, 49.67 kilograms of soybean polyoses, 16 kilograms of inputs of the isomalt Multidimensionblender, the progression of control Multidimensionblender is 800rpm, mixed 40 minutes, obtain the mixed material of antierythrite, soybean polyoses and isomalt, granularity is between 80 ~ 130 orders;
(2) 14 kilograms of 8.33 kilograms of Sucraloses, remaining isomalt are mixed with deionized water, the intensification stirring and dissolving obtains the mixed aqueous solution of Sucralose and isomalt;
(3) mixed material of step (1) gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece is distributed to the continuous spraying of the prepared mixed aqueous solution of step (2) on the interior sugar alcohol granule of fluid bed, the EAT of control fluid bed is between 50 ~ 80 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the EAT of fluid bed between 80 ~ 110 ℃, carry out heated-air drying, last discharging obtains Fluffy powder grain compound sweetener.
The composite sweetener that adopts technical solution of the present invention to obtain, its main performance index sees Table 1.
Table 1
Figure 900745DEST_PATH_IMAGE002
Front sweet slow, the rear sweet heavy problem of Sucralose composite sweetener can effectively be covered and alleviate to composite sweetener of the present invention, when in the functional beverage that is applied to dietary fiber drink etc. and has denseer thick mouthfeel, can coordinate mutually with the beverage taste, when substituting traditional white granulated sugar, beverage be thinned out or affect original mouthfeel of beverage.
The present invention drops into the auxiliary sweetening material of the part of composite sweetener in the Multidimensionblender first and carries out tentatively mixing, then main sweetening material and remaining auxiliary sweetening material are dissolved into mixed aqueous solution, and disperse dry by the disposable spraying of advanced negative-pressure fluidized bed apparatus, make it to be coated on just mixed mixed material surface, obtain the Fluffy powder grain compound sweetener product.The present invention compares with the method for prior art simple blend, and the product instant capacity that obtains, sugariness dispersiveness etc. have significantly lifting, have good quality; And with prior art in batches spray-dired method compare, can greatly shorten the process-cycle again, the amount of saving energy, reduced production cost (about 60 ~ 90 minutes of product manufacturing cycle of the present invention, and about 2 ~ 3 hours of the manufacturing cycle of spray drying process in batches, and the present invention just the mixed power consumption that uses Multidimensionblender be approximately fluidized bed with spraying electricity consumption of equipment amount 1/24).
The sugariness degree of modification of composite sweetener of the present invention can be adjusted by the consumption of Sucralose according to actual needs, and the present invention is fit to the composite sweetener of 20~50 times of sucrose sweetness of preparation usually.
What need to understand is: the above only is preferred embodiment of the present invention; for those skilled in the art; under the prerequisite that does not break away from the principle of the invention, can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.

Claims (5)

1. one kind is adapted at the composite sweetener that uses in the dietary fiber drink, it is characterized in that comprising following percentage by weight composition: Sucralose 3.33~8.33%, antierythrite 5~15%, isomalt 25~30%, soluble dietary fiber 46.67~66.67%; Its preparation method comprises following processing step:
1. just antierythrite, soluble dietary fiber and the isomalt that accounts for total amount 40 ~ 60% drop in the Multidimensionblender, progression with 600 ~ 1000rpm mixed 20 ~ 50 minutes, the granularity of control mixed material obtains the mixed material of antierythrite, soluble dietary fiber and isomalt at 80 ~ 130 orders;
2. the isomalt with Sucralose and surplus is dissolved in the deionized water, obtains the mixed aqueous solution of Sucralose and isomalt;
3. with step 1. the mixed material of gained put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with step 2. prepared mixed aqueous solution continuously spraying be distributed on the sugar alcohol granule in the fluid bed, by heated-air drying, obtain described composite sweetener again.
2. a kind of composite sweetener of using in the dietary fiber drink of being adapted at according to claim 1, it is characterized in that: described soluble dietary fiber is konjaku flour or soybean polyoses.
3. a kind of preparation method who is adapted at the composite sweetener that uses in the dietary fiber drink claimed in claim 1 is characterized in that comprising following processing step:
1. just antierythrite, soluble dietary fiber and the isomalt that accounts for total amount 40 ~ 60% drop in the Multidimensionblender, progression with 600 ~ 1000rpm mixed 20 ~ 50 minutes, the granularity of control mixed material obtains the mixed material of antierythrite, soluble dietary fiber and isomalt at 80 ~ 130 orders;
2. the isomalt with Sucralose and surplus is dissolved in the deionized water, obtains the mixed aqueous solution of Sucralose and isomalt;
3. with step 1. the mixed material of gained put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with step 2. prepared mixed aqueous solution continuously spraying be distributed on the sugar alcohol granule in the fluid bed, by heated-air drying, obtain described composite sweetener again.
4. a kind of preparation method who is adapted at the composite sweetener that uses in the dietary fiber drink according to claim 3 is characterized in that: step 3. in, the EAT of fluid bed is controlled at 50 ~ 110 ℃.
5. a kind of preparation method who is adapted at the composite sweetener that uses in the dietary fiber drink according to claim 4, it is characterized in that: step 3. in, when the mixed aqueous solution spraying disperses, the EAT of control fluid bed is between 50 ~ 80 ℃, and the EAT of control fluid bed is at 80 ~ 110 ℃ during heated-air drying.
CN2012105007050A 2012-11-30 2012-11-30 Compound sweetener suitable for dietary fiber beverage and preparation method thereof Pending CN102960821A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108077589A (en) * 2017-12-18 2018-05-29 广州美瑞泰科生物工程技术有限公司 A kind of feed composite sweetener and preparation method thereof

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CN1969674A (en) * 2006-11-30 2007-05-30 吴江中怡实业有限公司 Food additive
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CN102499285A (en) * 2011-12-30 2012-06-20 内蒙古伊利实业集团股份有限公司 High-fiber sugar-free brown active lactic acid bacterial beverage and preparation method thereof
CN102669781A (en) * 2012-05-03 2012-09-19 重庆市彭水县天娇农业开发有限公司 Low-calorie nutrient konjac diet drink

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1969674A (en) * 2006-11-30 2007-05-30 吴江中怡实业有限公司 Food additive
CN102423062A (en) * 2011-12-15 2012-04-25 苏州工业园区尚融科技有限公司 Fluffy granular composite sugar-free sweetening material and preparation method thereof
CN102499285A (en) * 2011-12-30 2012-06-20 内蒙古伊利实业集团股份有限公司 High-fiber sugar-free brown active lactic acid bacterial beverage and preparation method thereof
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
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Application publication date: 20130313