CN102934785A - Low-sugar low-calorie compound sweetener suitable for tea beverages or coffees and preparation method of low-sugar low-calorie compound sweetener suitable for tea beverages or the coffees - Google Patents
Low-sugar low-calorie compound sweetener suitable for tea beverages or coffees and preparation method of low-sugar low-calorie compound sweetener suitable for tea beverages or the coffees Download PDFInfo
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Abstract
The invention relates to a low-sugar low-calorie compound sweetener suitable for tea beverages or coffees and a preparation method of the low-sugar low-calorie compound sweetener suitable for the tea beverages or the coffees. The low-sugar low-calorie compound sweetener comprises the following components by weight percent: 13.33-23.33% of stevioside RA97, 30-42% of erythritol, 35-50% of isomaltitol, 0.01-0.35% of citric acid, 0.05-0.2% of sodium citrate and 0.05-0.44% of lactic acid; and the low-sugar low-calorie compound sweetener comprises the processes of putting erythritol and isomaltitol into a multi-dimensional mixing machine to obtain mixed materials, wherein the weight of isomaltulose is 50-70% of that of total weight; dissolving stevioside RA97, citric acid, sodium citrate, lactic acid and the rest isomaltitol into deionized water to obtain mixed water solution; driving the mixed materials to enter a spraying fluidized bed from the bottom of the spraying fluidized bed under a positive pressure and flow from bottom to top in an accelerated manner, and boiling the mixed materials upwards and downwards in the fluidized bed to form fine sugar alcohol granules; continuously spraying and dispersing the mixed water solution onto the sugar alcohol granules in the fluidized bed to obtain the compound sweetener.
Description
Technical field
The present invention relates to a kind of food additives, be specifically related to applicable low-sugar-content and low-calorie composite sweetener of a kind of tea beverage or coffee and preparation method thereof.
Background technology
In the last few years, raising along with expanding economy and people's lives wealth, obesity, hypertension, diabetes, carious tooth etc. become the height morbidity among the crowd, and the generation of these high morbidities is considered to especially with the sucrose Excessive Intake substantial connection is arranged with eating habit and diet structure.Therefore, as the sweetener of food additives, one of its development priority is exactly safe, without nutritive value, empty calory or functional high sweetener extremely low in calories.The characteristics of functional high sweetener are use safe, and consumption is few, and sugariness is high, and use cost is generally all far below sucrose, and this also is the power place that Food Science man continually develops novel high-intensity sweetener.At present, about 20 kinds of the granted high sweetener in countries in the world obtains that kind that the majority state approval allows to use mainly contains that saccharin sodium, honey element, 3,4-Dihydro-6-methyl-1,2,3-oxathiazin-4-one 2,2-dioxide potassium salt, Aspartame, Sucralose, alitame, knob are sweet, glycyrrhizin, stevioside, Momordica grosvenori is sweet and Talin etc.These high sweeteners have plenty of artificial synthetic, and are sweet etc. such as Aspartame, Sucralose, knob; What have then is natural extract, sweet etc. such as sky chrysanthemum glycosides and arhat.No matter be artificial synthesis edulcorant or natural extraction sweetener, at sugariness, sweet taste, stable aspects its pluses and minuses arranged respectively all, therefore, want to give full play to the optimal efficacy of these sweeteners, reduce cost, the most frequently used means are exactly compound at present.By carrying out various sweeteners or sweet substance compound, bring into play may exist between the various sweeteners synergistic function, in the hope of as far as possible approaching or satisfy the requirement of desirable sweetener: safety non-toxic, sweet taste is pure similar to sucrose (this is to be popular generally accepted sweet tastes), high sugariness, low heat value or without calorific value, stable height, unlikely dental caries, reduction cost.
In the prior art, mostly the generation sugar that uses in tea beverage or the coffee is take Sucralose as main sweet composite sweetener, this class composite sweetener also has different with sucrose on mouthfeel, there is front sweet slow, rear sweet and pleasant impression problem heavily, in the time of in being applied to tea beverage or coffee, also can so that the hardship sense in the drink give prominence to, be difficult to cover, thereby so that these drinks can not be accepted by masses and like.
The preparation method of composite sweetener in the prior art, can be by method or the spray-dired method converted products of substep of simple blend, the composite sweetener that the simple blend method makes is with low cost, but be difficult to guarantee that main sweetening material can be uniformly dispersed, and this point can affect the quality of composite sweetener product to a great extent.The spray-dired method of substep is that substep is dissolved in main sweetening material and each auxiliary sweetening material in the deionized water in batches, then the method by the wet spray drying is coated on each composition material on the granular sweetener by spraying respectively, the composite sweetener product sweetness that this method makes is uniformly dispersed, instant capacity is good, quality is better than the composite sweetener product that additive method makes, but its shortcoming is: material loss is large, the loss of especially main sweetening material is larger, machinery equipment power consumption is too high, the cost of product is significantly increased, and therefore this method also has been subject to certain restriction in implementation process.
Summary of the invention
The objective of the invention is to overcome the deficiency that prior art exists, a kind of with low cost, sugariness is uniformly dispersed, the better tea beverage of mouthfeel or coffee are applicable low-sugar-content and low-calorie composite sweetener and preparation method thereof is provided.
Purpose of the present invention is achieved through the following technical solutions:
The low-sugar-content and low-calorie composite sweetener that a kind of tea beverage or coffee are applicable comprises following percentage by weight composition: stevia sugar RA 97 13.33%~23.33%, antierythrite 30~42%, isomalt 35~50%, citric acid 0.01~0.35%, natrium citricum 0.05~0.2%, lactic acid 0.05~0.44%; Its preparation method comprises following processing step:
1. antierythrite and the isomalt that accounts for total amount 50 ~ 70% are dropped in the Multidimensionblender, mixed 20 ~ 40 minutes with the progression of 600 ~ 1000rpm, the granularity of control mixed material obtains the mixed material of antierythrite and isomalt at 80 ~ 130 orders;
2. the isomalt with stevia sugar RA 97, citric acid, natrium citricum, lactic acid and surplus is dissolved in the deionized water, obtains mixed aqueous solution;
3. with step 1. the mixed material of gained put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with step 2. prepared mixed aqueous solution continuously spraying be distributed on the sugar alcohol granule in the fluid bed, by heated-air drying, obtain described composite sweetener again.
The preparation method of the low-sugar-content and low-calorie composite sweetener that a kind of tea beverage of the present invention or coffee are applicable comprises following processing step:
1. antierythrite and the isomalt that accounts for total amount 50 ~ 70% are dropped in the Multidimensionblender, mixed 20 ~ 40 minutes with the progression of 600 ~ 1000rpm, the granularity of control mixed material obtains the mixed material of antierythrite and isomalt at 80 ~ 130 orders;
2. the isomalt with stevia sugar RA 97, citric acid, natrium citricum, lactic acid and surplus is dissolved in the deionized water, obtains mixed aqueous solution;
3. with step 1. the mixed material of gained put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with step 2. prepared mixed aqueous solution continuously spraying be distributed on the sugar alcohol granule in the fluid bed, by heated-air drying, obtain described composite sweetener again.
Further, the preparation method of the low-sugar-content and low-calorie composite sweetener that above-mentioned a kind of tea beverage or coffee are applicable, step 3. in, the EAT of fluid bed is controlled at 45 ~ 95 ℃.
Again further, the preparation method of the low-sugar-content and low-calorie composite sweetener that above-mentioned a kind of tea beverage or coffee are applicable, step 3. in, when the mixed aqueous solution spraying disperses, the EAT of control fluid bed is between 45 ~ 80 ℃, and the EAT of control fluid bed is at 80 ~ 95 ℃ during heated-air drying.
The substantive distinguishing features that technical solution of the present invention is outstanding and significant progressive being mainly reflected in:
The present invention adopts stevia sugar RA 97 as main sweet, be aided with antierythrite, isomalt etc. auxiliary sweet carry out composite, and add citric acid and lactic acid etc. composite sweetener is carried out seasoning, the final stevioside type low-sugar-content and low-calorie composite sweetener that obtains, be fit to very much be applied in the beverages such as coffee or tea, it can substitute the sweet taste that white granulated sugar provides popular institute to like and accept for drink.
The present invention drops into the auxiliary sweetening material of the part of composite sweetener in the Multidimensionblender first and carries out tentatively mixing, then main sweetening material and remaining auxiliary sweetening material are dissolved into mixed aqueous solution, and disperse dry by the disposable spraying of advanced negative-pressure fluidized bed apparatus, make it to be coated on just mixed mixed material surface, obtain the Fluffy powder grain compound sweetener product.The present invention compares with the method for prior art simple blend, and the product instant capacity that obtains, sugariness dispersiveness etc. have significantly lifting, have good quality; And with prior art in batches spray-dired method compare, can greatly shorten the process-cycle again, the amount of saving energy has reduced production cost (about 60 ~ 80 minutes of product manufacturing cycle of the present invention, and in batches about 2 ~ 3 hours of the manufacturing cycle of spray drying process).
The specific embodiment
Composite sweetener of the present invention, its composition is: stevia sugar RA 97 13.33%~23.33%, antierythrite 30~42%, isomalt 35~50%, citric acid 0.01~0.35%, natrium citricum 0.05~0.2%, lactic acid 0.05~0.44%.
The preparation technology of composite sweetener: first antierythrite and the isomalt that accounts for total amount 50 ~ 70% are dropped in the Multidimensionblender, progression with 600 ~ 1000rpm mixed 20 ~ 40 minutes, the granularity of control mixed material obtains the mixed material of antierythrite and isomalt at 80 ~ 130 orders; Isomalt with stevia sugar RA 97, citric acid, natrium citricum, lactic acid and surplus is dissolved in the deionized water again, obtains mixed aqueous solution; Then mixed material is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, the EAT of fluid bed is controlled at 45 ~ 95 ℃, forms tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with prepared mixed aqueous solution continuously spraying be distributed on the sugar alcohol granule in the fluid bed, when the mixed aqueous solution spraying disperses, the EAT of control fluid bed is between 45 ~ 80 ℃, pass through again heated-air drying, the EAT of control fluid bed obtains described composite sweetener at 80 ~ 95 ℃ during heated-air drying.
Multidimensionblender used in the present invention adopts commercial 200 feather weight Multidimensionblenders, rotating speed level journey is 200 ~ 1800rpm, barrel is two taper, middle column, and during work, this Multidimensionblender can make the material in the barrel collide, pulverize and mix from a plurality of angles.
Embodiment 1:
(1) get in 37 kilograms of antierythrites, 30 kilograms of inputs of the isomalt Multidimensionblender, the progression of control Multidimensionblender is 800rpm, mixes 40 minutes, obtains the mixed material of antierythrite and isomalt, and granularity is between 80 ~ 130 orders;
(2) 19.42 kilograms of 13.33 kilograms of stevia sugar RAs 97,0.1 kilogram of citric acid, 0.05 kilogram of natrium citricum, 0.1 kilogram of lactic acid, remaining isomalt are mixed with deionized water, the intensification stirring and dissolving obtains mixed aqueous solution;
(3) mixed material of step (1) gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece is distributed to the continuous spraying of the prepared mixed aqueous solution of step (2) on the interior sugar alcohol granule of fluid bed, the EAT of control fluid bed is between 45 ~ 80 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the EAT of fluid bed between 80 ~ 95 ℃, carry out heated-air drying, last discharging obtains Fluffy powder grain compound sweetener.
Embodiment 2:
(1) get in 38 kilograms of antierythrites, 28.3 kilograms of inputs of the isomalt Multidimensionblender, the progression of control Multidimensionblender is 800rpm, mixes 40 minutes, obtains the mixed material of antierythrite and isomalt, and granularity is between 80 ~ 130 orders;
(2) 16.63 kilograms of 16.67 kilograms of stevia sugar RAs 97,0.15 kilogram of citric acid, 0.1 kilogram of natrium citricum, 0.15 kilogram of lactic acid, remaining isomalt are mixed with deionized water, the intensification stirring and dissolving obtains mixed aqueous solution;
(3) mixed material of step (1) gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece is distributed to the continuous spraying of the prepared mixed aqueous solution of step (2) on the interior sugar alcohol granule of fluid bed, the EAT of control fluid bed is between 45 ~ 80 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the EAT of fluid bed between 80 ~ 95 ℃, carry out heated-air drying, last discharging obtains Fluffy powder grain compound sweetener.
Embodiment 3:
(1) get in 35 kilograms of antierythrites, 27.3 kilograms of inputs of the isomalt Multidimensionblender, the progression of control Multidimensionblender is 800rpm, mixes 35 minutes, obtains the mixed material of antierythrite and isomalt, and granularity is between 80 ~ 130 orders;
(2) 17.18 kilograms of 20 kilograms of stevia sugar RAs 97,0.2 kilogram of citric acid, 0.12 kilogram of natrium citricum, 0.2 kilogram of lactic acid, remaining isomalt are mixed with deionized water, the intensification stirring and dissolving obtains mixed aqueous solution;
(3) mixed material of step (1) gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece is distributed to the continuous spraying of the prepared mixed aqueous solution of step (2) on the interior sugar alcohol granule of fluid bed, the EAT of control fluid bed is between 45 ~ 80 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the EAT of fluid bed between 80 ~ 95 ℃, carry out heated-air drying, last discharging obtains Fluffy powder grain compound sweetener.
Embodiment 4:
(1) get in 35 kilograms of antierythrites, 26.2 kilograms of inputs of the isomalt Multidimensionblender, the progression of control Multidimensionblender is 800rpm, mixes 30 minutes, obtains the mixed material of antierythrite and isomalt, and granularity is between 80 ~ 130 orders;
(2) 14.85 kilograms of 23.33 kilograms of stevia sugar RAs 97,0.22 kilogram of citric acid, 0.15 kilogram of natrium citricum, 0.25 kilogram of lactic acid, remaining isomalt are mixed with deionized water, the intensification stirring and dissolving obtains mixed aqueous solution;
(3) mixed material of step (1) gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece is distributed to the continuous spraying of the prepared mixed aqueous solution of step (2) on the interior sugar alcohol granule of fluid bed, the EAT of control fluid bed is between 45 ~ 80 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the EAT of fluid bed between 80 ~ 95 ℃, carry out heated-air drying, last discharging obtains Fluffy powder grain compound sweetener.
The composite sweetener that adopts technical solution of the present invention to obtain, its main performance index sees Table 1.
Table 1
The present invention adopts stevia sugar RA 97 as main sweet, be aided with antierythrite, isomalt etc. auxiliary sweet carry out composite, and add citric acid and lactic acid etc. composite sweetener is carried out seasoning, the final stevioside type composite sweetener that obtains, be fit to very much be applied in the beverages such as coffee or tea, it can substitute white granulated sugar and provide the popular sugariness taste of liking for drink.
The present invention drops into the auxiliary sweetening material of the part of composite sweetener in the Multidimensionblender first and carries out tentatively mixing, then main sweetening material and remaining auxiliary sweetening material are dissolved into mixed aqueous solution, and disperse dry by the disposable spraying of advanced negative-pressure fluidized bed apparatus, make it to be coated on just mixed mixed material surface, obtain the Fluffy powder grain compound sweetener product.The present invention compares with the method for prior art simple blend, and the product instant capacity that obtains, sugariness dispersiveness etc. have significantly lifting, have good quality; And with prior art in batches spray-dired method compare, can greatly shorten the process-cycle again, the amount of saving energy, reduced production cost (about 60 ~ 80 minutes of product manufacturing cycle of the present invention, and about 2 ~ 3 hours of the manufacturing cycle of spray drying process in batches, and the present invention just the mixed power consumption that uses Multidimensionblender be approximately fluidized bed with spraying electricity consumption of equipment amount 1/24).
The sugariness degree of modification of composite sweetener of the present invention can be adjusted by the consumption of stevia sugar RA 97 according to actual needs, and the present invention is fit to the composite sweetener of 20~35 times of sucrose sweetness of preparation usually.
What need to understand is: the above only is preferred embodiment of the present invention; for those skilled in the art; under the prerequisite that does not break away from the principle of the invention, can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (4)
1. the applicable low-sugar-content and low-calorie composite sweetener of tea beverage or coffee is characterized in that comprising following percentage by weight composition: stevia sugar RA 97 13.33%~23.33%, antierythrite 30~42%, isomalt 35~50%, citric acid 0.01~0.35%, natrium citricum 0.05~0.2%, lactic acid 0.05~0.44%; Its preparation method comprises following processing step:
1. antierythrite and the isomalt that accounts for total amount 50 ~ 70% are dropped in the Multidimensionblender, mixed 20 ~ 40 minutes with the progression of 600 ~ 1000rpm, the granularity of control mixed material obtains the mixed material of antierythrite and isomalt at 80 ~ 130 orders;
2. the isomalt with stevia sugar RA 97, citric acid, natrium citricum, lactic acid and surplus is dissolved in the deionized water, obtains mixed aqueous solution;
3. with step 1. the mixed material of gained put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with step 2. prepared mixed aqueous solution continuously spraying be distributed on the sugar alcohol granule in the fluid bed, by heated-air drying, obtain described composite sweetener again.
2. the preparation method of the applicable low-sugar-content and low-calorie composite sweetener of tea beverage claimed in claim 1 or coffee is characterized in that comprising following processing step:
1. antierythrite and the isomalt that accounts for total amount 50 ~ 70% are dropped in the Multidimensionblender, mixed 20 ~ 40 minutes with the progression of 600 ~ 1000rpm, the granularity of control mixed material obtains the mixed material of antierythrite and isomalt at 80 ~ 130 orders;
2. the isomalt with stevia sugar RA 97, citric acid, natrium citricum, lactic acid and surplus is dissolved in the deionized water, obtains mixed aqueous solution;
3. with step 1. the mixed material of gained put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with step 2. prepared mixed aqueous solution continuously spraying be distributed on the sugar alcohol granule in the fluid bed, by heated-air drying, obtain described composite sweetener again.
3. the preparation method of the applicable low-sugar-content and low-calorie composite sweetener of tea beverage according to claim 2 or coffee is characterized in that: step 3. in, the EAT of fluid bed is controlled at 45 ~ 95 ℃.
4. the preparation method of the applicable low-sugar-content and low-calorie composite sweetener of tea beverage according to claim 3 or coffee, it is characterized in that: step 3. in, when the mixed aqueous solution spraying disperses, the EAT of control fluid bed is between 45 ~ 80 ℃, and the EAT of control fluid bed is at 80 ~ 95 ℃ during heated-air drying.
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CN114271422A (en) * | 2022-01-07 | 2022-04-05 | 杭州民生健康药业股份有限公司 | Vitamin C bubble solid beverage |
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