CN101768378B - 干法研磨超细重质碳酸钙的方法 - Google Patents
干法研磨超细重质碳酸钙的方法 Download PDFInfo
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- CN101768378B CN101768378B CN 200910247413 CN200910247413A CN101768378B CN 101768378 B CN101768378 B CN 101768378B CN 200910247413 CN200910247413 CN 200910247413 CN 200910247413 A CN200910247413 A CN 200910247413A CN 101768378 B CN101768378 B CN 101768378B
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- Prior art keywords
- grinding
- calcium carbonate
- heavy calcium
- ammonium chloride
- add
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- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 title claims abstract description 52
- 238000000227 grinding Methods 0.000 title claims abstract description 39
- 238000000034 method Methods 0.000 title claims abstract description 27
- 229910000019 calcium carbonate Inorganic materials 0.000 title claims abstract description 26
- 239000000080 wetting agent Substances 0.000 claims abstract description 19
- 239000000843 powder Substances 0.000 claims abstract description 14
- CJZGTCYPCWQAJB-UHFFFAOYSA-L calcium stearate Chemical group [Ca+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O CJZGTCYPCWQAJB-UHFFFAOYSA-L 0.000 claims description 9
- 239000008116 calcium stearate Substances 0.000 claims description 9
- 235000013539 calcium stearate Nutrition 0.000 claims description 9
- 238000009837 dry grinding Methods 0.000 claims description 9
- 239000013543 active substance Substances 0.000 claims description 8
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims description 7
- 241000282326 Felis catus Species 0.000 claims description 6
- YMKDRGPMQRFJGP-UHFFFAOYSA-M cetylpyridinium chloride Chemical compound [Cl-].CCCCCCCCCCCCCCCC[N+]1=CC=CC=C1 YMKDRGPMQRFJGP-UHFFFAOYSA-M 0.000 claims description 5
- WOWHHFRSBJGXCM-UHFFFAOYSA-M cetyltrimethylammonium chloride Chemical compound [Cl-].CCCCCCCCCCCCCCCC[N+](C)(C)C WOWHHFRSBJGXCM-UHFFFAOYSA-M 0.000 claims description 5
- ZRZPJMDENUOXEC-UHFFFAOYSA-M ethenyl-dimethyl-(2-octadecylphenyl)azanium chloride Chemical compound [Cl-].C(CCCCCCCCCCCCCCCCC)C1=C(C=CC=C1)[N+](C=C)(C)C ZRZPJMDENUOXEC-UHFFFAOYSA-M 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 4
- SXPWTBGAZSPLHA-UHFFFAOYSA-M cetalkonium chloride Chemical compound [Cl-].CCCCCCCCCCCCCCCC[N+](C)(C)CC1=CC=CC=C1 SXPWTBGAZSPLHA-UHFFFAOYSA-M 0.000 claims description 3
- 229960000228 cetalkonium chloride Drugs 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 3
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims description 2
- KWIUHFFTVRNATP-UHFFFAOYSA-N Betaine Natural products C[N+](C)(C)CC([O-])=O KWIUHFFTVRNATP-UHFFFAOYSA-N 0.000 claims description 2
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims description 2
- LZZYPRNAOMGNLH-UHFFFAOYSA-M Cetrimonium bromide Chemical compound [Br-].CCCCCCCCCCCCCCCC[N+](C)(C)C LZZYPRNAOMGNLH-UHFFFAOYSA-M 0.000 claims description 2
- KWIUHFFTVRNATP-UHFFFAOYSA-O N,N,N-trimethylglycinium Chemical compound C[N+](C)(C)CC(O)=O KWIUHFFTVRNATP-UHFFFAOYSA-O 0.000 claims description 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 2
- KHSLHYAUZSPBIU-UHFFFAOYSA-M benzododecinium bromide Chemical compound [Br-].CCCCCCCCCCCC[N+](C)(C)CC1=CC=CC=C1 KHSLHYAUZSPBIU-UHFFFAOYSA-M 0.000 claims description 2
- JBIROUFYLSSYDX-UHFFFAOYSA-M benzododecinium chloride Chemical group [Cl-].CCCCCCCCCCCC[N+](C)(C)CC1=CC=CC=C1 JBIROUFYLSSYDX-UHFFFAOYSA-M 0.000 claims description 2
- 229960003237 betaine Drugs 0.000 claims description 2
- 229920001577 copolymer Polymers 0.000 claims description 2
- 229920002401 polyacrylamide Polymers 0.000 claims description 2
- SFVFIFLLYFPGHH-UHFFFAOYSA-M stearalkonium chloride Chemical compound [Cl-].CCCCCCCCCCCCCCCCCC[N+](C)(C)CC1=CC=CC=C1 SFVFIFLLYFPGHH-UHFFFAOYSA-M 0.000 claims description 2
- 239000004094 surface-active agent Substances 0.000 abstract 1
- 239000002245 particle Substances 0.000 description 11
- 238000002360 preparation method Methods 0.000 description 9
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 8
- 239000003995 emulsifying agent Substances 0.000 description 8
- 238000004519 manufacturing process Methods 0.000 description 6
- -1 amine salt Chemical class 0.000 description 5
- 238000005516 engineering process Methods 0.000 description 5
- 229910000029 sodium carbonate Inorganic materials 0.000 description 4
- 235000017550 sodium carbonate Nutrition 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 3
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
- 239000011575 calcium Substances 0.000 description 3
- 229910052791 calcium Inorganic materials 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
- 239000006185 dispersion Substances 0.000 description 3
- 238000009826 distribution Methods 0.000 description 3
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 3
- 238000012216 screening Methods 0.000 description 3
- HVUMOYIDDBPOLL-XWVZOOPGSA-N Sorbitan monostearate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O HVUMOYIDDBPOLL-XWVZOOPGSA-N 0.000 description 2
- 230000002776 aggregation Effects 0.000 description 2
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical group [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 2
- 239000000920 calcium hydroxide Substances 0.000 description 2
- 229910001861 calcium hydroxide Inorganic materials 0.000 description 2
- 239000000945 filler Substances 0.000 description 2
- 230000004927 fusion Effects 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 235000012204 lemonade/lime carbonate Nutrition 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 239000001587 sorbitan monostearate Substances 0.000 description 2
- 235000011076 sorbitan monostearate Nutrition 0.000 description 2
- 229940035048 sorbitan monostearate Drugs 0.000 description 2
- 238000001238 wet grinding Methods 0.000 description 2
- QSSXJPIWXQTSIX-UHFFFAOYSA-N 1-bromo-2-methylbenzene Chemical compound CC1=CC=CC=C1Br QSSXJPIWXQTSIX-UHFFFAOYSA-N 0.000 description 1
- FGHSOIHUQQWOCJ-UHFFFAOYSA-N ClC1=C(C=CC=C1O)C.[P] Chemical compound ClC1=C(C=CC=C1O)C.[P] FGHSOIHUQQWOCJ-UHFFFAOYSA-N 0.000 description 1
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 description 1
- 241000276489 Merlangius merlangus Species 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 235000021355 Stearic acid Nutrition 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 238000004220 aggregation Methods 0.000 description 1
- 150000003863 ammonium salts Chemical class 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 235000019439 ethyl acetate Nutrition 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 125000000623 heterocyclic group Chemical group 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 235000012054 meals Nutrition 0.000 description 1
- 238000005065 mining Methods 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 1
- HWGNBUXHKFFFIH-UHFFFAOYSA-I pentasodium;[oxido(phosphonatooxy)phosphoryl] phosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O HWGNBUXHKFFFIH-UHFFFAOYSA-I 0.000 description 1
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 description 1
- 229920000053 polysorbate 80 Polymers 0.000 description 1
- 229910052573 porcelain Inorganic materials 0.000 description 1
- 150000003242 quaternary ammonium salts Chemical class 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 235000019982 sodium hexametaphosphate Nutrition 0.000 description 1
- GCLGEJMYGQKIIW-UHFFFAOYSA-H sodium hexametaphosphate Chemical group [Na]OP1(=O)OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])O1 GCLGEJMYGQKIIW-UHFFFAOYSA-H 0.000 description 1
- 235000019832 sodium triphosphate Nutrition 0.000 description 1
- 239000000600 sorbitol Substances 0.000 description 1
- 239000008117 stearic acid Substances 0.000 description 1
- 239000001577 tetrasodium phosphonato phosphate Substances 0.000 description 1
- STCOOQWBFONSKY-UHFFFAOYSA-N tributyl phosphate Chemical group CCCCOP(=O)(OCCCC)OCCCC STCOOQWBFONSKY-UHFFFAOYSA-N 0.000 description 1
- 239000001226 triphosphate Substances 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
Landscapes
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
Abstract
Description
Claims (6)
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CN101768378B true CN101768378B (zh) | 2012-11-14 |
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Families Citing this family (22)
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CN102220032B (zh) * | 2011-03-29 | 2013-10-09 | 上海东升新材料有限公司 | 超细重质碳酸钙的干法研磨方法 |
CN102220033B (zh) * | 2011-03-29 | 2014-01-29 | 上海东升新材料有限公司 | 干法研磨超细重质碳酸钙的方法 |
CN102504608A (zh) * | 2011-10-20 | 2012-06-20 | 张家界恒亮新材料科技有限公司 | 一种微纳级表面改性重质碳酸钙的制备方法及其产品 |
EP2771412A1 (en) * | 2011-10-25 | 2014-09-03 | Imerys Minerals Limited | Particulate fillers |
CN103408797B (zh) * | 2013-07-03 | 2015-07-15 | 青阳县永诚钙业有限责任公司 | 一种地板砖用改性碳酸钙及其制备方法 |
CN103555000A (zh) * | 2013-09-28 | 2014-02-05 | 昆山市周市溴化锂溶液厂 | 超细重质碳酸钙的研磨方法 |
CN104448937A (zh) * | 2014-11-18 | 2015-03-25 | 江苏群鑫粉体材料有限公司 | 油漆用超细活性重质碳酸钙的生产方法 |
CN104403369A (zh) * | 2014-11-26 | 2015-03-11 | 甘振辉 | 丙烯酸共聚物重质碳酸钙超细粉制备方法 |
CN104403372A (zh) * | 2014-12-08 | 2015-03-11 | 广西利升石业有限公司 | 干法超细重质碳酸钙的制备方法 |
CN104987752A (zh) * | 2014-12-31 | 2015-10-21 | 李安平 | 丙烯酸共聚物重质碳酸钙超细粉制备方法 |
CN105154007B (zh) * | 2015-09-29 | 2017-05-24 | 唐山市龙亿科技开发有限公司 | 一种矿渣助磨剂母液的制备方法及使用方法 |
CN105238352A (zh) * | 2015-10-28 | 2016-01-13 | 徐福明 | 一种贵金属矿石助磨剂及其制备方法 |
CN107400258A (zh) * | 2017-07-31 | 2017-11-28 | 贺州钟山县双文碳酸钙新材料有限公司 | 一种分散性好的改性碳酸钙的制备工艺 |
CN107442250A (zh) * | 2017-08-10 | 2017-12-08 | 青阳县永诚钙业有限责任公司 | 一种白云石细粉的制备方法 |
CN107418252A (zh) * | 2017-08-14 | 2017-12-01 | 合肥裕亿农业技术开发有限公司 | 一种养生房用地板砖改性碳酸钙 |
CN108752979A (zh) * | 2018-05-10 | 2018-11-06 | 桂林永福恒达实业有限公司 | 一种湿法制备超微细碳酸钙的方法 |
CN109647339B (zh) * | 2019-01-25 | 2021-12-31 | 中国科学院兰州化学物理研究所 | 利用半焦制备霉菌毒素吸附剂的方法 |
CN110132787B (zh) * | 2019-06-04 | 2021-11-05 | 山鹰华南纸业有限公司 | 一种造纸用石灰石粉的检测方法 |
CN110465398A (zh) * | 2019-07-08 | 2019-11-19 | 惠州市三化新技术有限公司 | 一种季铵盐类化合物在粉末组合物中作为助磨剂的应用 |
CN111234778A (zh) * | 2020-03-04 | 2020-06-05 | 安徽江东科技粉业有限公司 | 一种重钙粉体助磨剂及其制备方法 |
CN114149696B (zh) * | 2021-12-17 | 2023-04-28 | 亚士创能科技(上海)股份有限公司 | 改性碳酸钙及制备方法、耐老化外墙涂料和应用 |
CN114426781B (zh) * | 2022-01-19 | 2023-05-09 | 江西广源化工有限责任公司 | 一种超细重质碳酸钙及其制备方法 |
Citations (1)
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CN101367963A (zh) * | 2008-08-15 | 2009-02-18 | 芜湖同达新材料科技有限公司 | 超细复合改性重质碳酸钙粉体、制备方法及其应用 |
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CN101367963A (zh) * | 2008-08-15 | 2009-02-18 | 芜湖同达新材料科技有限公司 | 超细复合改性重质碳酸钙粉体、制备方法及其应用 |
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