CN102934788A - Low-sugar low-calorie compound sweetening agent applicable to tea beverage or coffee and preparation method thereof - Google Patents
Low-sugar low-calorie compound sweetening agent applicable to tea beverage or coffee and preparation method thereof Download PDFInfo
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Abstract
The invention relates to low-sugar low-calorie compound sweetening agent applicable to a tea beverage or coffee and a preparation method thereof. The sweetening agent comprises the following components: 33.33%-66.67% of stevioside RA97, 15-42% of erythritol, 17-50% of isomaltitol, 0.01-0.35% of citric acid, 0.05-0.2% of sodium citrate, and 0.05-0.44% of lactic acid. The process comprises the following steps: putting the stevioside RA97, the erythritol, and the isomaltitol accounting for 40-60% of the total amount into a multi-dimensional mixing machine for primary mixing; dissolving the citric acid, the sodium citrate, the lactic acid and the rest isomaltitol into deionized water to obtain a mixed water solution; enabling mixed materials to enter a spray fluidized bed from the bottom of the fluidized bed at positive pressure and flowing from bottom to top at an accelerating speed, and the mixed materials boiling up and down in the fluidized bed to form fine sugar alcohol particles; and continuously spraying and dispersing the mixed water solution onto the fine sugar alcohol particles in the fluidized bed to obtain the compound sweetening agent.
Description
Technical field
The present invention relates to a kind of food additives, be specifically related to a kind of low-sugar-content and low-calorie composite sweetener of using in tea beverage or the coffee and preparation method thereof that is adapted at.
Background technology
In the last few years, raising along with expanding economy and people's lives wealth, obesity, hypertension, diabetes, carious tooth etc. become the height morbidity among the crowd, and the generation of these high morbidities is considered to especially with the sucrose Excessive Intake substantial connection is arranged with eating habit and diet structure.Therefore, as the sweetener of food additives, one of its development priority is exactly safe, without nutritive value, empty calory or functional high sweetener extremely low in calories.The characteristics of functional high sweetener are use safe, and consumption is few, and sugariness is high, and use cost is generally all far below sucrose, and this also is the power place that Food Science man continually develops novel high-intensity sweetener.At present, approximately 20 kinds of the granted high sweeteners in countries in the world obtain that kind that the majority state approval allows to use mainly contains that saccharin sodium, honey element, 3,4-Dihydro-6-methyl-1,2,3-oxathiazin-4-one 2,2-dioxide potassium salt, Aspartame, Sucralose, alitame, knob are sweet, glycyrrhizin, stevioside, Momordica grosvenori is sweet and Talin etc.These high sweeteners have plenty of artificial synthetic, and are sweet etc. such as Aspartame, Sucralose, knob; What have then is natural extract, sweet etc. such as sky chrysanthemum glycosides and arhat.No matter be artificial synthesis edulcorant or natural extraction sweetener, at sugariness, sweet taste, stable aspects its pluses and minuses arranged respectively all, therefore, want to give full play to the optimal efficacy of these sweeteners, reduce cost, the most frequently used means are exactly compound at present.By carrying out various sweeteners or sweet substance compound, bring into play may exist between the various sweeteners synergistic function, to as far as possible approaching or satisfy the requirement of desirable sweetener: safety non-toxic, sweet taste is pure similar to sucrose (this is to be popular generally accepted sweet tastes), high sugariness, low heat value or without calorific value, stable high, unlikely dental caries, reduction cost.
In the prior art, mostly the generation sugar that uses in tea beverage or the coffee is take Sucralose as main sweet composite sweetener, this class composite sweetener also has different with sucrose on mouthfeel, there is front sweet slow, rear sweet and pleasant impression problem heavily, in the time of in being applied to tea beverage or coffee, also can so that the hardship sense in the drink give prominence to, be difficult to cover, thereby so that these drinks can not be accepted by the public and like.
The preparation method of composite sweetener in the prior art, can be by method or the spray-dired method converted products of substep of simple blend, the composite sweetener that the simple blend method makes is with low cost, but be difficult to guarantee that main sweetening material can be uniformly dispersed, and this point can affect the quality of composite sweetener product to a great extent.The spray-dired method of substep is that substep is dissolved in main sweetening material and each auxiliary sweetening material in the deionized water in batches, then the method by the wet spray drying is coated on each composition material on the granular sweetener by spraying respectively, the composite sweetener product sweetness that this method makes is uniformly dispersed, instant capacity is good, quality is better than the composite sweetener product that additive method makes, but its shortcoming is: material loss is large, the loss of especially main sweetening material is larger, machinery equipment power consumption is too high, the cost of product is significantly increased, and therefore this method also has been subject to certain restriction in implementation process.
Summary of the invention
The objective of the invention is to overcome the deficiency that prior art exists, provide a kind of with low cost, sugariness is uniformly dispersed and be highly suitable for tea beverage or coffee in the low-sugar-content and low-calorie composite sweetener that uses and preparation method thereof.
Purpose of the present invention is achieved through the following technical solutions:
A kind of low-sugar-content and low-calorie composite sweetener of using in tea beverage or the coffee of being adapted at comprises following percentage by weight composition: stevia sugar RA 97 33.33%～66.67%, antierythrite 15～42%, isomalt 17～50%, citric acid 0.01～0.35%, natrium citricum 0.05～0.2%, lactic acid 0.05～0.44%; Its preparation method comprises following processing step:
1. stevia sugar RA 97, antierythrite and the isomalt that accounts for total amount 40 ~ 60% are dropped in the Multidimensionblender, progression with 600 ~ 1000rpm mixed 25 ~ 40 minutes, the granularity of control mixed material obtains the mixed material of stevia sugar RA 97, antierythrite and isomalt at 80 ~ 130 orders;
2. the isomalt with citric acid, natrium citricum, lactic acid and surplus is dissolved in the deionized water, obtains mixed aqueous solution;
3. with step 1. the mixed material of gained put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with step 2. prepared mixed aqueous solution continuously spraying be distributed on the sugar alcohol granule in the fluid bed, by heated-air drying, obtain described composite sweetener again.
The present invention is a kind of to be adapted at the preparation method of the low-sugar-content and low-calorie composite sweetener that uses in tea beverage or the coffee, comprises following processing step:
1. stevia sugar RA 97, antierythrite and the isomalt that accounts for total amount 40 ~ 60% are dropped in the Multidimensionblender, progression with 600 ~ 1000rpm mixed 25 ~ 40 minutes, the granularity of control mixed material obtains the mixed material of stevia sugar RA 97, antierythrite and isomalt at 80 ~ 130 orders;
2. the isomalt with citric acid, natrium citricum, lactic acid and surplus is dissolved in the deionized water, obtains mixed aqueous solution;
3. with step 1. the mixed material of gained put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with step 2. prepared mixed aqueous solution continuously spraying be distributed on the sugar alcohol granule in the fluid bed, by heated-air drying, obtain described composite sweetener again.
Further, above-mentioned a kind of preparation method who is adapted at the low-sugar-content and low-calorie composite sweetener that uses in tea beverage or the coffee, step 3. in, the EAT of fluid bed is controlled at 45 ~ 95 ℃.
Again further, above-mentioned a kind of preparation method who is adapted at the low-sugar-content and low-calorie composite sweetener that uses in tea beverage or the coffee, step 3. in, when the mixed aqueous solution spraying disperses, the EAT of control fluid bed is at 45 ~ 80 ℃, and the EAT of control fluid bed is at 80 ~ 95 ℃ during heated-air drying.
The substantive distinguishing features that technical solution of the present invention is outstanding and significant progressive being mainly reflected in:
The present invention adopts stevia sugar RA 97 as main sweet, be aided with antierythrite, isomalt etc. auxiliary sweet carry out composite, and add citric acid and lactic acid etc. composite sweetener is carried out seasoning, the final stevioside type low-sugar-content and low-calorie composite sweetener that obtains, be fit to very much be applied in the beverages such as coffee or tea, it can substitute the sweet taste that white granulated sugar provides popular institute to like and accept for drink.
The present invention will carry out tentatively mixing in composite sweetener master sweetening material and the auxiliary sweetening material input of the part Multidimensionblender first, then remaining auxiliary sweetening material is dissolved into the aqueous solution, and disperse dry by the disposable wet spray of advanced negative-pressure fluidized bed apparatus, make it to be coated on just mixed mixed material surface, obtain the Fluffy powder grain compound sweetener product.The present invention compares with the method for prior art simple blend, and the product instant capacity that obtains, sugariness dispersiveness etc. have significantly lifting, have good quality; And with prior art in batches spray-dired method compare, can greatly shorten the process-cycle again, reduce the loss of the especially main sweetening material of raw material, the amount of saving energy has reduced production cost.
The specific embodiment
Composite sweetener of the present invention, its composition is: stevia sugar RA 97 33.33%～66.67%, antierythrite 15～42%, isomalt 17～50%, citric acid 0.01～0.35%, natrium citricum 0.05～0.2%, lactic acid 0.05～0.44%; Ideal formulations is: stevia sugar RA 97 53.33%, antierythrite 25%, isomalt 21.02%, citric acid 0.25%, natrium citricum 0.1%, lactic acid 0.3%.
The preparation technology of this composite sweetener: first stevia sugar RA 97, antierythrite and the isomalt that accounts for total amount 40 ~ 60% are dropped in the Multidimensionblender, progression with 600 ~ 1000rpm mixed 25 ~ 40 minutes, the granularity of control mixed material obtains the mixed material of stevia sugar RA 97, antierythrite and isomalt at 80 ~ 130 orders; Isomalt with citric acid, natrium citricum, lactic acid and surplus is dissolved in the deionized water again, obtains mixed aqueous solution; The mixed material of gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, the EAT of fluid bed is controlled at 45 ~ 95 ℃, forms tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with prepared mixed aqueous solution continuously spraying be distributed on the sugar alcohol granule in the fluid bed, when the mixed aqueous solution spraying disperses, the EAT of control fluid bed is at 45 ~ 80 ℃, pass through again heated-air drying, the EAT of control fluid bed obtains described composite sweetener at 80 ~ 95 ℃ during heated-air drying.
Multidimensionblender used in the present invention adopts commercial 200 feather weight Multidimensionblenders, rotating speed level journey is 200 ~ 1800rpm, barrel is two taper, middle column, and during work, this Multidimensionblender can make the material in the barrel collide, pulverize and mix from a plurality of angles.
Embodiment 1:
(1) getting 33.33 kilograms of stevia sugar RAs 97,18 kilograms of antierythrites, 28 kilograms of isomalts drops in the Multidimensionblender, the progression of control Multidimensionblender is 800rpm, mixed 35 minutes, obtain the mixed material of stevia sugar RA 97, antierythrite and isomalt, granularity is between 80 ~ 130 orders;
(2) 20.42 kilograms of 0.1 kilogram of citric acids, 0.05 kilogram of natrium citricum, 0.1 kilogram of lactic acid, remaining isomalt are mixed with deionized water, the intensification stirring and dissolving obtains mixed aqueous solution;
(3) mixed material of step (1) gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece is distributed to the continuous spraying of the prepared mixed aqueous solution of step (2) on the interior sugar alcohol granule of fluid bed, the EAT of control fluid bed is between 45 ~ 80 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the EAT of fluid bed between 80 ~ 95 ℃, carry out heated-air drying, last discharging obtains Fluffy powder grain compound sweetener.
Embodiment 2:
(1) getting 43.33 kilograms of stevia sugar RAs 97,20 kilograms of antierythrites, 18.8 kilograms of isomalts drops in the Multidimensionblender, the progression of control Multidimensionblender is 800rpm, mixed 35 minutes, obtain the mixed material of stevia sugar RA 97, antierythrite and isomalt, granularity is between 80 ~ 130 orders;
(2) 17.37 kilograms of 0.2 kilogram of citric acids, 0.1 kilogram of natrium citricum, 0.2 kilogram of lactic acid, remaining isomalt are mixed with deionized water, the intensification stirring and dissolving obtains mixed aqueous solution;
(3) mixed material of step (1) gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece is distributed to the continuous spraying of the prepared mixed aqueous solution of step (2) on the interior sugar alcohol granule of fluid bed, the EAT of control fluid bed is between 45 ~ 80 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the EAT of fluid bed between 80 ~ 95 ℃, carry out heated-air drying, last discharging obtains Fluffy powder grain compound sweetener.
Embodiment 3:
(1) getting 53.33 kilograms of stevia sugar RAs 97,25 kilograms of antierythrites, 8.82 kilograms of isomalts drops in the Multidimensionblender, the progression of control Multidimensionblender is 1000rpm, mixed 35 minutes, obtain the mixed material of stevia sugar RA 97, antierythrite and isomalt, granularity is between 80 ~ 130 orders;
(2) 12.2 kilograms of 0.25 kilogram of citric acids, 0.1 kilogram of natrium citricum, 0.3 kilogram of lactic acid, remaining isomalt are mixed with deionized water, the intensification stirring and dissolving obtains mixed aqueous solution;
(3) mixed material of step (1) gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece is distributed to the continuous spraying of the prepared mixed aqueous solution of step (2) on the interior sugar alcohol granule of fluid bed, the EAT of control fluid bed is between 45 ~ 80 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the EAT of fluid bed between 80 ~ 95 ℃, carry out heated-air drying, last discharging obtains Fluffy powder grain compound sweetener.
Embodiment 4:
(1) getting 66.67 kilograms of stevia sugar RAs 97,15 kilograms of antierythrites, 7.1 kilograms of isomalts drops in the Multidimensionblender, the progression of control Multidimensionblender is 1000rpm, mixed 40 minutes, obtain the mixed material of stevia sugar RA 97, antierythrite and isomalt, granularity is between 80 ~ 130 orders;
(2) 10.33 kilograms of 0.3 kilogram of citric acids, 0.2 kilogram of natrium citricum, 0.4 kilogram of lactic acid, remaining isomalt are mixed with deionized water, the intensification stirring and dissolving obtains mixed aqueous solution;
(3) mixed material of step (1) gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece is distributed to the continuous spraying of the prepared mixed aqueous solution of step (2) on the interior sugar alcohol granule of fluid bed, the EAT of control fluid bed is between 45 ~ 80 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the EAT of fluid bed between 80 ~ 95 ℃, carry out heated-air drying, last discharging obtains Fluffy powder grain compound sweetener.
The composite sweetener that adopts technical solution of the present invention to obtain, its main performance index sees Table 1.
Table 1
The present invention adopts stevia sugar RA 97 as main sweet, be aided with antierythrite, isomalt etc. auxiliary sweet carry out composite, and add citric acid and lactic acid etc. composite sweetener is carried out seasoning, the final stevioside type low-sugar-content and low-calorie composite sweetener that obtains, be fit to very much be applied in the beverages such as coffee or tea, it can substitute the sweet taste that white granulated sugar provides popular institute to like and accept for drink.
The present invention will carry out tentatively mixing in composite sweetener master sweetening material and the auxiliary sweetening material input of the part Multidimensionblender first, then remaining auxiliary sweetening material is dissolved into the aqueous solution, and disperse dry by the disposable wet spray of advanced negative-pressure fluidized bed apparatus, make it to be coated on just mixed mixed material surface, obtain the Fluffy powder grain compound sweetener product.The present invention compares with the method for prior art simple blend, and the product instant capacity that obtains, sugariness dispersiveness etc. have significantly lifting, have good quality; And with prior art in batches spray-dired method compare, can greatly shorten the process-cycle again, reduce the loss of the especially main sweetening material of raw material, the amount of saving energy, reduced production cost (product manufacturing cycle of the present invention approximately 60 ~ 80 minutes, and the manufacturing cycle of spray drying process approximately 2 ~ 3 hours in batches, and the present invention just the mixed power consumption that uses Multidimensionblender approximately be fluidized bed with spraying electricity consumption of equipment amount 1/24).
The sugariness degree of modification of composite sweetener of the present invention can be adjusted by the consumption of stevia sugar RA 97 according to actual needs, and the present invention is fit to the composite sweetener of 50～100 times of sucrose sweetness of preparation usually.
What need to understand is: the above only is preferred embodiment of the present invention; for those skilled in the art; under the prerequisite that does not break away from the principle of the invention, can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (4)
1. be adapted at the low-sugar-content and low-calorie composite sweetener that uses in tea beverage or the coffee, it is characterized in that comprising following percentage by weight composition: stevia sugar RA 97 33.33%～66.67%, antierythrite 15～42%, isomalt 17～50%, citric acid 0.01～0.35%, natrium citricum 0.05～0.2%, lactic acid 0.05～0.44%; Its preparation method comprises following processing step:
1. stevia sugar RA 97, antierythrite and the isomalt that accounts for total amount 40 ~ 60% are dropped in the Multidimensionblender, progression with 600 ~ 1000rpm mixed 25 ~ 40 minutes, the granularity of control mixed material obtains the mixed material of stevia sugar RA 97, antierythrite and isomalt at 80 ~ 130 orders;
2. the isomalt with citric acid, natrium citricum, lactic acid and surplus is dissolved in the deionized water, obtains mixed aqueous solution;
3. with step 1. the mixed material of gained put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with step 2. prepared mixed aqueous solution continuously spraying be distributed on the sugar alcohol granule in the fluid bed, by heated-air drying, obtain described composite sweetener again.
2. the preparation method who is adapted at the low-sugar-content and low-calorie composite sweetener that uses in tea beverage or the coffee claimed in claim 1 is characterized in that comprising following processing step:
1. stevia sugar RA 97, antierythrite and the isomalt that accounts for total amount 40 ~ 60% are dropped in the Multidimensionblender, progression with 600 ~ 1000rpm mixed 25 ~ 40 minutes, the granularity of control mixed material obtains the mixed material of stevia sugar RA 97, antierythrite and isomalt at 80 ~ 130 orders;
2. the isomalt with citric acid, natrium citricum, lactic acid and surplus is dissolved in the deionized water, obtains mixed aqueous solution;
3. with step 1. the mixed material of gained put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with step 2. prepared mixed aqueous solution continuously spraying be distributed on the sugar alcohol granule in the fluid bed, by heated-air drying, obtain described composite sweetener again.
3. the preparation method who is adapted at the low-sugar-content and low-calorie composite sweetener that uses in tea beverage or the coffee according to claim 2 is characterized in that: step 3. in, the EAT of fluid bed is controlled at 45 ~ 95 ℃.
4. the preparation method who is adapted at the low-sugar-content and low-calorie composite sweetener that uses in tea beverage or the coffee according to claim 3, it is characterized in that: step 3. in, when the mixed aqueous solution spraying disperses, the EAT of control fluid bed is at 45 ~ 80 ℃, and the EAT of control fluid bed is at 80 ~ 95 ℃ during heated-air drying.
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Application publication date: 20130220 |