CN102987332A - Compound low-sugar sweetening agent and preparation method thereof - Google Patents
Compound low-sugar sweetening agent and preparation method thereof Download PDFInfo
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- CN102987332A CN102987332A CN2011104079663A CN201110407966A CN102987332A CN 102987332 A CN102987332 A CN 102987332A CN 2011104079663 A CN2011104079663 A CN 2011104079663A CN 201110407966 A CN201110407966 A CN 201110407966A CN 102987332 A CN102987332 A CN 102987332A
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Abstract
The invention relates to a compound low-sugar sweetening agent and a preparation method thereof. The compound low-sugar sweetening agent comprises the following ingredients in percentage by weight: 45 to 90 percent of dextrose monohydrate, 0 to 20 percent of sorbitol, 5 to 20 percent of maltodextrin and 3.33 to 16.7 percent of sucralose. The preparation method comprises the following steps of: adding the maltodextrin and the sucralose into a heating container respectively, adding deionized water into the heating container and mixing respectively, and raising the temperature to dissolve the maltodextrin and the sucralose; adding activated carbon into the solution respectively, filtering while the solution is hot, and collecting the filtrate into a storage tank respectively; and introducing a mixture of smashed dextrose monohydrate and sorbitol into a spray fluidized bed from the bottom of the spray fluidized bed by applying a positive pressure, enabling the mixture to flow in an acceleratory mode from bottom to top, applying a negative pressure to the upper part of the spray fluidized bed to ensure that the spray fluidized bed vibrates from top to bottom and the mixture boils up and down in the spray fluidized bed, continuously spraying and dispersing the prepared sucralose solution to the superfine dextrose monohydrate and sorbitol by using a plurality of spray guns which are arranged at the side part of the spray fluidized bed, pumping the maltodextrin solution, and continuously spraying and drying to obtain the low-sugar and low-calorie sweetening agent. The sweetness of the low-sugar sweetening agent is 20 to 100 times that of common sucrose.
Description
Technical field
The present invention relates to a kind of edible sweetener, relate in particular to a kind of composite low-sugar sweetener and preparation method thereof.
Background technology
Because of the increase with chronic metabolic disease such as the too much inferior health that brings of sugar and cardiovascular and cerebrovasculars, people's demand is safe, healthy low-sugar-content and low-calorie type sweetener along with people; Reach in production procedure from raw material and put into the advanced preparation technology that one step of finished product completes; Make between sweet substance sweet sense learn from other's strong points to offset one's weaknesses, have complementary advantages on formula for a product, can play during product uses cover, the effect of synergy and lifting mouthfeel, people crave for and are satisfying under the prerequisite that sugariness is high, heat is low, easy to useization, with cane-sugar taste safety and Health low-sugar-content and low-calorie type sweetener roughly the same.
Summary of the invention
The objective of the invention is to overcome the deficiency that prior art exists, a kind of composite low-sugar sweetener and preparation method thereof is provided, adopt the scientific technology of easy operation control, the molten speed of product, mouthfeel, sugariness are all higher than the prior art optimum value.
Purpose of the present invention is achieved through the following technical solutions:
A kind of composite low-sugar sweetener, characteristics are to comprise following percentage by weight composition: Dextrose Monohydrate 45~90%, D-sorbite 0~20%, maltodextrin 5~20%, Sucralose 3.33~16.7%; Its preparation method comprises following processing step:
1. by composition proportion, maltodextrin, Sucralose are joined respectively in heating container, add respectively deionized water to mix;
2. be warming up to respectively 45~100 ℃ of dissolvings, and stir;
3. add respectively active carbon in above-mentioned maltodextrin solution and sucralose solution, be incubated 10~20 minutes, filter while hot, filtrate is pooled to respectively in the storage tank of heat tracing stand-by;
4. put in the spray-fluidized bed apparatus after by composition proportion, D-sorbite and Dextrose Monohydrate being pulverized, the mixed material of Dextrose Monohydrate and D-sorbite enters fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and accelerates from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is first sprayed the above-mentioned sucralose solution that refines continuously and is distributed on fine sugar alcohol body, pump into again the above-mentioned maltodextrin solution that refines, continuous spray-drying, obtain a kind of composite low-sugar sweetener.
Further, above-mentioned a kind of composite low-sugar sweetener, wherein, Dextrose Monohydrate 70%, D-sorbite 19.5%, maltodextrin 5.5%, Sucralose 5%.
Further, above-mentioned a kind of composite low-sugar sweetener, described maltodextrin DE value is 10~20.
The preparation method of a kind of composite low-sugar sweetener of the present invention comprises following processing step:
1. maltodextrin, Sucralose are joined respectively in heating container, add respectively deionized water to mix;
2. be warming up to respectively 45~100 ℃ of dissolvings, and stir;
3. add respectively active carbon in above-mentioned maltodextrin solution and sucralose solution, be incubated 10~20 minutes, filter while hot, filtrate is pooled to respectively in the storage tank of heat tracing stand-by;
4. will put in the spray-fluidized bed apparatus after D-sorbite and Dextrose Monohydrate pulverizing, the mixed material of Dextrose Monohydrate and D-sorbite enters fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and accelerates from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is first sprayed the above-mentioned sucralose solution that refines continuously and is distributed on fine sugar alcohol body, pump into again the above-mentioned maltodextrin solution that refines, continuous spray-drying, obtain a kind of composite low-sugar sweetener.
again further, the preparation method of above-mentioned a kind of composite low-sugar sweetener joins maltodextrin, Sucralose respectively in container, adds respectively deionized water to mix, be warming up to respectively 60~100 ℃ of dissolvings, and stir, add respectively active carbon, be incubated 10 minutes, filter while hot, filtrate is pooled to respectively in storage tank with heat tracing, Dextrose Monohydrate and D-sorbite reach 100~120 orders through pulverizing, be sent in the spray-fluidized bed apparatus, the mixed material of Dextrose Monohydrate and D-sorbite enters fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and accelerates from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, control the fluidisation EAT at 45~120 ℃, the multiple spot spray gun of fluid bed sidepiece is first sprayed the above-mentioned sucralose solution that refines continuously and is distributed on fine sugar alcohol body, after the mixing of sugar alcohol fluidisation loses surperficial moisture content, pump into again the above-mentioned maltodextrin solution that refines, continuous spray drying granulation, obtain a kind of composite low-sugar sweetener.
Again further, the preparation method of above-mentioned a kind of composite low-sugar sweetener, the EAT scope of described fluidized bed with spraying is 45~120 ℃, wherein the EAT of phase I Sucralose spraying dispersion is 45~95 ℃, 60~120 ℃ of the EATs of second stage maltodextrin mist projection granulating.
Again further, the preparation method of above-mentioned a kind of composite low-sugar sweetener, within the phase I of described spraying mixed fluidized bed, the Sucralose spraying is dispersed in fluidisation and smashes on fine sugar alcohol crystal body; In second stage, the maltodextrin spray drying granulation is on the noncrystal of mixing sugar alcohol.
The substantive distinguishing features that technical solution of the present invention is outstanding and significant progressive being mainly reflected in:
The negative-pressure fluidized-bed fluidization technique of the formula of employing science, uses advanced is in conjunction with the multi-point atomizing method, and time sharing segment control appliance EAT efficiently solves Uniform Dispersion, coats the problems such as granulation, drying.Take Dextrose Monohydrate, D-sorbite, Sucralose, maltodextrin as primary raw material; modify uniformly and coat by preparation method to sugariness; make product sweetness reach 20~100 times of common sucrose; products obtained therefrom does not have smell, there is no color; soluble in water; this fluffy granular composite low-sugar low-calorie sweetener is easy to use, and its preparation process science is simple and easy to operate, is fit to very much large-scale production.
The specific embodiment
A kind of composite low-sugar sweetener of the present invention, its composition is: Dextrose Monohydrate 45~90%, D-sorbite 0~20%, maltodextrin 5~20%, Sucralose 3.33~16.7%.Ideal formulations is: Dextrose Monohydrate 70%, D-sorbite 19.5%, maltodextrin 5.5%, Sucralose 5%.
A kind of preparation technology of composite low-sugar sweetener: at first, maltodextrin, Sucralose are joined respectively in heating container, add respectively deionized water to mix; Be warming up to respectively 45~100 ℃ of dissolvings, and stir; Add respectively active carbon in above-mentioned maltodextrin solution and sucralose solution, be incubated 10~20 minutes, filter while hot, filtrate is pooled to respectively in the storage tank of heat tracing; at last, after being pulverized, Dextrose Monohydrate and D-sorbite put in the spray-fluidized bed apparatus (heating temperature control and by the sugar alcohol material the is circulated boiling of equipment positive/negative-pressure boiling technology again in fluid bed, mix that fluidisation is anhydrated and fluffy processing, passing through again following steps: mixed material → malleation material accelerates to flow from bottom to top → and negative pressure vibrates → makes material boiling up and down in fluid bed → by the fluid bed side multiple spot spray gun liquid material ejection fog-like liquid of naming a person for a particular job from top to bottom, be sprayed onto on the trickle solids mixing material of boiling), the mixed material of Dextrose Monohydrate and D-sorbite enters fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and accelerates from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is first sprayed the above-mentioned sucralose solution that refines continuously and is distributed on trickle mixture, the EAT of controlling Sucralose spraying dispersion is 45~95 ℃, the Sucralose even spraying is dispersed on the mixing sugar alcohol crystalline solid of powder, the rising EAT, at mixing sugar alcohol after fluidisation loses surface crystallization water, pump into again the above-mentioned maltodextrin solution that refines, continuous spray drying granulation, the EAT of maltodextrin mist projection granulating controlled well is 60~120 ℃, and the maltodextrin spray drying granulation is on the noncrystalline fluffy body of sugar alcohol, obtain the fluffy powder granular products that even sugariness is modified.
Embodiment 1:
5.5 kilograms of maltodextrins are dissolved in a stainless steel heating reaction pot with 15 kilograms of deionized waters, 5 kilograms of Sucraloses are also dissolved in another stainless steel heating reaction pot with 27 kilograms of deionized waters, in pot, material is heated to 85 ℃ by chuck, start stirring, add respectively 1 kilogram of active carbon, be incubated 10 minutes, filter while hot, filtrate collects in respectively in the storage tank of jacket heat-preservation stand-by, 70 kilograms of Dextrose Monohydrates, 19.5 kilograms of D-sorbites, pulverize through pulverizer and reach 120 orders, be sent in the spray-fluidized bed apparatus, the mixed material of Dextrose Monohydrate and D-sorbite enters fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and accelerates from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is first sprayed the above-mentioned sucralose solution that refines continuously and is distributed on fine sugar alcohol body, controlling the fluidisation EAT is 45~95 ℃, the Multipoint Uniform spraying disperses, after operation is completed, improve again EAT to 60~120 ℃, at Dextrose Monohydrate, after the mixing of D-sorbite fluidisation loses surface crystallization water, pump into the above-mentioned maltodextrin solution that refines, continuous spray drying granulation, control EAT and mist flow well, obtain the fluffy powder granular products that even sugariness is modified.
Embodiment 2:
7.5 kilograms of maltodextrins are dissolved in a stainless steel heating reaction pot with 15 kilograms of deionized waters, 8.33 kilograms of Sucraloses are also dissolved in another stainless steel heating reaction pot with 30 kilograms of deionizations, in pot, material is heated to 85 ℃ by chuck, start stirring, add respectively 1 kilogram of active carbon, be incubated 10 minutes, filter while hot, filtrate collects in respectively in the storage tank of jacket heat-preservation stand-by, 76.3 kilograms of Dextrose Monohydrates, 7.87 kilograms of D-sorbites, pulverize through pulverizer and reach 120 orders, be sent in the spray-fluidized bed apparatus, the mixed material of Dextrose Monohydrate and D-sorbite enters fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and accelerates from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is first sprayed the above-mentioned sucralose solution that refines continuously and is distributed on fine sugar alcohol body, controlling EAT is 45~95 ℃, the Multipoint Uniform spraying disperses, after operation is completed, improve again EAT to 60~120 ℃, at Dextrose Monohydrate, after the mixing of D-sorbite fluidisation loses surface crystallization water, pump into the above-mentioned maltodextrin solution that refines, continuous spray drying granulation, control EAT and mist flow well, obtain the fluffy powder granular products that even sugariness is modified.
Embodiment 3:
8.2 kilograms of maltodextrins are dissolved in a stainless steel heating reaction pot with 20 kilograms of deionized waters, 16.7 kilograms of Sucraloses are also dissolved in another stainless steel heating reaction pot with 35 kilograms of deionized waters, in pot, material is heated to 85 ℃ by chuck, start stirring, add respectively 1 kilogram of active carbon, be incubated 30 minutes, filter while hot, filtrate collects in respectively in the storage tank of jacket heat-preservation stand-by, 72.6 kilograms of Dextrose Monohydrates, 2.5 kilograms of D-sorbites, pulverize through pulverizer and reach 120 orders, be sent in the spray-fluidized bed apparatus, the mixed material of Dextrose Monohydrate and D-sorbite enters fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and accelerates from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is first sprayed the above-mentioned sucralose solution that refines continuously and is distributed on fine sugar alcohol body, controlling the fluidisation EAT is 45~95 ℃, the Multipoint Uniform spraying disperses, after operation is completed, improve again EAT to 60~120 ℃, at Dextrose Monohydrate, after the mixing of D-sorbite fluidisation loses surface crystallization water, pump into the above-mentioned maltodextrin solution that refines, continuous spray drying granulation, control EAT and mist flow well, obtain the fluffy granular product that even sugariness is modified.
After testing, the fluffy granular composite low-sugar and low-calorie sweetener that adopts technical solution of the present invention to obtain, its main performance index sees Table 1.
Table 1
Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 |
Particle size | 40~100 orders | 40~100 orders | 40~100 orders |
Sugariness (sucrose contrast) | 30 times | 50 times | 100 times |
Outward appearance | The white powder | The white powder | The white powder |
The stability test of sweetener is to check sweetener to guarantee within a certain period of time the ability that undergoes no deterioration, and the sweetener product of the embodiment of the present invention was stored 3 years at normal temperatures, the phenomenons such as rotten and sugariness reduction occur, and stability is very superior.
The sugariness degree of modification of a kind of composite low-sugar sweetener of the present invention, will the adjustment in consumption according to Sucralose, usually select the common sucrose sugariness 30~100 times, relatively be fit to the use needs of food enterprise, form according to formula, in same sugariness situation, people are only 1 of common sucrose to the absorption of heat
/30~1/100, low-sugar-content and low-calorie sweetening agent is the sweet taste product of low-calorie, and this sweetener can not cause blood sugar to raise, and satisfies three high crowds, the healthy people's of pursuit needs.
To sum up obviously show, the present invention adopts formula, uses advanced science and technology technique and the method for science, and products obtained therefrom does not have smell, evenly white, soluble in water, and it is very convenient that this a kind of composite low-sugar sweetener is used.Granularity, dissolution velocity, mouthfeel, sugariness all are much better than the prior art value, and preparation technology's simple flow of science is easily gone, and are fit to very much large-scale production, are worth wide popularization and application in the field of business.
What need to understand is: the above is only the preferred embodiment of the present invention; for those skilled in the art; under the prerequisite that does not break away from the principle of the invention, can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (6)
1. a composite low-sugar sweetener, is characterized in that comprising following percentage by weight composition: Dextrose Monohydrate 45~90%, D-sorbite 0~20%, maltodextrin 5~20%, Sucralose 3.33~16.7%; Its preparation method comprises following processing step:
1. by composition proportion, maltodextrin, Sucralose are joined respectively in heating container, add respectively deionized water to mix;
2. be warming up to respectively 45~100 ℃ of dissolvings, and stir;
3. add respectively active carbon in above-mentioned maltodextrin solution and sucralose solution, be incubated 10~20 minutes, filter while hot, filtrate is pooled to respectively in the storage tank of heat tracing stand-by;
4. put in the spray-fluidized bed apparatus after by composition proportion, D-sorbite and Dextrose Monohydrate being pulverized, the mixed material of Dextrose Monohydrate and D-sorbite enters fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and accelerates from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is first sprayed the above-mentioned sucralose solution that refines continuously and is distributed on fine sugar alcohol body, pump into again the above-mentioned maltodextrin solution that refines, continuous spray-drying, obtain a kind of composite low-sugar sweetener.
2. a kind of composite low-sugar sweetener according to claim 1, is characterized in that its component has following percentage by weight: Dextrose Monohydrate 70%, D-sorbite 19.5%, maltodextrin 5.5%, Sucralose 5%.
3. a kind of composite low-sugar sweetener according to claim 1 and 2, it is characterized in that: described maltodextrin DE value is 10~20.
4.4. the preparation method of a kind of composite low-sugar sweetener claimed in claim 1 is characterized in that comprising following processing step:
1. by composition proportion, maltodextrin, Sucralose are joined respectively in heating container, add respectively deionized water to mix;
2. be warming up to respectively 45~100 ℃ of dissolvings, and stir;
3. add respectively active carbon in above-mentioned maltodextrin solution and sucralose solution, be incubated 10~20 minutes, filter while hot, filtrate is pooled to respectively in the storage tank of heat tracing stand-by;
4. put in the spray-fluidized bed apparatus after by composition proportion, D-sorbite and Dextrose Monohydrate being pulverized, the mixed material of Dextrose Monohydrate and D-sorbite enters fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and accelerates from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is first sprayed the above-mentioned sucralose solution that refines continuously and is distributed on fine sugar alcohol body, pump into again the above-mentioned maltodextrin solution that refines, continuous spray-drying, obtain a kind of composite low-sugar sweetener.
5. the preparation method of a kind of composite low-sugar sweetener according to claim 4, is characterized in that: maltodextrin, Sucralose are joined respectively in container, add respectively deionized water to mix, be warming up to respectively 60~100 ℃ of dissolvings, and stir, add respectively active carbon, be incubated 10 minutes, filter while hot, filtrate is pooled to respectively in storage tank with heat tracing, Dextrose Monohydrate and D-sorbite reach 100~120 orders through pulverizing, be sent in the spray-fluidized bed apparatus, the mixed material of Dextrose Monohydrate and D-sorbite enters fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and accelerates from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, control the fluidisation EAT at 45~120 ℃, the multiple spot spray gun of fluid bed sidepiece is first sprayed the above-mentioned sucralose solution that refines continuously and is distributed on fine sugar alcohol body, after the mixing of sugar alcohol fluidisation loses surperficial moisture content, pump into again the above-mentioned maltodextrin solution that refines, continuous spray drying granulation, obtain a kind of composite low-sugar sweetener.
6. the preparation method of a kind of composite low-sugar sweetener according to claim 5, it is characterized in that: the EAT scope of described fluidized bed with spraying is 45~120 ℃, wherein the EAT of phase I Sucralose spraying dispersion is 45~95 ℃, and the EAT of second stage maltodextrin mist projection granulating is 60~120 ℃.
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CN101142978A (en) * | 2007-09-28 | 2008-03-19 | 赵西南 | Trichlorosucrose low calorie sugar and preparation method thereof |
CN101401634A (en) * | 2008-01-04 | 2009-04-08 | 湖州市菱湖新望化学有限公司 | Food sweetening agent |
CN101874591A (en) * | 2009-11-24 | 2010-11-03 | 苏州工业园区尚融科技有限公司 | Fluffy granular composite low-sugar and low-calorie sweetener and preparation method thereof |
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Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN101142978A (en) * | 2007-09-28 | 2008-03-19 | 赵西南 | Trichlorosucrose low calorie sugar and preparation method thereof |
CN101401634A (en) * | 2008-01-04 | 2009-04-08 | 湖州市菱湖新望化学有限公司 | Food sweetening agent |
CN101874591A (en) * | 2009-11-24 | 2010-11-03 | 苏州工业园区尚融科技有限公司 | Fluffy granular composite low-sugar and low-calorie sweetener and preparation method thereof |
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Application publication date: 20130327 |