CN101309751A - 一种用于生产多孔成形主体的工艺 - Google Patents
一种用于生产多孔成形主体的工艺 Download PDFInfo
- Publication number
- CN101309751A CN101309751A CNA2006800423245A CN200680042324A CN101309751A CN 101309751 A CN101309751 A CN 101309751A CN A2006800423245 A CNA2006800423245 A CN A2006800423245A CN 200680042324 A CN200680042324 A CN 200680042324A CN 101309751 A CN101309751 A CN 101309751A
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- Granted
Links
- 238000000034 method Methods 0.000 title abstract description 17
- 239000011148 porous material Substances 0.000 claims abstract description 37
- 238000001354 calcination Methods 0.000 claims abstract description 13
- 239000011230 binding agent Substances 0.000 claims abstract description 11
- 239000000203 mixture Substances 0.000 claims abstract description 10
- 239000002245 particle Substances 0.000 claims abstract description 10
- 239000000843 powder Substances 0.000 claims abstract description 10
- 238000005516 engineering process Methods 0.000 claims description 17
- 230000003197 catalytic effect Effects 0.000 claims description 11
- 239000003513 alkali Substances 0.000 claims description 7
- 239000007900 aqueous suspension Substances 0.000 claims description 6
- 239000007787 solid Substances 0.000 claims description 5
- 239000003054 catalyst Substances 0.000 claims description 4
- -1 polypropylene Polymers 0.000 claims description 4
- 239000000725 suspension Substances 0.000 claims description 4
- 239000004698 Polyethylene Substances 0.000 claims description 3
- 229920000573 polyethylene Polymers 0.000 claims description 3
- 238000012545 processing Methods 0.000 claims description 3
- 238000005245 sintering Methods 0.000 claims description 3
- 239000004743 Polypropylene Substances 0.000 claims description 2
- 239000004793 Polystyrene Substances 0.000 claims description 2
- 150000001875 compounds Chemical class 0.000 claims description 2
- 229920000642 polymer Polymers 0.000 claims description 2
- 229920002223 polystyrene Polymers 0.000 claims description 2
- 229920002635 polyurethane Polymers 0.000 claims description 2
- 239000004814 polyurethane Substances 0.000 claims description 2
- 229920001577 copolymer Polymers 0.000 claims 1
- 229920001155 polypropylene Polymers 0.000 claims 1
- 238000007493 shaping process Methods 0.000 abstract description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 7
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 6
- 239000000463 material Substances 0.000 description 6
- 229910017604 nitric acid Inorganic materials 0.000 description 6
- 239000011347 resin Substances 0.000 description 6
- 229920005989 resin Polymers 0.000 description 6
- 238000006555 catalytic reaction Methods 0.000 description 5
- 238000012805 post-processing Methods 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- 229910021536 Zeolite Inorganic materials 0.000 description 4
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 4
- 229910052500 inorganic mineral Inorganic materials 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 239000011707 mineral Substances 0.000 description 4
- 239000010457 zeolite Substances 0.000 description 4
- 238000009826 distribution Methods 0.000 description 3
- 239000000377 silicon dioxide Substances 0.000 description 3
- 229920000178 Acrylic resin Polymers 0.000 description 2
- 239000004925 Acrylic resin Substances 0.000 description 2
- NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 239000000084 colloidal system Substances 0.000 description 2
- 238000010790 dilution Methods 0.000 description 2
- 239000012895 dilution Substances 0.000 description 2
- 238000002347 injection Methods 0.000 description 2
- 239000007924 injection Substances 0.000 description 2
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 2
- 229910052753 mercury Inorganic materials 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 description 1
- 235000010724 Wisteria floribunda Nutrition 0.000 description 1
- ILRRQNADMUWWFW-UHFFFAOYSA-K aluminium phosphate Chemical compound O1[Al]2OP1(=O)O2 ILRRQNADMUWWFW-UHFFFAOYSA-K 0.000 description 1
- 229910003481 amorphous carbon Inorganic materials 0.000 description 1
- 229920006125 amorphous polymer Polymers 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 239000011324 bead Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910001593 boehmite Inorganic materials 0.000 description 1
- 238000010000 carbonizing Methods 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000001186 cumulative effect Effects 0.000 description 1
- 238000006073 displacement reaction Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 229910000267 dualite Inorganic materials 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 235000013312 flour Nutrition 0.000 description 1
- FAHBNUUHRFUEAI-UHFFFAOYSA-M hydroxidooxidoaluminium Chemical compound O[Al]=O FAHBNUUHRFUEAI-UHFFFAOYSA-M 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 229920000609 methyl cellulose Polymers 0.000 description 1
- 239000001923 methylcellulose Substances 0.000 description 1
- 239000002808 molecular sieve Substances 0.000 description 1
- 239000006259 organic additive Substances 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 229920005606 polypropylene copolymer Polymers 0.000 description 1
- 229920005990 polystyrene resin Polymers 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 230000001172 regenerating effect Effects 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 235000012239 silicon dioxide Nutrition 0.000 description 1
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 description 1
- 239000011949 solid catalyst Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
- B01J37/0018—Addition of a binding agent or of material, later completely removed among others as result of heat treatment, leaching or washing,(e.g. forming of pores; protective layer, desintegrating by heat)
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J29/00—Catalysts comprising molecular sieves
- B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
- B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J29/00—Catalysts comprising molecular sieves
- B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
- B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
- B01J29/40—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11, as exemplified by patent documents US3702886, GB1334243 and US3709979, respectively
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
- B01J2229/30—After treatment, characterised by the means used
- B01J2229/42—Addition of matrix or binder particles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J35/00—Catalysts, in general, characterised by their form or physical properties
- B01J35/30—Catalysts, in general, characterised by their form or physical properties characterised by their physical properties
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/26—Web or sheet containing structurally defined element or component, the element or component having a specified physical dimension
- Y10T428/268—Monolayer with structurally defined element
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Crystallography & Structural Chemistry (AREA)
- Catalysts (AREA)
Abstract
Description
孔隙直径 | %含量 |
7.5-14nm | 5-15 |
14-80nm | 8-35 |
80-1750nm | 55-85 |
1750-15000nm | 0.1-2 |
实施例中的成形主体 | |
标准粘结剂粘结剂含量(重量%)LOI a)(重量%)Na b(ppm wt)C b)(ppm wt)硬度 (kg/cm2)PV-Hg (cm3/g) | 1/16”挤出物二氧化硅201.4<4070+/-201.90.54 |
孔隙尺寸分布:>1750nm1750-80nm80-14nm14-7.5nmAPRSA g)(m2/g) | 0.7168.9621.58.83295 |
Claims (12)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE102005052016A DE102005052016B4 (de) | 2005-10-31 | 2005-10-31 | Verfahren zur Herstellung poröser Formkörper und Formkörper erhältlich durch das Verfahren |
DE102005052016.2 | 2005-10-31 | ||
PCT/EP2006/010486 WO2007051601A1 (de) | 2005-10-31 | 2006-10-31 | Verfahren zur herstellung poröser formkörper |
Publications (2)
Publication Number | Publication Date |
---|---|
CN101309751A true CN101309751A (zh) | 2008-11-19 |
CN101309751B CN101309751B (zh) | 2012-09-26 |
Family
ID=37635855
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN2006800423245A Expired - Fee Related CN101309751B (zh) | 2005-10-31 | 2006-10-31 | 一种用于生产多孔成形主体的工艺 |
Country Status (7)
Country | Link |
---|---|
US (1) | US20090162649A1 (zh) |
EP (1) | EP1943017B1 (zh) |
JP (1) | JP5060488B2 (zh) |
CN (1) | CN101309751B (zh) |
DE (1) | DE102005052016B4 (zh) |
DK (1) | DK1943017T3 (zh) |
WO (1) | WO2007051601A1 (zh) |
Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US8138386B2 (en) * | 2007-03-20 | 2012-03-20 | Mitsui Chemicals, Inc. | Method for converting hydrocarbons with zeolite shaped catalyst |
DE102007048313B4 (de) | 2007-10-09 | 2011-07-28 | Süd-Chemie AG, 80333 | Beschichtung von Substraten unter Gewährleistung einer hohen Porosität bei gleichzeitig hoher Abriebbeständigkeit der Beschichtung |
DE102007059129A1 (de) | 2007-12-07 | 2009-06-10 | Süd-Chemie AG | Katalysator mit erhöhter Olefinselektivität zur Umsetzung von Oxygenaten zu Olefinen |
DE102009056145B3 (de) | 2009-11-27 | 2011-07-28 | Süd-Chemie AG, 80333 | Beschichtungssuspension zur Beschichtung von Katalysatorsubstraten |
DE102014215112A1 (de) * | 2014-07-31 | 2016-02-04 | Johnson Matthey Public Limited Company | Verfahren zur Herstellung eines Katalysators sowie Katalysator-Artikel |
Family Cites Families (21)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4032433A (en) * | 1976-04-30 | 1977-06-28 | Uop Inc. | Hydrorefining asphaltenic petroleum charge stocks |
FR2431468A1 (fr) * | 1978-07-19 | 1980-02-15 | Lafarge Sa | Materiau microporeux utilisable notamment dans l'industrie ceramique |
JPS60102938A (ja) * | 1983-11-09 | 1985-06-07 | Res Assoc Petroleum Alternat Dev<Rapad> | 重質炭化水素油の水素化精製用触媒 |
US5100859A (en) * | 1991-01-22 | 1992-03-31 | Norton Company | Catalyst carrier |
DE4142897A1 (de) * | 1991-12-23 | 1993-06-24 | Sued Chemie Ag | Katalysator-formkoerper |
DE19533486A1 (de) * | 1995-09-12 | 1997-03-13 | Basf Ag | Monomodale und polymodale Katalysatorträger und Katalysatoren mit engen Porengrößenverteilungen und deren Herstellverfahren |
DE19533484A1 (de) * | 1995-09-12 | 1997-03-13 | Basf Ag | Monomodale und polymodale Katalysatorträger und Katalysatoren mit engen Porengrößenverteilungen und deren Herstellverfahren |
EP1069944B1 (en) * | 1998-03-31 | 2007-02-21 | Grace GmbH & Co. KG | Shaped body of zeolite, a process for its production and its use |
CA2414989A1 (en) * | 2000-07-03 | 2003-01-02 | Basf Aktiengesellschaft | Improved catalyst and method for producing polytetrahydrofurane |
DE10110139A1 (de) * | 2001-03-02 | 2002-09-12 | Basf Ag | Formkörper und Verfahren zu dessen Herstellung |
JP4266103B2 (ja) * | 2001-12-07 | 2009-05-20 | 日本碍子株式会社 | 多孔質セラミック体の製造方法 |
EP1323468A1 (en) * | 2001-12-31 | 2003-07-02 | Grace GmbH & Co. KG | Adsorbing material comprised of porous functional solid incorporated in a polymer matrix |
DE10219879A1 (de) * | 2002-05-03 | 2003-11-20 | Basf Ag | Katalysatorträger und Verfahren zu seiner Herstellung |
JP3829792B2 (ja) * | 2002-10-30 | 2006-10-04 | トヨタ自動車株式会社 | 排ガス浄化触媒用担体の製造方法 |
ES2316514T3 (es) * | 2002-12-01 | 2009-04-16 | Sud-Chemie Ag | Uso de un catalizador a base de aluminosilicato cristalino. |
JP4967111B2 (ja) * | 2003-03-20 | 2012-07-04 | 独立行政法人産業技術総合研究所 | アルミナ基多孔質セラミックス及びその製造方法 |
DE10314753A1 (de) * | 2003-04-01 | 2004-10-14 | Süd-Chemie AG | Synthetischer Zeolith, insbesondere für die katalytische Hydroisomerisierung von höheren Paraffinen |
US7304013B2 (en) * | 2003-06-30 | 2007-12-04 | Corning Incorporated | Metal oxide catalysts |
DE10356184A1 (de) * | 2003-12-02 | 2005-07-07 | Basf Ag | Zeolithisches Material vom Pentasil-Strukturtyp, seine Herstellung und seine Verwendung |
JP4488773B2 (ja) * | 2004-03-11 | 2010-06-23 | 勝 市川 | 低級炭化水素直接改質触媒の製造方法および低級炭化水素直接改質触媒 |
JP4524425B2 (ja) * | 2004-03-19 | 2010-08-18 | 独立行政法人産業技術総合研究所 | セラミックスナノ粒子被覆有機樹脂球粒子並びにその成形体、多孔質セラミックス及びそれらの製造方法 |
-
2005
- 2005-10-31 DE DE102005052016A patent/DE102005052016B4/de not_active Expired - Fee Related
-
2006
- 2006-10-31 CN CN2006800423245A patent/CN101309751B/zh not_active Expired - Fee Related
- 2006-10-31 DK DK06806646.3T patent/DK1943017T3/da active
- 2006-10-31 JP JP2008538296A patent/JP5060488B2/ja not_active Expired - Fee Related
- 2006-10-31 US US12/092,028 patent/US20090162649A1/en not_active Abandoned
- 2006-10-31 EP EP06806646A patent/EP1943017B1/de not_active Not-in-force
- 2006-10-31 WO PCT/EP2006/010486 patent/WO2007051601A1/de active Application Filing
Also Published As
Publication number | Publication date |
---|---|
DE102005052016A1 (de) | 2007-05-03 |
JP2009513478A (ja) | 2009-04-02 |
JP5060488B2 (ja) | 2012-10-31 |
EP1943017B1 (de) | 2012-06-06 |
WO2007051601A1 (de) | 2007-05-10 |
EP1943017A1 (de) | 2008-07-16 |
DE102005052016B4 (de) | 2009-05-20 |
US20090162649A1 (en) | 2009-06-25 |
DK1943017T3 (da) | 2012-09-24 |
CN101309751B (zh) | 2012-09-26 |
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Owner name: SC INTELLECTUAL PROPERTY JOINT LTD. Free format text: FORMER OWNER: SUED CHEMIE AG Effective date: 20130110 |
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Granted publication date: 20120926 Termination date: 20201031 |