CN102960683A - Sugar-free compound sweetener suitable for neutral solid beverage and preparation method of sugar-free compound sweetener - Google Patents
Sugar-free compound sweetener suitable for neutral solid beverage and preparation method of sugar-free compound sweetener Download PDFInfo
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- CN102960683A CN102960683A CN2012105007510A CN201210500751A CN102960683A CN 102960683 A CN102960683 A CN 102960683A CN 2012105007510 A CN2012105007510 A CN 2012105007510A CN 201210500751 A CN201210500751 A CN 201210500751A CN 102960683 A CN102960683 A CN 102960683A
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Abstract
The invention relates to a sugar-free compound sweetener suitable for neutral solid beverage and a preparation method of the sugar-free compound sweetener. The sugar-free compound sweetener comprises 3.33 to 8.33 percent of sucralose, 30 to 33 percent of erythritol, 48.67 to 57.67 percent of low-polymer isomaltitol and 13 to 18 percent of xylitol. The preparation process comprises the following steps of: feeding sugar alcohol and 60 to 70 percent of total low-polymer isomaltitol into a multi-dimensional mixing machine for preliminary mixing; dissolving the sucralose and the residual low-polymer isomaltitol into deionized water to obtain a mixed aqueous solution; enabling the mixture to enter a fluidized bed from the bottom of the spraying fluidized bed under positive pressure and flow at an accelerated speed from bottom to top, applying negative pressure to the upper part of the spraying fluidized bed, vibrating the mixture top to bottom so that the mixture overturns up and down in the fluidized bed to form fine sugar alcohol particles; and continuously spraying and dispersing the mixed aqueous solution to the small sugar alcohol particles in the fluidized bed through a multi-point spraying gun on the side part of the fluidized bed, and drying the small sugar alcohol particles by hot air to obtain the compound sweetener.
Description
Technical field
The present invention relates to a kind of food additives, be specifically related to applicable sugar-free composite sweetener of a kind of neutral solid beverage and preparation method thereof.
Background technology
In the last few years, raising along with expanding economy and people's lives wealth, obesity, hypertension, diabetes, carious tooth etc. become the height morbidity among the crowd, and the generation of these high morbidities is considered to especially with the sucrose Excessive Intake substantial connection is arranged with eating habit and diet structure.Therefore, as the sweetener of food additives, one of its development priority is exactly safe, without nutritive value, empty calory or functional high sweetener extremely low in calories.The characteristics of functional high sweetener are use safe, and consumption is few, and sugariness is high, and use cost is generally all far below sucrose, and this also is the power place that Food Science man continually develops novel high-intensity sweetener.At present, about 20 kinds of the granted high sweetener in countries in the world obtains that kind that the majority state approval allows to use mainly contains that saccharin sodium, honey element, 3,4-Dihydro-6-methyl-1,2,3-oxathiazin-4-one 2,2-dioxide potassium salt, Aspartame, Sucralose, alitame, knob are sweet, glycyrrhizin, stevioside, Momordica grosvenori is sweet and Talin etc.These high sweeteners have plenty of artificial synthetic, and are sweet etc. such as Aspartame, Sucralose, knob; What have then is natural extract, sweet etc. such as sky chrysanthemum glycosides and arhat.No matter be artificial synthesis edulcorant or natural extraction sweetener, at sugariness, sweet taste, stable aspects its pluses and minuses arranged respectively all, therefore, want to give full play to the optimal efficacy of these sweeteners, reduce cost, the most frequently used means are exactly compound at present.By carrying out various sweeteners or sweet substance compound, bring into play may exist between the various sweeteners synergistic function, in the hope of as far as possible approaching or satisfy the requirement of desirable sweetener: safety non-toxic, sweet taste is pure similar to sucrose (this is to be popular generally accepted sweet tastes), high sugariness, low heat value or without calorific value, stable height, unlikely dental caries, reduction cost.
In the prior art, have with the composite composite sweetener of Sucralose, antierythrite, xylitol and oligoisomaltose, when being applied in the neutral solid beverages such as milk tea, soya-bean milk when these composite sweeteners, mouthfeel is not fine, and effect is unsatisfactory; And all used more xylitol and antierythrite in these composite sweeteners, this has improved the cost of product virtually.
Composite sweetener take Sucralose as main sweetening material in the prior art, can process by method or the spray-dired method of substep of simple blend, the composite sweetener that the simple blend method makes is with low cost, but be difficult to guarantee that main sweetening material Sucralose can be uniformly dispersed, and this point can affect the quality of composite sweetener product to a great extent.The spray-dired method of substep is that substep is dissolved in main sweetening material and each auxiliary sweetening material in the deionized water in batches, then the method by the wet spray drying is coated on each composition material on the granular sweetener by spraying respectively, the composite sweetener product sweetness that this method makes is uniformly dispersed, instant capacity is good, quality is better than the composite sweetener product that additive method makes, but its shortcoming is: material loss, the loss of especially main sweetening material is larger, machinery equipment power consumption is too high, the cost of product is significantly increased, and therefore this method also has been subject to certain restriction in implementation process.
Summary of the invention
The objective of the invention is to overcome the deficiency that prior art exists, provide that a kind of cost is cheaper, mouthfeel is fit to sugar-free composite sweetener that soya-bean milk, milk tea etc. can use by the neutral solid beverage that pulvis reconstitutes and preparation method thereof more.
Purpose of the present invention is achieved through the following technical solutions:
The sugar-free composite sweetener that a kind of neutral solid beverage is applicable comprises following percentage by weight composition: Sucralose 3.33 ~ 8.33%, antierythrite 30 ~ 33%, oligoisomaltose 48.67 ~ 57.67%, xylitol 13 ~ 18%; Its preparation method comprises following processing step:
1. antierythrite, xylitol and the oligoisomaltose that accounts for total amount 60 ~ 70% are dropped in the Multidimensionblender, progression with 800 ~ 1000rpm mixed 35 ~ 45 minutes, the granularity of control mixed material obtains the mixed material of antierythrite, xylitol and oligoisomaltose at 80 ~ 130 orders;
2. the oligoisomaltose with Sucralose and surplus is dissolved in the deionized water, obtains the mixed aqueous solution of Sucralose and oligoisomaltose;
3. with step 1. the mixed material of gained put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with step 2. prepared mixed aqueous solution continuously spraying be distributed on the sugar alcohol granule in the fluid bed, by heated-air drying, obtain described composite sweetener again.
The preparation method of the sugar-free composite sweetener that a kind of neutral solid beverage of the present invention is applicable comprises following processing step:
1. antierythrite, xylitol and the oligoisomaltose that accounts for total amount 60 ~ 70% are dropped in the Multidimensionblender, progression with 800 ~ 1000rpm mixed 35 ~ 45 minutes, the granularity of control mixed material obtains the mixed material of antierythrite, xylitol and oligoisomaltose at 80 ~ 130 orders;
2. the oligoisomaltose with Sucralose and surplus is dissolved in the deionized water, obtains the mixed aqueous solution of Sucralose and oligoisomaltose;
3. with step 1. the mixed material of gained put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with step 2. prepared mixed aqueous solution continuously spraying be distributed on the sugar alcohol granule in the fluid bed, by heated-air drying, obtain described composite sweetener again.
Further, the preparation method of the sugar-free composite sweetener that above-mentioned a kind of neutral solid beverage is applicable, step 3. in, the EAT of fluid bed is controlled at 40 ~ 100 ℃.
Again further, the preparation method of the sugar-free composite sweetener that above-mentioned a kind of neutral solid beverage is applicable, step 3. in, when the mixed aqueous solution spraying disperses, the EAT of control fluid bed is between 40 ~ 70 ℃, and the EAT of control fluid bed is at 70 ~ 100 ℃ during heated-air drying.
The substantive distinguishing features that technical solution of the present invention is outstanding and significant progressive being mainly reflected in:
The present invention has controlled the ratio of composite sweetener mesoerythrit and xylitol subtly, when the sugariness multiple of composite sweetener and sucrose is in about 20 ~ 50 times scope, composite sweetener product of the present invention can be applied in the neutral solid beverages such as milk tea, soya-bean milk well, improves mouthfeel and the local flavor of application; In addition because composition of raw materials of the present invention has reduced the higher antierythrite of cost and the consumption of xylitol, also so that composite sweetener product of the present invention reduced about 10% ~ 15% than the cost of material of other like products.
The present invention drops into the auxiliary sweetening material of the part of composite sweetener in the Multidimensionblender first and carries out tentatively mixing, then main sweetening material and remaining auxiliary sweetening material are dissolved into mixed aqueous solution, and disperse dry by the disposable spraying of advanced negative-pressure fluidized bed apparatus, make it to be coated on just mixed mixed material surface, obtain the Fluffy powder grain compound sweetener product.The present invention compares with the method for prior art simple blend, and the product instant capacity that obtains, sugariness dispersiveness etc. have significantly lifting, have good quality; And with prior art in batches spray-dired method compare, can greatly shorten the process-cycle again, the amount of saving energy has reduced production cost (about 65 ~ 85 minutes of product manufacturing cycle of the present invention, and in batches about 2 ~ 3 hours of the manufacturing cycle of spray drying process).
The specific embodiment
The applicable sugar-free composite sweetener of the neutral solid beverage of the present invention, its composition is: Sucralose 3.33 ~ 8.33%, antierythrite 30 ~ 33%, oligoisomaltose 48.67 ~ 57.67%, xylitol 13 ~ 18%.
The preparation technology of this composite sweetener: first antierythrite, xylitol and the oligoisomaltose that accounts for total amount 60 ~ 70% are dropped in the Multidimensionblender, progression with 800 ~ 1000rpm mixed 35 ~ 45 minutes, the granularity of control mixed material obtains the mixed material of antierythrite, xylitol and oligoisomaltose at 80 ~ 130 orders; Oligoisomaltose with Sucralose and surplus is dissolved in the deionized water again, obtains the mixed aqueous solution of Sucralose and oligoisomaltose; Then mixed material is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, the EAT of fluid bed is controlled at 40 ~ 100 ℃, forms tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with prepared mixed aqueous solution continuously spraying be distributed on the sugar alcohol granule in the fluid bed, when the mixed aqueous solution spraying disperses, the EAT of control fluid bed is between 40 ~ 70 ℃, pass through again heated-air drying, the EAT of control fluid bed obtains described composite sweetener at 70 ~ 100 ℃ during heated-air drying.
Multidimensionblender used in the present invention adopts commercial 200 feather weight Multidimensionblenders, rotating speed level journey is 200 ~ 1800rpm, barrel is two taper, middle column, and during work, this Multidimensionblender can make the material in the barrel collide, pulverize and mix from a plurality of angles.
Embodiment 1:
(1) gets in 31 kilograms of antierythrites, 9.3 kilograms of xylitols and 36.37 kilograms of inputs of the oligoisomaltose Multidimensionblender, the progression of control Multidimensionblender is 800rpm, mixed 40 minutes, obtain the mixed material of antierythrite, xylitol and oligoisomaltose, granularity is between 80 ~ 130 orders;
(2) 20 kilograms of 3.33 kilograms of Sucraloses, remaining oligoisomaltose are mixed with deionized water, the intensification stirring and dissolving obtains the mixed aqueous solution of Sucralose and oligoisomaltose;
(3) mixed material of step (1) gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece is distributed to the continuous spraying of the prepared mixed aqueous solution of step (2) on the interior sugar alcohol granule of fluid bed, the EAT of control fluid bed is between 40 ~ 70 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the EAT of fluid bed between 70 ~ 100 ℃, carry out heated-air drying, last discharging obtains Fluffy powder grain compound sweetener.
Embodiment 2:
(1) gets in 32 kilograms of antierythrites, 9.5 kilograms of xylitols and 34.5 kilograms of inputs of the oligoisomaltose Multidimensionblender, the progression of control Multidimensionblender is 800rpm, mixed 40 minutes, obtain the mixed material of antierythrite, xylitol and oligoisomaltose, granularity is between 80 ~ 130 orders;
(2) 19 kilograms of 5 kilograms of Sucraloses, remaining oligoisomaltose are mixed with deionized water, the intensification stirring and dissolving obtains the mixed aqueous solution of Sucralose and oligoisomaltose;
(3) mixed material of step (1) gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece is distributed to the continuous spraying of the prepared mixed aqueous solution of step (2) on the interior sugar alcohol granule of fluid bed, the EAT of control fluid bed is between 40 ~ 70 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the EAT of fluid bed between 70 ~ 100 ℃, carry out heated-air drying, last discharging obtains Fluffy powder grain compound sweetener.
Embodiment 3:
(1) gets in 32 kilograms of antierythrites, 9.8 kilograms of xylitols and 33.53 kilograms of inputs of the oligoisomaltose Multidimensionblender, the progression of control Multidimensionblender is 800rpm, mixed 45 minutes, obtain the mixed material of antierythrite, xylitol and oligoisomaltose, granularity is between 80 ~ 130 orders;
(2) 18 kilograms of 6.67 kilograms of Sucraloses, remaining oligoisomaltose are mixed with deionized water, the intensification stirring and dissolving obtains the mixed aqueous solution of Sucralose and oligoisomaltose;
(3) mixed material of step (1) gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece is distributed to the continuous spraying of the prepared mixed aqueous solution of step (2) on the interior sugar alcohol granule of fluid bed, the EAT of control fluid bed is between 40 ~ 70 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the EAT of fluid bed between 70 ~ 100 ℃, carry out heated-air drying, last discharging obtains Fluffy powder grain compound sweetener.
Embodiment 4:
(1) gets in 32.5 kilograms of antierythrites, 10 kilograms of xylitols and 31.17 kilograms of inputs of the oligoisomaltose Multidimensionblender, the progression of control Multidimensionblender is 800rpm, mixed 35 minutes, obtain the mixed material of antierythrite, xylitol and oligoisomaltose, granularity is between 80 ~ 130 orders;
(2) 18 kilograms of 8.33 kilograms of Sucraloses, remaining oligoisomaltose are mixed with deionized water, the intensification stirring and dissolving obtains the mixed aqueous solution of Sucralose and oligoisomaltose;
(3) mixed material of step (1) gained is put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece is distributed to the continuous spraying of the prepared mixed aqueous solution of step (2) on the interior sugar alcohol granule of fluid bed, the EAT of control fluid bed is between 40 ~ 70 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the EAT of fluid bed between 70 ~ 100 ℃, carry out heated-air drying, last discharging obtains Fluffy powder grain compound sweetener.
The composite sweetener that adopts technical solution of the present invention to obtain, its main performance index sees Table 1.
Table 1
The present invention has controlled the ratio of composite sweetener mesoerythrit and xylitol subtly, when the sugariness multiple of composite sweetener and sucrose is in about 20 ~ 50 times scope, composite sweetener product of the present invention can be applied in the neutral solid beverage that milk tea, soya-bean milk etc. can reconstitute with pulvis well, improves mouthfeel and the local flavor of application; In addition because composition of raw materials of the present invention has reduced the higher antierythrite of cost and the consumption of xylitol, also so that composite sweetener product of the present invention than the cost of other like products about 10% ~ 15%.
The present invention drops into the auxiliary sweetening material of the part of composite sweetener in the Multidimensionblender first and carries out tentatively mixing, then main sweetening material and remaining auxiliary sweetening material are dissolved into mixed aqueous solution, and disperse dry by the disposable spraying of advanced negative-pressure fluidized bed apparatus, make it to be coated on just mixed mixed material surface, obtain the Fluffy powder grain compound sweetener product.The present invention compares with the method for prior art simple blend, and the product instant capacity that obtains, sugariness dispersiveness etc. have significantly lifting, have good quality; And with prior art in batches spray-dired method compare, can greatly shorten the process-cycle again, the amount of saving energy, reduced production cost (about 60 ~ 90 minutes of product manufacturing cycle of the present invention, and about 2 ~ 3 hours of the manufacturing cycle of spray drying process in batches, and the present invention just the mixed power consumption that uses Multidimensionblender be approximately fluidized bed with spraying electricity consumption of equipment amount 1/24).
The sugariness degree of modification of composite sweetener of the present invention can be adjusted by the consumption of Sucralose according to actual needs, and the present invention is fit to the sugar-free composite sweetener of 20～50 times of sucrose sweetness of preparation usually.
What need to understand is: the above only is preferred embodiment of the present invention; for those skilled in the art; under the prerequisite that does not break away from the principle of the invention, can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (4)
1. the sugar-free composite sweetener that neutral solid beverage is applicable is characterized in that comprising following percentage by weight composition: Sucralose 3.33 ~ 8.33%, antierythrite 30 ~ 33%, oligoisomaltose 48.67 ~ 57.67%, xylitol 13 ~ 18%; Its preparation method comprises following processing step:
1. antierythrite, xylitol and the oligoisomaltose that accounts for total amount 60 ~ 70% are dropped in the Multidimensionblender, progression with 800 ~ 1000rpm mixed 35 ~ 45 minutes, the granularity of control mixed material obtains the mixed material of antierythrite, xylitol and oligoisomaltose at 80 ~ 130 orders;
2. the oligoisomaltose with Sucralose and surplus is dissolved in the deionized water, obtains the mixed aqueous solution of Sucralose and oligoisomaltose;
3. with step 1. the mixed material of gained put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with step 2. prepared mixed aqueous solution continuously spraying be distributed on the sugar alcohol granule in the fluid bed, by heated-air drying, obtain described composite sweetener again.
2. the preparation method of the applicable sugar-free composite sweetener of a kind of neutral solid beverage claimed in claim 1 is characterized in that comprising following processing step:
1. antierythrite, xylitol and the oligoisomaltose that accounts for total amount 60 ~ 70% are dropped in the Multidimensionblender, progression with 800 ~ 1000rpm mixed 35 ~ 45 minutes, the granularity of control mixed material obtains the mixed material of antierythrite, xylitol and oligoisomaltose at 80 ~ 130 orders;
2. the oligoisomaltose with Sucralose and surplus is dissolved in the deionized water, obtains the mixed aqueous solution of Sucralose and oligoisomaltose;
3. with step 1. the mixed material of gained put in the spray-fluidized bed apparatus, making mixed material enter the fluid bed with malleation from the bottom of fluidized bed with spraying and accelerate from bottom to top flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make mixed material in fluid bed up and down the boiling, form tiny sugar alcohol granule; Multiple spot spray gun by the fluid bed sidepiece with step 2. prepared mixed aqueous solution continuously spraying be distributed on the sugar alcohol granule in the fluid bed, by heated-air drying, obtain described composite sweetener again.
3. the preparation method of the applicable sugar-free composite sweetener of a kind of neutral solid beverage according to claim 2 is characterized in that: step 3. in, the EAT of fluid bed is controlled at 40 ~ 100 ℃.
4. the preparation method of the applicable sugar-free composite sweetener of a kind of neutral solid beverage according to claim 3, it is characterized in that: step 3. in, when the mixed aqueous solution spraying disperses, the EAT of control fluid bed is between 40 ~ 70 ℃, and the EAT of control fluid bed is at 70 ~ 100 ℃ during heated-air drying.
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| CN101874606A (en) * | 2009-12-04 | 2010-11-03 | 苏州工业园区尚融科技有限公司 | Fluffy granular composite sugar-free table sweetener and preparation method thereof |
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Application publication date: 20130313 |