CN102960822A - Compound sweetening agent suitable to be used in sour maize juice and preparation method thereof - Google Patents
Compound sweetening agent suitable to be used in sour maize juice and preparation method thereof Download PDFInfo
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Abstract
The invention relates to a suitable to be used in sour maize juice and a preparation method thereof. The compound sweetening agent comprises the following components: 1.5%-3.125% of neotame, 5-9.0% of sodium 2-(4-methoxyphenoxy) propionate, 2-7.6% of beta-cyclodextrin, 5-14.5% of table salt, 16-41% of erythritol, and 25-50% of maltodextrin. The process comprises the following steps: putting the neotame, the erythritol and the maltodextrin accounting for 50-70% of the total amount into a multi-dimensional mixing machine for primary mixing; dissolving the sodium 2-(4-methoxyphenoxy) propionate, the beta-cyclodextrin, the table salt and the rest maltodextrin in deionized water to obtain a mixed water solution; causing the mixed materials to enter a spray fluidized bed and flow from bottom to top at an accelerating speed, so that the mixed materials boil up and down in the fluidized bed to form fine sugar alcohol particles; and continuously spraying and dispersing the mixed water solution onto the fine sugar alcohol particles in the fluidized bed to obtain the compound sweetening agent. By adopting the compound sweetening agent, the product instant solubility and sweetness dispersibility are greatly improved.
Description
Technical field
The present invention relates to a kind of food additives, be specifically related to a kind of composite sweetener of using in the sour corn juice and preparation method thereof that is adapted at.
Background technology
In the last few years, raising along with expanding economy and people's lives wealth, obesity, hypertension, diabetes, carious tooth etc. become the height morbidity among the crowd, and the generation of these high morbidities is considered to especially with the sucrose Excessive Intake substantial connection is arranged with eating habit and diet structure.Therefore, as the sweetener of food additives, one of its development priority is exactly safe, without nutritive value, empty calory or functional high sweetener extremely low in calories.The characteristics of functional high sweetener are use safe, and consumption is few, and sugariness is high, and use cost is generally all far below sucrose, and this also is the power place that Food Science man continually develops novel high-intensity sweetener.At present, about 20 kinds of the granted high sweetener in countries in the world obtains that kind that the majority state approval allows to use mainly contains that saccharin sodium, honey element, 3,4-Dihydro-6-methyl-1,2,3-oxathiazin-4-one 2,2-dioxide potassium salt, Aspartame, Sucralose, alitame, knob are sweet, glycyrrhizin, stevioside, Momordica grosvenori is sweet and Talin etc.These high sweeteners have plenty of artificial synthetic, and are sweet etc. such as Aspartame, Sucralose, knob; What have then is natural extract, sweet etc. such as sky chrysanthemum glycosides and arhat.No matter be artificial synthesis edulcorant or natural extraction sweetener, at sugariness, sweet taste, stable aspects its pluses and minuses arranged respectively all, therefore, want to give full play to the optimal efficacy of these sweeteners, reduce cost, the most frequently used means are exactly compound at present.By carrying out various sweeteners or sweet substance compound, bring into play may exist between the various sweeteners synergistic function, in the hope of as far as possible approaching or satisfy the requirement of desirable sweetener: safety non-toxic, sweet taste is pure similar to sucrose (this is to be popular generally accepted sweet tastes), high sugariness, low heat value or without calorific value, stable height, unlikely dental caries, reduction cost.
Being applied in the prior art has Sucralose type composite sweetener for sugar in the sour corn juice, or the sweet type composite sweetener of knob.Compare, the sweet unit of knob sugariness cost is lower, but when being applied in the acidic beverages such as sour corn juice take the sweet composite sweetener as main sweetener of knob, sweet heavy, problem that pleasant impression is difficult to cover after also existing, be trapped in and cause easily sweet soapy feeling in the oral cavity, therefore meeting is not liked by masses so that the mouthfeel of drink is bad and is accepted.
The preparation method of composite sweetener in the prior art, can be by method or the spray-dired method converted products of substep of simple blend, the composite sweetener that the simple blend method makes is with low cost, but be difficult to guarantee that main sweetening material can be uniformly dispersed, and this point can affect the quality of composite sweetener product to a great extent.The spray-dired method of substep is that substep is dissolved in main sweetening material and each auxiliary sweetening material in the deionized water in batches, then the method by the wet spray drying is coated on each composition material on the granular sweetener by spraying respectively, the composite sweetener product sweetness that this method makes is uniformly dispersed, instant capacity is good, quality is better than the composite sweetener product that additive method makes, but its shortcoming is: material loss is large, the loss of especially main sweetening material is larger, machinery equipment power consumption is too high, the cost of product is significantly increased, and therefore this method also has been subject to certain restriction in implementation process.
Summary of the invention
The objective of the invention is to overcome the deficiency that prior art exists, provide a kind of with low cost, sugariness is uniformly dispersed, mouthfeel better is adapted at composite sweetener that uses in the sour corn juice and preparation method thereof.
Purpose of the present invention is achieved through the following technical solutions:
A kind of composite sweetener of using in the sour corn juice of being adapted at comprises following percentage by weight composition: knob is sweet 1.5%～3.125%, 2-(4-methoxyphenoxy)-sodium propionate 5～9.0%, beta-schardinger dextrin-2～7.6%, salt 5～14.5%, antierythrite 16～41%, maltodextrin 25～50%; Its preparation method comprises following processing step:
1. knob is sweet, antierythrite and the maltodextrin that accounts for total amount 50 ~ 70% drop in the Multidimensionblender, progression with 600 ~ 1000rpm mixed 20 ~ 40 minutes, the granularity of control mixed material is at 80 ~ 130 orders, obtains that knob is sweet, the mixed material of antierythrite and maltodextrin;
2. the maltodextrin with 2-(4-methoxyphenoxy)-sodium propionate, beta-schardinger dextrin-, salt and surplus is dissolved in the deionized water, obtains mixed aqueous solution;
3. with step 1. the mixed material of gained put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with step 2. prepared mixed aqueous solution continuously spraying be distributed on the sugar alcohol granule in the fluid bed, by heated-air drying, obtain described composite sweetener again.
The present invention is a kind of to be adapted at the preparation method of the composite sweetener that uses in the sour corn juice, comprises following processing step:
1. knob is sweet, antierythrite and the maltodextrin that accounts for total amount 50 ~ 70% drop in the Multidimensionblender, progression with 600 ~ 1000rpm mixed 20 ~ 40 minutes, the granularity of control mixed material is at 80 ~ 130 orders, obtains that knob is sweet, the mixed material of antierythrite and maltodextrin;
2. the maltodextrin with 2-(4-methoxyphenoxy)-sodium propionate, beta-schardinger dextrin-, salt and surplus is dissolved in the deionized water, obtains mixed aqueous solution;
3. with step 1. the mixed material of gained put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with step 2. prepared mixed aqueous solution continuously spraying be distributed on the sugar alcohol granule in the fluid bed, by heated-air drying, obtain described composite sweetener again.
Further, above-mentioned a kind of preparation method who is adapted at the composite sweetener that uses in the sour corn juice, step 3. in, the EAT of fluid bed is controlled at 40 ~ 100 ℃.
Further, above-mentioned a kind of preparation method who is adapted at the composite sweetener that uses in the sour corn juice, step 3. in, when the mixed aqueous solution spraying disperses, the EAT of control fluid bed is at 40 ~ 80 ℃, and the EAT of control fluid bed is at 70 ~ 100 ℃ during heated-air drying
The substantive distinguishing features that technical solution of the present invention is outstanding and significant progressive being mainly reflected in:
The present invention selects knob sweet in main sweetener, be aided with the mutually collaborative seasoning such as antierythrite, a small amount of 2-(4-methoxyphenoxy)-sodium propionate and salt, repeatedly optimization through prescription, so that each composition material matching is reasonable, pro rate is at optimum range, when composite sweetener of the present invention is applied in the sour corn juice, can effectively cover the sweet sweet greasy aftertaste of knob, make the drink mouthfeel better, meet popular taste demand.
The present invention will carry out tentatively mixing in composite sweetener master sweetening material and the auxiliary sweetening material input of the part Multidimensionblender first, then remaining auxiliary sweetening material is dissolved into the aqueous solution, and disperse dry by the disposable wet spray of advanced negative-pressure fluidized bed apparatus, make it to be coated on just mixed mixed material surface, obtain the Fluffy powder grain compound sweetener product.The present invention compares with the method for prior art simple blend, and the product instant capacity that obtains, sugariness dispersiveness etc. have significantly lifting, have good quality; And with prior art in batches spray-dired method compare, can greatly shorten the process-cycle again, reduce the loss of the especially main sweetening material of raw material, the amount of saving energy has reduced production cost.
The specific embodiment
Composite sweetener of the present invention, its composition is: knob is sweet 1.5%～3.125%, 2-(4-methoxyphenoxy)-sodium propionate 5～9.0%, beta-schardinger dextrin-2～7.6%, salt 5～14.5%, antierythrite 16～41%, maltodextrin 25～50%; Ideal formulations is: knob is sweet 2.25%, 2-(4-methoxyphenoxy)-sodium propionate 7.3%, beta-schardinger dextrin-5%, salt 9%, antierythrite 35%, maltodextrin 41.45%.
The preparation technology of composite sweetener: knob is sweet, antierythrite and the maltodextrin that accounts for total amount 50 ~ 70% drop in the Multidimensionblender first, progression with 600 ~ 1000rpm mixed 20 ~ 40 minutes, the granularity of control mixed material is at 80 ~ 130 orders, obtains that knob is sweet, the mixed material of antierythrite and maltodextrin; Maltodextrin with 2-(4-methoxyphenoxy)-sodium propionate, beta-schardinger dextrin-, salt and surplus is dissolved in the deionized water again, obtains mixed aqueous solution; The mixed material of gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, the EAT of fluid bed is controlled at 40 ~ 100 ℃, forms tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with prepared mixed aqueous solution continuously spraying be distributed on the sugar alcohol granule in the fluid bed, when the mixed aqueous solution spraying disperses, the EAT of control fluid bed is at 40 ~ 80 ℃, pass through again heated-air drying, the EAT of control fluid bed obtains described composite sweetener at 70 ~ 100 ℃ during heated-air drying.
Multidimensionblender used in the present invention adopts commercial 200 feather weight Multidimensionblenders, rotating speed level journey is 200 ~ 1800rpm, barrel is two taper, middle column, and during work, this Multidimensionblender can make the material in the barrel collide, pulverize and mix from a plurality of angles.
Embodiment 1:
(1) gets in sweet 1.5 kilograms of knob, 35 kilograms of antierythrites and 29.4 kilograms of inputs of the maltodextrin Multidimensionblender, the progression of control Multidimensionblender is 800rpm, mixed 30 minutes, and obtained that knob was sweet, the mixed material of antierythrite and maltodextrin, granularity is between 80 ~ 130 orders;
(2) 19.6 kilograms of 2-(4-methoxyphenoxy)-5 kilograms of sodium propionates, 3 kilograms of beta-schardinger dextrin-s, 6.5 kilograms of salt, remaining maltodextrin are mixed with deionized water, the intensification stirring and dissolving obtains mixed aqueous solution;
(3) mixed material of step (1) gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece is distributed to the continuous spraying of the prepared mixed aqueous solution of step (2) on the interior sugar alcohol granule of fluid bed, the EAT of control fluid bed is between 40 ~ 80 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the EAT of fluid bed between 70 ~ 100 ℃, carry out heated-air drying, last discharging obtains Fluffy powder grain compound sweetener.
Embodiment 2:
(1) gets in sweet 1.875 kilograms of knob, 36 kilograms of antierythrites and 26.775 kilograms of inputs of the maltodextrin Multidimensionblender, the progression of control Multidimensionblender is 800rpm, mixed 30 minutes, and obtained that knob was sweet, the mixed material of antierythrite and maltodextrin, granularity is between 80 ~ 130 orders;
(2) 17.85 kilograms of 2-(4-methoxyphenoxy)-6 kilograms of sodium propionates, 4 kilograms of beta-schardinger dextrin-s, 7.5 kilograms of salt, remaining maltodextrin are mixed with deionized water, the intensification stirring and dissolving obtains mixed aqueous solution;
(3) mixed material of step (1) gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece is distributed to the continuous spraying of the prepared mixed aqueous solution of step (2) on the interior sugar alcohol granule of fluid bed, the EAT of control fluid bed is between 40 ~ 80 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the EAT of fluid bed between 70 ~ 100 ℃, carry out heated-air drying, last discharging obtains Fluffy powder grain compound sweetener.
Embodiment 3:
(1) gets in sweet 2.25 kilograms of knob, 35 kilograms of antierythrites and 24.45 kilograms of inputs of the maltodextrin Multidimensionblender, the progression of control Multidimensionblender is 800rpm, mixed 30 minutes, and obtained that knob was sweet, the mixed material of antierythrite and maltodextrin, granularity is between 80 ~ 130 orders;
(2) 17 kilograms of 2-(4-methoxyphenoxy)-7.3 kilograms of sodium propionates, 5 kilograms of beta-schardinger dextrin-s, 9 kilograms of salt, remaining maltodextrin are mixed with deionized water, the intensification stirring and dissolving obtains mixed aqueous solution;
(3) mixed material of step (1) gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece is distributed to the continuous spraying of the prepared mixed aqueous solution of step (2) on the interior sugar alcohol granule of fluid bed, the EAT of control fluid bed is between 40 ~ 80 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the EAT of fluid bed between 70 ~ 100 ℃, carry out heated-air drying, last discharging obtains Fluffy powder grain compound sweetener.
Embodiment 4:
(1) gets in sweet 2.75 kilograms of knob, 36 kilograms of antierythrites and 22.45 kilograms of inputs of the maltodextrin Multidimensionblender, the progression of control Multidimensionblender is 800rpm, mixed 30 minutes, and obtained that knob was sweet, the mixed material of antierythrite and maltodextrin, granularity is between 80 ~ 130 orders;
(2) 14.8 kilograms of 2-(4-methoxyphenoxy)-8 kilograms of sodium propionates, 6 kilograms of beta-schardinger dextrin-s, 10 kilograms of salt, remaining maltodextrin are mixed with deionized water, the intensification stirring and dissolving obtains mixed aqueous solution;
(3) mixed material of step (1) gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece is distributed to the continuous spraying of the prepared mixed aqueous solution of step (2) on the interior sugar alcohol granule of fluid bed, the EAT of control fluid bed is between 40 ~ 80 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the EAT of fluid bed between 70 ~ 100 ℃, carry out heated-air drying, last discharging obtains Fluffy powder grain compound sweetener.
Embodiment 5:
(1) gets in sweet 3.125 kilograms of knob, 34 kilograms of antierythrites and 21.075 kilograms of inputs of the maltodextrin Multidimensionblender, the progression of control Multidimensionblender is 800rpm, mixed 30 minutes, and obtained that knob was sweet, the mixed material of antierythrite and maltodextrin, granularity is between 80 ~ 130 orders;
(2) 14 kilograms of 2-(4-methoxyphenoxy)-9 kilograms of sodium propionates, 7.3 kilograms of beta-schardinger dextrin-s, 11.5 kilograms of salt, remaining maltodextrin are mixed with deionized water, the intensification stirring and dissolving obtains mixed aqueous solution;
(3) mixed material of step (1) gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece is distributed to the continuous spraying of the prepared mixed aqueous solution of step (2) on the interior sugar alcohol granule of fluid bed, the EAT of control fluid bed is between 40 ~ 80 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the EAT of fluid bed between 70 ~ 100 ℃, carry out heated-air drying, last discharging obtains Fluffy powder grain compound sweetener.
The composite sweetener that adopts technical solution of the present invention to obtain, its main performance index sees Table 1.
Table 1
The present invention selects knob sweet in main sweetener, be aided with the mutually collaborative seasonings such as antierythrite, salt and 2-(4-methoxyphenoxy)-sodium propionate, repeatedly optimization through prescription, so that each composition material matching is reasonable, pro rate is at optimum range, when composite sweetener of the present invention is applied in the sour corn juice, can effectively cover the sweet sweet greasy aftertaste of knob, make the drink mouthfeel better, meet popular taste demand.
The present invention will carry out tentatively mixing in composite sweetener master sweetening material and the auxiliary sweetening material input of the part Multidimensionblender first, then remaining auxiliary sweetening material is dissolved into the aqueous solution, and disperse dry by the disposable wet spray of advanced negative-pressure fluidized bed apparatus, make it to be coated on just mixed mixed material surface, obtain the Fluffy powder grain compound sweetener product.The present invention compares with the method for prior art simple blend, and the product instant capacity that obtains, sugariness dispersiveness etc. have significantly lifting, have good quality; And with prior art in batches spray-dired method compare, can greatly shorten the process-cycle again, reduce the loss of the especially main sweetening material of raw material, the amount of saving energy, reduced production cost (about 60 ~ 90 minutes of product manufacturing cycle of the present invention, and about 2 ~ 3 hours of the manufacturing cycle of spray drying process in batches, and the present invention just the mixed power consumption that uses Multidimensionblender be approximately fluidized bed with spraying electricity consumption of equipment amount 1/24).
The sugariness degree of modification of composite sweetener of the present invention can be adjusted by the sweet consumption of knob according to actual needs, and the present invention is fit to the composite sweetener of 120～250 times of sucrose sweetness of preparation usually.
What need to understand is: the above only is preferred embodiment of the present invention; for those skilled in the art; under the prerequisite that does not break away from the principle of the invention, can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (4)
1. be adapted at the composite sweetener that uses in the sour corn juice, it is characterized in that comprising following percentage by weight composition: knob is sweet 1.5%～3.125%, 2-(4-methoxyphenoxy)-sodium propionate 5～9.0%, beta-schardinger dextrin-2～7.6%, salt 5～14.5%, antierythrite 16～41%, maltodextrin 25～50%; Its preparation method comprises following processing step:
1. knob is sweet, antierythrite and the maltodextrin that accounts for total amount 50 ~ 70% drop in the Multidimensionblender, progression with 600 ~ 1000rpm mixed 20 ~ 40 minutes, the granularity of control mixed material is at 80 ~ 130 orders, obtains that knob is sweet, the mixed material of antierythrite and maltodextrin;
2. the maltodextrin with 2-(4-methoxyphenoxy)-sodium propionate, beta-schardinger dextrin-, salt and surplus is dissolved in the deionized water, obtains mixed aqueous solution;
3. with step 1. the mixed material of gained put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with step 2. prepared mixed aqueous solution continuously spraying be distributed on the sugar alcohol granule in the fluid bed, by heated-air drying, obtain described composite sweetener again.
2. the preparation method who is adapted at the composite sweetener that uses in the sour corn juice claimed in claim 1 is characterized in that comprising following processing step:
1. knob is sweet, antierythrite and the maltodextrin that accounts for total amount 50 ~ 70% drop in the Multidimensionblender, progression with 600 ~ 1000rpm mixed 20 ~ 40 minutes, the granularity of control mixed material is at 80 ~ 130 orders, obtains that knob is sweet, the mixed material of antierythrite and maltodextrin;
2. the maltodextrin with 2-(4-methoxyphenoxy)-sodium propionate, beta-schardinger dextrin-, salt and surplus is dissolved in the deionized water, obtains mixed aqueous solution;
3. with step 1. the mixed material of gained put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with step 2. prepared mixed aqueous solution continuously spraying be distributed on the sugar alcohol granule in the fluid bed, by heated-air drying, obtain described composite sweetener again.
3. the preparation method who is adapted at the composite sweetener that uses in the sour corn juice according to claim 2 is characterized in that: step 3. in, the EAT of fluid bed is controlled at 40 ~ 100 ℃.
4. the preparation method who is adapted at the composite sweetener that uses in the sour corn juice according to claim 3, it is characterized in that: step 3. in, when the mixed aqueous solution spraying disperseed, the EAT of control fluid bed was at 40 ~ 80 ℃, and the EAT of control fluid bed is at 70 ~ 100 ℃ during heated-air drying.
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Application publication date: 20130313 |