CN101874607A - Granular composite low-sugar low-calorie sweetener and preparation method thereof - Google Patents
Granular composite low-sugar low-calorie sweetener and preparation method thereof Download PDFInfo
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- CN101874607A CN101874607A CN2009102520550A CN200910252055A CN101874607A CN 101874607 A CN101874607 A CN 101874607A CN 2009102520550 A CN2009102520550 A CN 2009102520550A CN 200910252055 A CN200910252055 A CN 200910252055A CN 101874607 A CN101874607 A CN 101874607A
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- 239000002131 composite material Substances 0.000 title claims abstract description 27
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 235000013615 non-nutritive sweetener Nutrition 0.000 title claims abstract description 14
- 238000005507 spraying Methods 0.000 claims abstract description 57
- 229920002774 Maltodextrin Polymers 0.000 claims abstract description 43
- 235000019408 sucralose Nutrition 0.000 claims abstract description 43
- SPFMQWBKVUQXJV-BTVCFUMJSA-N (2r,3s,4r,5r)-2,3,4,5,6-pentahydroxyhexanal;hydrate Chemical compound O.OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C=O SPFMQWBKVUQXJV-BTVCFUMJSA-N 0.000 claims abstract description 40
- 235000010447 xylitol Nutrition 0.000 claims abstract description 39
- 239000000463 material Substances 0.000 claims abstract description 37
- 239000005913 Maltodextrin Substances 0.000 claims abstract description 36
- 229940035034 maltodextrin Drugs 0.000 claims abstract description 36
- 229960000673 dextrose monohydrate Drugs 0.000 claims abstract description 33
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 claims abstract description 32
- TVXBFESIOXBWNM-UHFFFAOYSA-N Xylitol Natural products OCCC(O)C(O)C(O)CCO TVXBFESIOXBWNM-UHFFFAOYSA-N 0.000 claims abstract description 32
- HEBKCHPVOIAQTA-UHFFFAOYSA-N meso ribitol Natural products OCC(O)C(O)C(O)CO HEBKCHPVOIAQTA-UHFFFAOYSA-N 0.000 claims abstract description 32
- 239000000811 xylitol Substances 0.000 claims abstract description 32
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 claims abstract description 32
- 229960002675 xylitol Drugs 0.000 claims abstract description 32
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 30
- 150000005846 sugar alcohols Chemical class 0.000 claims abstract description 23
- 238000010438 heat treatment Methods 0.000 claims abstract description 21
- 239000008367 deionised water Substances 0.000 claims abstract description 20
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 20
- 238000002156 mixing Methods 0.000 claims abstract description 14
- 239000000706 filtrate Substances 0.000 claims abstract description 13
- 238000003860 storage Methods 0.000 claims abstract description 13
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000004376 Sucralose Substances 0.000 claims description 33
- BAQAVOSOZGMPRM-QBMZZYIRSA-N sucralose Chemical compound O[C@@H]1[C@@H](O)[C@@H](Cl)[C@@H](CO)O[C@@H]1O[C@@]1(CCl)[C@@H](O)[C@H](O)[C@@H](CCl)O1 BAQAVOSOZGMPRM-QBMZZYIRSA-N 0.000 claims description 33
- 239000012530 fluid Substances 0.000 claims description 28
- 238000009835 boiling Methods 0.000 claims description 16
- 238000005243 fluidization Methods 0.000 claims description 16
- 239000007921 spray Substances 0.000 claims description 15
- 238000003756 stirring Methods 0.000 claims description 12
- 238000005469 granulation Methods 0.000 claims description 11
- 230000003179 granulation Effects 0.000 claims description 11
- 238000010298 pulverizing process Methods 0.000 claims description 11
- 238000001694 spray drying Methods 0.000 claims description 11
- 239000003595 mist Substances 0.000 claims description 10
- 239000000203 mixture Substances 0.000 claims description 10
- 229910052799 carbon Inorganic materials 0.000 claims description 7
- 238000010792 warming Methods 0.000 claims description 5
- 239000006185 dispersion Substances 0.000 claims description 3
- 239000000047 product Substances 0.000 abstract description 18
- 235000003599 food sweetener Nutrition 0.000 abstract description 10
- 239000003765 sweetening agent Substances 0.000 abstract description 10
- 229930006000 Sucrose Natural products 0.000 abstract description 6
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 abstract description 6
- 229960004793 sucrose Drugs 0.000 abstract description 6
- 238000001035 drying Methods 0.000 abstract description 5
- 238000005086 pumping Methods 0.000 abstract description 4
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 abstract 3
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 abstract 2
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- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 7
- 238000005516 engineering process Methods 0.000 description 7
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Abstract
The invention relates to a granular composite low-sugar low-calorie sweetener and a preparation method thereof. The sweetener comprises the following components in percentage by weight: 30 to 55 percent of dextrose monohydrate, 20 to 25 percent of sorbitol, 10 to 20 percent of xylitol, 2 to 4 percent of maltodextrin, and 8 to 35 percent of splenda. The preparation method comprises the steps of: adding the maltodextrin and the splenda into heating containers respectively, adding deionized water into the heating containers and mixing respectively, and heating to dissolve the solution; adding activated carbon into the solution respectively, filtering the solution when the solution is hot, and collecting the filtrate in the two heating containers into a storage tank; allowing the mixed materials of crushed dextrose monohydrate, xylitol, and sorbitol to enter a spraying fluidized bed from the bottom with positive pressure and accelerating the flow from bottom to top, and applying negative pressure to the upper part of the spraying fluidized bed to vibrate from top to down, so that the materials boil up and down in the spraying fluidized bed; and continuously spraying and dispersing refined solution of splenda on superfine sugar alcohol by using a multipoint spay gun on the side of the fluidized bed, pumping solution of maltodextrin, and continuously spraying and drying to obtain the low-sugar low-calorie sweetener. The sweetness of the product is 50 to 200 times that of the common cane sugar.
Description
Technical field
The present invention relates to a kind of edible sweetener, relate in particular to a kind of fluffy granular composite low-sugar and low-calorie sweetener and preparation method thereof.
Background technology
Along with the increase of people because of too much bringing disease, people's demand safety, healthy low-sugar-content and low-calorie type sweetener with sugar; In production procedure, reach from raw material and put into the advanced preparation technology that finished product one step finishes; It is learnt from other's strong points to offset one's weaknesses, has complementary advantages to make between the sugar alcohol sweet taste on the formula for a product, can play during product uses and cover the effect that promotes mouthfeel with synergy, people thirst for satisfying under the low prerequisite of sugariness height, heat, and occupation modeization, with cane-sugar taste safety and Health low-sugar-content and low-calorie type sweetener roughly the same.
Summary of the invention
The objective of the invention is to overcome the deficiency that prior art exists, a kind of fluffy granular composite low-sugar and low-calorie sweetener and preparation method thereof is provided, adopt the scientific technology of easy operation control, the molten speed of product, mouthfeel, sugariness all are higher than the prior art optimum value.
Purpose of the present invention is achieved through the following technical solutions:
A kind of granular composite low-sugar low-calorie sweetner, characteristics are to comprise following composition (percentage by weight): Dextrose Monohydrate 30~55%, D-sorbite 20~25%, xylitol 10~20%, maltodextrin 2~4%, Sucralose 8~35%.
Further, above-mentioned a kind of granular composite low-sugar low-calorie sweetner, wherein, Dextrose Monohydrate 30%, D-sorbite 20%, maltodextrin 5%, xylitol 10%, Sucralose 35%.
Further, above-mentioned a kind of granular composite low-sugar low-calorie sweetner, described maltodextrin DE value is 10~20.
The preparation method of granular composite low-sugar low-calorie sweetner of the present invention comprises following processing step:
1. maltodextrin, Sucralose are joined respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 52~80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned maltodextrin solution and the sucralose solution, be incubated 25~30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank of heat tracing;
4. with Dextrose Monohydrate, xylitol and D-sorbite are put in the spray-fluidized bed apparatus after pulverizing, Dextrose Monohydrate, the mixed material of xylitol and D-sorbite enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, pump into the above-mentioned maltodextrin solution that refines again, spray-drying obtains fluffy granular composite low-sugar and low-calorie sweetener continuously.
Again further, the preparation method of above-mentioned a kind of granular composite low-sugar low-calorie sweetner joins maltodextrin, Sucralose respectively in the heating container, adds deionized water respectively and mixes; Be warming up to 60~80 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank that has heat tracing; Dextrose Monohydrate and D-sorbite reach 120~180 orders through pulverizing, be sent in the spray-fluidized bed apparatus, Dextrose Monohydrate, the mixed material of xylitol and D-sorbite enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, control fluidized-bed layer temperature is at 35~80 ℃, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, after the mixing of sugar alcohol fluidisation loses surperficial moisture content, pump into the above-mentioned maltodextrin solution that refines again, spray drying granulation obtains fluffy granular composite low-sugar and low-calorie sweetener continuously.
Again further, the preparation method of above-mentioned a kind of granular composite low-sugar low-calorie sweetner, the bed temperature scope of described fluidized bed with spraying is 35~80 ℃, wherein the bed temperature of phase I Sucralose spraying dispersion is 35~50 ℃, and the bed temperature of second stage maltodextrin mist projection granulating is 50~80 ℃.
Again further, the preparation method of above-mentioned a kind of granular composite low-sugar low-calorie sweetner, in the phase I of described spraying mixed fluidized bed, the Sucralose spraying is dispersed in fluidisation and smashes on the fine sugar alcohol crystal body; In second stage, the maltodextrin spray drying granulation is on the noncrystal of mixing sugar alcohol.
Substantive distinguishing features and obvious improvement that technical solution of the present invention is outstanding are mainly reflected in:
The negative pressure fluid bed fluidization technique that adopts scientific formula, uses advanced is in conjunction with the multi-point atomizing method, and time sharing segment control appliance bed temperature efficiently solves even dispersion, coats problems such as granulation, drying.With Dextrose Monohydrate, D-sorbite, xylitol, Sucralose is primary raw material; modify uniformly and coat by preparation method to sugariness; make product sweetness reach 50~200 times of common sucrose; products obtained therefrom does not have smell, does not have color; soluble in water; this fluffy granular composite low-sugar and low-calorie sweetener is easy to use, and its preparation process science is simple and easy to operate, is fit to very much large-scale production.
Description of drawings
Below in conjunction with accompanying drawing technical solution of the present invention is described further:
Fig. 1: process chart of the present invention.
The specific embodiment
Fluffy granular composite low-sugar and low-calorie sweetener of the present invention, its composition is: Dextrose Monohydrate 30~55%, D-sorbite 20~25%, xylitol 10~20%, maltodextrin 2~4%, Sucralose 8~35%.Ideal formulations is: Dextrose Monohydrate 30%, D-sorbite 20%, maltodextrin 5%, xylitol 10%, Sucralose 35%.
As shown in Figure 1, the preparation technology of fluffy granular composite low-sugar and low-calorie sweetener: at first, maltodextrin, Sucralose are joined respectively in the heating container, add deionized water respectively and mix; Be warming up to 52~80 ℃ of dissolvings respectively, and stir; Add active carbon in above-mentioned maltodextrin solution and the sucralose solution respectively, be incubated 25~30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank of heat tracing; At last, with Dextrose Monohydrate, put into after xylitol and D-sorbite are pulverized in the spray-fluidized bed apparatus (heating temperature control and by the positive negative pressure boiling of equipment technology with the boiling that in fluid bed, circulates of sugar alcohol material, mix that fluidisation is anhydrated and fluffy processing, sugar alcohol mixtures material → malleation material quickens to flow from bottom to top → and negative pressure vibrates → makes material boiling up and down in fluid bed → by the fluid bed side multiple spot spray gun liquid material ejection fog-like liquid of naming a person for a particular job from top to bottom, be sprayed onto on the trickle solid material body of boiling), Dextrose Monohydrate, the mixed material of xylitol and D-sorbite enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, the bed temperature that the spraying of control Sucralose disperses is 35~50 ℃, and the Sucralose even spraying is dispersed on the mixing sugar alcohol crystalline solid of powder; The rising bed temperature, at mixing sugar alcohol after fluidisation loses surface crystallization water, pump into the above-mentioned maltodextrin solution that refines again, continuous spray drying granulation, the bed temperature of maltodextrin mist projection granulating controlled well is 50~80 ℃, and the maltodextrin spray drying granulation is on the noncrystalline fluffy body of sugar alcohol; Obtain fluffy the shape product that even sugariness is modified.
Embodiment 1:
5 kilograms of maltodextrins and deionized water are dissolved in a stainless steel heating reaction pot for 20 kilograms, 8.8 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel heating reaction pot for 27 kilograms, material is heated to 62 ℃ by chuck in the pot, start stirring, add 1 kilogram of active carbon respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; 55 kilograms of Dextrose Monohydrates, 21.2 kilograms of D-sorbites, 10 kilograms of xylitols, pulverizing reaches 130 orders through pulverizer, be sent in the spray-fluidized bed apparatus, Dextrose Monohydrate, the mixed material of xylitol and D-sorbite enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, control fluidized-bed layer temperature is 35~50 ℃, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50~80 ℃ again, at Dextrose Monohydrate, xylitol, after the mixing of D-sorbite alcohol fluidisation loses surface crystallization water, pump into the above-mentioned maltodextrin solution that refines, continuously spray drying granulation, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
Embodiment 2:
2.5 kilograms of maltodextrins and deionized water are dissolved in a stainless steel heating reaction pot for 25 kilograms, 17.5 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel reaction pot for 25 kilograms, material is heated to 52 ℃ by chuck in the pot, start stirring, add 2 kilograms of active carbons respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; 50 kilograms of Dextrose Monohydrates, 20 kilograms of D-sorbites, 10 kilograms of xylitols, reach 150 orders through pulverizing, be sent to and carry out the fluidisation mixing in the spray-fluidized bed apparatus, Dextrose Monohydrate, the mixed material of xylitol and D-sorbite enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, 35~40 ℃ of control fluidized-bed layer temperature, even spraying is disperseed, after operation is finished, improve bed temperature to 50~80 ℃ again, make Dextrose Monohydrate, xylitol, after the mixing of D-sorbite alcohol fluidisation loses surface crystallization water, pumping into the above-mentioned maltodextrin solution that refines, continuously spray granulating and drying, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
Embodiment 3:
3 kilograms of maltodextrins and deionized water are dissolved in a stainless steel heating reaction pot for 25 kilograms, 26.4 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel heating reaction pot for 30 kilograms, material is heated to 60 ℃ by chuck in the pot, start stirring, add 3.0 kilograms of active carbons respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; 33.6 kilograms of Dextrose Monohydrates, 20 kilograms of D-sorbites, 17 kilograms of xylitols, pulverizing reaches 160 orders through pulverizer, be sent in the spray-fluidized bed apparatus, Dextrose Monohydrate, the mixed material of xylitol and D-sorbite enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, control 35~42 ℃ of fluidized-bed layer temperature well, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50~80 ℃ again, at Dextrose Monohydrate, xylitol, after the mixing of D-sorbite alcohol fluidisation loses surface crystallization water, pump into the above-mentioned maltodextrin solution that refines, continuously spray drying granulation, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
Embodiment 4:
5 kilograms of maltodextrins and deionized water are dissolved in a stainless steel heating reaction pot for 25 kilograms, 50 kilograms also another dissolves in stainless steel heating reaction pot with 35 kilograms of Sucraloses and deionized water, material is heated to 80 ℃ by chuck in the pot, start stirring, add 3.0 kilograms of active carbons respectively, be incubated 35 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; 30 kilograms of Dextrose Monohydrates, 20 kilograms of D-sorbites, 10 kilograms of xylitols, pulverizing reaches 180 orders through pulverizer, be sent to fluidisation in the spray-fluidized bed apparatus, Dextrose Monohydrate, the mixed material of xylitol and D-sorbite enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, control 35~50 ℃ of fluidized-bed layer temperature well, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50~80 ℃ again, at Dextrose Monohydrate, xylitol, after D-sorbite alcohol fluidisation loses surface crystallization water, pumping into the above-mentioned maltodextrin solution that refines, the combination drying granulation of spraying continuously, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is adornd.
Embodiment 5:
5 kilograms of maltodextrins and deionized water are dissolved in a stainless steel heating reaction pot for 20 kilograms, 10 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel heating reaction pot for 27 kilograms, material is heated to 62 ℃ by chuck in the pot, start stirring, add 1 kilogram of active carbon respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; 55 kilograms of Dextrose Monohydrates, 20 kilograms of D-sorbites, 10 kilograms of xylitols, pulverizing reaches 130 orders through pulverizer, be sent in the spray-fluidized bed apparatus, Dextrose Monohydrate, the mixed material of xylitol and D-sorbite enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, control fluidized-bed layer temperature is 35~50 ℃, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50~80 ℃ again, at Dextrose Monohydrate, xylitol, after the mixing of D-sorbite alcohol fluidisation loses surface crystallization water, pump into the above-mentioned maltodextrin solution that refines, continuously spray drying granulation, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
Embodiment 6:
5 kilograms of maltodextrins and deionized water are dissolved in a stainless steel heating reaction pot for 25 kilograms, 20 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel reaction pot for 30 kilograms, material is heated to 52 ℃ by chuck in the pot, start stirring, add 2 kilograms of active carbons respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; 45 kilograms of Dextrose Monohydrates, 20 kilograms of D-sorbites, 10 kilograms of xylitols, reach 150 orders through pulverizing, be sent to and carry out the fluidisation mixing in the spray-fluidized bed apparatus, Dextrose Monohydrate, the mixed material of xylitol and D-sorbite enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, 35~40 ℃ of control fluidized-bed layer temperature, even spraying is disperseed, after operation is finished, improve bed temperature to 50~80 ℃ again, make Dextrose Monohydrate, xylitol, after the mixing of D-sorbite alcohol fluidisation loses surface crystallization water, pumping into the above-mentioned maltodextrin solution that refines, continuously spray granulating and drying, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
Embodiment 7:
4 kilograms of maltodextrins and deionized water are dissolved in a stainless steel heating reaction pot for 20 kilograms, 30 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel heating reaction pot for 40 kilograms, material is heated to 60 ℃ by chuck in the pot, start stirring, add 3.0 kilograms of active carbons respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; 36 kilograms of Dextrose Monohydrates, 20 kilograms of D-sorbites, 10 kilograms of xylitols, pulverizing reaches 160 orders through pulverizer, be sent in the spray-fluidized bed apparatus, Dextrose Monohydrate, the mixed material of xylitol and D-sorbite enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, control 35~42 ℃ of fluidized-bed layer temperature well, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50~80 ℃ again, at Dextrose Monohydrate, xylitol, after the mixing of D-sorbite alcohol fluidisation loses surface crystallization water, pump into the above-mentioned maltodextrin solution that refines, continuously spray drying granulation, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
After testing, the fluffy granular composite low-sugar and low-calorie sweetener that adopts technical solution of the present invention to obtain, its main performance index sees Table 1.
Table 1
Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Embodiment 6 | Embodiment 7 |
Particle size | 30~60 orders | 30~60 orders | 30~60 orders | 30~60 orders | 30~60 orders | 30~60 orders | 30~60 orders |
Sugariness (sucrose contrast) | 50 times | 120 times | 150 times | 200 times | 80 times | 120 times | 180 times |
Outward appearance | White particle | White particle | White particle | White particle | White particle | White particle | White particle |
Bulk density (g/mm 3) | ??0.61 | ??0.62 | ??0.63 | ??0.66 | ??0.60 | ??0.62 | ??0.64 |
The stability test of sweetener is to check sweetener to guarantee the ability that undergoes no deterioration within a certain period of time, and the sweetener product of the embodiment of the invention was stored 3 years at normal temperatures, phenomenons such as rotten and sugariness reduction occur, and stability is very superior.
The sugariness degree of modification of fluffy granular composite low-sugar and low-calorie sweetener of the present invention, will be according to the adjustment of Sucralose in consumption, usually select the common sucrose sugariness for use 50~200 times, the use needs that relatively are fit to food enterprise, form according to prescription, under same sugariness situation, people only are 1/50~1/200 of common sucrose to the absorption of heat, low-sugar-content and low-calorie sweetening agent is the sweet taste product of low-calorie, this sweetener can not cause blood sugar to raise, and satisfies three high crowds, the healthy people's of pursuit needs.
Show obviously that to sum up the present invention adopts scientific formula, uses advanced science and technology technology and method, products obtained therefrom does not have smell, do not have color, and is soluble in water, and it is very convenient that this fluffy granular low-sugar-content and low-calorie sweetening agent is used.Granularity, molten speed, mouthfeel, sugariness all are much better than the prior art value, and the scientific preparation process simple flow is easily gone, and are fit to very much large-scale production, are worth wide popularization and application in the field of business.
What need understand is: the above only is a preferred implementation of the present invention; for those skilled in the art; under the prerequisite that does not break away from the principle of the invention, can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (6)
1. a granular composite low-sugar low-calorie sweetner is characterized in that comprising following composition (percentage by weight): Dextrose Monohydrate 30~55%, D-sorbite 20~25%, xylitol 10~20%, maltodextrin 2~4%, Sucralose 8~35%.
2. a kind of granular composite low-sugar low-calorie sweetner according to claim 1 is characterized in that its component has following percentage by weight: Dextrose Monohydrate 30%, D-sorbite 20%, maltodextrin 5%, xylitol 10%, Sucralose 35%.
3. a kind of granular composite low-sugar low-calorie sweetner according to claim 1 and 2 is characterized in that: described maltodextrin DE value is 10~20.
4. the preparation method of the described a kind of granular composite low-sugar low-calorie sweetner of claim 1 is characterized in that: comprise following processing step---
1. maltodextrin, Sucralose are joined respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 52~80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned maltodextrin solution and the sucralose solution, be incubated 25~30 minutes, filter while hot, filtrate is pooled in the storage tank of heat tracing stand-by respectively;
4. with Dextrose Monohydrate, xylitol and D-sorbite are put in the spray-fluidized bed apparatus after pulverizing, Dextrose Monohydrate, the mixed material of xylitol and D-sorbite enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, pump into the above-mentioned maltodextrin solution that refines again, spray-drying obtains fluffy granular composite low-sugar and low-calorie sweetener continuously.
5. the preparation method of a kind of granular composite low-sugar low-calorie sweetner according to claim 4 is characterized in that: maltodextrin, Sucralose are joined respectively in the container, add deionized water respectively and mix; Be warming up to 60~80 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank that has heat tracing; Dextrose Monohydrate, xylitol and D-sorbite reach 120~180 orders through pulverizing, be sent in the spray-fluidized bed apparatus, Dextrose Monohydrate, the mixed material of xylitol and D-sorbite enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, control fluidized-bed layer temperature is at 35~80 ℃, the multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously earlier and is distributed on the fine sugar alcohol body, after the mixing of sugar alcohol fluidisation loses surperficial moisture content, pump into the above-mentioned maltodextrin solution that refines again, spray drying granulation obtains fluffy granular composite low-sugar and low-calorie sweetener continuously.
6. the preparation method of a kind of granular composite low-sugar low-calorie sweetner according to claim 5, it is characterized in that: the bed temperature scope of described fluidized bed with spraying is 35~80 ℃, wherein the bed temperature of phase I Sucralose spraying dispersion is 35~50 ℃, and the bed temperature of second stage maltodextrin mist projection granulating is 50~80 ℃.
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Cited By (5)
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CN102429029A (en) * | 2011-12-20 | 2012-05-02 | 苏州工业园区尚融科技有限公司 | Production method of low-sugar fruit juice milk |
CN102940236A (en) * | 2012-11-30 | 2013-02-27 | 苏州工业园区尚融科技有限公司 | Compound sweetener suitable for refreshing neutral beverage and preparation method thereof |
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CN102429029A (en) * | 2011-12-20 | 2012-05-02 | 苏州工业园区尚融科技有限公司 | Production method of low-sugar fruit juice milk |
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CN102960700A (en) * | 2012-11-30 | 2013-03-13 | 苏州工业园区尚融科技有限公司 | Compound sweetener suitable for neutral beverage and preparation method thereof |
CN106723059A (en) * | 2017-02-10 | 2017-05-31 | 苏州工业园区尚融科技有限公司 | A kind of low-calorie health sugar and preparation method thereof |
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