CN101874606A - Fluffy granular composite sugar-free table sweetener and preparation method thereof - Google Patents
Fluffy granular composite sugar-free table sweetener and preparation method thereof Download PDFInfo
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- CN101874606A CN101874606A CN2009102520546A CN200910252054A CN101874606A CN 101874606 A CN101874606 A CN 101874606A CN 2009102520546 A CN2009102520546 A CN 2009102520546A CN 200910252054 A CN200910252054 A CN 200910252054A CN 101874606 A CN101874606 A CN 101874606A
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Abstract
The invention relates to a fluffy granular composite sugar-free table sweetener and a preparation method. The sweetener comprises the following components: 20-30% of xylitol, 20-35% of erythritol, 35-55% of isomaltooligosaccharide and 0.8-1.2% of sucralose. The process comprises the following steps: respectively adding 8% of isomaltooligosaccharide and the sucralose to a heating container and respectively adding deionized water for mixing; raising the temperature until dissolution; adding activated carbon to the solution respectively, filtering the mixture while the mixture is hot and collecting the filtrates respectively in storage tanks; and pumping the ground mixture of the xylitol, the erythritol and the isomaltooligosaccharide into a fluidized bed with spraying from the bottom of the bed under positive pressure and ensuring the mixture to flow at high speed from bottom to top, applying negative pressure to the upper part of the fluidized bed with spraying so that the bed vibrates from top to bottom to ensure the materials to boil in the bed; using a multipoint spray gun at the side of the fluidized bed to continuously spray and disperse the refined sucralose solution on superfine sugar alcohols, then pumping the isomaltooligosaccharide solution and carrying out continuous spray drying, thus obtaining the sugar-free table sweetener. The preparation flow is simple and convenient and the sweetness of the product is 5-10 times that of the common sucrose.
Description
Technical field
The present invention relates to a kind of edible sweetener, relate in particular to a kind of fluffy granular composite sugar-free table sweetener and preparation method thereof.
Background technology
Along with the increase of people because of too much bringing disease, people's demand safety, healthy Sugarless type dining table sweetener with sugar; In production procedure, reach from raw material and put into the advanced preparation technology that finished product one step finishes; It is learnt from other's strong points to offset one's weaknesses, has complementary advantages to make between the sugar alcohol sweet taste on the formula for a product, can play during product uses and cover the effect that promotes mouthfeel with synergy, people thirst for satisfying under the low prerequisite of sugariness height, heat, and occupation modeization, with cane-sugar taste safety and Health Sugarless type dining table sweetener roughly the same.
Summary of the invention
The objective of the invention is to overcome the deficiency that prior art exists, a kind of fluffy granular composite sugar-free table sweetener and preparation method thereof is provided, adopt the scientific technology of easy operation control, the molten speed of product, mouthfeel, sugariness all are higher than the prior art optimum value.
Purpose of the present invention is achieved through the following technical solutions:
Fluffy granular composite sugar-free table sweetener, characteristics are to comprise following composition (percentage by weight): xylitol 20～30%, antierythrite 20～35%, oligoisomaltose 35～55%, Sucralose 0.8～1.2%.
Further, above-mentioned fluffy granular composite sugar-free table sweetener, wherein, xylitol 25%, antierythrite 30%, oligoisomaltose 43.83%, Sucralose 1.17%.
The preparation method of fluffy granular composite sugar-free table sweetener of the present invention comprises following processing step:
1. with 8% oligoisomaltose, Sucralose joins respectively in the heating container, adds deionized water respectively and mixes;
2. be warming up to 52～80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned oligoisomaltose solution and the sucralose solution, be incubated 25～30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank of heat tracing;
4. with xylitol, antierythrite and oligoisomaltose are put in the spray-fluidized bed apparatus after pulverizing, xylitol, the mixed material of antierythrite and oligoisomaltose enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, pump into the above-mentioned oligoisomaltose solution that refines again, spray-drying obtains fluffy granular composite sugar-free table sweetener continuously.
Again further, the preparation method of above-mentioned fluffy granular composite sugar-free table sweetener joins 8% oligoisomaltose, Sucralose respectively in the heating container, adds deionized water respectively and mixes; Be warming up to 60～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank that has heat tracing; Xylitol, antierythrite and oligoisomaltose reach 120～180 orders through pulverizing, be sent in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, control fluidized-bed layer temperature is at 35～80 ℃, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, after the mixing of sugar alcohol fluidisation loses surperficial moisture content, pump into the above-mentioned oligoisomaltose solution that refines again, spray drying granulation obtains fluffy granular composite sugar-free table sweetener continuously.
Again further, the preparation method of above-mentioned fluffy granular composite sugar-free table sweetener, the bed temperature scope of described fluidized bed with spraying is 35～80 ℃, wherein the bed temperature of phase I Sucralose spraying dispersion is 35～50 ℃, and the bed temperature of second stage oligoisomaltose mist projection granulating is 50～80 ℃.
Again further, the preparation method of above-mentioned fluffy granular composite sugar-free table sweetener, in the phase I of described spraying mixed fluidized bed, the Sucralose spraying is dispersed in fluidisation and smashes on the fine sugar alcohol crystal body; In second stage, the oligoisomaltose spray drying granulation is on the noncrystal of mixing sugar alcohol.
Substantive distinguishing features and obvious improvement that technical solution of the present invention is outstanding are mainly reflected in:
The negative pressure fluid bed fluidization technique that adopts scientific formula, uses advanced is in conjunction with the multi-point atomizing method, and time sharing segment control appliance bed temperature efficiently solves even dispersion, coats problems such as granulation, drying.With xylitol, antierythrite, oligoisomaltose, Sucralose is primary raw material; modify uniformly and coat by preparation method to sugariness; make product sweetness reach 5～10 times of common sucrose; products obtained therefrom does not have smell, does not have color; soluble in water; this fluffy granular composite sugar-free table sweetener is easy to use, and its preparation process science is simple and easy to operate, is fit to very much large-scale production.
Description of drawings
Below in conjunction with accompanying drawing technical solution of the present invention is described further:
Fig. 1: process chart of the present invention.
The specific embodiment
Fluffy granular composite sugar-free table sweetener of the present invention, its composition is: xylitol 20～30%, antierythrite 20～35%, oligoisomaltose 35～55%, Sucralose 0.8～1.2%.Ideal formulations is: xylitol 25%, antierythrite 30%, oligoisomaltose 43.83%, Sucralose 1.17%.
As shown in Figure 1, the preparation technology of fluffy granular composite sugar-free table sweetener: at first, with 8% oligoisomaltose, Sucralose joins respectively in the heating container, adds deionized water respectively and mixes; Be warming up to 52～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively in above-mentioned oligoisomaltose solution and the sucralose solution, be incubated 25～30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank of heat tracing; At last, with xylitol, put into after antierythrite and oligoisomaltose are pulverized in the spray-fluidized bed apparatus (heating temperature control and by the positive negative pressure boiling of equipment technology with the boiling that in fluid bed, circulates of sugar alcohol material, mix that fluidisation is anhydrated and fluffy processing, sugar alcohol mixtures material → malleation material quickens to flow from bottom to top → and negative pressure vibrates → makes material boiling up and down in fluid bed → by the fluid bed side multiple spot spray gun liquid material ejection fog-like liquid of naming a person for a particular job from top to bottom, be sprayed onto on the trickle solid material body of boiling), the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, the bed temperature that the spraying of control Sucralose disperses is 35～50 ℃, and the Sucralose even spraying is dispersed on the mixing sugar alcohol crystalline solid of powder; The rising bed temperature, at mixing sugar alcohol after fluidisation loses surface crystallization water, pump into the above-mentioned oligoisomaltose solution that refines again, continuous spray drying granulation, the bed temperature of maltodextrin mist projection granulating controlled well is 50～80 ℃, and the maltodextrin spray drying granulation is on the noncrystalline fluffy body of sugar alcohol; Obtain fluffy the shape product that even sugariness is modified.
Embodiment 1:
8 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel heating reaction pot for 20 kilograms, 0.83 kilogram of Sucralose and deionized water are also dissolved in another stainless steel heating reaction pot for 10 kilograms, material is heated to 62 ℃ by chuck in the pot, start stirring, add 1 kilogram of active carbon respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; 24 kilograms of xylitols, 35 kilograms of antierythrites, 32.17 kilograms of oligoisomaltoses, pulverizing reaches 130 orders through pulverizer, be sent in the spray-fluidized bed apparatus, xylitol, the mixed material of antierythrite and oligoisomaltose enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, control fluidized-bed layer temperature is 35～50 ℃, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, at xylitol, antierythrite, after the mixing of oligoisomaltose alcohol fluidisation loses surface crystallization water, pump into the above-mentioned oligoisomaltose solution that refines, continuously spray drying granulation, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
Embodiment 2:
8 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel heating reaction pot for 25 kilograms, 1.17 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel reaction pot for 15 kilograms, material is heated to 52 ℃ by chuck in the pot, start stirring, add 2 kilograms of active carbons respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; 25 kilograms of xylitols, 30 kilograms of antierythrites, 35.83 kilograms of oligoisomaltoses, reach 150 orders through pulverizing, be sent to and carry out the fluidisation mixing in the spray-fluidized bed apparatus, xylitol, the mixed material of antierythrite and oligoisomaltose enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, 35～40 ℃ of control fluidized-bed layer temperature, even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, after making the mixing of above-mentioned various sugar alcohol alcohol fluidisation lose surface crystallization water, pumping into the above-mentioned oligoisomaltose solution that refines, continuously spray granulating and drying, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
Embodiment 3:
8 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel heating reaction pot for 25 kilograms, 1 kilogram of Sucralose and deionized water are also dissolved in another stainless steel heating reaction pot for 15 kilograms, material is heated to 60 ℃ by chuck in the pot, start stirring, add 2.0 kilograms of active carbons respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; 21 kilograms of xylitols, 23 kilograms of antierythrites, 47 kilograms of oligoisomaltoses, pulverizing reaches 160 orders through pulverizer, be sent in the spray-fluidized bed apparatus, xylitol, the mixed material of antierythrite and oligoisomaltose enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, control 35～42 ℃ of fluidized-bed layer temperature well, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, after the mixing of above-mentioned various sugar alcohol alcohol fluidisations loses surface crystallization water, pump into the above-mentioned oligoisomaltose solution that refines, continuously spray drying granulation, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
Embodiment 4:
8 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel heating reaction pot for 25 kilograms, 15 kilograms also another dissolves in stainless steel heating reaction pot with 1.17 kilograms of Sucraloses and deionized water, material is heated to 80 ℃ by chuck in the pot, start stirring, add 2.0 kilograms of active carbons respectively, be incubated 35 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; 28.83 kilograms of xylitols, 35 kilograms of antierythrites, 27 kilograms of oligoisomaltoses, pulverizing reaches 180 orders through pulverizer, be sent to fluidisation in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, control 35～50 ℃ of fluidized-bed layer temperature well, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, after above-mentioned various sugar alcohol alcohol fluidisations lose surface crystallization water, pumping into the above-mentioned oligoisomaltose solution that refines, the combination drying granulation of spraying continuously, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is adornd.
Embodiment 5:
8 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel heating reaction pot for 20 kilograms, 1.34 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel heating reaction pot for 15 kilograms, material is heated to 62 ℃ by chuck in the pot, start stirring, add 2 kilograms of active carbons respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; 20 kilograms of xylitols, 30 kilograms of antierythrites, 40.76 kilograms of oligoisomaltoses, pulverizing reaches 130 orders through pulverizer, be sent in the spray-fluidized bed apparatus, xylitol, the mixed material of antierythrite and oligoisomaltose enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, control fluidized-bed layer temperature is 35～50 ℃, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, at xylitol, antierythrite, after the mixing of oligoisomaltose alcohol fluidisation loses surface crystallization water, pump into the above-mentioned oligoisomaltose solution that refines, continuously spray drying granulation, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
Embodiment 6:
8 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel heating reaction pot for 25 kilograms, 1.66 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel reaction pot for 20 kilograms, material is heated to 52 ℃ by chuck in the pot, start stirring, add 2 kilograms of active carbons respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; 20 kilograms of xylitols, 23.34 kilograms of antierythrites, 47 kilograms of oligoisomaltoses, reach 150 orders through pulverizing, be sent to and carry out the fluidisation mixing in the spray-fluidized bed apparatus, xylitol, the mixed material of antierythrite and oligoisomaltose enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, 35～40 ℃ of control fluidized-bed layer temperature, even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, after making the mixing of above-mentioned various sugar alcohol alcohol fluidisation lose surface crystallization water, pumping into the above-mentioned oligoisomaltose solution that refines, continuously spray granulating and drying, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
After testing, the fluffy granular composite low-sugar and low-calorie sweetener that adopts technical solution of the present invention to obtain, its main performance index sees Table 1.
Table 1
| Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Embodiment 6 |
| Particle size | 30～60 orders | 30～60 orders | 30～60 orders | 30～60 orders | 30～60 orders | 30～60 orders |
| Sugariness (sucrose contrast) | 5 times | 7 times | 6 times | 7 times | 8 times | 10 times |
| Outward appearance | White particle | White particle | White particle | White particle | White particle | White particle |
| Bulk density (g/mm 3) | ??0.60 | ??0.62 | ??0.63 | ??0.66 | ??0.60 | ??0.62 |
The stability test of sweetener is to check sweetener to guarantee the ability that undergoes no deterioration within a certain period of time, and the sweetener product of the embodiment of the invention was stored 3 years at normal temperatures, phenomenons such as rotten and sugariness reduction occur, and stability is very superior.
The sugariness degree of modification of fluffy granular composite sugar-free table sweetener of the present invention, will be according to the adjustment of Sucralose in consumption, in use unrestricted, usually select the common sucrose sugariness for use 5～10 times, the use needs that relatively are fit to people, form according to prescription, under same sugariness situation, people are almost nil to the absorption of heat, Sugarless mensal sweetening material is the sweet taste product of low-calorie, this dining table sweetener can not cause blood sugar to raise, and does not participate in metabolism, not carious tooth, satisfy diabetes patient, three high crowds, pursue healthy people's needs.
Show obviously that to sum up the present invention adopts scientific formula, uses advanced science and technology technology and method, products obtained therefrom does not have smell, do not have color, and is soluble in water, and it is very convenient that this fluffy granule-shaped sugar-free dining table sweetener is used.Granularity, molten speed, mouthfeel, sugariness all are much better than the prior art value, and the scientific preparation process simple flow is easily gone, and are fit to very much large-scale production, are worth wide popularization and application in the field of business.
What need understand is: the above only is a preferred implementation of the present invention; for those skilled in the art; under the prerequisite that does not break away from the principle of the invention, can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (5)
1. fluffy granular composite sugar-free table sweetener is characterized in that comprising following composition (percentage by weight): xylitol 20～30%, antierythrite 20～35%, oligoisomaltose 35～55%, Sucralose 0.8～1.2%.
2. fluffy granular composite sugar-free table sweetener according to claim 1 is characterized in that its component has following percentage by weight: xylitol 25%, antierythrite 30%, oligoisomaltose 43.83%, Sucralose 1.17%.
3. the preparation method of the described fluffy granular composite sugar-free table sweetener of claim 1 is characterized in that: comprise following processing step---
1. with 8% oligoisomaltose, Sucralose joins respectively in the heating container, adds deionized water respectively and mixes;
2. be warming up to 52～80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned maltodextrin solution and the sucralose solution, be incubated 25～30 minutes, filter while hot, filtrate is pooled in the storage tank of heat tracing stand-by respectively;
4. with xylitol, antierythrite and oligoisomaltose are put in the spray-fluidized bed apparatus after pulverizing, xylitol, the mixed material of antierythrite and oligoisomaltose enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, pump into the above-mentioned oligoisomaltose solution that refines again, spray-drying obtains fluffy granular composite sugar-free table sweetener continuously.
4. the preparation method of fluffy granular composite sugar-free table sweetener according to claim 3, it is characterized in that: with 8% oligoisomaltose, Sucralose joins respectively in the container, adds deionized water respectively and mixes; Be warming up to 60～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank that has heat tracing; Xylitol, antierythrite and oligoisomaltose reach 120～180 orders through pulverizing, be sent in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, control fluidized-bed layer temperature is at 35～80 ℃, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, after the mixing of sugar alcohol fluidisation loses surperficial moisture content, pump into the above-mentioned oligoisomaltose solution that refines again, spray drying granulation obtains fluffy granular composite sugar-free table sweetener continuously.
5. the preparation method of fluffy granular composite sugar-free table sweetener according to claim 4, it is characterized in that: the bed temperature scope of described fluidized bed with spraying is 35～80 ℃, wherein the bed temperature of phase I Sucralose spraying dispersion is 35～50 ℃, and the bed temperature of second stage oligoisomaltose mist projection granulating is 50～80 ℃.
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| CN102423062A (en) * | 2011-12-15 | 2012-04-25 | 苏州工业园区尚融科技有限公司 | Fluffy granular composite sugar-free sweetening material and preparation method thereof |
| CN102429204A (en) * | 2011-12-09 | 2012-05-02 | 苏州工业园区尚融科技有限公司 | Fluffy granular compound sugar-free sweetening agent and preparation method thereof |
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| CN102440370A (en) * | 2011-12-20 | 2012-05-09 | 苏州工业园区尚融科技有限公司 | Composite sugar-free sweetener and preparation method thereof |
| CN102440348A (en) * | 2011-12-09 | 2012-05-09 | 苏州工业园区尚融科技有限公司 | Fluffy powdery composite sugar-free table sugar and preparation method thereof |
| CN102960683A (en) * | 2012-11-30 | 2013-03-13 | 苏州工业园区尚融科技有限公司 | Sugar-free compound sweetener suitable for neutral solid beverage and preparation method of sugar-free compound sweetener |
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| CN1226948C (en) * | 2003-06-10 | 2005-11-16 | 郑书旺 | Sanlitian harmonious sugar composition-stevia rebaudianum |
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| CN102429204A (en) * | 2011-12-09 | 2012-05-02 | 苏州工业园区尚融科技有限公司 | Fluffy granular compound sugar-free sweetening agent and preparation method thereof |
| CN102440369A (en) * | 2011-12-09 | 2012-05-09 | 苏州工业园区尚融科技有限公司 | Fluffy powdery composite sugar-free sweetener and preparation method thereof |
| CN102440348A (en) * | 2011-12-09 | 2012-05-09 | 苏州工业园区尚融科技有限公司 | Fluffy powdery composite sugar-free table sugar and preparation method thereof |
| CN102423062A (en) * | 2011-12-15 | 2012-04-25 | 苏州工业园区尚融科技有限公司 | Fluffy granular composite sugar-free sweetening material and preparation method thereof |
| CN102440370A (en) * | 2011-12-20 | 2012-05-09 | 苏州工业园区尚融科技有限公司 | Composite sugar-free sweetener and preparation method thereof |
| CN103190555A (en) * | 2012-01-05 | 2013-07-10 | 桂林三金集团股份有限公司 | Sugar cubes and preparation method thereof |
| CN103190555B (en) * | 2012-01-05 | 2014-06-04 | 桂林三金集团股份有限公司 | Sugar cubes and preparation method thereof |
| CN102960683A (en) * | 2012-11-30 | 2013-03-13 | 苏州工业园区尚融科技有限公司 | Sugar-free compound sweetener suitable for neutral solid beverage and preparation method of sugar-free compound sweetener |
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